CN112539643B - Alkali metal air chamber with high drying efficiency and drying method thereof - Google Patents

Alkali metal air chamber with high drying efficiency and drying method thereof Download PDF

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Publication number
CN112539643B
CN112539643B CN202011374026.4A CN202011374026A CN112539643B CN 112539643 B CN112539643 B CN 112539643B CN 202011374026 A CN202011374026 A CN 202011374026A CN 112539643 B CN112539643 B CN 112539643B
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tail pipe
air chamber
transparent
alkali metal
air
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CN112539643A (en
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周斌权
池浩湉
袁珩
陆吉玺
王亚翔
彭金鹏
尚慧宁
王学磊
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Beihang University
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Beihang University
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    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26DRYING
    • F26BDRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B21/00Arrangements or duct systems, e.g. in combination with pallet boxes, for supplying and controlling air or gases for drying solid materials or objects
    • F26B21/14Arrangements or duct systems, e.g. in combination with pallet boxes, for supplying and controlling air or gases for drying solid materials or objects using gases or vapours other than air or steam, e.g. inert gases
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26DRYING
    • F26BDRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B21/00Arrangements or duct systems, e.g. in combination with pallet boxes, for supplying and controlling air or gases for drying solid materials or objects
    • F26B21/004Nozzle assemblies; Air knives; Air distributors; Blow boxes

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Drying Of Solid Materials (AREA)

Abstract

According to the alkali metal air chamber with high drying efficiency and the drying method thereof, the air inlet tail pipe and the air outlet tail pipe which are staggered and tangent with the air chamber main body are arranged, so that inert gases such as dry nitrogen and the like form cyclone-shaped airflow along the inner wall of the air chamber main body under the action of gravity and tangential force, and the residual cleaning solution on the surface of the inner wall of the air chamber is dried efficiently. The alkali metal air chamber with high drying efficiency can ensure the cleanliness of the alkali metal air chamber, is not influenced by the cleanliness of a drying operation environment, shortens the drying time of the air chamber, and has great significance in improving the quality of the anti-relaxation coating in the alkali metal air chamber.

