CN112077252A - A kind of forging die and free forging processing method of near-net-shaped titanium strip slab - Google Patents

A kind of forging die and free forging processing method of near-net-shaped titanium strip slab Download PDF

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CN112077252A
CN112077252A CN202011015913.2A CN202011015913A CN112077252A CN 112077252 A CN112077252 A CN 112077252A CN 202011015913 A CN202011015913 A CN 202011015913A CN 112077252 A CN112077252 A CN 112077252A
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forging
ingot
wall surface
side wall
titanium
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乔恩利
张晓勇
张起
岳旭
同晓乐
顾忠明
王双礼
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Xinjiang Xiangrun New Material Technology Co ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21JFORGING; HAMMERING; PRESSING METAL; RIVETING; FORGE FURNACES
    • B21J13/00Details of machines for forging, pressing, or hammering
    • B21J13/02Dies or mountings therefor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21JFORGING; HAMMERING; PRESSING METAL; RIVETING; FORGE FURNACES
    • B21J1/00Preparing metal stock or similar ancillary operations prior, during or post forging, e.g. heating or cooling
    • B21J1/06Heating or cooling methods or arrangements specially adapted for performing forging or pressing operations
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21JFORGING; HAMMERING; PRESSING METAL; RIVETING; FORGE FURNACES
    • B21J5/00Methods for forging, hammering, or pressing; Special equipment or accessories therefor
    • B21J5/002Hybrid process, e.g. forging following casting
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21JFORGING; HAMMERING; PRESSING METAL; RIVETING; FORGE FURNACES
    • B21J5/00Methods for forging, hammering, or pressing; Special equipment or accessories therefor
    • B21J5/02Die forging; Trimming by making use of special dies ; Punching during forging
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22FCHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
    • C22F1/00Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
    • C22F1/16Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of other metals or alloys based thereon
    • C22F1/18High-melting or refractory metals or alloys based thereon
    • C22F1/183High-melting or refractory metals or alloys based thereon of titanium or alloys based thereon

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Abstract

本发明公开的一种近净成形钛带板坯的锻造用模具,包括有底板,底板的一端端部由下至上依次设置有过渡挡板及竖直挡板,过渡挡板的第一侧壁面及竖直挡板的第二侧壁面同侧,第一侧壁面、第二侧壁面及上表面均为模具与坯料的接触面;第一侧壁面及第二侧壁面均为弧面,第一底板的上表面为矩形平面,第一侧壁面通过第二侧壁面过渡与上表面平滑连接;底板的侧壁面上设置有若干个吊装孔。还公开了应用该模具的一种近净成形钛带板坯的自由锻造加工方法,该方法在保证加工过程简单、生产效率显著提高的前提下,使成品率大幅提高。

Figure 202011015913

The invention discloses a forging die for near-net-shape titanium strip slabs, which includes a bottom plate, one end of the bottom plate is provided with a transition baffle and a vertical baffle in sequence from bottom to top, and a first side wall surface of the transition baffle is provided. On the same side as the second side wall surface of the vertical baffle, the first side wall surface, the second side wall surface and the upper surface are the contact surfaces between the mold and the blank; the first side wall surface and the second side wall surface are arc surfaces, the first The upper surface of the bottom plate is a rectangular plane, and the first side wall surface is smoothly connected to the upper surface through the transition of the second side wall surface; a number of hoisting holes are arranged on the side wall surface of the bottom plate. Also disclosed is a free forging processing method for near-net-shape titanium strip slabs using the die, which greatly improves the yield on the premise of ensuring a simple processing process and significantly improved production efficiency.

Figure 202011015913

Description

一种近净成形钛带板坯的锻造用模具及自由锻造加工方法A kind of forging die and free forging processing method of near-net-shaped titanium strip slab

技术领域technical field

本发明属于材料加工技术领域,具体涉及一种近净成形钛带板坯的锻造用模具,还涉及一种近净成形钛带板坯的自由锻造加工方法。The invention belongs to the technical field of material processing, in particular to a forging die for near-net-shape titanium strip slabs, and also relates to a free forging processing method for near-net-shape titanium strip slabs.

背景技术Background technique

钛及钛合金因其比强度高、密度小、无磁、耐腐蚀性优异等特点,被广泛应用于舰船和海洋工程等领域。钛及钛合金带材由于比重小、耐蚀性好、耐高温、稳定性好等诸多优点,被大量使用在化工行业、舰船行业、航空航天、高档建筑外装饰等多种行业,使用范围及用量逐年上升。但钛及钛合金由于原材料价格昂贵、加工难度大,加工工艺路线长,成品率低等因素影响,终端材料价格还是偏高。Titanium and titanium alloys are widely used in ships and marine engineering due to their high specific strength, low density, non-magnetic, and excellent corrosion resistance. Titanium and titanium alloy strips are widely used in chemical industry, ship industry, aerospace, high-end building exterior decoration and other industries due to their advantages of small specific gravity, good corrosion resistance, high temperature resistance, and good stability. And the amount is increasing year by year. However, due to the high price of raw materials, difficult processing, long processing route and low yield of titanium and titanium alloys, the price of terminal materials is still high.

为了解决这一矛盾,使钛及钛合金更大范围普及,近年来,国内外钛加工领域研究人员做出了大量的研究和努力,虽然取得了一些成绩,但距离目标还相去胜远。In order to solve this contradiction and make titanium and titanium alloys popular in a wider range, in recent years, researchers in the field of titanium processing at home and abroad have made a lot of research and efforts. Although some achievements have been made, they are still far from the goal.

目前,国内外生产钛带材有两种基本工艺,一种是从简化工艺思路考虑,使用冷床炉熔炼工艺,将铸锭熔炼成直接可以轧制的方坯尺寸,省去中间环节,进行直接轧制。其优点是省去了中间加工环节,成品率得到一定提高,但由于熔炼造成的铸态组织无法得到有效改善,直接遗留至成品带材,造成带材无法正常使用,特别是薄带材,其孔洞、疏松等缺陷尤为明显。因此,此种工艺只能少量生产厚度较大,要求较低的低端钛带。另一种是通过自耗电极熔炼成圆锭,通过自由锻造成钛带坯料,再轧制成钛带材。此种工艺生产的钛带,由于自由锻造过程对铸态组织进行了充分破碎和压实,使材料的组织形貌得到根本改变,轧制出的各种规格钛带质量优异,能满足各种市场需求,其唯一缺点就是需经过自由锻造过程,导致钛带材综合成品率较低,钛带材价格偏高。At present, there are two basic processes for the production of titanium strips at home and abroad. One is to use the cooling-bed furnace smelting process to smelt the ingot into a billet size that can be rolled directly, eliminating the need for intermediate links. direct rolling. The advantage is that the intermediate processing links are omitted, and the yield is improved to a certain extent. However, the as-cast structure caused by smelting cannot be effectively improved, and it is directly left to the finished strip, resulting in the strip cannot be used normally, especially for thin strips. Defects such as holes and porosity are particularly obvious. Therefore, this process can only produce low-end titanium strips with larger thicknesses and lower requirements in small quantities. The other is to smelt into round ingots through consumable electrodes, form titanium strip billets through free forging, and then roll them into titanium strips. The titanium strip produced by this process is completely broken and compacted by the free forging process, so that the structure and morphology of the material are fundamentally changed. The rolled titanium strips of various specifications have excellent quality and can meet various The only disadvantage of the market demand is that it needs to go through the free forging process, resulting in a low comprehensive yield of titanium strips and a high price of titanium strips.

为此,本发明是在第二种工艺路线下,一方面根据工艺要求设计制造专用工模具,使工业化生产过程简单、有效,生产效率大幅提高;另一方面通过钛带板坯自由锻造过程工艺参数控制,使钛带板坯自由锻造制坯环节成品率提高10%以上,达到98%。该技术突破了国内、外钛带板坯制备关键技术瓶颈,从而最终获得一种近净成形钛带板坯的自由锻造加工方法。Therefore, the present invention is based on the second process route. On the one hand, special tooling and dies are designed and manufactured according to process requirements, so that the industrialized production process is simple and effective, and the production efficiency is greatly improved; on the other hand, the titanium strip slab free forging process technology is adopted. The parameter control increases the yield of the free forging of the titanium strip slab by more than 10% to 98%. This technology breaks through the key technical bottleneck of the preparation of domestic and foreign titanium strip slabs, and finally obtains a free forging processing method of near-net-shaped titanium strip slabs.

