CN114503983A - Preparation method and application of ionic oxygen disinfectant - Google Patents
Preparation method and application of ionic oxygen disinfectant Download PDFInfo
- Publication number
- CN114503983A CN114503983A CN202210104009.1A CN202210104009A CN114503983A CN 114503983 A CN114503983 A CN 114503983A CN 202210104009 A CN202210104009 A CN 202210104009A CN 114503983 A CN114503983 A CN 114503983A
- Authority
- CN
- China
- Prior art keywords
- oxygen
- water
- disinfectant
- deionized water
- parts
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000001301 oxygen Substances 0.000 title claims abstract description 63
- 229910052760 oxygen Inorganic materials 0.000 title claims abstract description 63
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 title claims abstract description 61
- 239000000645 desinfectant Substances 0.000 title claims abstract description 25
- 238000002360 preparation method Methods 0.000 title abstract description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 49
- 239000008367 deionised water Substances 0.000 claims abstract description 24
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 24
- 238000002156 mixing Methods 0.000 claims abstract description 17
- 239000003223 protective agent Substances 0.000 claims abstract description 15
- 239000007787 solid Substances 0.000 claims abstract description 15
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000010936 titanium Substances 0.000 claims abstract description 10
- 229910052719 titanium Inorganic materials 0.000 claims abstract description 10
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims abstract description 9
- 239000003054 catalyst Substances 0.000 claims abstract description 9
- 229910052751 metal Inorganic materials 0.000 claims abstract description 9
- 239000002184 metal Substances 0.000 claims abstract description 9
- 238000000926 separation method Methods 0.000 claims abstract description 9
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 9
- 239000011734 sodium Substances 0.000 claims abstract description 9
- 239000004372 Polyvinyl alcohol Substances 0.000 claims abstract description 7
- 229920002451 polyvinyl alcohol Polymers 0.000 claims abstract description 7
- 239000002552 dosage form Substances 0.000 claims abstract description 5
- 239000000463 material Substances 0.000 claims abstract description 5
- 239000007788 liquid Substances 0.000 claims description 8
- 238000005507 spraying Methods 0.000 claims description 8
- 238000000034 method Methods 0.000 claims description 7
- 239000011248 coating agent Substances 0.000 claims description 6
- 238000000576 coating method Methods 0.000 claims description 6
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 claims description 6
- 238000002791 soaking Methods 0.000 claims description 4
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 3
- 239000000084 colloidal system Substances 0.000 claims description 3
- 229910052802 copper Inorganic materials 0.000 claims description 3
- 239000010949 copper Substances 0.000 claims description 3
- 229910052697 platinum Inorganic materials 0.000 claims description 3
- 239000002994 raw material Substances 0.000 claims description 3
- 230000003247 decreasing effect Effects 0.000 claims description 2
- 238000004090 dissolution Methods 0.000 claims description 2
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 claims 1
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 abstract description 6
- 150000002500 ions Chemical class 0.000 abstract description 6
- 239000000047 product Substances 0.000 abstract description 6
- 230000003647 oxidation Effects 0.000 abstract description 5
- 238000007254 oxidation reaction Methods 0.000 abstract description 5
- 239000001569 carbon dioxide Substances 0.000 abstract description 3
- 229910002092 carbon dioxide Inorganic materials 0.000 abstract description 3
- VUZPPFZMUPKLLV-UHFFFAOYSA-N methane;hydrate Chemical compound C.O VUZPPFZMUPKLLV-UHFFFAOYSA-N 0.000 abstract description 3
- 239000006227 byproduct Substances 0.000 abstract description 2
- 238000004659 sterilization and disinfection Methods 0.000 description 13
- 230000001954 sterilising effect Effects 0.000 description 11
- 241000894006 Bacteria Species 0.000 description 8
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 7
- 230000000694 effects Effects 0.000 description 7
- 238000007865 diluting Methods 0.000 description 5
- 230000000844 anti-bacterial effect Effects 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- 241000222122 Candida albicans Species 0.000 description 3
- 241000588724 Escherichia coli Species 0.000 description 3
- 241000191967 Staphylococcus aureus Species 0.000 description 3
