CN113799414B - Large grid cylinder and vacuum-assisted RTM (real time kinematic) forming method thereof - Google Patents

Large grid cylinder and vacuum-assisted RTM (real time kinematic) forming method thereof Download PDF

Info

Publication number
CN113799414B
CN113799414B CN202111022904.0A CN202111022904A CN113799414B CN 113799414 B CN113799414 B CN 113799414B CN 202111022904 A CN202111022904 A CN 202111022904A CN 113799414 B CN113799414 B CN 113799414B
Authority
CN
China
Prior art keywords
glue
cylinder
vacuum
grid
grid cylinder
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN202111022904.0A
Other languages
Chinese (zh)
Other versions
CN113799414A (en
Inventor
周栋
史文锋
沈辉
黄文煜
杨浩
吴文平
叶周军
刘图远
姜璐
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shanghai Composite Material Science and Technology Co Ltd
Original Assignee
Shanghai Composite Material Science and Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shanghai Composite Material Science and Technology Co Ltd filed Critical Shanghai Composite Material Science and Technology Co Ltd
Priority to CN202111022904.0A priority Critical patent/CN113799414B/en
Publication of CN113799414A publication Critical patent/CN113799414A/en
Application granted granted Critical
Publication of CN113799414B publication Critical patent/CN113799414B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C70/00Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts
    • B29C70/04Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts comprising reinforcements only, e.g. self-reinforcing plastics
    • B29C70/28Shaping operations therefor
    • B29C70/40Shaping or impregnating by compression not applied
    • B29C70/42Shaping or impregnating by compression not applied for producing articles of definite length, i.e. discrete articles
    • B29C70/46Shaping or impregnating by compression not applied for producing articles of definite length, i.e. discrete articles using matched moulds, e.g. for deforming sheet moulding compounds [SMC] or prepregs
    • B29C70/48Shaping or impregnating by compression not applied for producing articles of definite length, i.e. discrete articles using matched moulds, e.g. for deforming sheet moulding compounds [SMC] or prepregs and impregnating the reinforcements in the closed mould, e.g. resin transfer moulding [RTM], e.g. by vacuum
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C70/00Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts
    • B29C70/04Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts comprising reinforcements only, e.g. self-reinforcing plastics
    • B29C70/28Shaping operations therefor
    • B29C70/54Component parts, details or accessories; Auxiliary operations, e.g. feeding or storage of prepregs or SMC after impregnation or during ageing
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E30/00Energy generation of nuclear origin
    • Y02E30/30Nuclear fission reactors

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Composite Materials (AREA)
  • Mechanical Engineering (AREA)
  • Injection Moulding Of Plastics Or The Like (AREA)

Abstract

The application provides a vacuum auxiliary RTM forming method of a large grid cylinder, which comprises the following steps: manufacturing a vacuum bag along the molding surface of the mold by using the grid cylinder product prefabricated member; the plastic outlet tank is connected with a plurality of plastic outlets of the cylinder body for vacuumizing; injecting glue to the grating cylinder from bottom to top in a layered manner, and when the height of the layer and the circumferential glue injection are finished and the glue outlet of the lower layer begins to be out, controlling the glue outlet of the lower layer to switch from vacuumizing to RTM glue injection through a three-way switching valve, and finishing the process from bottom to top in a layered manner through an annular runner until the top is completely soaked and the glue begins to be out; when a large amount of glue is discharged from a glue outlet at the top of the grid cylinder, reversely pressurizing from a glue discharge tank; closing the interface of the glue injection pipeline, and continuously vacuumizing the glue outlet until the subsequent furnace feeding is heated and solidified to obtain the large grid barrel. The method can ensure the full infiltration of the residual dead angle of the prefabricated part of the grid cylinder under the condition of higher required fiber volume content, reduce the air holes in the product, improve the product quality and ensure that the porosity of the product is lower than 2 percent.

