CN112546936A - Temperature monitoring system for inorganic-organic composite material mixing equipment - Google Patents

Temperature monitoring system for inorganic-organic composite material mixing equipment Download PDF

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Publication number
CN112546936A
CN112546936A CN202011368435.3A CN202011368435A CN112546936A CN 112546936 A CN112546936 A CN 112546936A CN 202011368435 A CN202011368435 A CN 202011368435A CN 112546936 A CN112546936 A CN 112546936A
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CN
China
Prior art keywords
temperature
tank
stirring
modification
monitoring system
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Pending
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CN202011368435.3A
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Chinese (zh)
Inventor
刘刚
孙江波
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Beijing Aikemet New Material Development Co ltd
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Beijing Aikemet New Material Development Co ltd
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Priority to CN202011368435.3A priority Critical patent/CN112546936A/en
Publication of CN112546936A publication Critical patent/CN112546936A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00Other mixers; Mixing plants; Combinations of mixers
    • B01F33/80Mixing plants; Combinations of mixers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/808Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with stirrers driven from the bottom of the receptacle
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/90Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with paddles or arms 
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00Other mixers; Mixing plants; Combinations of mixers
    • B01F33/80Mixing plants; Combinations of mixers
    • B01F33/81Combinations of similar mixers, e.g. with rotary stirring devices in two or more receptacles
    • B01F33/811Combinations of similar mixers, e.g. with rotary stirring devices in two or more receptacles in two or more consecutive, i.e. successive, mixing receptacles or being consecutively arranged
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00Other mixers; Mixing plants; Combinations of mixers
    • B01F33/80Mixing plants; Combinations of mixers
    • B01F33/836Mixing plants; Combinations of mixers combining mixing with other treatments
    • B01F33/8362Mixing plants; Combinations of mixers combining mixing with other treatments with chemical reactions
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/20Measuring; Control or regulation
    • B01F35/21Measuring
    • B01F35/211Measuring of the operational parameters
    • B01F35/2115Temperature
    • B01F35/21151Temperature using infrared radiation thermometer or pyrometer or infrared sensors for temperature measurement without contact

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Glanulating (AREA)
  • Accessories For Mixers (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The invention relates to the field of organic inorganic powder particle preparation, and particularly provides a temperature monitoring system for inorganic-organic composite material mixing equipment, which comprises: a first high-temperature modification stirring tank (1), a second high-temperature modification stirring tank (2) and a third high-temperature mixing reaction tank (3); the first high-temperature modification stirring tank is provided with a first temperature sensing device, the second high-temperature modification stirring tank is provided with a second temperature sensing device, and the third high-temperature mixing reaction tank is provided with a third temperature sensing device. The invention realizes the full composite reaction of the inorganic powder material and the organic material by carrying out the initial high-temperature stirring modification, the thorough high-temperature stirring modification and the thorough mixing reaction on the inorganic powder material to form the organic-inorganic composite material. In the process from modification stirring to mixing reaction, the state and temperature of the materials are accurately grasped, so that thorough modification and thorough reaction are realized, and the yield and the working efficiency are ensured.

Description

Temperature monitoring system for inorganic-organic composite material mixing equipment
Technical Field
The invention relates to the field of organic inorganic powder particle preparation, in particular to a temperature monitoring system for inorganic-organic composite material mixing equipment for mixing organic powder and inorganic powder in the preparation process of organic inorganic powder particles.
Background
In the preparation process of the organic inorganic powder particles, because inorganic powder needs to be stirred and modified at high temperature and to be mixed and reacted with organic materials, the inorganic powder and the organic powder need to be heated at high temperature, and the inorganic powder and the organic material need to be kept at high temperature before the reaction to form organic inorganic powder (i.e. organic powder) is completed, so as to ensure that the inorganic powder is fully modified and fully mixed and reacted with the organic material.
When the existing material mixing equipment is used for mixing two materials at high temperature, an independent temperature sensor or a thermometer is usually only arranged on a reaction kettle to monitor the temperature inside the reaction kettle, the temperature monitoring is usually only suitable for temperature detection of materials (such as liquid and the like) with larger volume or easy temperature detection, but for powder materials, the whole state and temperature condition of the materials in the reaction kettle cannot be accurately and effectively monitored only by arranging one temperature sensor or temperature timing, so that the monitoring effect is not ideal, and the subsequent operation cannot be carried out as reference.
