Full-automatic graphite is cleared up tail gas processing apparatus for appearance
Technical Field
The invention relates to the technical field of tail gas treatment, in particular to a tail gas treatment device for a full-automatic graphite digestion instrument.
Background
The graphite digestion instrument is a common laboratory device, is used for sample pretreatment, sample pretreatment links in various fields of quality inspection, environment, food, biology, agriculture, mining industry, industry and the like, is applied to baking, drying, digestion and the like of samples, and can also be used for replacing the samples treated by the microwave digestion instrument to dare acid.
In chemical experiments, gases which are toxic and harmful to human bodies are often generated, once the gases are inhaled by people, serious threats can be brought to the life health of people, aldehyde gases and acid gases have great harm to the human bodies and great damage to the environment, a fume cupboard is normally used for collecting and treating tail gas in general experiments, the fume cupboard is generally provided with a treatment box for storing purifying liquid to achieve a treatment effect, but the treatment box has a poor absorption effect on the aldehyde gases and has a poor neutralization effect on gases with low chemical valence, such as nitrogen monoxide gases, sulfur trioxide gases and the like which are generated or volatilized in certain reactions, the gases with low chemical valence, such as the nitrogen monoxide gases, the sulfur trioxide and the like, can be completely and quickly neutralized by oxidation, the gases with low chemical valence, such as the nitrogen monoxide gases, the sulfur trioxide and the like are directly introduced into the treatment box, the treatment time can be delayed, and the neutralization liquid is wasted, thereby affecting the treatment effect.
Disclosure of Invention
The invention aims to provide a tail gas treatment device for a full-automatic graphite digestion instrument, which aims to solve the problems in the background technology.
In order to achieve the purpose, the invention provides the following technical scheme:
a tail gas treatment device for a full-automatic graphite digestion instrument comprises a graphite digestion instrument body, a digestion working area is arranged on the graphite digestion instrument body, the graphite digestion instrument body is arranged on the upper surface of the bottom plate, the two sides of the upper surface of the bottom plate are fixedly connected with top plates through symmetrical side plates, the upper surface of the top plate is fixedly provided with a treatment box through a bracket, the bottom of the treatment box is communicated with the position right above the digestion working area through an air exhaust assembly, and the top of the treatment box is provided with an air outlet for discharging treated gas, the air outlet is fixedly communicated with a neutralization tank through a pipeline, a dust filtering net and an active carbon filtering net are respectively and fixedly connected with the inner lower side and the inner upper side of the treatment box, a photocatalyst plate is arranged between the dust filter screen and the active carbon filter screen, the photocatalyst plate is fixedly arranged at the corresponding position of the inner wall of the treatment box, and an ultraviolet lamp is also arranged right above the photocatalyst plate and is fixedly arranged on the inner side wall of the treatment box.
As a further scheme of the invention: the projection of the ultraviolet lamp on the upper surface of the photocatalyst plate is just coincided with the middle line of the photocatalyst plate.
As a further scheme of the invention: the photocatalyst plate consists of two layers of three-dimensional honeycomb ceramic nets with titanium dioxide coatings loaded on the surfaces and porous particles loaded with nano titanium dioxide and filled between the two layers of honeycomb ceramic nets.
As a further scheme of the invention: the neutralizing tank is fixedly arranged on the upper surface of the top plate, strong acid liquid and strong alkali liquid are arranged in the neutralizing tank, and a plurality of air outlet pipes are arranged at the top of the neutralizing tank.
As a further scheme of the invention: the subassembly of bleeding is including dispelling the gas collecting cover that sets up directly over the working area, the interior middle part of gas collecting cover has the fan through mounting bracket fixed mounting, and the small-bore end of gas collecting cover is fixed to be communicated with global down in the activity ring, the last global fixed connection plastic bellow's of activity ring one end, and plastic bellow's the other end is vertical global down of up and the solid fixed ring of fixed connection, and solid fixed ring's last fixed surface installs the lower surface at the roof and corresponds the position, gu fixed ring inner circle corresponds the roof surface simultaneously and sets up the trompil that supplies the air duct lower extreme to be linked together, the sealed and fastening intercommunication in top of air duct is on the air inlet that the bottom of handling the case was seted up, still be provided with the adjustment.
