CN111848090A - Preparation method of low-cost humidity-adjusting plastering gypsum - Google Patents
Preparation method of low-cost humidity-adjusting plastering gypsum Download PDFInfo
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- CN111848090A CN111848090A CN202010772144.4A CN202010772144A CN111848090A CN 111848090 A CN111848090 A CN 111848090A CN 202010772144 A CN202010772144 A CN 202010772144A CN 111848090 A CN111848090 A CN 111848090A
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/14—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing calcium sulfate cements
- C04B28/142—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing calcium sulfate cements containing synthetic or waste calcium sulfate cements
- C04B28/144—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing calcium sulfate cements containing synthetic or waste calcium sulfate cements the synthetic calcium sulfate being a flue gas desulfurization product
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B11/00—Calcium sulfate cements
- C04B11/02—Methods and apparatus for dehydrating gypsum
- C04B11/028—Devices therefor characterised by the type of calcining devices used therefor or by the type of hemihydrate obtained
- C04B11/036—Devices therefor characterised by the type of calcining devices used therefor or by the type of hemihydrate obtained for the dry process, e.g. dehydrating in a fluidised bed or in a rotary kiln, i.e. to obtain beta-hemihydrate
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B14/00—Use of inorganic materials as fillers, e.g. pigments, for mortars, concrete or artificial stone; Treatment of inorganic materials specially adapted to enhance their filling properties in mortars, concrete or artificial stone
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B18/00—Use of agglomerated or waste materials or refuse as fillers for mortars, concrete or artificial stone; Treatment of agglomerated or waste materials or refuse, specially adapted to enhance their filling properties in mortars, concrete or artificial stone
- C04B18/04—Waste materials; Refuse
- C04B18/18—Waste materials; Refuse organic
- C04B18/24—Vegetable refuse, e.g. rice husks, maize-ear refuse; Cellulosic materials, e.g. paper, cork
- C04B18/241—Paper, e.g. waste paper; Paper pulp
- C04B18/243—Waste from paper processing or recycling paper, e.g. de-inking sludge
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B22/00—Use of inorganic materials as active ingredients for mortars, concrete or artificial stone, e.g. accelerators, shrinkage compensating agents
- C04B22/06—Oxides, Hydroxides
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B24/00—Use of organic materials as active ingredients for mortars, concrete or artificial stone, e.g. plasticisers
- C04B24/12—Nitrogen containing compounds organic derivatives of hydrazine
- C04B24/14—Peptides; Proteins; Derivatives thereof
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2103/00—Function or property of ingredients for mortars, concrete or artificial stone
- C04B2103/10—Accelerators; Activators
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/00474—Uses not provided for elsewhere in C04B2111/00
- C04B2111/00482—Coating or impregnation materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/50—Mortars, concrete or artificial stone characterised by specific physical values for the mechanical strength
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/50—Reuse, recycling or recovery technologies
- Y02W30/91—Use of waste materials as fillers for mortars or concrete
Abstract
The invention discloses a preparation method of low-cost humidity-regulating plastering gypsum, which is characterized in that desulfurized gypsum is calcined to obtain beta-type semi-hydrated gypsum, the beta-semi-hydrated gypsum, causticized white sludge are uniformly stirred, and then uniformly stirred with hydroxypropyl methyl cellulose, lignocellulose, zinc oxide, Bonaite and ultrahigh-gel-degree protein powder. The low-cost humidity-regulating plastering gypsum can be replaced by causticized white sludge and ultrahigh-gel-degree protein powder without adding expensive imports of a dispersing rubber powder and a retarder, not only can achieve the strength of the plastering gypsum, but also has low cost and cannot cause the phenomenon of shrinkage cracking. In the invention, a small amount of bonite is added, so that the strength of the plastering gypsum can be effectively improved, and a small amount of zinc oxide is added as a catalyst, thereby being beneficial to adjusting the humidity.
Description
Technical Field
The invention relates to the technical field of plastering gypsum, in particular to a preparation method of low-cost humidity-regulating plastering gypsum.
Background
The currently marketed bottom layer plastering gypsum is usually manufactured by mixing outsourced mixed sand and surface layer plastering gypsum in proportion, the product performance produced by the method has higher dependence degree on the stability of the sand, and if the supply quality of the sand is unstable, the product performance is greatly influenced. The thickness and mixing ratio of the sand, i.e., the sand grains of different grain sizes, greatly affect the performance of the plastering gypsum because of: in concrete, the surface of the sand needs to be covered by gypsum slurry, and the greater the total surface area of the sand, the more gypsum slurry needs to be covered on the surface of the sand. Under the condition of the same dosage, the total surface area of the fine sand is larger, and the total surface area of the coarse sand is smaller, while the traditional process usually adopts powdery quartz sand, and the powdery quartz sand brings the reduction of the cracking resistance after exceeding a certain thickness.