Description

Large grid cylinder and vacuum-assisted RTM (real time kinematic) forming method thereof
Technical Field
The application relates to the technical field of composite material forming, in particular to a large-scale grating cylinder and a vacuum-assisted RTM forming method suitable for the large-scale grating cylinder.
Background
As an innovative material, the composite material has the advantages of designability, light weight, high strength, high modulus, stable chemical property, good mechanical property and the like, and is widely applied to various fields of national economy. In the age of rapid development of aerospace industry, the aerospace industry aims at the huge advantages of composite materials, in the projects of space stations, manned lunar climbing and the like, large-scale composite material grid barrels with large size and large bearing characteristics are gradually developed, and the bearing efficiency and the bearing capacity of a large-scale grid structure can be improved through winding sequence, layering angles, layer numbers and process design. The low expansion target of the structural member in all directions can be achieved through winding and layering design, the light weight can be achieved, and meanwhile, high structural rigidity can be maintained under high-low temperature alternation in the service process. The large composite material grating cylinder has long molding period, and the dry winding preformed piece is preferable in the molding method, but the porosity is high, so that the molding quality of the product cannot be ensured.
Disclosure of Invention
Aiming at the defects in the prior art, the application aims to provide a vacuum-assisted RTM forming method suitable for a large grid barrel. So as to solve the problem of long product forming period, reduce product pores and ensure product quality.
The application aims at realizing the following scheme:
a vacuum-assisted RTM molding method suitable for a large grid cylinder comprises the following steps:
s1, manufacturing a vacuum bag along the molding surface of a mold by using a grid cylinder product prefabricated member;
step S2, connecting a glue outlet tank through a plurality of glue outlets of the cylinder body, and vacuumizing; the glue outlet tank is provided with a glue solution storage function, a vacuum system is protected, the glue outlet tank is used as a glue injection device for pressurizing in the subsequent direction, and the vacuum degree of the product is monitored by adopting a measurement mode of suction measurement and separation;
s3, injecting glue into the grid cylinder prefabricated member from the bottom to the top in a layered mode, when the height of the layer (the first layer) and the circumferential glue injection are finished, and the glue outlet of the second layer starts to be out, controlling the conversion from vacuumizing to RTM glue injection of the glue outlet through a three-way switching valve by a plurality of glue outlets of the second layer, finishing the process from the bottom to the top in a layered mode through an annular runner, and controlling the glue injection rate until the top is completely soaked and the glue outlet starts to be out; setting observation intervals along the height direction of the barrel section of the grid barrel prefabricated member, the tank bodies of the glue inlet tank and the glue outlet tank, the pipeline flow channels and the like, monitoring the glue injection condition in real time, and adjusting the glue injection rate accordingly;
s4, when a large amount of glue is discharged from a glue outlet at the top of the grid cylinder prefabricated member, reversely pressurizing the glue from the glue outlet of the glue discharge tank to the inside of the grid cylinder prefabricated member; fiber infiltration is increased, and air holes are reduced;
and S5, closing the interface of the glue injection pipeline, continuously vacuumizing the glue outlet, and further removing air holes until the subsequent furnace feeding is heated and solidified to obtain the large grid barrel.
Preferably, in the step S2, the vacuum degree of the product is also monitored by adopting a measurement mode of separated suction measurement.
Preferably, in the step S2, the vacuum degree of the separated product is less than or equal to-0.097 MPa.
Preferably, in the step S3, the glue injection rate is completed layer by layer according to the height of 200mm/4h of each layer.
Preferably, in the step S3, the resin system used for injecting the glue is an epoxy TDE-85 resin system, and the normal temperature viscosity is 200mpa·s to 300mpa·s.
Preferably, in the step S3, the grid cylinder prefabricated member is subjected to glue injection by 10 layers from bottom to top.
Preferably, in the step S4, the pressure of the reverse pressurization is 0.1MPa.
Preferably, the basic properties of the resin casting body adopted by the large grid barrel are as follows: the tensile strength is more than or equal to 55MPa, and the tensile modulus is more than or equal to 3.5GPa; the bending strength is more than or equal to 110MPa, and the bending modulus is more than or equal to 3.5GPa.
Preferably, the grid cylinder prefabricated part has the diameter of phi 3800mm and the height of 2000mm.
Preferably, 30 glue injection ports are uniformly arranged in the height direction and the circumferential direction of the grid cylinder prefabricated member.
Compared with the prior art, the application has the following beneficial effects:
1. the method of the application not only can solve the problem of the applicability period of wet winding resin under the condition of long winding period, but also can reduce the pores between the product fiber and the resin and ensure the molding quality of the product.
2. According to the method, the multiple glue outlets are connected with the glue outlet tank for vacuumizing, so that the vacuumizing efficiency is improved, and the authenticity and accuracy of the vacuum degree of the product are improved by adopting a vacuumizing separation method;
3. according to the method, the problem of short resin pot life of the wet winding piece can be perfectly solved by using the dry winding post-injection glue.
4. The method of the application adopts the measures of layer-by-layer glue injection and reverse pressing, can ensure the full infiltration of the residual dead angle of the prefabricated part of the grating cylinder under the condition of higher required fiber volume content, further reduces the air holes in the product, improves the quality of the grating cylinder product, ensures that the porosities of two products molded by the method meet the requirement of being superior to 2 percent in design, and is lower than the index of 3 to 4 percent of the porosities of the conventional RTM products. The porosity of the product is lower than 2%. The ultrasonic nondestructive inspection device is used for detecting the material, meets the C-level standard in GJB2895, and has stable molding quality.