Disclosure of Invention
The present invention is directed to solving at least one of the problems of the background art and to providing a temperature monitoring system for an inorganic-organic composite material mixing apparatus.
In order to achieve the above object, the present invention provides a temperature monitoring system for an inorganic-organic composite material mixing device, comprising: the system comprises a first high-temperature modification stirring tank, a second high-temperature modification stirring tank and a third high-temperature mixing reaction tank;
the first high-temperature modification stirring tank is provided with a first temperature sensing device, the second high-temperature modification stirring tank is provided with a second temperature sensing device, and the third high-temperature mixing reaction tank is provided with a third temperature sensing device.
According to one aspect of the invention, the first high-temperature modification stirring tank comprises a first tank body and a first cover body for covering the first tank body, and a first heating sleeve structure is arranged on the periphery of the first tank body.
According to one aspect of the invention, the first temperature sensing device comprises an infrared sensor disposed on the first cover and disposed facing the inner bottom of the first tank and a temperature sensor disposed on a side wall of the first tank.
According to an aspect of the present invention, the first temperature sensing means includes three temperature sensors provided at three positions of an upper portion, a middle portion and a lower portion of the side wall of the first tank, respectively.
According to one aspect of the invention, the second high-temperature modification stirring tank comprises a second tank body and a second cover body for covering the second tank body, and a second heating sleeve structure is arranged on the periphery of the second tank body.
According to one aspect of the invention, the second temperature sensing means comprises an infrared sensor disposed on the second cover and disposed facing the inner bottom of the second tank and a temperature sensor disposed on a side wall of the second tank.
According to an aspect of the present invention, the second temperature sensing means includes three temperature sensors provided at three positions of an upper portion, a middle portion and a lower portion of the side wall of the second tank, respectively.
According to one aspect of the invention, the third high-temperature mixing reaction tank comprises a third tank body and a third cover body for covering the third tank body, and a third heating sleeve structure is arranged on the periphery of the third tank body.
According to one aspect of the invention, the third temperature sensing device comprises an infrared sensor disposed on the third cover and disposed facing the inner bottom of the third tank and a temperature sensor disposed on a side wall of the third tank.
According to one aspect of the present invention, the first temperature sensing device includes an infrared sensor and a temperature sensor, wherein the infrared sensor is disposed on the first cover, and it is critical that the infrared sensor is disposed opposite to the bottom of the first tank, so as to monitor the state and temperature of the inorganic powder material from top to bottom of the first tank. Further, the temperature sensor is arranged on the side wall of the first tank body. Preferably, the first temperature sensing device includes three temperature sensors respectively disposed at three positions of an upper portion, a middle portion and a lower portion of the sidewall of the first tank. So set up, can be so that the inorganic powder material of being stirred by high temperature in the first jar body obtains comprehensive three-dimensional temperature monitoring for the temperature of the material that is in three positions about in the stirring process all can be monitored by accurate. The problem of when stirring inorganic powder material, because the accurate average temperature of the internal material of jar can't accurately be learnt when the powder volume of stirring is great, lead to the material not to conform to the demand at the internal preliminary modified stirring of first jar, carry out follow-up stirring preparation process after the ejection of compact and go wrong like this, lead to the reduction of product percent of pass is solved. Moreover, use infrared ray sensor at the internal mode from last to penetrating through stirring material of jar to monitoring jar internal material down, can further the accurate temperature condition and the modified state of learning jar internal all materials (including jar internal atomizing degree, loose degree and flight speed information etc.) through infrared ray sensor and three temperature sensor's cooperation like this, can obtain the accurate information of jar internal material, make the preliminary modification of material can reach the demand state, can not produce any problem that influences the product percent of pass during the ejection of compact.