The invention has strict requirements on the quality of the sand, and carries out deep research and analysis on the gradation of the sand, so that the prepared product has strong bonding force, effectively inhibits the shrinkage cracking phenomenon in plastering, and better solves the common problems of hollowing cracking, falling off and the like of cement mortar and mixed mortar plastering. In order to reduce the cost and effectively prevent the shrinkage cracking, it is necessary to research a low-cost preparation method of the humidity-controlling plastering gypsum.
Disclosure of Invention
Based on the technical problems in the background art, the invention provides a preparation method of low-cost humidity-regulating plastering gypsum.
The technical scheme of the invention is as follows:
a preparation method of low-cost humidity-regulating plastering gypsum comprises the following steps:
A. after being pre-dried at the temperature of 80-90 ℃, the desulfurized gypsum enters a boiling calciner, is calcined at the temperature of 120-130 ℃, is added into an impact type flour mill for grinding, and is aged after being cooled;
B. uniformly stirring the aged desulfurized gypsum and the causticized white sludge, repeatedly grinding, and sieving by a 325-mesh sieve;
C. then adding hydroxypropyl methyl cellulose, lignocellulose, zinc oxide, bonite and ultrahigh-gel-degree protein powder, uniformly stirring, grinding and sieving with a 200-mesh sieve.
Preferably, the aging time in the step A is 7 to 10 days.
Preferably, in the step B, the causticized white slime is paper-making alkali recovery causticized white slime with the water content of 8-15%.
Preferably, in the step C, the raw material of the ultrahigh-gelation-degree protein powder is eggs.
More preferably, in the step C, the gel degree of the ultrahigh gel degree protein powder is 1200-1400g cm-2。
Preferably, the low-cost humidity-regulating plastering gypsum consists of the following components in percentage by weight: 8-15% of causticized white sludge, 1-3% of hydroxypropyl methyl cellulose, 2-5% of lignocellulose, 1-2% of ultrahigh-gel-degree protein powder, 0.02-0.05% of zinc oxide, 0.2-0.5% of Bonaite and the balance of desulfurized gypsum.
Bonite is a new synthetic dense refractory aggregate based on a mineral phase of calcium hexaluminate (CA 6). CA6 has the following main properties: high refractoriness; high stability in reducing atmosphere (such as carbon monoxide); the chemical stability in alkaline environment is good; has low wettability to molten metal and slag.
The invention has the advantages that: the preparation method of the low-cost humidity-regulating plastering gypsum adopts the desulfurized gypsum to calcine to obtain the beta-semi-hydrated gypsum, uniformly mixes the beta-semi-hydrated gypsum with causticized white sludge, mixes the beta-semi-hydrated gypsum with hydroxypropyl methyl cellulose, lignocellulose, zinc oxide, bonite and ultrahigh-gelation-degree protein powder, and uniformly mixes the beta-semi-hydrated gypsum with the causticized white sludge to obtain the low-cost humidity-regulating plastering gypsum. The low-cost humidity-regulating plastering gypsum can be replaced by causticized white sludge and ultrahigh-gel-degree protein powder without adding expensive imports of a dispersing rubber powder and a retarder, not only can achieve the strength of the plastering gypsum, but also has low cost and cannot cause the phenomenon of shrinkage cracking. In the invention, a small amount of bonite is added, so that the strength of the plastering gypsum can be effectively improved, and a small amount of zinc oxide is added as a catalyst, thereby being beneficial to adjusting the humidity.
Detailed Description
Example 1
A preparation method of low-cost humidity-regulating plastering gypsum comprises the following steps:
A. after being pre-dried at the temperature of 82 ℃, the desulfurized gypsum enters a boiling calciner, is calcined at the temperature of 128 ℃, is added into an impact type pulverizer for grinding, and is aged after being cooled;
B. uniformly stirring the aged desulfurized gypsum and the causticized white sludge, repeatedly grinding, and sieving by a 325-mesh sieve;
C. then adding hydroxypropyl methyl cellulose, lignocellulose, zinc oxide, bonite and ultrahigh-gel-degree protein powder, uniformly stirring, grinding and sieving with a 200-mesh sieve.