As a further scheme of the invention: the adjustment subassembly includes activity ring upper surface both sides fixed connection's one end of acting as go-between, and the other end of acting as go-between wears the duplex winding from the line hole of seting up on the roof and connects on the bobbin, and two bobbins are fixed the dress respectively in the both sides of changeing the post, and the commentaries on classics post rotates and runs through on the air duct, and the one end of changeing the post passes through coupling joint on gear motor's output shaft, gear motor fixed mounting is at the upper surface of roof.
As a further scheme of the invention: the perforation that supplies the rotary column to run through is seted up to gas duct week portion bilateral symmetry position, and the inner peripheral portion complex connection of perforation has the sealing ring of round, and the inner peripheral fixed mounting of sealing ring has the bearing, and the bearing is used for rotating suit rotary column.
As a further scheme of the invention: the interior bottom of handling the case has the draught fan through mounting bracket fixed mounting, the inlet end of draught fan down and with air duct top intercommunication, and the end of giving vent to anger of draught fan directly over towards, the top of draught fan still is provided with a horizontal rotation axis simultaneously, the both ends of rotation axis are all rotated and are connected in the corresponding inner wall of handling the case, and the fixed cover of peripheral portion at the rotation axis is equipped with the paddle, the paddle is located the draught fan and gives vent to anger directly over the end, it gets rid of the one end of rope to go back fixed connection in the both sides of rotation axis simultaneously, and the other end fixedly connected.
As a further scheme of the invention: the tail end of each blade of the paddle is provided with a wind gathering bent part bent towards one side.
As a further scheme of the invention: the length of the throwing rope is larger than the shortest distance from the rotating shaft to the dust filter screen.
Compared with the prior art, the invention has the beneficial effects that:
1. according to the invention, the tail gas generated in the work process of the digestion work area is pumped into the treatment box through the air pumping assembly, the tail gas firstly passes through the dust filtering net, larger particulate matters such as dust and the like in the tail gas are filtered, then passes through the photocatalyst plate under the irradiation of the ultraviolet lamp, harmful gases in the tail gas are catalyzed and oxidized, such as aldehyde gases, and the photocatalyst plate has a strong oxidation function, so that the tail gas can oxidize acid-containing gases containing substances such as nitrogen, sulfur and the like into stable nitrogen-containing oxides and sulfur-containing oxides with the highest chemical valence, then the tail gas is reacted through strong acid and strong base in the neutralization tank in sequence, and finally the treated gas is discharged to the atmosphere, so that the effect of automatic purification is achieved.
2. According to the invention, the speed reduction motor is started to drive the rotary column and the bobbin to rotate, then the bobbin is rotated and wound, the pull wire is utilized to upwards pull the movable ring, the movable ring is lifted and simultaneously can drive the gas gathering cover to synchronously lift, and the height of the gas gathering cover relative to the digestion working area can be adjusted within a certain range due to the scalability of the plastic corrugated pipe, so that the gas gathering cover can be adjusted to a height which does not interfere with a normal experiment and can suck tail gas as much as possible according to the use requirements of different test tube heights in the digestion working area, and the practicability of the invention is greatly improved.
Drawings
FIG. 1 is a schematic structural view of the present invention;
FIG. 2 is a schematic view of the structure of a photocatalyst plate in the present invention;
FIG. 3 is a schematic view of the structure of the airway tube of the present invention;
FIG. 4 is an enlarged view of the structure at A in FIG. 1;
FIG. 5 is a schematic view of the structure of a blade according to the present invention;
fig. 6 is a schematic view of the installation of the gas collecting cover and the plastic corrugated pipe in the present invention.