发明内容SUMMARY OF THE INVENTION

本发明的目的是提供一种近净成形钛带板坯的锻造用模具,使钛带板坯的头尾棱角缺肉现象得到解决,使钛带用自由锻造板坯锻造成品率大幅提高。The purpose of the present invention is to provide a forging die for near-net-shaped titanium strip slabs, so that the phenomenon of lack of flesh at the head and tail edges and corners of the titanium strip slabs can be solved, and the forging yield of titanium strip free forging slabs can be greatly improved.

本发明的另一个目的是一种近净成形钛带板坯的自由锻造加工方法,该方法在保证加工过程简单、生产效率显著提高的前提下,使成品率大幅提高。Another object of the present invention is a free forging processing method for near-net-shaped titanium strip slabs, which can greatly improve the yield on the premise of ensuring a simple processing process and significantly improved production efficiency.

本发明所采用的技术方案是,一种近净成形钛带板坯的锻造用模具,包括有底板,底板的一端端部由下至上依次设置有过渡挡板及竖直挡板,过渡挡板的第一侧壁面及竖直挡板的第二侧壁面同侧,第一侧壁面、第二侧壁面及上表面均为模具与坯料的接触面;The technical scheme adopted in the present invention is a forging die for near-net-shape titanium strip slabs, comprising a bottom plate, one end of the bottom plate is provided with a transition baffle and a vertical baffle sequentially from bottom to top, and the transition baffle The first side wall surface and the second side wall surface of the vertical baffle are on the same side, and the first side wall surface, the second side wall surface and the upper surface are the contact surfaces of the mold and the blank;

第一侧壁面及第二侧壁面均为弧面,第一底板的上表面为矩形平面,第一侧壁面通过第二侧壁面过渡与上表面平滑连接;底板的侧壁面上设置有若干个吊装孔。The first side wall surface and the second side wall surface are both arc surfaces, the upper surface of the first bottom plate is a rectangular plane, and the first side wall surface is smoothly connected to the upper surface through the transition of the second side wall surface; the side wall surface of the bottom plate is provided with several hoisting devices hole.

本发明的特征还在于,The present invention is also characterized in that,

第一侧壁面的弧度对应的半径R=50~100mm;第二侧壁面的弧度对应的半径R=3000~4000mm。The radius corresponding to the curvature of the first side wall surface is R=50-100mm; the radius corresponding to the curvature of the second side wall surface is R=3000-4000mm.

第一侧壁面、第二侧壁面及上表面的表面光洁度Ra均不大于3.2μm;底板的厚度不小于200mm;竖直挡板的厚度为200~400mm。The surface roughness Ra of the first side wall surface, the second side wall surface and the upper surface is not more than 3.2μm; the thickness of the bottom plate is not less than 200mm; the thickness of the vertical baffle is 200-400mm.

底板、过渡挡板及竖直挡板均为5CrMnMo板。The bottom plate, transition baffle and vertical baffle are all 5CrMnMo plates.

本发明所采用的第二个技术方案是,一种近净成形钛带板坯的自由锻造加工方法,具体按以下步骤实施:The second technical solution adopted by the present invention is a free forging processing method of a near-net-shaped titanium strip slab, which is specifically implemented according to the following steps:

步骤(1)铸锭制备:将原料钛及钛合金铸锭经过外圆周方向扒皮,去除熔炼过程中产生的表面氧化皮及皮下气孔缺陷,再将铸锭头部进行车平处理,去除熔炼过程中铸锭冒口位置产生的珊瑚状熔瘤缺陷,其次将铸锭底部端面缺陷去除干净,再对铸锭头尾进行圆角处理;Step (1) ingot preparation: peel the raw material titanium and titanium alloy ingots through the outer circumferential direction, remove the surface oxide scale and subcutaneous pore defects generated during the smelting process, and then carry out the flattening treatment on the head of the ingot to remove the smelting process The coral-like molten tumor defect generated at the riser position of the middle ingot, and then the end face defects at the bottom of the ingot are removed, and then the head and tail of the ingot are rounded;

步骤(2)铸锭加热:按照一定的加热工艺为铸锭加热;Step (2) ingot heating: heating the ingot according to a certain heating process;

步骤(3)开坯锻造:将加热好的铸锭移送至锻造压机上,采用先轻轻锻造一至两遍,然后加大压下量进行锻造,将加热好的铸锭锻造至厚度在800mm时,将坯料进行翻面,再加大压下量进行锻造,锻造过程中尽量保证上下面变形一致,最终将厚度尺寸控制在600~700mm区间;Step (3) Billeting forging: transfer the heated ingot to the forging press, first lightly forge one to two times, and then increase the reduction for forging, and forge the heated ingot to a thickness of 800mm During the forging process, the billet is turned over, and the reduction is increased for forging. During the forging process, try to ensure that the upper and lower deformations are consistent, and finally control the thickness size within the range of 600-700mm;

步骤(4)专用工模具控制锻造:对锻造至600~700mm尺寸区间的坯料,采用上述的模具进行锻造变形;Step (4) Control forging with special tool and die: For the blank forged to a size range of 600-700 mm, the above-mentioned die is used for forging deformation;

步骤(5)回火加热:将步骤(4)锻造后的热坯料进行回火加热处理,加热温度为900~950℃,保温时间为90~200分钟得中间坯料;Step (5) tempering and heating: perform tempering and heating treatment on the hot billet after forging in step (4), the heating temperature is 900-950° C., and the holding time is 90-200 minutes to obtain an intermediate billet;

步骤(6)成形锻造:将步骤(5)回火加热好的中间坯料在快锻机上进行锻造,得到钛及钛合金钛带板坯成品坯。Step (6) forming and forging: the intermediate billet tempered and heated in step (5) is forged on a fast forging machine to obtain finished billets of titanium and titanium alloy titanium strip slabs.

本发明的特征还在于,The present invention is also characterized in that,

步骤(1)中使用的原料钛及钛合金铸锭牌号为TA1、TA2、TA3、TA4或TA10。The grades of raw material titanium and titanium alloy ingots used in step (1) are TA1, TA2, TA3, TA4 or TA10.

步骤(1)中,使用的钛及钛合金铸锭为经过真空自耗电弧法二次熔炼,直径为Φ1000mm及以上锭型。In step (1), the titanium and titanium alloy ingots used are secondary smelting by vacuum consumable arc method, and the diameters are ingot shapes of Φ1000mm and above.

步骤(1)中,铸锭头尾圆角半径R=15mm~20mm。In step (1), the radius R of the head and tail of the ingot is 15mm-20mm.

步骤(2)中,铸锭加热工艺流程为:先由室温升温到800~850℃,升温时间150~180分钟;然后在800~850℃下保温,保温时间180~250分钟;再升温到1000~1050℃,升温时间180~250分钟;最后在1000~1050℃保温,保温时间180~250分钟。In step (2), the ingot heating process is as follows: firstly, the temperature is raised from room temperature to 800~850°C, and the temperature rise time is 150~180 minutes; then the temperature is kept at 800~850°C for 180~250 minutes; ~1050°C, the heating time is 180~250 minutes; finally, the temperature is kept at 1000~1050°C for 180~250 minutes.

步骤(3)中,铸锭开始轻压一至两遍时,压下量控制在30~50mm,再加大压下量进行锻造,压下量控制在单边80~100mm;步骤(4)的具体实施步骤为:对锻造至600~700mm的坯料进行锻造时,使坯料端面靠近专用工模具的第二侧壁面(3-1)处,通过每次压下100~120mm反复压制,将坯料锻造至厚度在300~400mm尺寸之间;步骤(6)中,得到的钛及钛合金钛带板坯成品坯尺寸为:厚度×宽度×长度=180mm~250mm×1000mm~1600mm×5000mm~9000mm的钛带用板坯。In step (3), when the ingot is lightly pressed one to two times, the reduction is controlled at 30-50 mm, and the reduction is further increased for forging, and the reduction is controlled at 80-100 mm on one side; step (4) The specific implementation steps are as follows: when forging a billet with a thickness of 600-700 mm, make the end face of the billet close to the second side wall surface (3-1) of the special tool and die, and repeatedly press down by 100-120 mm each time to forge the billet. To the thickness between 300~400mm size; in step (6), the obtained titanium and titanium alloy titanium strip slab finished blank size is: thickness×width×length=180mm~250mm×1000mm~1600mm×5000mm~9000mm of titanium With slabs.

