CN111617534A - A purification and separation system for catalytic gasification catalyst recovery of MTO device - Google Patents
A purification and separation system for catalytic gasification catalyst recovery of MTO device Download PDFInfo
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- B01D29/50—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with multiple filtering elements, characterised by their mutual disposition
- B01D29/52—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with multiple filtering elements, characterised by their mutual disposition in parallel connection
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- B01D29/66—Regenerating the filter material in the filter by flushing, e.g. counter-current air-bumps
- B01D29/68—Regenerating the filter material in the filter by flushing, e.g. counter-current air-bumps with backwash arms, shoes or nozzles
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- B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
- B01D29/88—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor having feed or discharge devices
- B01D29/94—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor having feed or discharge devices for discharging the filter cake, e.g. chutes
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Abstract
本发明属于MTO装置节能环保技术领域,公开了一种用于MTO装置催化气化催化剂回收的净化分离系统,至少包括一组净化分离过滤器、自动控制单元和阀组;净化分离过滤器设置有入口、出口、反吹清洗口和排渣卸灰口,净化分离过滤器内部安装有过滤分离元件和反吹清洁元件,自动控制单元能够控制阀组中任意自动控制阀的开启和关闭,阀组包括第一自动控制阀、第二自动控制阀、第三自动控制阀和第四自动控制阀,第一控制阀设置在净化分离过滤器的入口管路上,第二自动控制阀设置在净化分离过滤器的出口管路上,第三自动控制阀设置在净化分离过滤器的反吹清洗口管路上,第四自动控制阀设置在净化分离过滤器的排渣卸灰口管路上。
The invention belongs to the technical field of energy saving and environmental protection of MTO devices, and discloses a purification and separation system for the recovery of catalytic gasification catalysts of MTO devices, which comprises at least one set of purification and separation filters, an automatic control unit and a valve group; The inlet, outlet, backflushing cleaning port and slag discharge and ash discharge port are installed inside the purification separation filter with filtering separation elements and backflushing cleaning elements. The automatic control unit can control the opening and closing of any automatic control valve in the valve group. The valve group It includes a first automatic control valve, a second automatic control valve, a third automatic control valve and a fourth automatic control valve. The first control valve is set on the inlet pipeline of the purification and separation filter, and the second automatic control valve is set on the purification and separation filter. On the outlet pipeline of the filter, the third automatic control valve is arranged on the backflushing and cleaning port pipeline of the purification and separation filter, and the fourth automatic control valve is arranged on the slag discharge and ash discharge outlet pipeline of the purification and separation filter.
Description
技术领域technical field
本发明涉及MTO装置节能环保技术领域,具体涉及一种用于MTO装置催化气化催化剂回收的净化分离系统。The invention relates to the technical field of energy saving and environmental protection of MTO devices, in particular to a purification and separation system used for the recovery of catalytic gasification catalysts of MTO devices.
背景技术Background technique
目前,MTO工艺是煤化工产业链中最新研发的生产工艺技术,国内在建的装置不足5套,已建成的装置目前尚处于試运行阶段,远未达产平稳运行。At present, the MTO process is the latest production technology developed in the coal chemical industry chain. There are less than 5 units under construction in China, and the completed units are still in the trial operation stage, far from reaching production and running smoothly.
现有的MTO装置催化气化催化剂溶液净化处理工艺中,基本都是采用板框压滤机设备进行滤渣处理,压滤机为开放式的设备,在运行时会因挤压导致液体飞溅、气味扩散,导致工作环境较差;且压滤设备体积庞大、滤布数量多、清洗更换频率高、停车频繁,不论是前期投资还是后期维护,费用极大;受限于现有的滤布材料,一般过滤精度不高,难以满足后续工艺设备的进料要求。In the existing MTO device catalytic gasification catalyst solution purification process, the plate and frame filter press equipment is basically used for filter residue treatment. The filter press is an open type equipment, which will cause liquid splashing and odor due to extrusion during operation. Diffusion, resulting in poor working environment; and the filter press equipment is bulky, the number of filter cloths is large, the frequency of cleaning and replacement is high, and the parking lot is frequent. Whether it is early investment or post-maintenance, the cost is very high; limited by the existing filter cloth materials, Generally, the filtration accuracy is not high, and it is difficult to meet the feeding requirements of subsequent process equipment.
因此,本领域需要一种用于MTO装置催化气化催化剂回收的净化分离系统来解决上述问题。Therefore, there is a need in the art for a purification and separation system for catalytic gasification catalyst recovery of MTO devices to solve the above problems.