Description

Alkali metal air chamber with high drying efficiency and drying method thereof
Technical Field
The invention relates to an alkali metal air chamber, in particular to an alkali metal air chamber with high drying efficiency and a drying method thereof.
Background
The alkali metal gas chamber is a special transparent glass bubble for performing ultra-high-sensitivity magnetic field and inertia measurement by utilizing the property of alkali metal atom spinning, and is widely applied to a plurality of research fields such as an atom gyroscope, an atom clock, an atom magnetometer and the like. The inside of the alkali metal gas chamber is provided with an anti-relaxation coating for inhibiting collision relaxation between alkali metal atoms and the inner wall of the gas chamber. The quality of the anti-relaxation coating can affect the quality of the alkali metal gas cell. In the process of manufacturing the relaxation-resistant coating, the inner wall of the air chamber needs to be dried for many times. For example, taking the fabrication of a "dry film" Octadecyltrichlorosilane (OTS) coating as an example, the fabrication process includes four steps: cleaning, coating, filling and curing. In the step of "cleaning", a strong oxidizing Piranha (Piranha) solution is usually used to clean the inner wall of the alkali metal gas chamber to remove impurities attached to the inner wall of the gas chamber, and to form a layer of hydroxyl groups on the inner wall of the gas chamber, thereby facilitating the film formation of the OTS molecules on the surface of the inner wall of the gas chamber. The cleaning step is wet cleaning, and after the cleaning is finished, the inner wall of the air chamber needs to be dried, and then the film coating operation can be carried out. At present, the inner wall of the air chamber is dried by adopting a vacuum oven or a blowing method of inert gases such as nitrogen and the like. When the inner wall of the air chamber is dried by adopting a vacuum oven drying mode, the inner wall of the glass air chamber is polluted and the manufacture of the relaxation-resistant coating and the final quality of the alkali metal air chamber are influenced because the inner wall of the glass air chamber needs to be taken out after being cooled after being dried, namely the drying time is long. When the inner wall of the air chamber is dried by adopting a blowing drying mode of inert gases such as nitrogen and the like, the traditional alkali metal air chamber has the structure that only one tail pipe of the alkali metal air chamber is used for leading the inert gases such as nitrogen and the like to be difficult to enter the air chamber; or two alkali metal gas chamber tail pipes which are directly and oppositely distributed are arranged, inert gases such as nitrogen and the like are difficult to traverse the inner wall of the whole gas chamber, the difficulty of drying the inner wall of the gas chamber by a blowing drying mode of the inert gases such as nitrogen and the like is high, and the inner wall of the whole gas chamber cannot be effectively dried.
Disclosure of Invention
The invention provides an alkali metal air chamber with high drying efficiency and a drying method thereof, aiming at the defects or shortcomings in the prior art, the alkali metal air chamber with high drying efficiency is provided with an air inlet tail pipe and an air outlet tail pipe which are staggered and tangent with an air chamber main body, so that inert gases such as dry nitrogen and the like form cyclone-shaped airflow along the inner wall of the air chamber main body under the action of gravity and tangential force, and residual cleaning liquid on the surface of the inner wall of the air chamber is dried with high efficiency. The alkali metal air chamber with high drying efficiency can ensure the cleanliness of the alkali metal air chamber, is not influenced by the cleanliness of a drying operation environment, shortens the drying time of the air chamber, and has great significance in improving the quality of the anti-relaxation coating in the alkali metal air chamber.
The technical scheme of the invention is as follows:
an alkali metal air chamber with high drying efficiency comprises a cylindrical transparent air chamber shell, and an air inlet tail pipe and an air outlet tail pipe which are communicated with the inside of the transparent air chamber shell, wherein the side surfaces of the air inlet tail pipe and the air outlet tail pipe are tangent to the cylindrical side surface of the transparent air chamber shell, and the axial lines of the air inlet tail pipe and the air outlet tail pipe are parallel to each other and are vertical to the axial line of the transparent air chamber shell; the axes of the air inlet tail pipe and the air outlet tail pipe are not on the same cross section of the transparent air chamber shell, the axis of the air inlet tail pipe is close to the upper bottom surface of the transparent air chamber shell, and the axis of the air outlet tail pipe is close to the lower bottom surface of the transparent air chamber shell. Preferably, the axial section of the transparent gas chamber shell perpendicular to the axes of the inlet tail pipe and the outlet tail pipe is an interface, and the inlet tail pipe and the outlet tail pipe are respectively positioned at two sides of the interface.