- 229940095731 candida albicans Drugs 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 3
- 239000002131 composite material Substances 0.000 description 3
- 230000000249 desinfective effect Effects 0.000 description 3
- 239000007800 oxidant agent Substances 0.000 description 3
- 230000001590 oxidative effect Effects 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 239000000725 suspension Substances 0.000 description 3
- 229920000742 Cotton Polymers 0.000 description 2
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 2
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 2
- KFSLWBXXFJQRDL-UHFFFAOYSA-N Peracetic acid Chemical compound CC(=O)OO KFSLWBXXFJQRDL-UHFFFAOYSA-N 0.000 description 2
- 238000013329 compounding Methods 0.000 description 2
- 238000012258 culturing Methods 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 238000010790 dilution Methods 0.000 description 2
- 239000012895 dilution Substances 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 229910052748 manganese Inorganic materials 0.000 description 2
- 239000011572 manganese Substances 0.000 description 2
- 210000003928 nasal cavity Anatomy 0.000 description 2
- -1 oxygen ions Chemical class 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 244000025254 Cannabis sativa Species 0.000 description 1
- 235000012766 Cannabis sativa ssp. sativa var. sativa Nutrition 0.000 description 1
- 235000012765 Cannabis sativa ssp. sativa var. spontanea Nutrition 0.000 description 1
- 241000233866 Fungi Species 0.000 description 1
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 description 1
- 241000700605 Viruses Species 0.000 description 1
- 230000001580 bacterial effect Effects 0.000 description 1
- 244000052616 bacterial pathogen Species 0.000 description 1
- 229960002233 benzalkonium bromide Drugs 0.000 description 1
- KHSLHYAUZSPBIU-UHFFFAOYSA-M benzododecinium bromide Chemical compound [Br-].CCCCCCCCCCCC[N+](C)(C)CC1=CC=CC=C1 KHSLHYAUZSPBIU-UHFFFAOYSA-M 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 235000009120 camo Nutrition 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 235000005607 chanvre indien Nutrition 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- MAYPHUUCLRDEAZ-UHFFFAOYSA-N chlorine peroxide Inorganic materials ClOOCl MAYPHUUCLRDEAZ-UHFFFAOYSA-N 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- OSVXSBDYLRYLIG-UHFFFAOYSA-N dioxidochlorine(.) Chemical compound O=Cl=O OSVXSBDYLRYLIG-UHFFFAOYSA-N 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000011487 hemp Substances 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 230000005923 long-lasting effect Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 210000004400 mucous membrane Anatomy 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 244000052769 pathogen Species 0.000 description 1
- 230000001717 pathogenic effect Effects 0.000 description 1
- 230000003449 preventive effect Effects 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 239000008399 tap water Substances 0.000 description 1
- 235000020679 tap water Nutrition 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 239000003053 toxin Substances 0.000 description 1
- 231100000765 toxin Toxicity 0.000 description 1
- 108700012359 toxins Proteins 0.000 description 1
Images
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/22—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing ingredients stabilising the active ingredients
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K33/00—Medicinal preparations containing inorganic active ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
- A61K47/02—Inorganic compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
- A61K47/06—Organic compounds, e.g. natural or synthetic hydrocarbons, polyolefins, mineral oil, petrolatum or ozokerite
- A61K47/16—Organic compounds, e.g. natural or synthetic hydrocarbons, polyolefins, mineral oil, petrolatum or ozokerite containing nitrogen, e.g. nitro-, nitroso-, azo-compounds, nitriles, cyanates
- A61K47/18—Amines; Amides; Ureas; Quaternary ammonium compounds; Amino acids; Oligopeptides having up to five amino acids
- A61K47/183—Amino acids, e.g. glycine, EDTA or aspartame
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
- A61K47/30—Macromolecular organic or inorganic compounds, e.g. inorganic polyphosphates
- A61K47/32—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds, e.g. carbomers, poly(meth)acrylates, or polyvinyl pyrrolidone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P31/00—Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
- A61P31/02—Local antiseptics
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P31/00—Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