发明内容SUMMARY OF THE INVENTION
现有的MTO装置催化气化催化剂溶液净化处理工艺中,基本都是采用板框压滤机设备进行滤渣处理,压滤机为开放式的设备,在运行时会因挤压导致液体飞溅、气味扩散,导致工作环境较差;且压滤设备体积庞大、滤布数量多、清洗更换频率高、停车频繁,不论是前期投资还是后期维护,费用极大;受限于现有的滤布材料,一般过滤精度不高,难以满足后续工艺设备的进料要求。为了解决现有技术中的上述问题,本发明提供了一种用于MTO装置催化气化催化剂回收的净化分离系统,至少包括一组净化分离过滤器、自动控制单元和阀组;净化分离过滤器设置有入口、出口、反吹清洗口和排渣卸灰口,净化分离过滤器内部安装有滤芯和反吹清洁元件,自动控制单元能够控制任意自动控制阀的开启和关闭,阀组包括第一自动控制阀、第二自动控制阀、第三自动控制阀和第四自动控制阀,第一控制阀设置在净化分离过滤器的入口管路上,第二自动控制阀设置在净化分离过滤器的出口管路上,第三自动控制阀设置在净化分离过滤器的反吹清洗口管路上,第四自动控制阀设置在在净化分离过滤器的排渣卸灰口管路上。In the existing MTO device catalytic gasification catalyst solution purification process, the plate and frame filter press equipment is basically used for filter residue treatment. The filter press is an open type equipment, which will cause liquid splashing and odor due to extrusion during operation. Diffusion, resulting in poor working environment; and the filter press equipment is bulky, the number of filter cloths is large, the frequency of cleaning and replacement is high, and the parking lot is frequent. Whether it is early investment or post-maintenance, the cost is very high; limited by the existing filter cloth materials, Generally, the filtration accuracy is not high, and it is difficult to meet the feeding requirements of subsequent process equipment. In order to solve the above-mentioned problems in the prior art, the present invention provides a purification and separation system for the recovery of catalytic gasification catalysts of an MTO device, which at least includes a set of purification and separation filters, an automatic control unit and a valve group; the purification and separation filters It is provided with inlet, outlet, backflushing cleaning port and slag discharge and ash discharge port. The filter element and backflushing cleaning element are installed inside the purification separation filter. The automatic control unit can control the opening and closing of any automatic control valve. The valve group includes the first Automatic control valve, second automatic control valve, third automatic control valve and fourth automatic control valve, the first control valve is arranged on the inlet pipeline of the purification separation filter, and the second automatic control valve is arranged at the outlet of the purification separation filter On the pipeline, the third automatic control valve is arranged on the backflushing and cleaning port pipeline of the purification and separation filter, and the fourth automatic control valve is arranged on the slag discharge and ash discharge outlet pipeline of the purification and separation filter.
在上述用于MTO装置催化气化催化剂回收的净化分离系统的优选技术方案中,净化分离过滤器内部设置有孔板,滤芯安装在孔板上,孔板将过滤器分为第一腔室和第二腔室,第一腔室室设置有入口,第二腔室设置有出口,第一腔室底部设置有排渣卸灰口,第二腔室设置有反吹清洗口。In the above preferred technical solution of the purification and separation system for the recovery of catalytic gasification catalysts of MTO devices, the purification and separation filter is provided with an orifice plate, the filter element is installed on the orifice plate, and the orifice plate divides the filter into a first chamber and a The second chamber, the first chamber is provided with an inlet, the second chamber is provided with an outlet, the bottom of the first chamber is provided with a slag discharge port, and the second chamber is provided with a backflushing cleaning port.
在上述用于MTO装置催化气化催化剂回收的净化分离系统的优选技术方案中,滤芯为圆筒状结构,滤芯的第一端为封闭结构,第二端为开口结构;滤芯材质为金属材质,滤芯在受到外力作用后,改变原有形状,当外力撤消后,滤芯会恢复原有形状。In the above-mentioned preferred technical solution of the purification and separation system for the recovery of catalytic gasification catalyst of an MTO device, the filter element is a cylindrical structure, the first end of the filter element is a closed structure, and the second end is an open structure; the filter element material is a metal material, The filter element changes its original shape after being subjected to external force. When the external force is removed, the filter element will return to its original shape.
在上述用于MTO装置催化气化催化剂回收的净化分离系统的优选技术方案中,自动控制单元为PLC自动控制单元,PLC自动控制单元分别与第一自动控制阀、第二自动控制阀、第三自动控制阀和第四自动控制阀电连接,PLC自动控制单元能够控制第一自动控制阀、第二自动控制阀、第三自动控制阀和第四自动控制阀的打开和关闭。In the above preferred technical solution of the purification and separation system for the recovery of catalytic gasification catalysts of MTO devices, the automatic control unit is a PLC automatic control unit, and the PLC automatic control unit is respectively connected with the first automatic control valve, the second automatic control valve, the third automatic control valve, and the third automatic control valve The automatic control valve and the fourth automatic control valve are electrically connected, and the PLC automatic control unit can control the opening and closing of the first automatic control valve, the second automatic control valve, the third automatic control valve and the fourth automatic control valve.