本发明的有益效果是:The beneficial effects of the present invention are:

(1)本发明方法通过在自由锻生产过程中合理借助专用工模具,突破了国内、外钛带板坯制备关键技术瓶颈,最终获得一种近净成形钛带板坯的自由锻造加工方法。(1) The method of the present invention breaks through the key technical bottleneck of the preparation of domestic and foreign titanium strip slabs by reasonably using special tools and dies in the free forging production process, and finally obtains a free forging processing method for near-net-shaped titanium strip slabs.

(2)本发明方法通过在自由锻生产过程中合理借助专用工模具,使钛带用自由锻造板坯锻造成品率由行业现有水平的88%提高到98%,成品率大幅提高;(2) The method of the present invention increases the forging yield of free forging slabs for titanium strips from 88% to 98% from the industry's existing level by reasonably using special tools and dies in the free forging production process, and the yield is greatly improved;

(3)本发明方法通过在自由锻生产过程中合理借助专用工模具,使钛带板坯的头尾棱角缺肉现象彻底解决;(3) The method of the present invention completely solves the phenomenon of lack of flesh at the head and tail edges and corners of the titanium strip slab by reasonably using special tools and dies in the free forging production process;

(4)本发明方法通过在自由锻生产过程中合理借助专用工模具,使锻造过程中采用较大变形,使铸锭的铸态组织得到充分破碎和压实,使板坯的组织形貌得到根本改变,板坯内在质量显著提高;(4) The method of the present invention adopts a large deformation in the forging process through reasonable use of special tools and dies in the production process of free forging, so that the as-cast structure of the ingot is fully broken and compacted, and the structure and morphology of the slab are obtained. Fundamentally changed, the internal quality of the slab is significantly improved;

(5)本发明方法通过在自由锻生产过程中合理借助专用工模具,在大幅提高成品率的前提下,使生产时间显著缩短,生产效率比现有国内、外制备工艺显著提高。(5) The method of the present invention significantly shortens the production time and significantly improves the production efficiency compared with the existing domestic and foreign preparation processes under the premise of greatly improving the yield by reasonably using special tools and dies in the free forging production process.

附图说明Description of drawings

图1为本发明一种近净成形钛带板坯的锻造用模具的结构示意图;Fig. 1 is the structural representation of the forging die of a kind of near-net-shape titanium strip slab of the present invention;

图2为本发明方法实施前铸锭头部形貌图;Fig. 2 is the topography diagram of the head of the ingot before the method of the present invention is implemented;

图3为经本发明方法步骤1实施后铸锭头部形貌图;3 is a topography diagram of the head of the ingot after the implementation of the method step 1 of the present invention;

图4为本发明方法实施前成品板坯头部表面形貌图;Fig. 4 is the topography of the surface of the finished slab head before the method of the present invention is implemented;

图5为经本发明方法实施后成品板坯头部表面形貌图;Fig. 5 is the surface topography diagram of the finished slab head after the method of the present invention is implemented;

图6为本发明方法实施前成品板坯头部需切除部分形貌图;Fig. 6 is the topography diagram of the part to be removed from the head of the finished slab before the method of the present invention is implemented;

图7为经本发明方法实施后成品板坯头部需切除或铣削部分形貌图;Fig. 7 is the topography diagram of the part to be cut or milled at the head of the finished slab after the method of the present invention is implemented;

图8为本发明方法实施前板坯头部切除部分实物图;FIG. 8 is a physical view of the cut part of the slab head before the method of the present invention is implemented;

图9为经本发明方法实施后板坯头部切除部分实物图;Fig. 9 is the actual picture of the cut part of the slab head after the method of the present invention is implemented;

图10为经本发明方法实施后成品板坯实物图。Figure 10 is a physical view of the finished slab after the method of the present invention is implemented.

图中,1.底板,2.过渡挡板,3.竖直挡板,4.吊装孔,1-1.上表面,2-1.第一侧壁面,3-1.第二侧壁面。In the figure, 1. bottom plate, 2. transition baffle, 3. vertical baffle, 4. hoisting hole, 1-1. upper surface, 2-1. first side wall surface, 3-1. second side wall surface.

具体实施方式Detailed ways

下面结合附图和具体实施方式对本发明进行详细说明。The present invention will be described in detail below with reference to the accompanying drawings and specific embodiments.

本发明提供一种近净成形钛带板坯的锻造用模具,如图1所示,包括有底板1,底板1的一端端部由下至上依次设置有过渡挡板2及竖直挡板3,过渡挡板2的第一侧壁面2-1及竖直挡板3的第二侧壁面3-1同侧,第一侧壁面2-1、第二侧壁面3-1及上表面1-1均为模具与坯料的接触面;The present invention provides a forging die for near-net-shape titanium strip slabs. As shown in FIG. 1 , it includes a bottom plate 1, and one end of the bottom plate 1 is sequentially provided with a transition baffle 2 and a vertical baffle 3 from bottom to top. , the first side wall surface 2-1 of the transition baffle 2 and the second side wall surface 3-1 of the vertical baffle 3 are on the same side, the first side wall surface 2-1, the second side wall surface 3-1 and the upper surface 1- 1 is the contact surface between the mold and the blank;

第一侧壁面2-1及第二侧壁面3-1均为弧面,第一底板1的上表面1-1为矩形平面,第一侧壁面2-1通过第二侧壁面3-1过渡与上表面1-1平滑连接;底板1的侧壁面上设置有若干个吊装孔4。The first side wall surface 2-1 and the second side wall surface 3-1 are both arc surfaces, the upper surface 1-1 of the first bottom plate 1 is a rectangular plane, and the first side wall surface 2-1 transitions through the second side wall surface 3-1 It is smoothly connected with the upper surface 1-1; the side wall surface of the bottom plate 1 is provided with several hoisting holes 4.

第一侧壁面2-1的弧度对应的半径R=50~100mm;第二侧壁面3-1的弧度对应的半径R=3000~4000mm。The radius corresponding to the radian of the first side wall surface 2-1 is R=50-100 mm; the radius corresponding to the radian of the second side wall surface 3-1 is R=3000-4000 mm.

第一侧壁面2-1、第二侧壁面3-1及上表面1-1的表面光洁度Ra均不大于3.2μm;底板1的厚度不小于200mm;竖直挡板3的厚度为200~400mm。The surface finish Ra of the first side wall surface 2-1, the second side wall surface 3-1 and the upper surface 1-1 is not greater than 3.2 μm; the thickness of the bottom plate 1 is not less than 200 mm; the thickness of the vertical baffle 3 is 200-400 mm .

底板1、过渡挡板2及竖直挡板3均为5CrMnMo板。The bottom plate 1, the transition baffle 2 and the vertical baffle 3 are all 5CrMnMo plates.