- A61P31/04—Antibacterial agents
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P31/00—Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
- A61P31/10—Antimycotics
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/46—Removing components of defined structure
- B01D53/72—Organic compounds not provided for in groups B01D53/48 - B01D53/70, e.g. hydrocarbons
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/74—General processes for purification of waste gases; Apparatus or devices specially adapted therefor
- B01D53/76—Gas phase processes, e.g. by using aerosols
Landscapes
- Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Medicinal Chemistry (AREA)
- Animal Behavior & Ethology (AREA)
- Pharmacology & Pharmacy (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Epidemiology (AREA)
- Inorganic Chemistry (AREA)
- Organic Chemistry (AREA)
- Communicable Diseases (AREA)
- Oncology (AREA)
- Environmental & Geological Engineering (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Plant Pathology (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Biomedical Technology (AREA)
- Agronomy & Crop Science (AREA)
- Analytical Chemistry (AREA)
- Toxicology (AREA)
- Proteomics, Peptides & Aminoacids (AREA)
- Dispersion Chemistry (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a preparation method and application of an ionic oxygen disinfectant, wherein the preparation method comprises the following steps: firstly, adding deionized water into a sterilized container; adding solid oxygen, an EDTA2 sodium protective agent, a polyvinyl alcohol protective agent, water-soluble nano titanium, a separation aid and a metal catalyst one by one, and uniformly mixing to fully dissolve; covering with a cover, slightly ventilating, dissolving all the materials gradually, dissolving a large amount of fine oxygen bubbles in water gradually, and storing at below 33 deg.C. The ion oxygen disinfectant has the innovative characteristics that: the effective concentration is very low (0.03%), the dosage is small, the final products of oxidation are carbon dioxide and water, no harmful by-products are left, and the disinfectant is the safest, efficient and multipurpose product in the current disinfectants; compared with similar strong oxidizers, the strong oxidizers are safe, have more dosage forms, are suitable for a wide range of application, and have the advantages that the common temperature is changed (0-40 ℃), the pH value of an article is not influenced, and the cost price is lower than that of a market article.
Description
Technical Field
The invention relates to the field of sanitation and disinfection, in particular to a preparation method and application of an ionic oxygen disinfectant.
Background
"oxygen" is closely related to life, is unnecessary and has strong effect, and chemical research has already clarified that almost all organic matters can be vigorously combusted in oxygen to generate carbon dioxide and water. I.e. can be inactivated against almost all complex microorganisms. However, the oxygen in the air in nature generally has a slow and not strong enough oxidation sterilization effect, and a high-tech treatment is required to improve the strong oxidation effect of the oxygen.
The oxygen-containing strong oxidants currently used in the market are: peracetic acid, chlorine peroxide, hydrogen peroxide and ozone, which are all very effective against a wide variety of pathogenic bacteria, fungi and viruses. But has not been widely used during current epidemic situations. The main reasons are that the strong oxidants are unsafe and unstable and damage human bodies and objects. The application range and conditions are limited, etc. Therefore, the composite material structure of the strong oxidant is researched and improved, the characteristics of oxidizing and efficiently killing bacteria and toxins are kept, toxic and side effects and defects are removed, the composite material can be widely used, and the composite material plays a role in epidemic situations.
Disclosure of Invention
It is an object of the present invention to provide a method for producing an ionic oxygen disinfectant which separates oxygen bound in a fixed oxide to form ionic oxygen having a energetically stable strong oxidizing action, rather than negative oxygen ions.
The technical scheme for realizing the purpose of the invention is as follows:
the invention relates to an ionic oxygen disinfectant, which comprises the following raw materials in parts by weight:
solid oxygen 6-10
Metal catalyst 0.1-0.3
0.1-0.5% of separation aid
Polyvinyl alcohol protective agent 0.2-0.5
EDTA2 sodium protective agent 1.0-2.0
Water soluble nano titanium 0.5-1.0
86-94 parts of deionized water.