In the figure: 1. a graphite digestion instrument body; 2. clearing up a working area; 3. a base plate; 4. a side plate; 5. a top plate; 6. a gas gathering cover; 7. a fan; 8. a pull wire; 9. a fixing ring; 10. a movable ring; 11. a plastic bellows; 12. an air inlet; 13. an induced draft fan; 14. a paddle; 15. a rotating shaft; 16. a metal bead; 17. a treatment tank; 18. an active carbon filter screen; 19. an air outlet; 20. an ultraviolet lamp; 21. a photocatalyst plate; 22. a dust filter screen; 23. an air duct; 24. a bobbin; 25. a reduction motor; 26. a honeycomb ceramic mesh; 27. porous particles; 28. turning the column; 29. perforating; 30. a seal ring; 31. a bearing; 32. a neutralization tank; 33. and (4) throwing the rope.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Referring to fig. 1 to 6, in the embodiment of the present invention, a tail gas treatment device for a full-automatic graphite digestion instrument includes a graphite digestion instrument body 1 having a digestion work area 2, where the digestion work area 2 is a position where the graphite digestion instrument body 1 generates tail gas when working, the graphite digestion instrument body 1 is disposed on an upper surface of a bottom plate 3, two sides of the upper surface of the bottom plate 3 are fixedly connected with top plates 5 through symmetrical side plates 4, the upper surface of the top plate 5 is fixedly mounted with a treatment box 17 through a bracket, the bottom of the treatment box 17 is communicated with the right above the digestion work area 2 through an air exhaust assembly, the top of the treatment box 17 is provided with an air outlet 19 for discharging treated gas, the air outlet 19 is fixedly communicated with a neutralization tank 32 through a pipeline, a dust filtering net 22 and an activated carbon filtering net 18 are respectively and fixedly connected with an inner lower side and an upper side of the treatment box 17, a photocatalyst plate 21 is arranged between the dust filter 22 and the activated carbon filter 18, the photocatalyst plate 21 is fixedly arranged at a corresponding position on the inner wall of the treatment box 17, an ultraviolet lamp 20 is arranged right above the photocatalyst plate 21, the ultraviolet lamp 20 is fixedly arranged at the position on the inner side wall of the treatment box 17, exhaust gas generated during the operation of the digestion work area 2 is pumped into the treatment box 17 through an exhaust component, the exhaust gas firstly passes through the dust filter 22, dust and other large particulate matters in the exhaust gas are filtered, then the exhaust gas passes through the photocatalyst plate 21 under the irradiation of the ultraviolet lamp 20, harmful gases in the exhaust gas are catalyzed and oxidized, such as aldehyde gases, and due to the strong oxidation function of the photocatalyst plate 21, the exhaust gas containing nitrogen, sulfur and other substances can be oxidized into stable nitrogen and sulfur containing oxides with the highest chemical valence, and then the exhaust gas sequentially passes through strong acid and strong base in the neutralization tank to react, finally, the treated gas is discharged to the atmosphere, so that the effect of automatic purification is achieved.
Further, the projection of the ultraviolet lamp 20 on the upper surface of the photocatalyst plate 21 is exactly coincident with the central line of the photocatalyst plate 21, so that the light source emitted by the ultraviolet lamp 20 can be irradiated on the photocatalyst plate 21 comprehensively and uniformly, the catalysis rate of the porous particles 27 in the photocatalyst plate 21 is increased, and the catalytic oxidation effect on harmful gases is improved.
Further, the photocatalyst plate 21 is composed of two layers of three-dimensional honeycomb ceramic nets 26 with titanium dioxide coatings loaded on the surfaces and porous particles 27 filled between the two layers of honeycomb ceramic nets 26 and loaded with nano titanium dioxide, and the honeycomb ceramic nets 26 have the effect of increasing the contact area with airflow, so that the reaction is more sufficient, and the purification treatment effect is improved.
Further, the neutralization tank 32 is fixedly arranged on the upper surface of the top plate 5, strong acid liquor and strong alkali liquor are arranged in the neutralization tank 32, and a plurality of air outlet pipes are arranged at the top of the neutralization tank 32.
Further, the air exhaust assembly comprises an air collecting cover 6 arranged right above the digestion working area 2, a fan 7 is fixedly arranged in the middle of the air collecting cover 6 through a mounting frame, a small-caliber end of the air collecting cover 6 is fixedly communicated with the lower peripheral surface of the movable ring 10, one end of a plastic corrugated pipe 11 is fixedly connected with the upper peripheral surface of the movable ring 10, the other end of the plastic corrugated pipe 11 is vertically upward and fixedly connected with the lower peripheral surface of the fixed ring 9, the upper surface of the fixed ring 9 is fixedly arranged at a corresponding position of the lower surface of the top plate 5, meanwhile, an opening for communicating the lower end of an air duct 23 is formed in the inner ring of the fixed ring 9 corresponding to the surface of the top plate 5, the top end of the air duct 23 is hermetically and fixedly communicated with an air inlet 12 formed in the bottom of the processing box 17, when the graphite digestion instrument body 1 works, the fan 7 is immediately started, the air collecting cover, then the gas is introduced into a treatment box 17 for purification treatment, and an adjusting component for adjusting the height of the gas gathering cover 6 is also arranged on the top plate 5.