本发明模具采用5CrMnMo材料制作,设计各点及受力面应完全满足使用过程工艺要求。其中,图1中竖直挡板3的厚度为200~400mm,该处厚度主要考虑板坯端部成形过程中承受来自坯料流动所产生的横向压力,设计中考虑其受力不小于坯料流动所产生的最大横向压力,设计厚度根据最大横向压力确定。此面与坯料不接触,应此对表面光洁度不做要求。图1中第二侧壁面3-1为钛带头尾端面成形的主要工作面,为了在成品钛带板坯头尾基本实现平齐,此面设计应采用弧面设计,表面光洁度Ra不大于小于3.2μm,弧度设计范围应控制在R=3000~4000mm之间,否则将导致成品板坯头尾凹陷,端头不平。图1中第一侧壁面2-1应考虑圆弧设计,表面光洁度Ra应不大于3.2μm,弧度设计范围应控制在R=50~100mm之间,其目的主要考虑钛带坯料成形过程中,此处坯料流动较难到达。其次,如采用直角设计,易在此处产生较严重的应力集中,导致工模具从此处断裂。图1中坯料成形过程中长度、宽度方向接触面,接触面最大,受力也最大,设计主要考虑该上表面1-1应满足的坯料长度、宽度方向变形过程中尺寸要求。同时,应充分考虑底面在坯料变形过程中长期使用的整体平整度应不大于10mm。图1中,专用工模具底面的厚度,其受力主要为上、下锤头之间对坯料锻打的垂直力,其厚度不小于200mm。图1中吊装孔4,设计考虑工模具在使用中的方便吊装。图1中,模具中,不与坯料接触的侧壁面,由于坯料要从600~700mm尺寸区间锻造至300~400mm,应此,设计时应考虑与底面接触净高度不小于坯料尺寸。The mold of the present invention is made of 5CrMnMo material, and the design points and the force-bearing surface should fully meet the technological requirements of the use process. Among them, the thickness of the vertical baffle 3 in Figure 1 is 200-400mm. The thickness of the slab end mainly considers the lateral pressure generated by the flow of the blank during the forming process of the slab end. In the design, it is considered that the force is not less than that caused by the flow of the blank. The maximum transverse pressure generated, the design thickness is determined according to the maximum transverse pressure. This surface is not in contact with the blank, so there is no requirement for surface finish. In Figure 1, the second side wall surface 3-1 is the main working surface for forming the head and tail end faces of the titanium strip. In order to basically achieve the head and tail of the finished titanium strip slab, the design of this surface should be cambered, and the surface finish Ra is not greater than or less than 3.2μm, the arc design range should be controlled between R = 3000 ~ 4000mm, otherwise it will cause the head and tail of the finished slab to sag and the end to be uneven. The first side wall surface 2-1 in Figure 1 should consider the arc design, the surface finish Ra should not be greater than 3.2μm, and the arc design range should be controlled between R=50~100mm. The purpose is mainly to consider the titanium strip blank forming process, Here the billet flow is more difficult to reach. Secondly, if the right-angle design is adopted, it is easy to produce serious stress concentration here, which will cause the tool and die to break from here. In Figure 1, the contact surface in the length and width directions of the blank forming process has the largest contact surface and the largest force. The design mainly considers the size requirements of the blank length and width direction deformation process that the upper surface 1-1 should meet. At the same time, it should be fully considered that the overall flatness of the bottom surface used for a long time in the process of blank deformation should not be greater than 10mm. In Figure 1, the thickness of the bottom surface of the special tool and die, its force is mainly the vertical force between the upper and lower hammer heads on the blank forging, and its thickness is not less than 200mm. The hoisting hole 4 in Fig. 1 is designed considering the convenient hoisting of the tool and die in use. In Figure 1, in the mold, the side wall surface that is not in contact with the billet, since the billet has to be forged from the size range of 600-700mm to 300-400mm, therefore, the design should consider that the net height in contact with the bottom surface is not less than the size of the billet.

本发明还提供一种近净成形钛带板坯的自由锻造加工方法,如图2-10所示,具体按以下步骤实施:The present invention also provides a free forging processing method for near-net-shaped titanium strip slabs, as shown in Figure 2-10, which is specifically implemented according to the following steps:

步骤(1)铸锭制备:将原料钛及钛合金铸锭经过外圆周方向扒皮,去除熔炼过程中产生的表面氧化皮及皮下气孔缺陷,再将铸锭头部进行车平处理,去除熔炼过程中铸锭冒口位置产生的珊瑚状熔瘤缺陷,其次将铸锭底部端面缺陷去除干净,再对铸锭头尾进行圆角处理(见图2);Step (1) ingot preparation: peel the raw material titanium and titanium alloy ingots through the outer circumferential direction, remove the surface oxide scale and subcutaneous pore defects generated during the smelting process, and then carry out the flattening treatment on the head of the ingot to remove the smelting process For the coral-like molten tumor defect generated at the riser position of the middle ingot, then remove the end surface defects at the bottom of the ingot, and then round the head and tail of the ingot (see Figure 2);

步骤(1)中使用的原料钛及钛合金铸锭牌号为TA1、TA2、TA3、TA4或TA10。The grades of raw material titanium and titanium alloy ingots used in step (1) are TA1, TA2, TA3, TA4 or TA10.

步骤(1)中,使用的钛及钛合金铸锭为经过真空自耗电弧法二次熔炼,直径为Φ1000mm及以上锭型。In step (1), the titanium and titanium alloy ingots used are secondary smelting by vacuum consumable arc method, and the diameters are ingot shapes of Φ1000mm and above.

步骤(1)中,铸锭头尾圆角半径R=15mm~20mm。In step (1), the radius R of the head and tail of the ingot is 15mm-20mm.

步骤(2)铸锭加热:铸锭加热应采用科学合理的工艺及加热曲线,才能确保铸锭加热均匀及实现锻造过程。按照一定的加热工艺为铸锭加热;Step (2) ingot heating: scientific and reasonable process and heating curve should be adopted for ingot heating, so as to ensure uniform heating of ingot and realize the forging process. Heating the ingot according to a certain heating process;

步骤(2)中,铸锭加热工艺流程为:先由室温升温到800~850℃,升温时间150~180分钟;然后在800~850℃下保温,保温时间180~250分钟;再升温到1000~1050℃,升温时间180~250分钟;最后在1000~1050℃保温,保温时间180~250分钟。In step (2), the ingot heating process is as follows: firstly, the temperature is raised from room temperature to 800~850°C, and the temperature rise time is 150~180 minutes; then the temperature is kept at 800~850°C for 180~250 minutes; ~1050°C, the heating time is 180~250 minutes; finally, the temperature is kept at 1000~1050°C for 180~250 minutes.

步骤(3)开坯锻造:将加热好的铸锭移送至锻造压机上,采用先轻轻锻造一至两遍,然后加大压下量进行锻造,将加热好的铸锭锻造至厚度在800mm时,将坯料进行翻面,再加大压下量进行锻造,锻造过程中尽量保证上下面变形一致,最终将厚度尺寸控制在600~700mm区间;Step (3) Billeting forging: transfer the heated ingot to the forging press, first lightly forge one to two times, and then increase the reduction for forging, and forge the heated ingot to a thickness of 800mm During the forging process, the billet is turned over, and the reduction is increased for forging. During the forging process, try to ensure that the upper and lower deformations are consistent, and finally control the thickness size within the range of 600-700mm;

步骤(3)中,铸锭开始轻压一至两遍时,压下量控制在30~50mm,再加大压下量进行锻造,压下量控制在单边80~100mm;In step (3), when the ingot is lightly pressed for one to two times, the reduction is controlled at 30-50 mm, and the reduction is further increased for forging, and the reduction is controlled at 80-100 mm on one side;

步骤(4)专用工模具控制锻造:对锻造至600~700mm尺寸区间的坯料,采用上述的模具进行锻造变形;步骤(4)利用金属最小阻力定律变形原理,应采用翻面压制成形;Step (4) Control forging with special tool and die: For the blank forged to the size range of 600-700mm, the above-mentioned die is used for forging deformation; Step (4) Using the deformation principle of the metal minimum resistance law, it should be formed by turning over and pressing;

步骤(4)的具体实施步骤为:对锻造至600~700mm的坯料进行锻造时,使坯料端面靠近专用工模具的第二侧壁面3-1处,通过每次压下100~120mm反复压制,并利用金属最小阻力定律变形原理,将坯料锻造至厚度在300~400mm尺寸之间,得到满足工艺要求的端面形状为凹形的中间坯料;The specific implementation steps of step (4) are: when forging the blank forged to 600-700mm, make the end face of the blank close to the second side wall surface 3-1 of the special tool die, and repeatedly press by pressing down 100-120mm each time, And using the deformation principle of the metal minimum resistance law, the billet is forged to a thickness of 300-400mm, and an intermediate billet with a concave end face shape that meets the process requirements is obtained;

步骤(5)回火加热:制定合理的加热温度曲线,将步骤(4)锻造后的热坯料进行回火加热处理,加热温度为900~950℃,保温时间为90~200分钟得中间坯料;Step (5) tempering heating: formulate a reasonable heating temperature curve, and perform tempering heating treatment on the hot billet after forging in step (4), the heating temperature is 900-950 ° C, and the holding time is 90-200 minutes to obtain an intermediate billet;

步骤(6)成形锻造:将步骤(5)回火加热好的中间坯料在快锻机上进行锻造,得到无板舌、表面无缺陷的钛及钛合金钛带板坯成品坯,如图10所示。无板舌钛带用板坯,应为板坯头尾端面锻后基本平齐,不需要锯切或头尾锯切后锻造成品率不低于98%。Step (6) Forming and forging: the intermediate billet tempered and heated in step (5) is forged on a fast forging machine to obtain a finished billet of titanium and titanium alloy titanium strips without tongue and surface defects, as shown in Figure 10. Show. The slab used for the titanium strip without plate tongue should be basically flush with the head and tail end faces of the slab after forging, without sawing or the forging yield after head and tail sawing is not less than 98%.