The solid oxygen in the formula is 3.5 solid oxygen.
The metal catalyst in the formulation comprises copper, manganese and platinum.
The auxiliary release agent in the formula is 101 auxiliary release agent, and the dosage of the auxiliary release agent can be increased or decreased with the dosage according to the use condition.
The preparation method of the ionic oxygen disinfectant comprises the following steps:
(1) adding 20 parts by weight of deionized water into a sterilized container;
(2) adding solid oxygen, and slowly waiting for dissolution;
(3) adding an EDTA2 sodium protective agent, and uniformly mixing with the deionized water obtained in the step (1) to fully dissolve the EDTA2 sodium protective agent;
(4) adding a polyvinyl alcohol protective agent and 20 parts by weight of deionized water, and uniformly mixing to fully dissolve;
(5) adding water-soluble nano titanium and 20 parts by weight of deionized water, and uniformly mixing to fully dissolve the water-soluble nano titanium and the deionized water;
(6) adding a separation aid and 20 parts by weight of deionized water, and uniformly mixing to fully dissolve;
(7) adding a metal catalyst and the rest deionized water, and uniformly mixing to fully dissolve;
(8) covering with a cover, slightly ventilating, dissolving all the materials gradually, dissolving a large amount of fine oxygen bubbles in water gradually, and storing at below 33 deg.C.
The above-mentioned compounding process can not be heated.
The invention also aims to provide application of the ionic oxygen disinfectant, and the dosage form and the application method thereof are as follows:
(1) solid: can be subpackaged, broadcast sowed, fumigated, added with water at any time and converted into liquid;
(2) liquid: preparing the solution with various concentrations, and is suitable for different purposes, such as spraying, atomizing, wiping and soaking;
(3) colloid: the slow release of the coating is prepared.
The ion oxygen disinfectant has the innovative characteristics that:
(1) the method separates oxygen bound in the fixed oxide to form ionic oxygen with a multi-energy stable strong oxidation effect, but not negative oxygen ions, which cannot be mixed.
(2) The effective concentration is very low (0.03%), the dosage is small, the final products of oxidation are carbon dioxide and water, no harmful by-products are left, and the disinfectant is the safest, efficient and multipurpose product in the current disinfectants;
(3) compared with similar strong oxidizers, the strong oxidizers are safe, have more dosage forms, are suitable for a wide range of application, and the pH value of an article is not influenced when the common temperature is changed (0-40 ℃);
(4) compared with medical disinfecting alcohol, 84 disinfectant, benzalkonium bromide and the like commonly used in the market, the disinfectant has the advantages of good and lasting effect, wide application range, no peculiar smell, safety, good sense, and the like, and the cost price is lower than that of market products.
Drawings
FIG. 1 is a reference diagram of a rapid sterilization test in an example of application of the present invention.
Detailed Description
The invention is further illustrated by the following examples, which are not intended to limit the scope of the invention.
Example (b):
the invention relates to a preparation method of an ionic oxygen disinfectant, which comprises the following steps:
(1) preparing materials: the following raw materials are respectively weighed according to the weight portion: 3.5 solid oxygen 6-10, metal catalyst (copper, manganese and platinum) 0.1-0.3, 101 separation aid 0.1-0.5, polyvinyl alcohol protective agent 0.2-0.5, EDTA2 sodium protective agent 1.0-2.0, water-soluble nano titanium 0.5-1.0, and deionized water 86-94;
(2) adding solid oxygen, slowly dissolving, and not heating
(3) Adding 20 parts by weight of deionized water into a sterilized pure transparent container;
(4) adding an EDTA2 sodium protective agent, and uniformly mixing with the deionized water obtained in the step (1) to fully dissolve the EDTA2 sodium protective agent;
(5) adding a polyvinyl alcohol protective agent and 20 parts by weight of deionized water, and uniformly mixing to fully dissolve;
(6) adding water-soluble nano titanium and 20 parts by weight of deionized water, and uniformly mixing to fully dissolve the water-soluble nano titanium and the deionized water;
(7) adding a separation aid and 20 parts by weight of deionized water, and uniformly mixing to fully dissolve;
(8) adding a metal catalyst and the rest deionized water, and uniformly mixing to fully dissolve;
(9) covering with a cover, slightly ventilating, dissolving all the materials gradually, dissolving a large amount of fine oxygen bubbles in water gradually, and storing at below 33 deg.C.