According to one scheme of the invention, the second temperature sensing device comprises an infrared sensor and a temperature sensor, the infrared sensor is arranged on the second cover body, and the key point is that the infrared sensor needs to be arranged opposite to the bottom of the inner tank of the second tank body, so that the state and the temperature condition of the inorganic powder material of the whole second tank body from top to bottom can be monitored. Further, the temperature sensor is arranged on the side wall of the second tank body. Preferably, the second temperature sensing device includes three temperature sensors respectively disposed at three positions of an upper portion, a middle portion and a lower portion of the sidewall of the second tank. So set up, can be so that the inorganic powder material by high temperature stirring in the second jar body obtains comprehensive three-dimensional temperature monitoring for the temperature of the material that is in three positions about in the stirring process all can be monitored by accurate. The problem of when stirring inorganic powder material, because the accurate average temperature of the internal material of jar can't accurately be learnt when the powder volume of stirring is great, lead to the material inhomogeneous thorough in the internal modification stirring of second jar, carry out follow-up stirring preparation process after the ejection of compact and go wrong, lead to the reduction of product percent of pass is solved like this. Moreover, use infrared ray sensor at the internal mode from last to penetrating through stirring material of jar to monitoring jar internal material down, can further the accurate temperature condition and the modified state of learning jar internal all materials (including jar internal atomizing degree, loose degree and flight speed etc. information), like this through infrared ray sensor and three temperature sensor's cooperation, can obtain the accurate information of jar internal material, make the material modify thoroughly, can reach the demand state, can not produce any problem that influences the product percent of pass during the ejection of compact.
According to the scheme of the invention, the inorganic powder material is subjected to initial high-temperature stirring modification, thorough high-temperature stirring modification and thorough mixing reaction to realize the sufficient composite reaction of the inorganic powder material and the organic material so as to form the organic-inorganic composite material. The key point of the process is that the process is realized by a first temperature sensing device arranged on a first high-temperature modification stirring tank, a second temperature sensing device arranged on a second high-temperature modification stirring tank and a third temperature sensing device arranged on a third high-temperature mixing reaction tank respectively, and the state and the temperature of the materials are accurately grasped in the process from modification stirring to mixing reaction, so that complete modification and complete reaction are realized. Thus, the yield and the working efficiency are ensured.
Drawings
Fig. 1 schematically shows a structural view of a temperature monitoring system for an inorganic-organic composite material mixing apparatus according to an embodiment of the present invention.
Detailed Description
The technical solutions in the embodiments of the present invention are clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the scope of the present invention.
Fig. 1 schematically shows a structural view of a temperature monitoring system for an inorganic-organic composite material mixing apparatus according to an embodiment of the present invention. As shown in fig. 1, in the temperature monitoring system for an inorganic-organic composite material mixing apparatus according to the present invention, the inorganic-organic composite material mixing apparatus includes: a first high-temperature modification stirring tank 1, a second high-temperature modification stirring tank 2 and a third high-temperature mixing reaction tank 3. The temperature monitoring system also comprises: a first temperature sensing device is arranged on the first high-temperature modification stirring tank 1, a second temperature sensing device is arranged on the second high-temperature modification stirring tank 2, and a third temperature sensing device is arranged on the third high-temperature mixing reaction tank 3. So set up and to make first high temperature modified agitator tank 1, second high temperature modified agitator tank 2 and third high temperature mixing retort 3 all can obtain temperature monitoring, can guarantee like this that the material all possesses temperature monitoring at every stage of the in-process of modifying to mixing reaction, guarantee the temperature and the state of material in the within range that needs, guarantee material modification quality and abundant reaction, for example guarantee inorganic powder's abundant modification, and inorganic powder and organic material's abundant reaction form organic inorganic powder (be organic powder).
Further, as shown in fig. 1, in the present embodiment, the first high-temperature reforming agitation tank 1 includes a first tank 101 and a first lid 102 for closing the first tank 101. A first heating sleeve structure (not shown) is disposed on the periphery of the first tank 101, and the inorganic powder filled in the first high-temperature modified stirring tank 1 is heated at a high temperature by introducing a heating medium (e.g., heat transfer oil) into the first heating sleeve structure. The inorganic powder is stirred at high temperature in the first high-temperature modification stirring tank 1 to realize primary change of the original activity, and then the inorganic powder enters the second high-temperature modification stirring tank 2 in a high-temperature state.