步骤(6)中,得到的钛及钛合金钛带板坯成品坯尺寸为:厚度×宽度×长度=180mm~250mm×1000mm~1600mm×5000mm~9000mm的钛带用板坯。In step (6), the obtained titanium and titanium alloy titanium strip slabs have the following dimensions: thickness×width×length=180mm~250mm×1000mm~1600mm×5000mm~9000mm slabs for titanium strips.

钛铸锭在熔炼过程中,其头部均会产生熔瘤现象(见图2),而此熔瘤在后期的钛带板坯生产过程中,将对成品板坯的表面产生严重的表面缺陷。为了避免铸锭熔瘤对板坯表面产生的严重缺陷,本发明方法在对步骤1的铸锭制备过程进行了详细描述,通过铸锭制备过程实施,使熔瘤等铸锭缺陷得到有效控制,实施后铸锭头部形貌明显改善,如3所示。During the smelting process of the titanium ingot, the head of the ingot will produce a lump phenomenon (see Figure 2), and this lump will cause serious surface defects on the surface of the finished slab in the later production process of the titanium strip slab. . In order to avoid serious defects caused by ingot melting on the slab surface, the method of the present invention is described in detail in the ingot preparation process in step 1, and the ingot preparation process is implemented to effectively control ingot defects such as melting nodules. After the implementation, the shape of the head of the ingot is obviously improved, as shown in 3.

本发明铸锭制备过程未实施前,制备板坯过程中,铸锭端面熔瘤翻转到板坯表面,对成品板坯表面产生严重影响,导致板坯头部较长部分无法使用,见图4。Before the ingot preparation process of the present invention is implemented, in the process of preparing the slab, the end face of the ingot is turned over to the surface of the slab, which has a serious impact on the surface of the finished slab, so that the longer part of the slab head cannot be used, see Figure 4 .

本发明铸锭制备过程实施后,铸锭端面熔瘤得到有效去除,铸锭端面熔瘤在制备板坯过程中,对成品板坯表面不再造成严重影响,生产出来的板坯头部表面质量较好,如图5所示。After the ingot preparation process of the present invention is carried out, the end face fusion of the ingot is effectively removed, and the ingot end face fusion no longer has a serious impact on the surface of the finished slab during the slab preparation process, and the surface quality of the produced slab head is Better, as shown in Figure 5.

本发明方法实施前,由于钛带板坯在生产过程中,其铸锭的端面变形过程是自由变形,因此,在上、下锤头的锻打之下,其端面发生自由变形,均产生较大的凸出舌头,而该凸出舌头只能作为废料被切除掉(见图6直线外部分),对成品率影响很大。Before the implementation of the method of the present invention, since the deformation process of the end face of the ingot of the titanium strip slab is free deformation during the production process, under the forging of the upper and lower hammer heads, the end face of the titanium strip is freely deformed, and all of them produce relatively large deformations. The large protruding tongue, which can only be removed as scrap (see the outer part of the straight line in Figure 6), has a great impact on the yield.

为了能最大限度减少头部凸出舌头部分产生的废料损失,本发明方法的步骤4实施过程中,对坯料在变形过程的某一阶段,采用专用工模具对坯料端部的变形实现有效干预,使成品板坯的端部实现平齐,切除极少头部或不切除直接进行端部轻微铣削,大大减少废料损失(见图7直线外部分),最终大幅提高钛带板坯成品率。In order to minimize the waste loss caused by the protruding tongue portion of the head, during the implementation of step 4 of the method of the present invention, at a certain stage of the deformation process of the blank, a special tool and die are used to effectively intervene in the deformation of the end of the blank. The end of the finished slab is flushed, and the end is slightly milled without cutting off or without cutting, which greatly reduces the waste loss (see the outer part of the straight line in Figure 7), and finally greatly improves the yield of the titanium strip slab.

由图8可以看到,实施前板坯头部板舌凸出严重、表面熔瘤等缺陷很多,根本无法使用,因此,切除部分很大,每块板坯头部切掉部分平均在600~700公斤之间,坯料损失很严重,也导致该产品成品率很低。As can be seen from Figure 8, before the implementation of the slab head, the tongue protrudes seriously, and there are many defects such as surface melting, and it cannot be used at all. Therefore, the cut part is very large, and the cut part of the head of each slab is 600~ Between 700 kg, the loss of blanks is very serious, which also leads to a very low yield of the product.

由图9可以看到,实施后板坯头部基本平齐、无凸出板舌,表面熔瘤等缺陷也得到了很好控制,因此,板坯头部切除很小,每块板坯头部切掉或铣掉部分平均在40~80公斤之间,坯料损失很小,成品率显著提高。As can be seen from Figure 9, after the implementation, the slab head is basically flush, there is no protruding plate tongue, and the defects such as surface fusion have been well controlled. Therefore, the slab head is cut very small, and each slab head The average cut or milled part is between 40 and 80 kg, the blank loss is very small, and the yield is significantly improved.

实施例1Example 1

一种近净成形钛带板坯的自由锻造加工方法,具体按以下步骤实施:A method for free forging processing of near-net-shaped titanium strip slabs, which is specifically implemented according to the following steps:

步骤(1)铸锭制备:将真空自耗电弧炉二次熔炼的钛及钛合金铸锭,经过重型车床沿圆周方向扒皮。再将铸锭头部及底部端面缺陷去除干净(特别是铸锭冒口位置产生的珊瑚状缺陷)。其次对铸锭头尾进行圆角处理。Step (1) Ingot preparation: The titanium and titanium alloy ingots smelted by the vacuum consumable electric arc furnace for the second time are peeled along the circumferential direction by a heavy-duty lathe. Then remove the defects on the head and bottom end faces of the ingot (especially the coral-like defects at the riser position of the ingot). Secondly, the head and tail of the ingot are rounded.

步骤(1)中,使用的钛及钛合金铸锭为经过真空自耗电弧法二次熔炼,牌号为TA1,直径为Φ1020mm,,重量为8995kg。In step (1), the titanium and titanium alloy ingots used are secondary smelting by vacuum consumable arc method, the grade is TA1, the diameter is Φ1020mm, and the weight is 8995kg.

步骤(1)中,铸锭头尾圆角半径R=15mm。In step (1), the radius of the rounded corners of the head and tail of the ingot is R=15mm.

步骤(2)铸锭加热:先由室温升温到800℃,升温时间150分钟;然后在800℃下保温,保温时间180分钟;再升温到1000℃,升温时间180分钟;最后在1000℃保温,保温时间180分钟。Step (2) ingot heating: firstly, the temperature is raised from room temperature to 800°C, and the heating time is 150 minutes; then the temperature is kept at 800°C for 180 minutes; the temperature is then raised to 1000°C, and the heating time is 180 minutes; Holding time 180 minutes.

步骤(3)开坯锻造:将加热好的铸锭移送至锻造压机上,采用先轻轻锻造一至两遍,然后加大压下量进行锻造,将加热好的铸锭锻造至厚度在800mm时,将坯料进行翻面,再加大压下量进行锻造,锻造过程中尽量保证上下面变形一致,最终将厚度尺寸控制在600mm区间;Step (3) Billeting forging: transfer the heated ingot to the forging press, first lightly forge one to two times, and then increase the reduction for forging, and forge the heated ingot to a thickness of 800mm During the forging process, the blank is turned over, and the reduction is increased for forging. During the forging process, try to ensure that the upper and lower deformations are consistent, and finally control the thickness size within the range of 600mm;

步骤(3)中,铸锭开始轻压一至两遍时,压下量控制30mm,再加大压下量进行锻造,压下量控制在单边800mm;In step (3), when the ingot is lightly pressed one to two times, the reduction is controlled to 30mm, and the reduction is further increased for forging, and the reduction is controlled at 800mm on one side;

步骤(4)专用工模具控制锻造:对锻造至600mm的坯料进行锻造时,使坯料端面靠近专用工模具的第二侧壁面3-1处,通过每次压下100mm反复压制,并利用金属最小阻力定律变形原理,将坯料锻造至厚度在300mm尺寸之间,得到满足工艺要求的端面形状为凹形的中间坯料;Step (4) Control forging by special tool and die: When forging the blank forged to 600mm, make the end face of the blank close to 3-1 of the second side wall surface of the special tool and die, repeat pressing by pressing down 100mm each time, and use the minimum metal According to the deformation principle of the resistance law, the blank is forged to a thickness of 300mm to obtain an intermediate blank with a concave end face that meets the process requirements;

步骤(5)回火加热:制定合理的加热温度曲线,将步骤(4)锻造后的热坯料进行回火加热处理,加热温度为900℃,保温时间为90分钟得中间坯料;Step (5) tempering heating: formulate a reasonable heating temperature curve, carry out tempering heating treatment on the hot billet after forging in step (4), the heating temperature is 900 ° C, and the holding time is 90 minutes to obtain an intermediate billet;

步骤(6)成形锻造:将回火加热好的中间坯料在锻造压机上进行自由锻造,此过程中应注意板坯整体尺寸、棱角等满足工艺要求,最终得到成品尺寸为:成品尺寸为220(厚度)×1280(宽度)×6970(长度)mm的无板舌钛带用板坯。Step (6) Forming and forging: The tempered and heated intermediate billet is free forged on a forging press. During this process, attention should be paid to the overall size, edges and corners of the slab to meet the technological requirements, and the final finished product size is: the finished product size is 220 (thickness) x 1280 (width) x 6970 (length) mm of slabs for lingual titanium strips.