The aging time in the step A is 9 days.
In the step B, the causticized white slime is papermaking alkali recovery causticized white slime with the water content of 12 percent.
In the step C, the raw material of the ultrahigh-gelation-degree protein powder is eggs. In the step C, the gel degree of the protein powder with the ultrahigh gel degree is 1300g cm-2。
The low-cost humidity-regulating plastering gypsum consists of the following components in percentage by weight: 12% of causticized white sludge, 2% of hydroxypropyl methylcellulose, 4% of lignocellulose, 1.5% of ultrahigh-gelation-degree protein powder, 0.03% of zinc oxide, 0.3% of Bonaite and the balance of desulfurized gypsum.
Example 2
A preparation method of low-cost humidity-regulating plastering gypsum comprises the following steps:
A. after being pre-dried at the temperature of 90 ℃, the desulfurized gypsum enters a boiling calciner, is calcined at the temperature of 120 ℃, is added into an impact type pulverizer for grinding, and is aged after being cooled;
B. uniformly stirring the aged desulfurized gypsum and the causticized white sludge, repeatedly grinding, and sieving by a 325-mesh sieve;
C. then adding hydroxypropyl methyl cellulose, lignocellulose, zinc oxide, bonite and ultrahigh-gel-degree protein powder, uniformly stirring, grinding and sieving with a 200-mesh sieve.
The aging time in the step A is 7 days.
In the step B, the causticized white slime is papermaking alkali recovery causticized white slime with the water content of 15 percent.
In the step C, the raw material of the ultrahigh-gelation-degree protein powder is eggs. In the step C, the gel degree of the ultrahigh-gel-degree protein powder is 1200g cm-2。
The low-cost humidity-regulating plastering gypsum consists of the following components in percentage by weight: 15% of causticized white sludge, 3% of hydroxypropyl methylcellulose, 2% of lignocellulose, 1% of ultrahigh-gelation-degree protein powder, 0.05% of zinc oxide, 0.2% of Bonet and the balance of desulfurized gypsum.
Example 3
A preparation method of low-cost humidity-regulating plastering gypsum comprises the following steps:
A. after being pre-dried at the temperature of 80 ℃, the desulfurized gypsum enters a boiling calciner, is calcined at the temperature of 130 ℃, is added into an impact type pulverizer for grinding, and is aged after being cooled;
B. uniformly stirring the aged desulfurized gypsum and the causticized white sludge, repeatedly grinding, and sieving by a 325-mesh sieve;
C. then adding hydroxypropyl methyl cellulose, lignocellulose, zinc oxide, bonite and ultrahigh-gel-degree protein powder, uniformly stirring, grinding and sieving with a 200-mesh sieve.
The aging time in the step A is 10 days.
In the step B, the causticized white slime is papermaking alkali recovery causticized white slime with the water content of 8 percent.
In the step C, the raw material of the ultrahigh-gelation-degree protein powder is eggs. In the step C, the gel degree of the ultrahigh-gel-degree protein powder is 1400g cm-2。
The low-cost humidity-regulating plastering gypsum consists of the following components in percentage by weight: 8% of causticized white sludge, 1% of hydroxypropyl methylcellulose, 5% of lignocellulose, 2% of ultrahigh-gel-degree protein powder, 0.02% of zinc oxide, 0.5% of Bonaite and the balance of desulfurized gypsum.
Example 4
A preparation method of low-cost humidity-regulating plastering gypsum comprises the following steps:
A. after being pre-dried at the temperature of 88 ℃, the desulfurized gypsum enters a boiling calciner, is calcined at the temperature of 122 ℃, is added into an impact type pulverizer for grinding, and is aged after being cooled;
B. uniformly stirring the aged desulfurized gypsum and the causticized white sludge, repeatedly grinding, and sieving by a 325-mesh sieve;
C. then adding hydroxypropyl methyl cellulose, lignocellulose, zinc oxide, bonite and ultrahigh-gel-degree protein powder, uniformly stirring, grinding and sieving with a 200-mesh sieve.
The aging time in the step A is 7 days.
In the step B, the causticized white slime is papermaking alkali recovery causticized white slime with the water content of 10 percent.
In the step C, the raw material of the ultrahigh-gelation-degree protein powder is eggs. In the step C, the gel degree of the ultrahigh-gel-degree protein powder is 1320g cm-2。
The low-cost humidity-regulating plastering gypsum consists of the following components in percentage by weight: 10% of causticized white sludge, 2.5% of hydroxypropyl methylcellulose, 3.5% of lignocellulose, 1.2% of ultrahigh-gel-degree protein powder, 0.03% of zinc oxide, 0.3% of bonite and the balance of desulfurized gypsum.