Drawings
Other features, objects and advantages of the present application will become more apparent upon reading of the detailed description of non-limiting embodiments, given with reference to the accompanying drawings in which:
FIG. 1 is a schematic diagram of a grid cylinder mold glue injection system according to the present application.
FIG. 2 is a schematic view of the injection port of the grid cylinder mold of the present application.
Detailed Description
The present application will be described in detail with reference to specific examples. The following examples will assist those skilled in the art in further understanding the present application, but are not intended to limit the application in any way. It should be noted that variations and modifications could be made by those skilled in the art without departing from the inventive concept. These are all within the scope of the present application.
The present application will be described in detail with reference to specific embodiments and fig. 1 and 2.
Examples
A vacuum-assisted RTM molding method suitable for a large grid cylinder comprises the following steps:
s1, manufacturing a vacuum bag from a grid cylinder product prefabricated member to an outer flange surface by using a pressure equalizing plate and other auxiliary materials;
s2, connecting 30 glue injection ports 2 and three glue outlet ports 1 (as shown in figure 2, 3 glue injection ports are uniformly distributed along the circumferential direction, ten glue outlet ports are formed in each row, and the vacuum degree of a product is monitored by adopting a measurement mode of sampling and measuring separation) with a vacuum pipeline interface 3 of a glue outlet tank for vacuumizing; wherein, 3 glue outlets 1 are only used for glue outlet and are arranged at the positions of the nodes where the glue outlet is difficult;
s3, injecting glue into 10 layers of grid cylinder prefabricated parts from bottom to top, starting to discharge the glue from an outlet of a glue injection tank 6, connecting 3 glue injection ports of a bottom flange of a product mold through a three-way switching valve, wherein 3 rows of cylinder bodies are divided into 30 glue injection ports (as shown in FIG. 2, 3 rows of glue injection ports are uniformly distributed along the circumferential direction, 10 glue injection ports are arranged in each row, and meanwhile, the function of the glue injection ports) are kept in a vacuumizing state, when three glue outlet ports of a second layer of the product in the circumferential direction start to discharge the glue, switching from vacuumizing to RTM glue injection of the second layer of the glue outlet ports is controlled through a three-way valve switch, finishing from bottom to top by level through an annular runner, respectively controlling the glue injection time to be 200mm/4h according to the height of each layer, finishing level by level until the top is completely soaked and starting to discharge the glue;
s4, arranging glass observation windows 5 on the barrel section of the grid barrel prefabricated member along the height direction, the glue injection tank body and the glue outlet tank body, using a transparent pipeline 7 as an observation section for a pipeline runner, monitoring the glue injection condition in real time, and adjusting the glue injection rate accordingly;
s5, when a large amount of glue is discharged from a glue outlet at the top of the grid cylinder prefabricated member, pressurizing the glue outlet tank 4 reversely by 0.1MPa, pressurizing the glue solution of the glue outlet tank reversely from 33 paths of vacuum pipelines of the glue outlet to the inside of the grid cylinder, maintaining the pressure for 3 hours, increasing fiber infiltration, and reducing air holes;
s6, closing an interface of the glue injection pipeline, continuously vacuumizing a glue outlet, and further removing air holes until the glue outlet is heated and solidified after the glue inlet is subsequently fed into a furnace, wherein the vacuum degree is less than or equal to-0.097 MPa;
the application discloses a vacuum auxiliary RTM forming method suitable for a large grid barrel, wherein the grid barrel is a large composite material part with the diameter phi 3800mm and the height 2000mm and composed of variable density grid ribs, a skin and a flange. In the method, the vacuum pumping efficiency is improved by adopting a plurality of glue outlets to connect the glue outlet tanks for vacuum pumping, and the authenticity and the accuracy of the vacuum degree of the product are improved by adopting a method of vacuum testing and separation; the problem of short resin pot life of the wet winding piece can be perfectly solved by using the dry winding post-injection glue. The measures of layer-by-layer glue injection and reverse pressing are applied, so that under the condition of high-requirement fiber volume content, the full infiltration of residual dead angles of the prefabricated parts of the grid cylinder can be ensured, the air holes in the product are further reduced, the quality of the product of the grid cylinder is improved, and the porosity of the product is lower than 2%.
In the description of the present application, it should be understood that the terms "upper", "lower", "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outer", etc. indicate orientations or positional relationships based on the orientations or positional relationships shown in the drawings, are merely for convenience in describing the present application and simplifying the description, and do not indicate or imply that the devices or elements referred to must have a specific orientation, be configured and operated in a specific orientation, and thus should not be construed as limiting the present application.
The foregoing describes specific embodiments of the present application. It is to be understood that the application is not limited to the particular embodiments described above, and that various changes or modifications may be made by those skilled in the art within the scope of the appended claims without affecting the spirit of the application. The embodiments of the application and the features of the embodiments may be combined with each other arbitrarily without conflict.