Before entering the second high-temperature modification stirring tank 2, when the inorganic powder is subjected to high-temperature modification stirring in the first high-temperature modification stirring tank 1, the temperature and the state of the inorganic powder in the first tank 101 are monitored through the first temperature sensing device. Specifically, the first temperature sensing device includes an infrared sensor and a temperature sensor, wherein the infrared sensor is disposed on the first cover 102, and it is critical that the infrared sensor is disposed opposite to the bottom of the first tank 101, so as to monitor the state and temperature of the inorganic powder material from top to bottom of the first tank 101. Further, the temperature sensor is disposed on a side wall of the first tank 101. Preferably, the first temperature sensing means includes three temperature sensors respectively disposed at three positions of an upper portion, a middle portion and a lower portion of the sidewall of the first tank 101. So set up, can be so that the inorganic powder material of being stirred by high temperature in the first jar of body 101 obtains comprehensive three-dimensional temperature monitoring for the temperature of the material that is in three positions about in the stirring process all can be monitored by accurate. The problem of when stirring inorganic powder material, because the accurate average temperature of the internal material of jar can't accurately be learnt when the powder volume of stirring is great, lead to the material not to conform to the demand at the preliminary modified stirring of first jar of body 101, carry out follow-up stirring preparation process after the ejection of compact and go wrong like this, lead to the reduction of product percent of pass is solved. Moreover, use infrared ray sensor at the internal mode from last to penetrating through stirring material of jar to monitoring jar internal material down, can further the accurate temperature condition and the modified state of learning jar internal all materials (including jar internal atomizing degree, loose degree and flight speed information etc.) through infrared ray sensor and three temperature sensor's cooperation like this, can obtain the accurate information of jar internal material, make the preliminary modification of material can reach the demand state, can not produce any problem that influences the product percent of pass during the ejection of compact.
When inorganic powder enters the second high-temperature modification stirring tank 2 after being preliminarily modified and stirred by the first high-temperature modification stirring tank 1, the second high-temperature modification stirring tank 2 thoroughly and uniformly modifies the inorganic powder, and the modification is realized by accelerating the stirring speed, the temperature and other conditions. Of course, the second high-temperature modification stirring tank 2 comprises a second tank 201 and a second cover 202 for covering the second tank 201, and a second heating sleeve structure is arranged on the periphery of the second tank 201.
In the second high-temperature modification stirring tank 2, the temperature and the state of the inorganic powder in the second tank 201 are monitored by a second temperature sensing device. Specifically, the second temperature sensing device includes infrared sensor and temperature sensor, and infrared sensor sets up on second lid 202 to the key is, and infrared sensor needs to set up towards the inside tank bottoms of the second jar of body 201, can monitor the state and the temperature condition of whole second jar of body 201 from last inorganic powder material down like this. Further, a temperature sensor is provided on a sidewall of the second tank 201. Preferably, the second temperature sensing means includes three temperature sensors respectively provided at three positions of an upper portion, a middle portion and a lower portion of the sidewall of the second tank 201. So set up, can be so that the inorganic powder material by high temperature stirring in the second jar body 201 obtains comprehensive three-dimensional temperature monitoring for the temperature of the material that is in three positions about in the stirring process all can be monitored by accurate. The problem of when stirring inorganic powder material, because the accurate average temperature of the internal material of jar can't accurately be learnt when the powder volume of stirring is great, lead to the material inhomogeneous thorough of the modified stirring in the second jar body 201, carry out follow-up stirring preparation process after the ejection of compact and go wrong, lead to the reduction of product percent of pass is solved like this. Moreover, use infrared ray sensor at the internal mode from last to penetrating through stirring material of jar to monitoring jar internal material down, can further the accurate temperature condition and the modified state of learning jar internal all materials (including jar internal atomizing degree, loose degree and flight speed etc. information), like this through infrared ray sensor and three temperature sensor's cooperation, can obtain the accurate information of jar internal material, make the material modify thoroughly, can reach the demand state, can not produce any problem that influences the product percent of pass during the ejection of compact.
After the inorganic powder material is modified by thorough high-temperature stirring, the inorganic powder material enters the third high-temperature mixing reaction tank 3 from the second high-temperature modification stirring tank 2, and in the third high-temperature mixing reaction tank 3, the inorganic powder and the organic material added in addition need to be subjected to high-temperature mixing stirring, so that the inorganic powder and the organic material can be uniformly and thoroughly reacted to form organic inorganic powder (namely, organic powder and organic-inorganic composite material). In the process, the temperature of the materials in the tank body still needs to be monitored so as to ensure that the temperature and the state of the materials reach the state of the accuracy requirement.