The above-mentioned compounding process can not be heated.
The application example is as follows: application of ionic oxygen
Dosage forms and methods of use:
❶ solid: can be subpackaged, broadcast sowed, fumigated, added with water at any time and converted into liquid;
❷ liquid: preparing the solution with various concentrations, and is suitable for different purposes, such as spraying, atomizing, wiping and soaking;
❸ colloid: the slow release of the coating is prepared.
Brief description of the application
(1) Preventive disinfection, 0.3-0.6% of ion oxygen water, and is used in office, meeting room, classroom, ward, movable room, vehicle and other indoor places. The experimental group is tried on the bus, and after the guest finishes, close door and window, arrange 3 culture dish points, after 15 minutes with the ion oxygen water spraying, open the plate and contact with the air, cultivate the detection, do not discover the live bacteria, no pungent smell in the car, no peculiar smell.
(2) Rapidly disinfecting the epidemic rooms: firstly, conveying solid combined powder to a destination, adding tap water into a powder bag (5 kilograms of water/bag), quickly spraying a large amount of nascent oxygen, and immediately connecting spray disinfection; ② spraying with 1 percent of ionized oxygen water. Can quickly kill pathogen and block transmission.
(3) 0.5-0.6% of ionized oxygen water is sprayed, wiped, soaked and disinfected. The sterilization device is used for sterilizing express delivery pieces on trial, and does not damage articles and packages.
(4) 0.6-0.8% of the disinfectant is superior to alcohol and other disinfectants in cleaning and disinfecting by wiping fingers, and has long lasting effect, smoothness and no bad stimulation. The product is used for students and shopping staff to clean and disinfect the fingers of hundreds of people, and has good reaction.
(5) 0.5% of ionized oxygen water, eliminating indoor chemical pollution and purifying air
Safety of ion oxygen sterilization
1. Skin, mucous membrane: before the nasal cavity or the gum is wiped by soaking 0.2-0.6% ionized oxygen water in a cotton swab, the nasal cavity or the gum has no irritation and pain.
2. An object: ❶ no damage and no color change after three days of observation of 0.5% ionic oxygen water spraying of textile (cotton, hemp, thread, silk, chemical fiber); ❷ stainless steel, wooden furniture, electric fan, 0.5% spraying, and observing for three days without damage.
3. The ingredients of the ingredients are safe and nontoxic when being checked
Ionic oxygen water antibacterial test for antibacterial effect
(one), quick sterilization (blind second kill) test: (as shown in figure 1) the uncleaned fingers were moved up and down and wiped with ionized oxygen water; no. 5 indicates that the wiping is performed by diluting 5 times by using ionized oxygen water; number 4 refers to wipe with 75% alcohol; one finger (No. 3) was not wiped with anything, the other finger (No. 6) was wiped with ionized oxygen diluted 21 times with pure water, and cultured rapidly for 24 hours, and it was observed that the fingers No. 1, 2, 5 wiped with ionized oxygen water and the finger No. 4 wiped with sterilized alcohol were aseptically grown, and the finger No. 3 and the finger No. 6 diluted 21 times were overgrown with bacteria, and the test was repeated 5 times, the test showed that: firstly, the ionic oxygen can be quickly sterilized; ② the sterilization is ineffective after diluting the sterilized alcohol, the rapid sterilization effect is still achieved after diluting 5-10 times of the sterilized alcohol by the ion oxygen, and the efficacy is superior to that of the alcohol.