在上述用于MTO装置催化气化催化剂回收的净化分离系统的优选技术方案中,净化分离过滤器均设置有多个在线反吹清洁管,反吹清洁管设置在净化分离过滤器的反吹清洗口处。In the above preferred technical solution of the purification and separation system for the recovery of catalytic gasification catalysts of MTO devices, the purification and separation filters are all provided with a plurality of online backflushing cleaning pipes, and the backflushing cleaning pipes are arranged in the backflushing cleaning of the purification separation filter. mouth.
在上述用于MTO装置催化气化催化剂回收的净化分离系统的优选技术方案中,净化分离过滤器的入口管道和出口管道均设置有压力测量装置,压力测量装置与自动控制单元电连接,将压力信号反馈给自动控制单元。In the above-mentioned preferred technical solution of the purification and separation system for catalytic gasification catalyst recovery of the MTO device, the inlet pipe and the outlet pipe of the purification and separation filter are both provided with a pressure measuring device, and the pressure measuring device is electrically connected with the automatic control unit to connect the pressure The signal is fed back to the automatic control unit.
在上述用于MTO装置催化气化催化剂回收的净化分离系统的优选技术方案中,净化分离过滤器的入口管道处的压力测量装置为第一压力测量装置,第一压力测量装置设置在入口管道上,且位于第一自动控制阀的后端。In the above-mentioned preferred technical solution of the purification and separation system for the recovery of catalytic gasification catalysts of MTO devices, the pressure measurement device at the inlet pipe of the purification separation filter is the first pressure measurement device, and the first pressure measurement device is arranged on the inlet pipe , and is located at the rear end of the first automatic control valve.
在上述用于MTO装置催化气化催化剂回收的净化分离系统的优选技术方案中,净化分离过滤器的出口管道处的压力测量装置为第二压力测量装置,第二压力测量装置设置在出口管道上,且位于第二自动控制阀的前端。In the above preferred technical solution of the purification and separation system for the recovery of catalytic gasification catalysts of MTO devices, the pressure measurement device at the outlet pipe of the purification separation filter is a second pressure measurement device, and the second pressure measurement device is arranged on the outlet pipe , and is located at the front end of the second automatic control valve.
在上述用于MTO装置催化气化催化剂回收的净化分离系统的优选技术方案中,净化分离过滤器的本体设置有温度测量装置,温度测量装置与自动控制单元电连接,将温度信号反馈给自动控制单元。In the preferred technical solution of the above purification and separation system for catalytic gasification catalyst recovery of MTO devices, the body of the purification and separation filter is provided with a temperature measuring device, and the temperature measuring device is electrically connected to the automatic control unit, and the temperature signal is fed back to the automatic control unit. unit.
在上述用于MTO装置催化气化催化剂回收的净化分离系统的优选技术方案中,自动控制单元采用压差控制和时间控制相互协同的控制方式,所述压差控制和时间控制相互协同的控制方式是多台并联安装运行的净化分离的过滤器通过检测入口、出口压差来控制反吹清洗口处第三自动控制阀的开启,同时设定反吹清洗的时间值,在达到该时间值时,即使入口和出口的压差值未达到反吹清洗口开启的条件,自动控制单元依然开始执行对过滤元件进行反吹清洁的动作。In the above preferred technical solution of the purification and separation system for the recovery of catalytic gasification catalysts in MTO devices, the automatic control unit adopts a control mode in which pressure difference control and time control are coordinated with each other, and the pressure difference control and time control are in a coordinated control mode with each other. It is a filter for purification and separation installed and operated in parallel to control the opening of the third automatic control valve at the backflushing cleaning port by detecting the pressure difference between the inlet and the outlet, and at the same time set the time value of the backflushing cleaning. When the time value is reached , even if the pressure difference between the inlet and the outlet does not reach the condition that the backflushing cleaning port is opened, the automatic control unit still starts to perform the action of backflushing and cleaning the filter element.