Preferably, the axial section of the transparent air chamber shell, which is perpendicular to the axes of the inlet tail pipe and the outlet tail pipe, is an interface, the inlet tail pipe and the outlet tail pipe are respectively positioned at the same side of the interface, the free end of the inlet tail pipe extends perpendicularly towards the upper bottom surface of the transparent air chamber shell and is provided with an inlet branch pipe, and the free end of the outlet tail pipe extends perpendicularly towards the lower bottom surface of the transparent air chamber shell and is provided with an outlet branch pipe.
Preferably, the projections of the axes of the inlet tail pipe and the outlet tail pipe on the cross section of the transparent air chamber shell are mutually coincident.
Preferably, the side surface of the air inlet tail pipe is tangent to the upper bottom surface of the transparent air chamber shell, and the side surface of the air outlet tail pipe is tangent to the lower bottom surface of the transparent air chamber shell.
The inner wall of the alkali metal air chamber with high drying efficiency is dried in an inert gas blow-drying mode, the upper bottom surface of a transparent air chamber shell faces upwards, inert gas enters the transparent air chamber shell from the air inlet tail pipe in a tangential direction, traverses the inner wall of the whole transparent air chamber shell under the action of gravity and tangential force, and is finally discharged through the air outlet tail pipe.
Compared with the prior art, the invention has the advantages that: the alkali metal air chamber with high drying efficiency and the drying method thereof are characterized in that the air inlet tail pipe and the air outlet tail pipe are communicated with the cylindrical transparent air chamber shell in a tangent mode, inert gas used for drying the inner wall of the transparent air chamber shell of the alkali metal air chamber enters from the air inlet tail pipe, moves along the inner wall of the transparent air chamber shell in a circular mode under the action of the tangential force and moves downwards under the action of gravity to form cyclone-shaped air flow, the inner wall of the whole transparent air chamber shell can be efficiently traversed to dry cleaning liquid remained on the inner wall of the transparent air chamber shell, drying time is shortened, manufacturing time of the alkali metal air chamber is shortened, the drying process is not influenced by operating environment, cleanliness of the inside of the alkali metal air chamber is effectively guaranteed, and quality of an anti-relaxation coating in the alkali metal air chamber is improved.
Drawings
FIG. 1 is a three-dimensional structural view of an alkali metal gas cell of example 1 of the present invention having high drying efficiency;
FIG. 2 is a front view of an embodiment 1 of an alkali metal gas cell of the present invention with high drying efficiency;
FIG. 3 is a top view of an embodiment 1 of a high drying efficiency alkali metal chamber of the present invention;
FIG. 4 is a left side view of an alkali metal gas cell embodiment 1 of the present invention with high drying efficiency;
FIG. 5 is a front view of an alkali metal chamber embodiment 2 of the present invention with high drying efficiency;
FIG. 6 is a top view of an alkali metal chamber embodiment 2 of the present invention having high drying efficiency;
FIG. 7 is a left side view of an alkali metal gas cell embodiment 2 of the present invention with high drying efficiency;
FIG. 8 is a front view of an alkali metal chamber embodiment 3 of the present invention with high drying efficiency;
FIG. 9 is a top view of an alkali metal chamber embodiment 3 of the present invention having high drying efficiency;
FIG. 10 is a left side view of an alkali metal gas cell embodiment 3 of the present invention with high drying efficiency;
FIG. 11 is a front view of an alkali metal chamber embodiment 4 of the present invention with high drying efficiency;
FIG. 12 is a top view of an alkali metal chamber embodiment 4 of the present invention having high drying efficiency;
FIG. 13 is a left side view of an alkali metal cell embodiment 4 of the present invention with high drying efficiency.
The reference numbers are listed below: 1-a tail pipe; 2-air outlet tail pipe; 3-a transparent air chamber shell; 31-upper bottom surface; 32-lower bottom surface; 33-cylindrical side; 34-interface.
Detailed Description
To facilitate an understanding of the invention, the invention is described in more detail below with reference to figures 1-2 and the specific examples.
Example 1