Claims (6)

1. The vacuum-assisted RTM forming method for the large grid cylinder is characterized by comprising the following steps of:
s1, manufacturing a vacuum bag along the molding surface of a mold by using a grid cylinder product prefabricated member;
step S2, connecting a glue outlet tank through a plurality of glue outlets of the cylinder body, and vacuumizing;
s3, injecting glue to the grid cylinder prefabricated member from bottom to top in a layered mode, when the first layer of height direction and the annular glue injection are completed, and the glue outlet of the second layer begins to discharge glue, controlling the glue outlet of the second layer to switch from vacuumizing to RTM glue injection through a three-way switching valve, and completing the process from bottom to top in a layered mode through an annular runner until the top is completely soaked and glue discharge begins; the glue injection rate is finished layer by layer according to the height of each layer of 200mm/4 h; the resin system used for injecting glue is an epoxy TDE-85 resin system, and the normal temperature viscosity is 200 mPas to 300 mPas; injecting glue into 10 layers of the grid cylinder prefabricated member from bottom to top, and uniformly arranging 30 glue injection ports in the height direction and the circumferential direction of the grid cylinder prefabricated member;
s4, when a large amount of glue is discharged from a glue outlet at the top of the grid cylinder prefabricated member, reversely pressurizing the glue from the glue outlet of the glue discharge tank to the inside of the grid cylinder prefabricated member; the pressure of the reverse pressurization is 0.1MPa;
and S5, closing the interface of the glue injection pipeline, and continuously vacuumizing the glue outlet until the glue outlet is heated and solidified in a subsequent furnace to obtain the large grid barrel.
2. The method for forming a large grid cylinder according to claim 1, wherein in step S2, the vacuum degree of the product is monitored by a measurement method of separation by suction measurement.
3. The method for vacuum assisted RTM molding of a large grating cylinder according to claim 2, wherein in the step S2, the vacuum degree of the vacuum separation monitoring product is less than or equal to-0.097 MPa.
4. The method for vacuum assisted RTM molding of large grating cylinders according to claim 1, wherein the basic properties of the resin casting body used for the large grating cylinder preform satisfy: the tensile strength is more than or equal to 55MPa, and the tensile modulus is more than or equal to 3.5GPa; the bending strength is more than or equal to 110MPa, and the bending modulus is more than or equal to 3.5GPa.
5. The method of vacuum assisted RTM molding of large grating cylinders according to claim 1, wherein the grating cylinder preform is 3800mm in diameter and 2000mm in height.
6. A large grating cylinder prepared by the vacuum assisted RTM molding method of any one of claims 1 to 5.
CN202111022904.0A 2021-09-01 2021-09-01 Large grid cylinder and vacuum-assisted RTM (real time kinematic) forming method thereof Active CN113799414B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202111022904.0A CN113799414B (en) 2021-09-01 2021-09-01 Large grid cylinder and vacuum-assisted RTM (real time kinematic) forming method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202111022904.0A CN113799414B (en) 2021-09-01 2021-09-01 Large grid cylinder and vacuum-assisted RTM (real time kinematic) forming method thereof