实施例2Example 2

步骤(1)中使用的钛及钛合金铸锭为经过真空自耗电弧法二次熔炼,牌号为TA1,直径为Φ1020mm,,重量为8960kg。其余锻造方法及工艺参数均与实施例1相同,得到的成品尺寸为:220(厚度)×1280(宽度)×6940(长度)mm。The titanium and titanium alloy ingots used in the step (1) are secondary smelting by vacuum consumable arc method, the grade is TA1, the diameter is Φ1020mm, and the weight is 8960kg. The remaining forging methods and process parameters are the same as in Example 1, and the size of the obtained product is: 220 (thickness)×1280 (width)×6940 (length) mm.

实施例3Example 3

步骤(1)中使用的钛及钛合金铸锭为经过真空自耗电弧法二次熔炼,牌号为TA1,直径为Φ1020mm,,重量为8990kg。其余锻造方法及工艺参数均与实施例1相同,得到的成品尺寸为:220(厚度)×1280(宽度)×6970(长度)mm。The titanium and titanium alloy ingots used in the step (1) are secondary smelting by vacuum consumable arc method, the grade is TA1, the diameter is Φ1020mm, and the weight is 8990kg. The remaining forging methods and process parameters are the same as those in Example 1, and the size of the obtained finished product is: 220 (thickness)×1280 (width)×6970 (length) mm.

实施例1-3效果验证:Example 1-3 Effect verification:

经对实施例1-3得到的三个钛带用板坯进行效果验证,数据如下:After effect verification is carried out to the slabs for three titanium strips obtained in Example 1-3, the data are as follows:

Figure BDA0002699053270000121
Figure BDA0002699053270000121

由验证数据可以看出,三个铸锭锻后成品率较实施前的88%提高了10.42%,达到了98.42%。以年产2万吨该规格钛带产品、目前市场价格为8.5万元/t、残料3万元/t计算,则:20000×10.42%×(8.5-3.0)=11462万元;年可为企业创造经济效益为1.1462亿元。It can be seen from the verification data that the yield of the three ingots after forging has increased by 10.42% compared with 88% before implementation, reaching 98.42%. With an annual output of 20,000 tons of titanium belt products of this specification, the current market price is 85,000 yuan / t, and the residual material is 30,000 yuan / t, then: 20,000 × 10.42% × (8.5-3.0) = 114.62 million yuan; The economic benefit created for the enterprise is 114.62 million yuan.

实施例4Example 4

一种近净成形钛带板坯的自由锻造加工方法,具体按以下步骤实施:A method for free forging processing of near-net-shaped titanium strip slabs, which is specifically implemented according to the following steps:

步骤(1)铸锭制备:将原料钛及钛合金铸锭经过外圆周方向扒皮,去除熔炼过程中产生的表面氧化皮及皮下气孔缺陷,再将铸锭头部进行车平处理,去除熔炼过程中铸锭冒口位置产生的珊瑚状熔瘤缺陷,其次将铸锭底部端面缺陷去除干净,再对铸锭头尾进行圆角处理(见图2);Step (1) ingot preparation: peel the raw material titanium and titanium alloy ingots through the outer circumferential direction, remove the surface oxide scale and subcutaneous pore defects generated during the smelting process, and then carry out the flattening treatment on the head of the ingot to remove the smelting process For the coral-like molten tumor defect generated at the riser position of the middle ingot, then remove the end surface defects at the bottom of the ingot, and then round the head and tail of the ingot (see Figure 2);

步骤(1)中使用的原料钛及钛合金铸锭牌号为TA2,直径为Φ1020mm,重量为9000kg。The raw material titanium and titanium alloy ingots used in the step (1) have a grade of TA2, a diameter of Φ1020mm, and a weight of 9000kg.

步骤(1)中,使用的钛及钛合金铸锭为经过真空自耗电弧法二次熔炼,直径为Φ1500mm。In step (1), the titanium and titanium alloy ingots used are secondary smelted by vacuum consumable arc method, and the diameter is Φ1500mm.

步骤(1)中,铸锭头尾圆角半径R=20mm。In step (1), the radius of the ingot head and tail fillet is R=20mm.

步骤(2)铸锭加热:铸锭加热应采用科学合理的工艺及加热曲线,才能确保铸锭加热均匀及实现锻造过程。按照一定的加热工艺为铸锭加热;Step (2) ingot heating: scientific and reasonable process and heating curve should be adopted for ingot heating, so as to ensure uniform heating of ingot and realize the forging process. Heating the ingot according to a certain heating process;

步骤(2)中,铸锭加热工艺流程为:先由室温升温到850℃,升温时间180分钟;然后在850℃下保温,保温时间250分钟;再升温到1050℃,升温时间250分钟;最后在1050℃保温,保温时间250分钟。In step (2), the ingot heating process is as follows: firstly, the temperature is raised from room temperature to 850°C, and the temperature rise time is 180 minutes; then the temperature is kept at 850°C, and the temperature rise time is 250 minutes; Incubate at 1050°C for 250 minutes.

步骤(3)开坯锻造:将加热好的铸锭移送至锻造压机上,采用先轻轻锻造一至两遍,然后加大压下量进行锻造,将加热好的铸锭锻造至厚度在800mm时,将坯料进行翻面,再加大压下量进行锻造,锻造过程中尽量保证上下面变形一致,最终将厚度尺寸控制在700mm区间;Step (3) Billeting forging: transfer the heated ingot to the forging press, first lightly forge one to two times, and then increase the reduction for forging, and forge the heated ingot to a thickness of 800mm During the forging process, the blank is turned over, and the reduction is increased for forging. During the forging process, the upper and lower deformations are kept as consistent as possible, and the thickness size is finally controlled within the 700mm range;

步骤(3)中,铸锭开始轻压一至两遍时,压下量控制在50mm,再加大压下量进行锻造,压下量控制在单边100mm;In step (3), when the ingot is lightly pressed one to two times, the reduction is controlled at 50mm, and the reduction is further increased for forging, and the reduction is controlled at 100mm on one side;

步骤(4)专用工模具控制锻造:对锻造至700mm尺寸区间的坯料,采用上述的模具进行锻造变形;步骤(4)利用金属最小阻力定律变形原理,应采用翻面压制成形;Step (4) Control forging with special tool and die: For the blank forged to the size range of 700mm, the above-mentioned die is used for forging deformation; Step (4) utilizes the deformation principle of the law of least resistance of metal, and should be turned over to press and form;

步骤(4)的具体实施步骤为:对锻造至700mm的坯料进行锻造时,使坯料端面靠近专用工模具的第二侧壁面3-1处,通过每次压下120mm反复压制,并利用金属最小阻力定律变形原理,将坯料锻造至厚度在400mm尺寸之间,得到满足工艺要求的端面形状为凹形的中间坯料;The specific implementation steps of step (4) are as follows: when forging the blank forged to 700mm, make the end face of the blank close to the second side wall surface 3-1 of the special tool and die, and repeatedly press down by 120mm each time, and use the metal minimum. According to the deformation principle of the resistance law, the blank is forged to a thickness of 400mm to obtain an intermediate blank with a concave end face that meets the process requirements;

步骤(5)回火加热:制定合理的加热温度曲线,将步骤(4)锻造后的热坯料进行回火加热处理,加热温度为950℃,保温时间为200分钟得中间坯料;Step (5) tempering heating: formulate a reasonable heating temperature curve, carry out tempering heating treatment on the hot blank after forging in step (4), the heating temperature is 950 ° C, and the holding time is 200 minutes to obtain an intermediate blank;

步骤(6)成形锻造:将步骤(5)回火加热好的中间坯料在快锻机上进行锻造,得到无板舌、表面无缺陷的钛及钛合金钛带板坯成品坯,如图10所示。无板舌钛带用板坯,应为板坯头尾端面锻后基本平齐,不需要锯切或头尾锯切后锻造成品率不低于98%。Step (6) Forming and forging: the intermediate billet tempered and heated in step (5) is forged on a fast forging machine to obtain a finished billet of titanium and titanium alloy titanium strips without tongue and surface defects, as shown in Figure 10. Show. The slab used for the titanium strip without plate tongue should be basically flush with the head and tail end faces of the slab after forging, without sawing or the forging yield after head and tail sawing is not less than 98%.