Specifically, the third high-temperature mixing reaction tank 3 includes a third tank 301 and a third cover 302 for covering the third tank 301, and a third heating sleeve structure is provided on the periphery of the third tank 301. In this embodiment, the third temperature sensing device includes an infrared sensor and a temperature sensor, the infrared sensor is disposed on the third cover 302, and the key point is that the infrared sensor needs to be disposed opposite to the inner tank bottom of the third tank 301, so as to monitor the state and temperature condition of the organic inorganic powder material from top to bottom of the third tank 301. Further, a temperature sensor is provided on a sidewall of the second tank 201. So set up, for thoroughly inorganic powder of modification lies in organic material mixing stirring reaction, the change of matter has taken place to its state, so no longer need set up many places temperature sensor on the jar body, only need set up on the jar body can monitor jar internal temperature one temperature sensor, cooperation through infrared ray sensor and temperature sensor, can obtain the accurate information of the organic inorganic powder material of jar internal, make the material composite reaction thoroughly, can reach the demand state, can not produce any problem that influences the product percent of pass during the ejection of compact, lay solid material foundation for preparing qualified material granule, yield and effective work efficiency have been guaranteed.
In summary, the invention realizes the full composite reaction of the inorganic powder material and the organic material by performing the initial high-temperature stirring modification, the thorough high-temperature stirring modification and the thorough mixing reaction on the inorganic powder material to form the organic-inorganic composite material. The key point of the process is that the process is realized by a first temperature sensing device arranged on the first high-temperature modification stirring tank 1, a second temperature sensing device arranged on the second high-temperature modification stirring tank 2 and a third temperature sensing device arranged on the third high-temperature mixing reaction tank 3 respectively, and because the state and the temperature of the material are accurately grasped in the process from modification stirring to mixing reaction, the thorough modification and the thorough reaction are realized, so that the yield and the working efficiency are ensured.
Finally, it is noted that the above-mentioned preferred embodiments illustrate rather than limit the invention, and that, although the invention has been described in detail with reference to the above-mentioned preferred embodiments, it will be understood by those skilled in the art that various changes in form and detail may be made therein without departing from the scope of the invention as defined by the appended claims.

Claims (9)

1. The utility model provides an inorganic organic composite material temperature monitoring system for mixing apparatus which characterized in that includes: a first high-temperature modification stirring tank (1), a second high-temperature modification stirring tank (2) and a third high-temperature mixing reaction tank (3);
the device is characterized in that a first temperature sensing device is arranged on the first high-temperature modification stirring tank (1), a second temperature sensing device is arranged on the second high-temperature modification stirring tank (2), and a third temperature sensing device is arranged on the third high-temperature mixing reaction tank (3).
2. The temperature monitoring system according to claim 1, wherein the first high-temperature modified stirring tank (1) comprises a first tank body (101) and a first cover body (102) for covering the first tank body (101), and a first heating sleeve structure is arranged on the periphery of the first tank body (101).
3. The temperature monitoring system according to claim 2, wherein the first temperature sensing means comprises an infrared sensor and a temperature sensor, the infrared sensor being arranged on the first cover (102) and being arranged facing the inner tank bottom of the first tank (101), the temperature sensor being arranged on a side wall of the first tank (101).
4. The temperature monitoring system according to claim 3, wherein the first temperature sensing means comprises three temperature sensors respectively disposed at three positions of an upper portion, a middle portion and a lower portion of the side wall of the first tank (101).
5. The temperature monitoring system according to claim 1, wherein the second high-temperature modified stirring tank (2) comprises a second tank body (201) and a second cover body (202) for covering the second tank body (201), and a second heating sleeve structure is arranged on the periphery of the second tank body (201).
6. The temperature monitoring system according to claim 5, wherein the second temperature sensing means comprises an infrared sensor and a temperature sensor, the infrared sensor being arranged on the second cover (202) and being arranged facing the inner tank bottom of the second tank (201), the temperature sensor being arranged on a side wall of the second tank (201).
7. The temperature monitoring system according to claim 6, wherein the second temperature sensing means comprises three temperature sensors respectively disposed at three positions of an upper portion, a middle portion and a lower portion of the sidewall of the second tank (201).
8. The temperature monitoring system according to claim 1, wherein the third high-temperature mixing reaction tank (3) comprises a third tank body (301) and a third cover body (302) for covering the third tank body (301), and a third heating sleeve structure is arranged on the periphery of the third tank body (301).
9. The temperature monitoring system according to claim 6, characterized in that said third temperature sensing means comprises an infrared sensor and a temperature sensor, said infrared sensor being arranged on said third cover (302) and being arranged facing the inner tank bottom of said third tank (301), said temperature sensor being arranged on the side wall of said third tank (301).
CN202011368435.3A 2020-11-30 2020-11-30 Temperature monitoring system for inorganic-organic composite material mixing equipment Pending CN112546936A (en)

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Application publication date: 20210326