And (II) antibacterial test, namely mixing Escherichia coli, staphylococcus aureus and candida albicans suspensions with sample ionic oxygen liquid for 5 minutes respectively for neutralization, culturing for 24 hours, and observing the result: no viable bacteria exist (all are killed), the test is repeated for 5 times, the effect is the same, and the sterilization effective rate is confirmed to be more than 99 percent.
And (III) antibacterial minimum effective concentration test, namely diluting the ionic oxygen solution by 1: 16,1:32,1:64. 1:128, (1: 256 is not observed) and each bacterial liquid are mixed and cultured for 24 hours in sequence, and the observation result shows that no viable bacteria exist (all are killed), the test is repeated for 3 times, and the sterilization effective rate of 65-128 times (the minimum effective concentration is 0.03%) of dilution can be determined to be more than 99%.
(IV) coating test: diluting the suspension of escherichia coli, staphylococcus aureus and candida albicans at a ratio of 1:10, coating and culturing for 24 hours, counting the number of the viable bacteria: escherichia coli > 300cfu/ml, staphylococcus aureus 36cfu/ml and candida albicans > 1000cfu/ml, wherein the ionic oxygen solution is mixed with the suspension of each bacterium in a dilution ratio of 1:10 respectively, and coating observation is carried out, so that no existing viable bacteria exist, and the list is as follows:
note: the sample is sent to a national institution for detection, and the sterilization efficiency is more than 99 percent.
Claims (6)
1. An ionic oxygen disinfectant is characterized in that: comprises the following raw materials in parts by weight:
solid oxygen 6-10
Metal catalyst 0.1-0.3
0.1-0.5% of separation aid
Polyvinyl alcohol protective agent 0.2-0.5
EDTA2 sodium protective agent 1.0-2.0
Water soluble nano titanium 0.5-1.0
86-94 parts of deionized water.
2. The ionic oxygen disinfectant as set forth in claim 1, wherein: the solid oxygen is 3.5 solid oxygen.
3. The ionic oxygen disinfectant as set forth in claim 1, wherein: the metal catalyst includes copper, manganese, and platinum.
4. The ionic oxygen disinfectant as set forth in claim 1, wherein: the separation aid is 101, and the dosage of the separation aid can be increased or decreased according to the using condition.
5. A method of preparing an ionic oxygen disinfectant as claimed in any one of claims 1 to 4, comprising the steps of:
(1) adding 20 parts by weight of deionized water into a sterilized container;
(2) adding solid oxygen, and slowly waiting for dissolution;
(3) adding EDTA2 sodium protectant, mixing, and dissolving completely;
(4) adding a polyvinyl alcohol protective agent and 20 parts by weight of deionized water, and uniformly mixing to fully dissolve;
(5) adding water-soluble nano titanium and 20 parts by weight of deionized water, and uniformly mixing to fully dissolve the water-soluble nano titanium and the deionized water;
(6) adding a separation aid and 20 parts by weight of deionized water, and uniformly mixing to fully dissolve;
(7) adding a metal catalyst and the rest deionized water, and uniformly mixing to fully dissolve;
(8) covering with a cover, slightly ventilating, dissolving all the materials gradually, dissolving a large amount of fine oxygen bubbles in water gradually, and storing at below 33 deg.C.