步骤(6)中,得到的钛及钛合金钛带板坯成品坯尺寸为:厚度×宽度×长度=250mm×1600mm×9000mm的钛带用板坯。In step (6), the size of the obtained titanium and titanium alloy titanium strip slabs is: thickness×width×length=250mm×1600mm×9000mm of titanium strip slabs.

实施例5Example 5

一种近净成形钛带板坯的自由锻造加工方法,具体按以下步骤实施:A method for free forging processing of near-net-shaped titanium strip slabs, which is specifically implemented according to the following steps:

步骤(1)铸锭制备:将原料钛及钛合金铸锭经过外圆周方向扒皮,去除熔炼过程中产生的表面氧化皮及皮下气孔缺陷,再将铸锭头部进行车平处理,去除熔炼过程中铸锭冒口位置产生的珊瑚状熔瘤缺陷,其次将铸锭底部端面缺陷去除干净,再对铸锭头尾进行圆角处理(见图2);Step (1) ingot preparation: peel the raw material titanium and titanium alloy ingots through the outer circumferential direction, remove the surface oxide scale and subcutaneous pore defects generated during the smelting process, and then carry out the flattening treatment on the head of the ingot to remove the smelting process For the coral-like molten tumor defect generated at the riser position of the middle ingot, then remove the end surface defects at the bottom of the ingot, and then round the head and tail of the ingot (see Figure 2);

步骤(1)中使用的原料钛及钛合金铸锭牌号为TA3,直径为Φ1020mm,重量为9000kg。The raw material titanium and the titanium alloy ingot used in the step (1) have a grade of TA3, a diameter of Φ1020mm, and a weight of 9000kg.

步骤(1)中,使用的钛及钛合金铸锭为经过真空自耗电弧法二次熔炼,直径为Φ1200mm。In step (1), the titanium and titanium alloy ingots used are secondary smelting by vacuum consumable arc method, and the diameter is Φ1200mm.

步骤(1)中,铸锭头尾圆角半径R=18mm。In step (1), the radius of the ingot head and tail fillet is R=18mm.

步骤(2)铸锭加热:铸锭加热应采用科学合理的工艺及加热曲线,才能确保铸锭加热均匀及实现锻造过程。按照一定的加热工艺为铸锭加热;Step (2) ingot heating: scientific and reasonable process and heating curve should be adopted for ingot heating, so as to ensure uniform heating of ingot and realize the forging process. Heating the ingot according to a certain heating process;

步骤(2)中,铸锭加热工艺流程为:先由室温升温到820℃,升温时间160分钟;然后在830℃下保温,保温时间200分钟;再升温到1030℃,升温时间200分钟;最后在1030℃保温,保温时间200分钟。In step (2), the ingot heating process is as follows: firstly, the temperature is raised from room temperature to 820° C., and the heating time is 160 minutes; then the temperature is kept at 830° C., and the heating time is 200 minutes; Incubate at 1030°C for 200 minutes.

步骤(3)开坯锻造:将加热好的铸锭移送至锻造压机上,采用先轻轻锻造一至两遍,然后加大压下量进行锻造,将加热好的铸锭锻造至厚度在800mm时,将坯料进行翻面,再加大压下量进行锻造,锻造过程中尽量保证上下面变形一致,最终将厚度尺寸控制在650mm区间;Step (3) Billeting forging: transfer the heated ingot to the forging press, first lightly forge one to two times, and then increase the reduction for forging, and forge the heated ingot to a thickness of 800mm During the forging process, the blank is turned over, and the reduction is increased for forging. During the forging process, try to ensure that the upper and lower deformations are consistent, and finally control the thickness size within the range of 650mm;

步骤(3)中,铸锭开始轻压一至两遍时,压下量控制在40mm,再加大压下量进行锻造,压下量控制在单边90mm;In step (3), when the ingot is lightly pressed one to two times, the reduction is controlled at 40mm, and the reduction is further increased for forging, and the reduction is controlled at 90mm on one side;

步骤(4)专用工模具控制锻造:对锻造至650mm尺寸区间的坯料,采用上述的模具进行锻造变形;步骤(4)利用金属最小阻力定律变形原理,应采用翻面压制成形;Step (4) Control forging with special tool and die: For the blank forged to the size range of 650mm, the above-mentioned die is used for forging deformation; Step (4) utilizes the deformation principle of the law of least resistance of metal, and should be turned over to press and form;

步骤(4)的具体实施步骤为:对锻造至650mm的坯料进行锻造时,使坯料端面靠近专用工模具的第二侧壁面3-1处,通过每次压下110mm反复压制,并利用金属最小阻力定律变形原理,将坯料锻造至厚度在350mm尺寸之间,得到满足工艺要求的端面形状为凹形的中间坯料;The specific implementation steps of step (4) are: when forging the blank forged to 650mm, make the end face of the blank close to the second side wall surface 3-1 of the special tool and die, and repeatedly press down by 110mm each time, and use the metal minimum. According to the deformation principle of the resistance law, the blank is forged to a thickness of 350mm to obtain an intermediate blank with a concave end face that meets the process requirements;

步骤(5)回火加热:制定合理的加热温度曲线,将步骤(4)锻造后的热坯料进行回火加热处理,加热温度为920℃,保温时间为100分钟得中间坯料;Step (5) tempering heating: formulate a reasonable heating temperature curve, and perform tempering heating treatment on the hot billet after forging in step (4), the heating temperature is 920 ° C, and the holding time is 100 minutes to obtain an intermediate billet;

步骤(6)成形锻造:将步骤(5)回火加热好的中间坯料在快锻机上进行锻造,得到无板舌、表面无缺陷的钛及钛合金钛带板坯成品坯,如图10所示。无板舌钛带用板坯,应为板坯头尾端面锻后基本平齐,不需要锯切或头尾锯切后锻造成品率不低于98%。Step (6) Forming and forging: the intermediate billet tempered and heated in step (5) is forged on a fast forging machine to obtain a finished billet of titanium and titanium alloy titanium strips without tongue and surface defects, as shown in Figure 10. Show. The slab used for the titanium strip without plate tongue should be basically flush with the head and tail end faces of the slab after forging, without sawing or the forging yield after head and tail sawing is not less than 98%.

步骤(6)中,得到的钛及钛合金钛带板坯成品坯尺寸为:厚度×宽度×长度=200mm×1500mm×6000mm的钛带用板坯。In step (6), the size of the obtained titanium and titanium alloy titanium strip slab blanks is: thickness×width×length=200mm×1500mm×6000mm of titanium strip slabs.