An alkali metal gas chamber with high drying efficiency is disclosed, as shown in fig. 1-4, comprising a cylindrical transparent gas chamber shell 3, and an inlet tail pipe 1 and an outlet tail pipe 2 communicated with the inside of the transparent gas chamber shell 3, wherein the side surfaces of the inlet tail pipe 1 and the outlet tail pipe 2 are tangent to the cylindrical side surface 33 of the transparent gas chamber shell 3, and the axes of the inlet tail pipe 1 and the outlet tail pipe 2 are parallel to each other and perpendicular to the axis of the transparent gas chamber shell 3; the axes of the inlet tail pipe 1 and the outlet tail pipe 2 are not on the same cross section of the transparent air chamber shell 3, the axis of the inlet tail pipe 1 is close to the upper bottom surface 31 of the transparent air chamber shell 1, and the axis of the outlet tail pipe 2 is close to the lower bottom surface 32 of the transparent air chamber shell 3. The air inlet tail pipe 1 and the air outlet tail pipe 2 are communicated with the cylindrical transparent air chamber shell 3 in a tangent mode, inert gas used for drying the inner wall of the transparent air chamber shell 3 of the alkali metal air chamber enters from the air inlet tail pipe 1, circular motion is conducted along the inner wall of the transparent air chamber shell 3 under the action of tangential force, meanwhile, the inert gas moves downwards under the action of gravity to form cyclone-shaped air flow, the inner wall of the transparent air chamber shell 3 can be efficiently traversed to dry cleaning liquid remained on the inner wall, drying time is shortened, manufacturing time of the alkali metal air chamber is shortened, the drying process is not affected by operating environment, cleanliness inside the alkali metal air chamber is effectively guaranteed, and quality of the relaxation-resistant coating in the alkali metal air chamber is improved. Preferably, the axial section of the transparent gas chamber shell 3 perpendicular to the axial lines of the inlet tail pipe 1 and the outlet tail pipe 2 is an interface 34, and the inlet tail pipe 1 and the outlet tail pipe 2 are respectively positioned at two sides of the interface 34. The tangent parts of the inlet tail pipe 1 and the outlet tail pipe 2 with the transparent air chamber shell 3 are on the same straight line, and the straight line is positioned at an interface 34.
Example 2
Unlike the above embodiments, as shown in fig. 5-7, the tangential positions of the inlet tail pipe 1 and the outlet tail pipe 2 to the transparent gas chamber shell 3 are not on the same straight line, but are located on the opposite side lines of the dividing plane 34.
Example 3
Unlike the previous embodiments, as shown in fig. 8-10, the inlet tail pipe 1 and the outlet tail pipe 2 are respectively located on the same side of the interface 34. And the tangential parts of the inlet tail pipe 1 and the outlet tail pipe 2 and the transparent air chamber shell 3 are not on the same straight line, and the straight line is positioned on a boundary surface 34. At this time, in order to facilitate the connection of the inert gas pipes to the inlet tail pipe 1 and the outlet tail pipe 2, the free end of the inlet tail pipe 1 is provided with an inlet branch pipe 11 extending vertically toward the upper bottom surface 31 of the transparent gas chamber housing 3, and the free end of the outlet tail pipe 2 is provided with an outlet branch pipe 21 extending vertically toward the lower bottom surface 32 of the transparent gas chamber housing 3.
Preferably, the side surface of the inlet tail pipe 1 is tangent to the upper bottom surface 31 of the transparent gas chamber shell 3, and the side surface of the outlet tail pipe 2 is tangent to the lower bottom surface 32 of the transparent gas chamber shell 3. In this case, the cyclone formed by the inert gas efficiently and completely traverses the inner wall of the transparent air chamber shell 3 from top to bottom to dry the cleaning solution remained on the inner wall.
Example 4
Unlike the previous embodiments, as shown in fig. 11-13, the inlet tail pipe 1 and the outlet tail pipe 2 are respectively located on the same side of the interface 34. And the tangential parts of the inlet tail pipe 1 and the outlet tail pipe 2 and the transparent air chamber shell 3 are on the same straight line and are respectively positioned on the opposite side lines of the interface 34. At this time, in order to facilitate the connection of the inert gas pipes to the inlet tail pipe 1 and the outlet tail pipe 2, the free end of the inlet tail pipe 1 is provided with an inlet branch pipe 11 extending vertically toward the upper bottom surface 31 of the transparent gas chamber housing 3, and the free end of the outlet tail pipe 2 is provided with an outlet branch pipe 21 extending vertically toward the lower bottom surface 32 of the transparent gas chamber housing 3.
Example 5
The inner wall of the alkali metal air chamber with high drying efficiency is dried in an inert gas blow-drying mode, the upper bottom surface 31 of the transparent air chamber shell 3 faces upwards, inert gas enters the transparent air chamber shell 3 from the air inlet tail pipe 1 in a tangential direction, traverses the inner wall of the whole transparent air chamber shell under the action of gravity and tangential force, and is finally discharged through the air outlet tail pipe 2.