本领域技术人员能够理解的是,在本发明的用于MTO装置催化气化催化剂回收的净化分离系统的优选技术方案中,该用于MTO装置催化气化催化剂回收的净化分离系统的净化分离过滤器采用高纳污、高承压、易清洁的高精密净化分离过滤元件代替现有的板框压滤设备,对MTO装置催化剂的回收、运行成本的降低及水资源的节约等都有着巨大的现实意义及可观的经济价值。该用于 MTO装置催化气化催化剂回收的净化分离系统能够实现净化分离过滤器的在线反吹再生,减少停车次数,大大降低运行成本。其解决现行MTO装置催化剂循环使用无法稳定运行的技术难题,为MTO装置实现连续稳定运行创造了可行的技术路线。Those skilled in the art can understand that, in the preferred technical solution of the purification and separation system for the recovery of the catalytic gasification catalyst of the MTO device of the present invention, the purification separation and filtration of the purification and separation system for the recovery of the catalytic gasification catalyst of the MTO device The filter adopts high-precision purification and separation filter elements with high pollution, high pressure and easy cleaning to replace the existing plate and frame filter press equipment, which has a huge impact on the recovery of MTO device catalyst, the reduction of operating costs and the saving of water resources. Practical significance and considerable economic value. The purification and separation system used for the recovery of catalytic gasification catalyst of the MTO device can realize the online backflushing regeneration of the purification and separation filter, reduce the number of shutdowns, and greatly reduce the operating cost. It solves the technical problem that the catalyst cycle of the current MTO device cannot run stably, and creates a feasible technical route for the MTO device to achieve continuous and stable operation.
(1)、现行板框压滤机工艺开放式作业,弥散飞溅液体、气体,工作环境差。本发明的净化分离系统可在密闭条件下进行,避免液体飞溅,气体弥散;(1) The current plate and frame filter press technology is open to work, dispersing splashing liquid and gas, and the working environment is poor. The purification and separation system of the present invention can be carried out under airtight conditions to avoid liquid splashing and gas dispersion;
(2)、传统工艺中板框压滤机中的滤布作为净化分离元件,安装更换劳动强度大,且布袋承压强度差,容易被坚硬颗粒刺穿,造成穿孔后,渣料进入后续系统,造成设备磨损、结垢等。本发明的净化分离系统以高精密金属滤芯作为净化分离元件,过滤面积大,设备体积小,耐高压,不会穿孔且耐腐蚀,设备整体寿命长。(2) In the traditional process, the filter cloth in the plate and frame filter press is used as a purification and separation element. The installation and replacement are labor-intensive, and the pressure strength of the cloth bag is poor, which is easy to be pierced by hard particles. , causing equipment wear, scaling, etc. The purification and separation system of the present invention uses a high-precision metal filter element as a purification and separation element, which has large filtering area, small equipment volume, high pressure resistance, no perforation and corrosion resistance, and long overall equipment life.
(3)、传统工艺中如有滤布被刺穿,由于布袋数量巨大,因此需要逐一检测每条滤袋并替换,劳动强度大。而本发明的净化分离系统中过滤元件耐高温,强度高,渣料颗粒被拦截在光滑表面,不会穿孔,使用寿命长,劳动强度低。(3) If the filter cloth is pierced in the traditional process, due to the huge number of cloth bags, it is necessary to detect each filter bag one by one and replace it, which is labor-intensive. On the other hand, in the purification and separation system of the present invention, the filter element has high temperature resistance and high strength, and the slag particles are intercepted on the smooth surface without perforation, the service life is long, and the labor intensity is low.
(4)、传统工艺滤布数量大、造价高,更换清洗频率高,耗水量大,产生大量清洗污水,清洗、安装及更换的操作劳动强度高,工作量大,人工成本高。本发明的净化分离系统可通过自动控制开启反吹口实现在线反吹,滤芯使用寿命长,减少进入设备检修的频次。过滤元件在设备内单支独立安装,检修时人员可进入设备单支拆装滤芯,不需要起重机械及吊车设备,更换操作简单,节省人力等。(4) The number of traditional filter cloths is large, the cost is high, the frequency of replacement and cleaning is high, the water consumption is large, and a large amount of cleaning sewage is generated. The operation of cleaning, installation and replacement is labor-intensive, workload is large, and labor costs are high. The purification and separation system of the invention can realize online backflushing by automatically controlling the opening of the backflushing port, the filter element has a long service life, and the frequency of entering equipment for maintenance is reduced. The filter element is installed independently in the equipment, and the personnel can enter the equipment to disassemble and assemble the filter element during maintenance, without the need for lifting machinery and crane equipment, the replacement operation is simple, and manpower is saved.
(5)、传统工艺滤布滤饼剥离困难,甚至需要添加助滤剂才能顺利脱落,如不能自行脱落需要认为检修剥离,工作过程不稳定,难以实现自动化运行。本发明的净化分离系统可通过自动控制系统开启反吹口实现在线反吹,完全实现自动化运行。(5) It is difficult to peel off the filter cake of the traditional process filter cloth, and even need to add filter aid to fall off smoothly. The purification and separation system of the present invention can realize online backflushing by opening the backflushing port through the automatic control system, and fully realize automatic operation.