Still further, the adjusting assembly includes one end of a stay wire 8 fixedly connected with both sides of the upper surface of the movable ring 10, the other end of the stay wire 8 is threaded through a wire hole opened on the top plate 5 and wound on a bobbin 24, two bobbins 24 are fixedly sleeved on both sides of a rotary post 28 respectively, the rotary post 28 is rotatably penetrated on the air duct 23, one end of the rotary post 28 is connected on an output shaft of a speed reducing motor 25 through a coupling, the speed reducing motor 25 is fixedly installed on the upper surface of the top plate 5, the purpose is that the rotary post 28 and the bobbin 24 are driven to rotate by starting the speed reducing motor 25, then in the process of the rotary winding of the bobbin 24, the movable ring 10 is pulled upwards by the stay wire 8, the movable ring 10 is lifted and simultaneously can drive the gas gathering cover 6 to synchronously lift, and the height of the gas gathering cover 6 relative to the digestion working area 2 can be adjusted within a certain range due to the scalability of the plastic corrugated pipe 11, therefore, the gas gathering cover 6 can be adjusted to a height which does not hinder a normal experiment and can pump in tail gas as far as possible according to the use requirements of different test tube heights on the digestion working area 2, and the practicability of the invention is greatly improved.
Still further, the bilateral symmetry position of the periphery of the air duct 23 is provided with a through hole 29 for the rotary column 28 to pass through, the inner periphery of the through hole 29 is compositely connected with a circle of sealing ring 30, the inner periphery of the sealing ring 30 is fixedly provided with a bearing 31, the bearing 31 is used for rotatably sleeving the rotary column 28, the sealing ring 30 has a sealing effect, the condition that the tail gas in the air duct 23 escapes can be avoided to the maximum extent, and the normal gas transmission function of the air duct 23 cannot be hindered.
Further, an induced draft fan 13 is fixedly installed at the inner bottom of the processing box 17 through an installation frame, an air inlet end of the induced draft fan 13 faces downwards and is communicated with the top of the air guide tube 23, an air outlet end of the induced draft fan 13 faces towards the upper side, a transverse rotating shaft 15 is further arranged above the induced draft fan 13, two ends of the rotating shaft 15 are rotatably connected to corresponding inner walls of the processing box 17, blades 14 are fixedly sleeved on the outer periphery of the rotating shaft 15, the blades 14 are located right above the air outlet end of the induced draft fan 13, one ends of throwing ropes 33 are fixedly connected to two sides of the rotating shaft 15, metal beads 16 are fixedly connected to the other ends of the throwing ropes 33, so that the blades 14 can drive the rotating shaft 15 to rotate by means of air flow blown by the induced draft fan 13, the throwing ropes 33 can intermittently flap the metal beads 16 onto the dust filter 22, and normal ventilation and dust-cutting functions are prevented, and after a period of time, the treatment box 17 is opened to clean and replace the dust filter 22, so that the actual use effect is improved.
Still further, the wind-gathering bent portion that bends to one side is all formed at each blade end of the paddle 14, and its purpose is that can carry out certain gathering effect to the air current that blows, improve the blade windage in the paddle 14 to improve the driving force, realize that wind drives the purpose that paddle 14 smoothly rotates.
Further, the length of the throwing rope 33 is greater than the shortest distance between the rotating shaft 15 and the dust filter 22, so that the throwing rope 33 can drive the metal beads 16 to throw and hit the lower surface of the dust filter 22, the dust filter 22 slightly vibrates, and large-particle impurities blocked on the dust filter 22 are shaken off with a certain probability.
In the description of the present invention, it should be noted that, unless otherwise explicitly specified or limited, the terms "mounted," "connected," and "connected" are to be construed broadly, e.g., as meaning either a fixed connection, a removable connection, or an integral connection; can be mechanically or electrically connected; they may be connected directly or indirectly through intervening media, or they may be interconnected between two elements. The specific meaning of the above terms in the present invention can be understood by those of ordinary skill in the art through specific situations.
Although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that various changes in the embodiments and/or modifications of the invention can be made, and equivalents and modifications of some features of the invention can be made without departing from the spirit and scope of the invention.