Claims (6)

1. The alkali metal gas chamber with high drying efficiency is characterized by comprising a cylindrical transparent gas chamber shell, and an air inlet tail pipe and an air outlet tail pipe which are communicated with the inside of the transparent gas chamber shell, wherein the side surfaces of the air inlet tail pipe and the air outlet tail pipe are tangent to the cylindrical side surface of the transparent gas chamber shell, and the axes of the air inlet tail pipe and the air outlet tail pipe are parallel to each other and are vertical to the axis of the transparent gas chamber shell; the axes of the air inlet tail pipe and the air outlet tail pipe are not on the same cross section of the transparent air chamber shell, the axis of the air inlet tail pipe is close to the upper bottom surface of the transparent air chamber shell, and the axis of the air outlet tail pipe is close to the lower bottom surface of the transparent air chamber shell.
2. The high drying efficiency alkali metal gas cell according to claim 1, wherein the cross section of the transparent gas cell casing perpendicular to the axes of the inlet tail pipe and the outlet tail pipe is an interface, and the inlet tail pipe and the outlet tail pipe are respectively disposed at both sides of the interface.
3. The alkali metal gas cell with high drying efficiency as claimed in claim 1, wherein the section of the transparent gas cell casing perpendicular to the axes of the inlet tail pipe and the outlet tail pipe is an interface, the inlet tail pipe and the outlet tail pipe are respectively located at the same side of the interface, the free end of the inlet tail pipe is provided with an inlet branch pipe extending perpendicularly to the upper bottom surface of the transparent gas cell casing, and the free end of the outlet tail pipe is provided with an outlet branch pipe extending perpendicularly to the lower bottom surface of the transparent gas cell casing.
4. The high drying efficiency alkali metal gas cell according to claim 2 or 3, wherein the projections of the axes of the inlet tail tube and the outlet tail tube on the cross section of the transparent gas cell shell are coincident with each other.
5. The high drying efficiency alkali metal gas cell according to claim 1, wherein the side surface of the inlet tail pipe is tangent to the upper bottom surface of the transparent gas cell housing, and the side surface of the outlet tail pipe is tangent to the lower bottom surface of the transparent gas cell housing.
6. A drying method of an alkali metal air chamber with high drying efficiency is characterized in that the inner wall of the alkali metal air chamber with high drying efficiency is dried by adopting an inert gas blow-drying mode according to any one of claims 1 to 5, the upper bottom surface of a shell of the transparent air chamber is upward, the inert gas enters the interior of the shell of the transparent air chamber from the air inlet tail pipe along the tangential direction, traverses the inner wall of the shell of the transparent air chamber under the action of gravity and tangential force, and is finally discharged through the air outlet tail pipe.
CN202011374026.4A 2020-11-30 2020-11-30 Alkali metal air chamber with high drying efficiency and drying method thereof Active CN112539643B (en)

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CN112539643B true CN112539643B (en) 2022-01-21

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2011192390A (en) * 2010-03-11 2011-09-29 Noritake Co Ltd Drying method and drying device of metal foil laminated body
CN108286894A (en) * 2018-02-06 2018-07-17 中国人民解放军第八医院 A kind of drying device of medical treatment specimen collection container
CN208349707U (en) * 2018-05-17 2019-01-08 成都星达铜业有限公司 A kind of copper wire drying device
CN208587921U (en) * 2018-01-23 2019-03-08 武汉凯迪绿色能源开发运营有限公司 A kind of cyclone dryer and biomass fuel drying device
CN111026177A (en) * 2019-12-18 2020-04-17 北京航空航天大学 System and method for controlling humidity in alkali metal air chamber

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2011192390A (en) * 2010-03-11 2011-09-29 Noritake Co Ltd Drying method and drying device of metal foil laminated body
CN208587921U (en) * 2018-01-23 2019-03-08 武汉凯迪绿色能源开发运营有限公司 A kind of cyclone dryer and biomass fuel drying device
CN108286894A (en) * 2018-02-06 2018-07-17 中国人民解放军第八医院 A kind of drying device of medical treatment specimen collection container
CN208349707U (en) * 2018-05-17 2019-01-08 成都星达铜业有限公司 A kind of copper wire drying device
CN111026177A (en) * 2019-12-18 2020-04-17 北京航空航天大学 System and method for controlling humidity in alkali metal air chamber

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