Claims (10)

1.一种近净成形钛带板坯的锻造用模具,其特征在于,包括有底板(1),所述底板(1)的一端端部由下至上依次设置有过渡挡板(2)及竖直挡板(3),过渡挡板(2)的第一侧壁面(2-1)及竖直挡板(3)的第二侧壁面(3-1)同侧,第一侧壁面(2-1)、第二侧壁面(3-1)及上表面(1-1)均为模具与坯料的接触面;1. A forging die for near-net-shaped titanium strip slabs, characterized in that it comprises a bottom plate (1), and one end of the bottom plate (1) is sequentially provided with a transition baffle plate (2) and The vertical baffle (3), the first side wall surface (2-1) of the transition baffle (2) and the second side wall surface (3-1) of the vertical baffle (3) are on the same side, and the first side wall surface ( 2-1), the second side wall surface (3-1) and the upper surface (1-1) are the contact surfaces between the mold and the blank; 第一侧壁面(2-1)及第二侧壁面(3-1)均为弧面,第一底板(1)的上表面(1-1)为矩形平面,第一侧壁面(2-1)通过第二侧壁面(3-1)过渡与上表面(1-1)平滑连接;底板(1)的侧壁面上设置有若干个吊装孔(4)。The first side wall surface (2-1) and the second side wall surface (3-1) are arc surfaces, the upper surface (1-1) of the first bottom plate (1) is a rectangular plane, and the first side wall surface (2-1) ) is smoothly connected to the upper surface (1-1) through the transition of the second side wall surface (3-1); a plurality of hoisting holes (4) are arranged on the side wall surface of the bottom plate (1). 2.根据权利要求1所述的一种近净成形钛带板坯的锻造用模具,其特征在于,第一侧壁面(2-1)的弧度对应的半径R=50~100mm;第二侧壁面(3-1)的弧度对应的半径R=3000~4000mm。2 . The forging die for near-net-shape titanium strip slabs according to claim 1 , wherein the radius corresponding to the curvature of the first side wall surface (2-1) is R=50-100 mm; the second side The radius R=3000~4000mm corresponding to the radian of the wall surface (3-1). 3.根据权利要求1所述的一种近净成形钛带板坯的锻造用模具,其特征在于,第一侧壁面(2-1)、第二侧壁面(3-1)及上表面(1-1)的表面光洁度Ra均不大于3.2μm;底板(1)的厚度不小于200mm;竖直挡板(3)的厚度为200~400mm。3. The forging die for a near-net-shape titanium strip slab according to claim 1, wherein the first side wall surface (2-1), the second side wall surface (3-1) and the upper surface ( The surface finish Ra of 1-1) is not greater than 3.2 μm; the thickness of the bottom plate (1) is not less than 200 mm; the thickness of the vertical baffle plate (3) is 200-400 mm. 4.根据权利要求1所述的一种近净成形钛带板坯的锻造用模具,其特征在于,底板(1)、过渡挡板(2)及竖直挡板(3)均为5CrMnMo板。4. The forging die of a near-net-shaped titanium strip slab according to claim 1, wherein the bottom plate (1), the transition baffle plate (2) and the vertical baffle plate (3) are all 5CrMnMo plates . 5.一种近净成形钛带板坯的自由锻造加工方法,其特征在于,具体按以下步骤实施:5. a free forging processing method of near-net-shaped titanium strip slab, is characterized in that, is specifically implemented according to the following steps: 步骤(1)铸锭制备:将原料钛及钛合金铸锭经过外圆周方向扒皮,去除熔炼过程中产生的表面氧化皮及皮下气孔缺陷,再将铸锭头部进行车平处理,去除熔炼过程中铸锭冒口位置产生的珊瑚状熔瘤缺陷,其次将铸锭底部端面缺陷去除干净,再对铸锭头尾进行圆角处理;Step (1) ingot preparation: peel the raw material titanium and titanium alloy ingots through the outer circumferential direction, remove the surface oxide scale and subcutaneous pore defects generated during the smelting process, and then carry out the flattening treatment on the head of the ingot to remove the smelting process The coral-like molten tumor defect generated at the riser position of the middle ingot, and then the end face defects at the bottom of the ingot are removed, and then the head and tail of the ingot are rounded; 步骤(2)铸锭加热:按照一定的加热工艺为铸锭加热;Step (2) ingot heating: heating the ingot according to a certain heating process; 步骤(3)开坯锻造:将加热好的铸锭移送至锻造压机上,采用先轻轻锻造一至两遍,然后加大压下量进行锻造,将加热好的铸锭锻造至厚度在800mm时,将坯料进行翻面,再加大压下量进行锻造,锻造过程中尽量保证上下面变形一致,最终将厚度尺寸控制在600~700mm区间;Step (3) Billeting forging: transfer the heated ingot to the forging press, first lightly forge one to two times, and then increase the reduction for forging, and forge the heated ingot to a thickness of 800mm During the forging process, the billet is turned over, and the reduction is increased for forging. During the forging process, try to ensure that the upper and lower deformations are consistent, and finally control the thickness size within the range of 600-700mm; 步骤(4)专用工模具控制锻造:对锻造至600~700mm尺寸区间的坯料,采用如权利要求1-4任意一项所述的模具进行锻造变形;Step (4) Controlling forging by special tool and die: forging the billet in the size range of 600-700mm, using the die according to any one of claims 1-4 to carry out forging deformation; 步骤(5)回火加热:将步骤(4)锻造后的热坯料进行回火加热处理,加热温度为900~950℃,保温时间为90~200分钟得中间坯料;Step (5) tempering and heating: perform tempering and heating treatment on the hot billet after forging in step (4), the heating temperature is 900-950° C., and the holding time is 90-200 minutes to obtain an intermediate billet; 步骤(6)成形锻造:将步骤(5)回火加热好的中间坯料在快锻机上进行锻造,得到钛及钛合金钛带板坯成品坯。Step (6) forming and forging: the intermediate billet tempered and heated in step (5) is forged on a fast forging machine to obtain finished billets of titanium and titanium alloy titanium strip slabs. 6.根据权利要求5所述的一种近净成形钛带板坯的自由锻造加工方法,其特征在于,步骤(1)中使用的原料钛及钛合金铸锭牌号为TA1、TA2、TA3、TA4或TA10。6. the free forging processing method of a kind of near-net-shape titanium strip slab according to claim 5, is characterized in that, the raw material titanium used in step (1) and titanium alloy ingot grades are TA1, TA2, TA3, TA4 or TA10. 7.根据权利要求5所述的一种近净成形钛带板坯的自由锻造加工方法,其特征在于,步骤(1)中,使用的钛及钛合金铸锭为经过真空自耗电弧法二次熔炼,直径为Φ1000mm及以上锭型。7. the free forging processing method of a kind of near-net-shape titanium strip slab according to claim 5, is characterized in that, in step (1), the titanium and titanium alloy ingots used are through vacuum consumable arc method Secondary smelting, ingots with a diameter of Φ1000mm and above. 8.根据权利要求5所述的一种近净成形钛带板坯的自由锻造加工方法,其特征在于,步骤(1)中,铸锭头尾圆角半径R=15mm~20mm。8 . The method for free forging of near-net-shaped titanium strip slabs according to claim 5 , wherein, in step (1), the radius of the head and tail fillets of the ingot is R=15mm~20mm. 9 . 9.根据权利要求5所述的一种近净成形钛带板坯的自由锻造加工方法,其特征在于,步骤(2)中,铸锭加热工艺流程为:先由室温升温到800~850℃,升温时间150~180分钟;然后在800~850℃下保温,保温时间180~250分钟;再升温到1000~1050℃,升温时间180~250分钟;最后在1000~1050℃保温,保温时间180~250分钟。9 . The free forging processing method of a near-net-shaped titanium strip slab according to claim 5 , wherein, in step (2), the ingot heating process is as follows: firstly, the temperature is raised from room temperature to 800-850° C. 9 . , the heating time is 150 to 180 minutes; then the temperature is kept at 800 to 850 ° C for 180 to 250 minutes; the temperature is then raised to 1000 to 1050 ° C, and the heating time is 180 to 250 minutes; ~250 minutes. 10.根据权利要求5所述的一种近净成形钛带板坯的自由锻造加工方法,其特征在于,步骤(3)中,铸锭开始轻压一至两遍时,压下量控制在30~50mm,再加大压下量进行锻造,压下量控制在单边80~100mm;步骤(4)的具体实施步骤为:对锻造至600~700mm的坯料进行锻造时,使坯料端面靠近专用工模具的第二侧壁面(3-1)处,通过每次压下100~120mm反复压制,将坯料锻造至厚度在300~400mm尺寸之间;步骤(6)中,得到的钛及钛合金钛带板坯成品坯尺寸为:厚度×宽度×长度=180mm~250mm×1000mm~1600mm×5000mm~9000mm的钛带用板坯。10. The free forging processing method of a near-net-shaped titanium strip slab according to claim 5, characterized in that, in step (3), when the ingot starts to be lightly pressed one to two times, the reduction is controlled at 30 ~50mm, and then increase the reduction amount for forging, and the reduction amount is controlled at 80 ~ 100mm on one side; the specific implementation steps of step (4) are: when forging the billet forged to 600 ~ 700mm, make the end face of the billet close to the special purpose At the second side wall surface (3-1) of the tool die, the blank is forged to a thickness of 300 to 400 mm by repeatedly pressing down 100 to 120 mm each time; in step (6), the obtained titanium and titanium alloy The size of the finished titanium strip slab is: thickness×width×length=180mm~250mm×1000mm~1600mm×5000mm~9000mm slab for titanium strip.
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