(6)、本发明的净化分离系统能够实现多台过滤器并联,各过滤器设备可互为备用设备,保证在反吹及单台设备检修时不影响系统正常过滤的进行;(6), the purification and separation system of the present invention can realize the parallel connection of multiple filters, and each filter device can be used as a backup device for each other, so as to ensure that the normal filtration of the system is not affected during backflushing and maintenance of a single device;
(7)、反吹气体采用氮气或压缩空气,也可采用滤后液,自出口管线上引入进行反吹(图1中虚线部分表示),节约能源;(7) The backflushing gas adopts nitrogen or compressed air, or the filtered liquid can be used to introduce backflushing from the outlet pipeline (represented by the dotted line in Figure 1) to save energy;
(8)、反吹出来的滤渣集中收集至集渣区,多次反吹后再进行一次集中处理,采用管道输送的方式排卸至指定位置,避免每台设备每次反吹时都需要排渣处理;(8) The filter residue from the backflushing is collected in the slag collecting area, and then subjected to a centralized treatment after multiple backflushing, and is discharged to the designated position by pipeline transportation, so as to avoid the need to discharge each equipment every time it is backflushed. slag treatment;
(9)、反吹所用气量小,时间短,反吹再生的效率高。(9) The amount of gas used for backflushing is small, the time is short, and the efficiency of backflushing and regeneration is high.
附图说明Description of drawings
下面参照附图来描述本发明的优选实施方式,附图中:Preferred embodiments of the present invention are described below with reference to the accompanying drawings, in which:
图1为本发明的用于MTO装置催化剂回收的净化分离系统的管线流程图一;Fig. 1 is the pipeline flow chart one of the purification separation system used for MTO device catalyst recovery of the present invention;
图2为本发明的用于MTO装置催化剂回收的净化分离系统的管线流程图二;Fig. 2 is the pipeline flow chart two of the purification separation system used for MTO device catalyst recovery of the present invention;
附图标记:1、净化分离过滤器;2、入口;3、出口;4、反吹清洗口;5、排渣卸灰口;6、滤芯;7、第一自动控制阀;8、第二自动控制阀;9、第三自动控制阀;10、第四自动控制阀;11、第一压力测量装置;12、第二压力测量装置;13、温度测量装置。Reference numerals: 1. Purification and separation filter; 2. Inlet; 3. Outlet; 4. Back-flushing cleaning port; 5. Slag discharge port; 6. Filter element; Automatic control valve; 9. Third automatic control valve; 10. Fourth automatic control valve; 11. First pressure measuring device; 12. Second pressure measuring device; 13. Temperature measuring device.
具体实施方式Detailed ways
以下由特定的具体实施例说明本发明的实施方式,熟悉此技术的人士可由本说明书所揭露的内容轻易地了解本发明的其他优点及功效,显然,所描述的实施例是本发明一部分实施例,而不是全部的实施例。基于本发明中的实施例,本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例,都属于本发明保护的范围。The embodiments of the present invention are described below by specific specific embodiments. Those who are familiar with the technology can easily understand other advantages and effects of the present invention from the contents disclosed in this specification. Obviously, the described embodiments are part of the present invention. , not all examples. Based on the embodiments of the present invention, all other embodiments obtained by those of ordinary skill in the art without creative efforts shall fall within the protection scope of the present invention.
需要说明的是,在本发明的描述中,术语“中”、“上”、“下”、“横”、“内”等指示的方向或位置关系的术语是基于附图所示的方向或位置关系,这仅仅是为了便于描述,而不是指示或暗示所述装置或元件必须具有特定的方位、以特定的方位构造和操作,因此不能理解为对本发明的限制。此外,术语“第一”、“第二”仅用于描述目的,而不能理解为指示或暗示相对重要性。It should be noted that, in the description of the present invention, the terms "middle", "upper", "lower", "horizontal", "inner", etc. indicate directions or terms in positional relationship based on the directions shown in the drawings or The positional relationship is only for the convenience of description, rather than indicating or implying that the device or element must have a specific orientation, be constructed and operated in a specific orientation, and therefore should not be construed as a limitation of the present invention. Furthermore, the terms "first" and "second" are used for descriptive purposes only and should not be construed to indicate or imply relative importance.
此外,还需要说明的是,在本发明的描述中,除非另有明确的规定和限定,术语“设置”、“安装”、“相连”、“连接”应做广义理解,例如,可以是固定连接,也可以是可拆卸连接,或一体地连接;可以是机械连接;可以是直接相连,也可以通过中间媒介间接相连,可以是两个元件内部的连通。对于本领域技术人员而言,可根据具体情况理解上述术语在本发明中的具体含义。In addition, it should be noted that, in the description of the present invention, unless otherwise expressly specified and limited, the terms "arranged", "installed", "connected" and "connected" should be understood in a broad sense, for example, it may be fixed The connection can also be a detachable connection, or an integral connection; it can be a mechanical connection; it can be a direct connection, or an indirect connection through an intermediate medium, and it can be the internal communication of two components. For those skilled in the art, the specific meanings of the above terms in the present invention can be understood according to specific situations.
基于背景技术指出的现有的MTO装置催化气化催化剂溶液净化处理工艺中,基本都是采用板框压滤机设备进行滤渣处理,压滤机为开放式的设备,在运行时会因挤压导致液体飞溅、气味扩散,导致工作环境较差;且压滤设备体积庞大、滤布数量多、清洗更换频率高、停车频繁,不论是前期投资还是后期维护,费用极大;受限于现有的滤布材料,一般过滤精度不高,难以满足后续工艺设备的进料要求。本发明的用于MTO装置催化气化催化剂回收的净化分离系统,净化分离过滤器采用高纳污、高承压、易清洁的高精密净化分离过滤元件代替或补充的现有的板框压滤设备,对MTO装置催化气化催化剂的回收、运行成本的降低及水资源的节约等都有着巨大的现实意义及可观的经济价值。该用于MTO装置催化气化催化剂回收的净化分离系统能够实现净化分离过滤器的在线反吹再生,减少停车次数,大大降低运行成本。其解决现行MTO装置催化气化催化剂循环使用无法稳定运行的技术难题,为MTO装置实现连续稳定运行创造了可行的技术路线。本发明的分离系统可在密闭条件下进行过滤,避免液体飞溅、气体弥散;本发明的分离系统以高精密金属滤芯作为净化分离元件,过滤面积大,且设备体积小,耐高压,不会穿孔且耐腐蚀,设备整体寿命长。本发明的分离系统中过滤元件耐高温,强度高,渣料颗粒被拦截在光滑表面,不会穿孔,使用寿命长,劳动强度低。本发明的过滤系统可通过自动控制开启反吹口实现在线反吹,滤芯使用寿命长,减少进入设备检修的频次。过滤元件在设备内单支独立安装,检修时人员可进入设备单支拆装滤芯,不需要起重机械及吊车设备,更换操作简单,节省人力等。本发明的净化分离系统的过滤系统可通过自动控制系统开启反吹口实现在线反吹,完全实现自动化运行。本发明的净化分离系统能够实现多台过滤器并联,各过滤器设备可互为备用设备,保证在反吹及单台设备检修时不影响系统正常过滤的进行;反吹气体采用氮气或压缩空气,也可采用滤后液,自出口管线上引入进行反吹,节约能源;反吹出来的滤渣集中收集至集渣区,多次反吹后再进行一次集中处理,采用管道输送的方式排卸至指定位置,避免每台设备每次反吹时都需要排渣处理;反吹所用气量小,时间短,反吹再生的效率高。In the existing MTO device catalytic gasification catalyst solution purification treatment process pointed out based on the background technology, the plate and frame filter press equipment is basically used for filter residue treatment. This leads to liquid splashing and odor diffusion, resulting in poor working environment; and the filter press equipment is bulky, the number of filter cloths is large, the frequency of cleaning and replacement is high, and the parking lot is frequent. Whether it is early investment or post-maintenance, the cost is very high; limited by the existing The filter cloth material is generally not high in filtration accuracy, and it is difficult to meet the feeding requirements of the subsequent process equipment. In the purification and separation system for the recovery of the catalytic gasification catalyst of the MTO device of the present invention, the purification and separation filter adopts a high-contamination, high-pressure, easy-to-clean high-precision purification and separation filter element to replace or supplement the existing plate and frame filter press The equipment has great practical significance and considerable economic value for the recovery of catalytic gasification catalysts of MTO units, the reduction of operating costs and the conservation of water resources. The purification and separation system for catalytic gasification catalyst recovery of an MTO device can realize online backflushing and regeneration of purification and separation filters, reduce the number of shutdowns, and greatly reduce operating costs. It solves the technical problem that the catalytic gasification catalyst of the current MTO device cannot be operated stably, and creates a feasible technical route for the continuous and stable operation of the MTO device. The separation system of the present invention can be filtered under airtight conditions to avoid liquid splashing and gas dispersion; the separation system of the present invention uses a high-precision metal filter element as a purification and separation element, which has a large filtering area, small equipment volume, high pressure resistance, and no perforation. And corrosion resistance, the overall life of the equipment is long. In the separation system of the invention, the filter element has high temperature resistance and high strength, the slag particles are intercepted on the smooth surface without perforation, the service life is long, and the labor intensity is low. The filtering system of the invention can realize online backflushing by automatically controlling the opening of the backflushing port, the filter element has a long service life, and the frequency of entering equipment for maintenance is reduced. The filter element is installed independently in the equipment, and the personnel can enter the equipment to disassemble and assemble the filter element during maintenance, without the need for lifting machinery and crane equipment, the replacement operation is simple, and manpower is saved. The filtration system of the purification and separation system of the present invention can realize online backflushing by opening the backflushing port through the automatic control system, and fully realize automatic operation. The purification and separation system of the invention can realize the parallel connection of multiple filters, and the filter devices can be used as backup devices for each other, so as to ensure that the normal filtration of the system is not affected during backflushing and maintenance of a single device; the backflushing gas adopts nitrogen or compressed air. , the filtered liquid can also be introduced from the outlet pipeline for backflushing to save energy; the filter residues from the backflushing are collected in the slag collecting area, and then subjected to a centralized treatment after multiple backflushing, and are discharged by pipeline transportation. To the designated position, to avoid the need for slag discharge treatment every time each equipment is backflushed; the amount of gas used for backflushing is small, the time is short, and the efficiency of backflushing and regeneration is high.
具体地,如图1和2所示,本发明的用于MTO装置催化气化催化剂回收的净化分离系统,至少包括一组净化分离过滤器1、自动控制单元和阀组(多组采用并联安装方式与主管路连接,各过滤器设备可互为备用设备,保证在反吹及单台设备检修时不影响系统正常过滤);净化分离过滤器1设置有入口2、出口3、反吹清洗口4和排渣卸灰口5,净化分离过滤器1内部安装有滤芯和反吹清洁元件,自动控制单元能够控制任意自动控制阀的开启和关闭,阀组包括第一自动控制阀7、第二自动控制阀8、第三自动控制阀9和第四自动控制阀10,第一控制阀设置在净化分离过滤器1的入口2管路上,第二自动控制阀8设置在净化分离过滤器1的出口管路3上,第三自动控制阀9设置在净化分离过滤器1的反吹清洗口管路4上,第四自动控制阀10设置在在净化分离过滤器1的排渣卸灰口管路5上。在本发明中,第一自动控制阀7、第二自动控制阀8、第三自动控制阀9和第四自动控制阀10为现有技术。具体工作过程为:脏催化剂溶液由净化分离过滤器1的入口2进入净化分离过滤器1,经过过滤分离元件(滤芯6)拦截渣料后,干净的催化剂溶液由出口3流出,过滤分离元件堵塞后由反吹清洗口4通入反吹气或滤后液对过滤分离元件进行在线清洗恢复,被拦截的吹扫下滤渣由排渣卸灰口5排出,多次反吹后再进行一次集中处理,采用管道输送的方式排卸至指定位置,避免每台设备每次反吹时都需要排渣处理。Specifically, as shown in Figures 1 and 2, the purification and separation system for catalytic gasification catalyst recovery of an MTO device of the present invention includes at least one group of purification and separation filters 1, an automatic control unit and a valve group (multiple groups are installed in parallel). The method is connected to the main pipeline, and each filter equipment can be used as backup equipment for each other to ensure that the normal filtration of the system will not be affected during backflushing and single equipment maintenance); purification and separation filter 1 is provided with inlet 2,
优选地,净化分离过滤器1内部设置有孔板,滤芯6安装在孔板上,孔板将过滤器分为第一腔室和第二腔室,第一腔室室设置有入口2,第二腔室设置有出口3,第一腔室底部设置有排渣卸灰口5,第二腔室设置有反吹清洗口4。Preferably, an orifice plate is arranged inside the purification and separation filter 1, the
在本发明中,过滤器的内部结构分为两种方案,第一方案如图1所示,第一腔室和第二腔室为上下设置,第一腔室在下,第二腔室在上,第一腔室设置有入口2,第二腔室设置有出口3,第一腔室底部设置有排渣卸灰口5,第二腔室顶部设置有反吹清洗口4;第二种方案如图2所示,第一腔室和第二腔室为内外设置,第二腔室在第一腔室内部,第一下腔室设置有入口2,第二上腔室设置有出口3,第一腔室底部设置有排渣卸灰口5,第二腔室设置有反吹清洗口4。这种两种方式就能实现本发明的目的,但是第二方案的吹扫效果要优于第一方案的效果。In the present invention, the internal structure of the filter is divided into two schemes. The first scheme is shown in Figure 1. The first chamber and the second chamber are arranged up and down, the first chamber is at the bottom, and the second chamber is at the top. , the first chamber is provided with an inlet 2, the second chamber is provided with an
优选地,滤芯6为圆筒状结构,滤芯6的第一端为封闭结构,第二端为开口结构;滤芯6材质为金属材质,滤芯6在受到外力作用后,改变原有形状,当外力撤消后,滤芯6会恢复原有形状。Preferably, the
优选地,自动控制单元为PLC自动控制单元,PLC控制单元可现场安装,也可远传连接DCS(集散控制系统),利用DCS集中控制。PLC自动控制单元分别与第一自动控制阀7、第二自动控制阀8、第三自动控制阀9和第四自动控制阀10电连接,PLC自动控制单元能够控制第一自动控制阀7、第二自动控制阀8、第三自动控制阀9和第四自动控制阀10的打开和关闭。Preferably, the automatic control unit is a PLC automatic control unit, and the PLC control unit can be installed on-site, and can also be connected to a DCS (distributed control system) by remote transmission, and the DCS can be used for centralized control. The PLC automatic control unit is respectively electrically connected with the first
优选地,净化分离过滤器1均设置有多个在线反吹清洁管,反吹清洁管设置在净化分离过滤器1的反吹清洗口处4。在线反吹清洁管口及管线可与过滤器出口3的洁净催化剂溶液总管连接,也可单独连接氮气或压缩空气的公用工程管线,使用氮气或压缩空气作为反吹清洁用气体介质。Preferably, each of the purification and separation filters 1 is provided with a plurality of online backflushing cleaning pipes, and the backflushing cleaning pipes are arranged at the backflushing cleaning port 4 of the purification and separation filter 1 . The nozzle and pipeline of online backflushing cleaning can be connected to the main pipe of clean catalyst solution at the
优选地,如图1所示,净化分离过滤器1的入口管道2和出口管道3均设置有压力测量装置,压力测量装置与自动控制单元电连接,将压力信号反馈给自动控制单元。在本发明中,压力测量装置为现有技术,压力测量装置为压力传感器。Preferably, as shown in FIG. 1 , both the inlet pipe 2 and the
优选地,如图1和2所示,净化分离过滤器1的入口管道2处的压力测量装置为第一压力测量装置11,第一压力测量装置11设置在入口管道2上,且位于第一自动控制阀7的后端。Preferably, as shown in FIGS. 1 and 2 , the pressure measurement device at the inlet pipe 2 of the purification separation filter 1 is a first pressure measurement device 11 , and the first pressure measurement device 11 is arranged on the inlet pipe 2 and located at the first The rear end of the
优选地,如图1和2所示,净化分离过滤器1的出口管道3处的压力测量装置为第二压力测量装置12,第二压力测量装置12设置在出口管道3上,且位于第二自动控制阀8的前端。Preferably, as shown in FIGS. 1 and 2 , the pressure measurement device at the
优选地,如图1和2所示,净化分离过滤器1的本体设置有温度测量装置 13,温度测量装置13与自动控制单元电连接,将温度信号反馈给自动控制单元。在本发明中,温度测量装置13为现有技术,温度测量装置13为温度传感器。Preferably, as shown in Figures 1 and 2, the body of the purification separation filter 1 is provided with a
优选地,自动控制单元采用压差控制和时间控制相互协同的控制方式,所述压差控制和时间控制相互协同的控制方式是多台并联安装运行的净化分离的过滤器通过检测入口2、出口3压差来控制反吹清洗口4处第三自动控制阀 9的开启,同时设定反吹清洗的时间值,在达到该时间值时,即使入口2和出口3的压差值未达到反吹清洗口4开启的条件,自动控制单元依然开始执行对过滤元件进行反吹清洁的动作。Preferably, the automatic control unit adopts a control method in which differential pressure control and time control cooperate with each other. 3 pressure difference to control the opening of the third
至此,已经结合附图所示的优选实施方式描述了本发明的技术方案,但是,本领域技术人员容易理解的是,本发明的保护范围显然不局限于这些具体实施方式。在不偏离本发明的原理的前提下,本领域技术人员可以对相关技术特征做出等同的更改或替换,这些更改或替换之后的技术方案都将落入本发明的保护范围之内。So far, the technical solutions of the present invention have been described with reference to the preferred embodiments shown in the accompanying drawings, however, those skilled in the art can easily understand that the protection scope of the present invention is obviously not limited to these specific embodiments. Without departing from the principle of the present invention, those skilled in the art can make equivalent changes or substitutions to the relevant technical features, and the technical solutions after these changes or substitutions will fall within the protection scope of the present invention.
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| CN112457888A (en) * | 2020-11-20 | 2021-03-09 | 宁夏神耀科技有限责任公司 | Gasification flash system of on-line self-cleaning condenser |
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| CN112755633B (en) * | 2021-01-26 | 2025-09-05 | 上海格氏流体设备科技有限公司 | Filtration system capable of online disinfection, detection and cleaning and control method |
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Application publication date: 20200904 |