6. The application of an ionic oxygen disinfectant comprises the following dosage forms and application methods:
(1) solid: can be subpackaged, broadcast sowed, fumigated, added with water at any time and converted into liquid;
(2) liquid: preparing the solution with various concentrations, and is suitable for different purposes, such as spraying, atomizing, wiping and soaking;
(3) colloid: the slow release of the coating is prepared.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210104009.1A CN114503983A (en) | 2022-01-28 | 2022-01-28 | Preparation method and application of ionic oxygen disinfectant |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210104009.1A CN114503983A (en) | 2022-01-28 | 2022-01-28 | Preparation method and application of ionic oxygen disinfectant |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN114503983A true CN114503983A (en) | 2022-05-17 |
Family
ID=81549794
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202210104009.1A Pending CN114503983A (en) | 2022-01-28 | 2022-01-28 | Preparation method and application of ionic oxygen disinfectant |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN114503983A (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101163784A (en) * | 2005-02-25 | 2008-04-16 | 生物医学解决方案有限责任公司 | Aqueous disinfectants and sterilants |
| CN102951691A (en) * | 2011-08-31 | 2013-03-06 | 黄泽平 | Oxygen supply scavenging agent for aquatic product culture |
| CN104445459A (en) * | 2014-11-13 | 2015-03-25 | 苏州市相城区盛胡特种养殖专业合作社 | High-efficiency nano water clarifying agent and preparation method thereof |
| CN113456671A (en) * | 2021-06-30 | 2021-10-01 | 武汉华欣美康新材料科技有限公司 | Friendly type durable antibacterial disinfection gel and preparation method thereof |
-
2022
- 2022-01-28 CN CN202210104009.1A patent/CN114503983A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101163784A (en) * | 2005-02-25 | 2008-04-16 | 生物医学解决方案有限责任公司 | Aqueous disinfectants and sterilants |
| CN102951691A (en) * | 2011-08-31 | 2013-03-06 | 黄泽平 | Oxygen supply scavenging agent for aquatic product culture |
| CN104445459A (en) * | 2014-11-13 | 2015-03-25 | 苏州市相城区盛胡特种养殖专业合作社 | High-efficiency nano water clarifying agent and preparation method thereof |
| CN113456671A (en) * | 2021-06-30 | 2021-10-01 | 武汉华欣美康新材料科技有限公司 | Friendly type durable antibacterial disinfection gel and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| EP1644010B1 (en) | Colloidal silver composition having antimicrobial properties | |
| JP4971198B2 (en) | Aqueous disinfectant and sterilant | |
| CN101522033B (en) | Disinfectant systems and methods | |
| JP6803896B2 (en) | Antimicrobial agent containing hypochlorous acid | |
| US20090148540A1 (en) | Antibacterial composition and method of production | |
| CN104824019A (en) | Aqueous sanitizers, disinfectants, and/or sterilants with low peroxygen content | |
| CN1918999A (en) | Preparation process of nano antibacterial agent | |
| CN111657299A (en) | Composite nano-ion bacteriostatic agent | |
| AU2011247875B1 (en) | Disinfectant Compositions and Uses Thereof | |
| CN111165478A (en) | Foam type sterilization, disinfection and air purification agent and preparation method and application thereof | |
| CN113287627B (en) | Cleaning disinfectant containing potassium hydrogen persulfate compound, and use method and application thereof | |
| CN110679607A (en) | Stable novel sterilization and disinfection solution and preparation method thereof | |
| CN113142240A (en) | Environment disinfectant and preparation method thereof | |
| CN111956665A (en) | Electrolytic silver ion disinfectant and preparation method thereof | |
| CN114503983A (en) | Preparation method and application of ionic oxygen disinfectant | |
| CN111226989A (en) | Folium artemisiae argyi composite disinfectant and preparation method thereof | |
| CN102648710B (en) | Compound glutaraldehyde disinfectant for body of dead person | |
| CN106689198A (en) | Compound hydrogen peroxide disinfectant as well as preparation method and application thereof<0} | |
| KR20200071200A (en) | Compositions for sterilization and disinfection using hydrogen peroxide | |
| JP2011502143A (en) | Bactericidal composition comprising peracid and acetylsalicylic acid | |
| KR102202917B1 (en) | Compositions for sterilization and disinfection and the manufacturing method thereof | |
| CN102461499B (en) | Disinfector for remains and preparation method thereof | |
| CN111165493A (en) | Mixed liquid deodorizing disinfectant and preparation method thereof | |
| CN111616148A (en) | High-efficiency disinfectant | |
| CN110721326A (en) | Manufacturing and application of multifunctional laboratory disinfection cleaning machine |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20220517 |
|
| RJ01 | Rejection of invention patent application after publication |