Example 5
A preparation method of low-cost humidity-regulating plastering gypsum comprises the following steps:
A. after being pre-dried at the temperature of 90 ℃, the desulfurized gypsum enters a boiling calciner, is calcined at the temperature of 130 ℃, is added into an impact type pulverizer for grinding, and is aged after being cooled;
B. uniformly stirring the aged desulfurized gypsum and the causticized white sludge, repeatedly grinding, and sieving by a 325-mesh sieve;
C. then adding hydroxypropyl methyl cellulose, lignocellulose, zinc oxide, bonite and ultrahigh-gel-degree protein powder, uniformly stirring, grinding and sieving with a 200-mesh sieve.
The aging time in the step A is 8 days.
In the step B, the causticized white slime is papermaking alkali recovery causticized white slime with the water content of 9 percent.
In the step C, the raw material of the ultrahigh-gelation-degree protein powder is eggs. In the step C, the gel content of the ultrahigh-gel-content protein powder is 1285g cm-2。
The low-cost humidity-regulating plastering gypsum consists of the following components in percentage by weight: 12.5 percent of causticized white sludge, 2.5 percent of hydroxypropyl methylcellulose, 3.5 percent of lignocellulose, 1.5 percent of ultrahigh-gel-degree protein powder, 0.04 percent of zinc oxide, 0.3 percent of Bonaite and the balance of desulfurized gypsum.
Comparative example 1
The ultra-high-gel-degree protein powder in the example 1 is removed, and the rest proportion and the preparation method are unchanged.
Comparative example 2
The ultra-high gel protein powder in the example 1 is replaced by the protein powder with the gel degree of 800g cm-2The rest proportion and the preparation method of the protein powder are unchanged.
Comparative example 3
The zinc oxide in example 1 was removed, and the rest of the formulation and preparation method were unchanged.
The plastering gypsum prepared in examples 1 to 5 and comparative examples 1 to 3 were examined as follows according to JC/T517-one 2004 plastering gypsum, the results of which are shown in Table 1.
The moisture absorption amount is tested under the test conditions of room temperature 25 ℃ and moisture absorption humidity of 75 percent in the above 24 h; the moisture release amount is tested under the test conditions of room temperature 25 ℃ and moisture release humidity of 35 percent after 24 h.
From the above test data, it can be seen that the low-cost humidity-conditioning render gypsum of the present invention can meet the standard requirements for render gypsum.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.
Claims (6)
1. A preparation method of low-cost humidity-regulating plastering gypsum is characterized by comprising the following steps:
A. after being pre-dried at the temperature of 80-90 ℃, the desulfurized gypsum enters a boiling calciner, is calcined at the temperature of 120-130 ℃, is added into an impact type flour mill for grinding, and is aged after being cooled;
B. uniformly stirring the aged desulfurized gypsum and the causticized white sludge, repeatedly grinding, and sieving by a 325-mesh sieve;
C. then adding hydroxypropyl methyl cellulose, lignocellulose, zinc oxide, bonite and ultrahigh-gel-degree protein powder, uniformly stirring, grinding and sieving with a 200-mesh sieve.
2. The method of preparing a low cost moisture controlled stucco gypsum of claim 1, wherein the aging time in step a is 7-10 days.
3. The method for preparing low-cost humidity-controlling plastering gypsum according to claim 1, wherein in the step B, the causticized white slime is paper-making alkali recovery causticized white slime with the water content of 8-15%.
4. The method for preparing low-cost moisture-controlling plastering gypsum according to claim 1, wherein in the step C, the raw material of the ultra-high gel strength protein powder is egg.
5. The method for preparing low-cost wet-adjustable render gypsum as claimed in claim 1, wherein the gel content of the ultra-high gel content protein powder in step C is 1200 g/cm and 1400 g/cm-2。
6. The method for preparing low-cost humidity-controlling plastering gypsum according to claim 1, wherein the low-cost humidity-controlling plastering gypsum consists of the following components in percentage by weight: 8-15% of causticized white sludge, 1-3% of hydroxypropyl methyl cellulose, 2-5% of lignocellulose, 1-2% of ultrahigh-gel-degree protein powder, 0.02-0.05% of zinc oxide, 0.2-0.5% of Bonaite and the balance of desulfurized gypsum.
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