Publications (2)

Publication Number Publication Date
CN113799414A CN113799414A (en) 2021-12-17
CN113799414B true CN113799414B (en) 2023-08-22

Family

ID=78942194

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202111022904.0A Active CN113799414B (en) 2021-09-01 2021-09-01 Large grid cylinder and vacuum-assisted RTM (real time kinematic) forming method thereof

Country Status (1)

Country Link
CN (1) CN113799414B (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114589943B (en) * 2022-03-23 2023-08-04 成都飞机工业(集团)有限责任公司 T-shaped rib glue injection mold for resin transfer molding

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101352925A (en) * 2008-08-25 2009-01-28 中国船舶重工集团公司第七二五研究所 Vacuum auxiliary molding technique produced by high-facade composite material for ship
CN105398064A (en) * 2015-11-30 2016-03-16 南京航空航天大学 Integral molding method and molding die for fiber-reinforced resin-based composite round pipe
CN111421858A (en) * 2020-05-18 2020-07-17 北京玻钢院复合材料有限公司 Composite material launching box and preparation method thereof
CN111572065A (en) * 2020-06-24 2020-08-25 福建省华辰管业科技有限公司 Improved glue injection mold for fiber woven winding pultrusion pipeline

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6818159B2 (en) * 2000-03-17 2004-11-16 Deutsches Zentrum Fuer Luft-Und Raumfahrt E.V. Process for the production of a composite consisting of a fiber reinforced material

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101352925A (en) * 2008-08-25 2009-01-28 中国船舶重工集团公司第七二五研究所 Vacuum auxiliary molding technique produced by high-facade composite material for ship
CN105398064A (en) * 2015-11-30 2016-03-16 南京航空航天大学 Integral molding method and molding die for fiber-reinforced resin-based composite round pipe
CN111421858A (en) * 2020-05-18 2020-07-17 北京玻钢院复合材料有限公司 Composite material launching box and preparation method thereof
CN111572065A (en) * 2020-06-24 2020-08-25 福建省华辰管业科技有限公司 Improved glue injection mold for fiber woven winding pultrusion pipeline

Also Published As

Publication number Publication date
CN113799414A (en) 2021-12-17

Similar Documents

Publication Publication Date Title
CN107215039B (en) Sandwich composite material and preparation method thereof
KR101151966B1 (en) Rtm molding method and device
Li et al. Process and performance evaluation of the vacuum-assisted process
US8834782B2 (en) Composite structures and methods of making same
CN102990940B (en) Composite stiffened liquid molding device and method
CN104589669B (en) A kind of composite liquid pressure forming method
CN101143492A (en) Compression type RTM forming method
CN113799414B (en) Large grid cylinder and vacuum-assisted RTM (real time kinematic) forming method thereof
CN105881932A (en) Method for forming large-sized composite material box
CN103273662A (en) Preparation method of low heat expansion carbon fiber reinforced resin matrix composite material mold
CN105479773B (en) Liquid resin transfer molding system and forming method thereof
US9481116B2 (en) Method and manufacturing device for manufacturing a fiber compound sandwich component
CN105398064A (en) Integral molding method and molding die for fiber-reinforced resin-based composite round pipe
US20090039566A1 (en) Composite structures and methods of making same
CN103448260A (en) Connecting method of shell plate made from composites and metal member
CN102990944A (en) Composite material vacuum bag forming method
CN105216342A (en) Automobile-used carbon fibre composite shape for hat beam preparation method and mould
CN104742382A (en) Pressure-assisted VARI (vacuum assisted resin infusion) forming device and method
CN1915154A (en) Composite compound bathtub, and fabricating technique
CN112497786A (en) Forming method and die for carbon fiber automobile parts
US20150014898A1 (en) Device and method for producing a moulded part from a composite material
CN205112423U (en) Automobile -used carbon -fibre composite shape for hat roof beam preparation mould
AU2011239964B2 (en) Method and apparatus for moulding parts made from composite materials
CN102179942A (en) Liquid forming method of composite material for closed die built-in resin flow distributor
CN107901448B (en) Large-diameter composite skirt compression curing method

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant