CN111548869A - Laundry detergent containing silk hydrolase and plant components - Google Patents
Laundry detergent containing silk hydrolase and plant components Download PDFInfo
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- CN111548869A CN111548869A CN202010396654.6A CN202010396654A CN111548869A CN 111548869 A CN111548869 A CN 111548869A CN 202010396654 A CN202010396654 A CN 202010396654A CN 111548869 A CN111548869 A CN 111548869A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/40—Products in which the composition is not well defined
- C11D7/46—Animal products
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/40—Products in which the composition is not well defined
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/40—Products in which the composition is not well defined
- C11D7/44—Vegetable products
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P21/00—Preparation of peptides or proteins
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- Health & Medical Sciences (AREA)
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- Bioinformatics & Cheminformatics (AREA)
- General Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Detergent Compositions (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a laundry detergent containing silk hydrolase and plant components, which consists of the following components in parts by weight: 1-3 parts of silk protein hydrolysate, 3-12 parts of essential oil, 3-20 parts of traditional Chinese medicine extract, 0.1-1 part of enzyme preparation, 0.1-1 part of aromatic, 0.05-1 part of emulsifier and a proper amount of water. The laundry detergent disclosed by the invention can be quickly cleaned, has a skin care function, can be used for effectively sterilizing and inhibiting bacteria, and can prevent residual germs on clothes from damaging the skin.
Description
Technical Field
The invention relates to the technical field of daily chemical articles, in particular to a laundry detergent containing silk hydrolase and plant components.
Background
Along with the requirement of people on health care life is higher and higher, many of the laundry detergents which are not environment-friendly and harmful to human bodies in the prior art can not meet the daily life needs of people, the traditional laundry detergents are free of oil and stain, and are used for sterilization and disinfection, and seem to provide a guarantee for the health of people. And because the environment worsens now, the clothing is placed in the room after the ordinary cleaner washs, because the indoor environment is moist, often breed a large amount of bacterium, serious harm to the human body, especially underwear and underwear. It is therefore desirable to prepare a laundry detergent that can solve the above problems.
Disclosure of Invention
The invention aims to: aiming at the problems mentioned in the background technology, the laundry detergent disclosed by the invention can be quickly cleaned, has a skin care function, can also be used for effectively sterilizing, and can prevent residual germs on clothes from hurting the skin.
In order to achieve the purpose of the invention, the technical scheme adopted by the invention is as follows:
a laundry detergent containing silk hydrolase and plant components comprises the following components in parts by weight: 1-3 parts of silk protein hydrolysate, 3-12 parts of essential oil, 3-20 parts of traditional Chinese medicine extract, 0.1-1 part of enzyme preparation, 0.1-1 part of aromatic, 0.05-1 part of emulsifier and a proper amount of water.
Further, the preparation method of the laundry detergent comprises the steps of adding essential oil and an emulsifier into the silk protein hydrolysate, adding a small amount of water, mixing and stirring for emulsification, sequentially adding the traditional Chinese medicine extract, the enzyme preparation and the aromatic agent after emulsification is finished, uniformly mixing, and adding water for dilution to obtain a finished product.
Further, the emulsification is carried out by high-speed stirring, and the emulsification time is 20-40 min.
Further, the method for hydrolyzing the fibroin comprises the following steps: removing silk, adding into enamel reactor, adding lemon juice, heating for hydrolysis, fermenting, cooling to room temperature, adjusting pH to neutral, decolorizing, removing impurities, filtering, concentrating, and sterilizing to obtain silk protein hydrolysate colloid.
Further, the lemon juice is freshly squeezed lemon juice directly from lemons, the hydrolysis temperature is 90-120 ℃, the hydrolysis time is 24-48 hours, the fermentation time is 1-5 days, and the fermentation temperature is 70-90 ℃.
10. Further, the plant extract comprises the following raw materials of fructus cnidii, scutellaria baicalensis, honeysuckle, tea trees and dianthus chinensis, and the weight ratio of the components is (10-20): (10-20): (15-30): (5-13): (12-20).
Further, the preparation method of the plant extract comprises the steps of weighing the raw materials according to the weight ratio, mixing, adding fermentation strains, heating for fermentation, stirring simultaneously in the fermentation process, filtering out the fermentation liquor after fermentation is finished, sterilizing and inactivating, and further filtering the strains to obtain viscous fermentation liquor, namely the plant extract.
Further, the fermentation time is 12-48h, the fermentation temperature is 40-60 ℃, and ultraviolet sterilization is adopted for sterilization.
Further, the aromatic is prepared by mixing lemon peel and lotus according to the weight ratio of 1:1, fermenting, filtering, and extracting with alcohol.
In summary, due to the adoption of the technical scheme, the invention has the beneficial effects that:
(1) compared with the traditional laundry detergent, the laundry detergent prepared by the invention has great superiority, the traditional laundry detergent has various surfactants as detergent and detergent, and individual surfactants contain ingredients which are bad for skin, can remain on clothes fabrics and can hurt the skin after contacting the skin.
(2) According to the invention, the silk hydrolase and the plant extract are used for compound sterilization, so that high-efficiency decontamination can be achieved without using harmful surfactants, harmful substance residues on fabrics can be prevented, and the harm to human skin is reduced;
(3) the silk hydrolyzed protein is colloidal protein obtained after silk hydrolysis and fermentation, and the hydrolyzed liquid contains protease, so that polluted fabrics can be effectively removed, and the silk hydrolyzed protein is very safe and has no residue;
(4) according to the invention, citric acid in lemon juice is used for hydrolysis in the silk hydrolysis process, and then fermentation is carried out, so that other chemical auxiliaries are prevented from being added and other impurities are prevented from being mixed;
(5) the laundry detergent disclosed by the invention is prepared by mixing and fermenting the lemon peel and the lotus flower as the aromatic, the combination of the lemon peel and the lotus flower has clear refreshing fragrance, and the laundry detergent is prepared by directly fermenting plants, so that active substances and fragrance in the plants are reserved.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention will be described in further detail below with reference to preferred embodiments. It should be noted, however, that the numerous details set forth in the description are merely for the purpose of providing the reader with a thorough understanding of one or more aspects of the present invention, which may be practiced without these specific details.
Example 1
A laundry detergent containing silk hydrolase and plant components comprises the following components in parts by weight: 1 part of silk protein hydrolysate, 3 parts of essential oil, 3 parts of traditional Chinese medicine extract, 0.1 part of enzyme preparation, 0.1 part of aromatic, 0.05 part of emulsifier and a proper amount of water.
Example 2
A laundry detergent containing silk hydrolase and plant components comprises the following components in parts by weight: 3 parts of silk protein hydrolysate, 12 parts of essential oil, 20 parts of traditional Chinese medicine extract, 1 part of enzyme preparation, 1 part of aromatic, 1 part of emulsifier and a proper amount of water.
Example 3
A laundry detergent containing silk hydrolase and plant components comprises the following components in parts by weight: 2 parts of silk protein hydrolysate, 8 parts of essential oil, 12 parts of traditional Chinese medicine extract, 0.5 part of enzyme preparation, 0.5 part of aromatic, 0.1 part of emulsifier and a proper amount of water.
Example 4
A liquid laundry detergent containing silk hydrolyzed protease and plant components is prepared by adding essential oil and emulsifier into silk hydrolyzed protein, adding small amount of water, mixing, stirring at high speed, emulsifying for 20min, sequentially adding Chinese medicinal extract, enzyme preparation and aromatic, mixing, and diluting with water to obtain the final product.
The method for hydrolyzing the fibroin comprises the following steps: removing silk, adding into an enamel reactor, adding lemon juice, heating for hydrolysis and fermentation, stirring, cooling to room temperature, adjusting pH to neutral, decolorizing, removing impurities, filtering, concentrating, and sterilizing to obtain silk protein hydrolysate colloid; the lemon juice is obtained by directly squeezing lemon, wherein the hydrolysis temperature is 90 ℃, the hydrolysis time is 48 hours, the fermentation time is 1 day, and the fermentation temperature is 90 ℃; the decolorization is to remove most of the fat-soluble pigment by adopting an alcohol extraction and water precipitation method, remove most of the fat-soluble pigment by adopting the alcohol extraction and water precipitation method and repeatedly circulate the two methods to completely remove the pigment in the fibroin; the concentration is direct heating and steaming, the sterilization is high temperature sterilization, and the high temperature sterilization is carried out when the heating, steaming and concentrating are carried out.
The plant extract comprises the following raw materials of common cnidium fruit, baical skullcap root, honeysuckle flower, tea tree and dianthus chinensis, and the weight ratio of each component is 20: 10: 15: 5: 12, the preparation method of the plant extract comprises the steps of firstly weighing the raw materials according to the weight ratio, mixing and adding fermentation strains, heating for fermentation, stirring simultaneously in the fermentation process, filtering out the fermentation liquor after the fermentation is finished, sterilizing and inactivating, and then further filtering the strains to obtain viscous fermentation liquor, namely the plant extract; the fermentation time is 12h, the fermentation temperature is 60 ℃, the sterilization adopts ultraviolet sterilization, and the wavelength of an ultraviolet sterilization lamp is 270 nm.
The aromatic is prepared by mixing lemon peel and flos Nelumbinis at a weight ratio of 1:1, fermenting, filtering, and extracting with ethanol to obtain filtrate, adding the filtrate into a large amount of ethanol, mixing, standing, layering, separating liquid, heating the substance dissolved in ethanol, and volatilizing ethanol to obtain extract.
Example 5
A liquid laundry detergent containing silk hydrolyzed protease and plant components is prepared by adding essential oil and emulsifier into silk hydrolyzed protein, adding small amount of water, mixing, stirring at high speed, emulsifying for 40min, sequentially adding Chinese medicinal extract, enzyme preparation and aromatic, mixing, and diluting with water to obtain the final product.
The method for hydrolyzing the fibroin comprises the following steps: removing silk, adding into an enamel reactor, adding lemon juice, heating for hydrolysis and fermentation, stirring, cooling to room temperature, adjusting pH to neutral, decolorizing, removing impurities, filtering, concentrating, and sterilizing to obtain silk protein hydrolysate colloid; the lemon juice is obtained by directly squeezing lemon, wherein the hydrolysis temperature is 120 ℃, the hydrolysis time is 24 hours, the fermentation time is 5 days, and the fermentation temperature is 70 ℃; the decolorization is to remove most of the fat-soluble pigment by adopting an alcohol extraction and water precipitation method, remove most of the fat-soluble pigment by adopting the alcohol extraction and water precipitation method and repeatedly circulate the two methods to completely remove the pigment in the fibroin; the concentration is direct heating and steaming, the sterilization is high temperature sterilization, and the high temperature sterilization is carried out when the heating, steaming and concentrating are carried out.
The plant extract comprises the following raw materials of fructus cnidii, scutellaria baicalensis, honeysuckle, tea trees and dianthus chinensis, and the weight ratio of each component is 10: 20: 30: 13: 20, the preparation method of the plant extract comprises the steps of firstly weighing the raw materials according to the weight ratio, mixing and adding fermentation strains, heating for fermentation, stirring simultaneously in the fermentation process, filtering out the fermentation liquor after the fermentation is finished, sterilizing and inactivating, and then further filtering the strains to obtain viscous fermentation liquor, namely the plant extract; the fermentation time is 48h, the fermentation temperature is 40 ℃, the sterilization adopts ultraviolet sterilization, and the wavelength of an ultraviolet sterilization lamp is 275 nm.
The aromatic is prepared by mixing lemon peel and flos Nelumbinis at a weight ratio of 1:1, fermenting, filtering, and extracting with ethanol to obtain filtrate, adding the filtrate into a large amount of ethanol, mixing, standing, layering, separating liquid, heating the substance dissolved in ethanol, and volatilizing ethanol to obtain extract.
Example 6
A liquid laundry detergent containing silk hydrolyzed protease and plant components is prepared by adding essential oil and emulsifier into silk hydrolyzed protein, adding small amount of water, mixing, stirring at high speed, emulsifying for 30min, sequentially adding Chinese medicinal extract, enzyme preparation and aromatic, mixing, and diluting with water to obtain the final product.
The method for hydrolyzing the fibroin comprises the following steps: removing silk, adding into an enamel reactor, adding lemon juice, heating for hydrolysis and fermentation, stirring, cooling to room temperature, adjusting pH to neutral, decolorizing, removing impurities, filtering, concentrating, and sterilizing to obtain silk protein hydrolysate colloid; the lemon juice is obtained by directly squeezing lemon, wherein the hydrolysis temperature is 100 ℃, the hydrolysis time is 36 hours, the fermentation time is 3 days, and the fermentation temperature is 80 ℃; the decolorization is to remove most of the fat-soluble pigment by adopting an alcohol extraction and water precipitation method, remove most of the fat-soluble pigment by adopting the alcohol extraction and water precipitation method and repeatedly circulate the two methods to completely remove the pigment in the fibroin; the concentration is direct heating and steaming, the sterilization is high temperature sterilization, and the high temperature sterilization is carried out when the heating, steaming and concentrating are carried out.
The plant extract comprises the following raw materials of fructus cnidii, scutellaria baicalensis, honeysuckle, tea trees and dianthus chinensis, and the weight ratio of the components is 15: 15: 23: 9: 18, the preparation method of the plant extract comprises the steps of firstly weighing the raw materials according to the weight ratio, mixing, adding fermentation strains, heating for fermentation, stirring simultaneously in the fermentation process, filtering out the fermentation liquor after the fermentation is finished, sterilizing and inactivating, and then further filtering the strains to obtain viscous fermentation liquor, namely the plant extract; the fermentation time is 36h, the fermentation temperature is 50 ℃, the sterilization adopts ultraviolet sterilization, and the wavelength of an ultraviolet sterilization lamp is 273 nm.
The aromatic is prepared by mixing lemon peel and flos Nelumbinis at a weight ratio of 1:1, fermenting, filtering, and extracting with ethanol to obtain filtrate, adding the filtrate into a large amount of ethanol, mixing, standing, layering, separating liquid, heating the substance dissolved in ethanol, and volatilizing ethanol to obtain extract.
The laundry detergents prepared in examples 1 to 6 are compared with three commercially available laundry detergents, namely comparative example 1, comparative example 2 and comparative example 3, and the sterilization efficiency and the decontamination rate of the laundry detergents are tested by performing a sterilization test according to the requirements of the sterilization technical specification published by the ministry of health in 2002, wherein the test mainly relates to the sterilization effect on escherichia coli, staphylococcus aureus and candida albicans, and the test results of the final sterilization and decontamination rates are shown in table 1.
TABLE 1 test data for each of the examples and comparative examples
The data in table 1 show that the laundry detergent prepared by the invention has better effects than the commercial laundry detergent products in terms of sterilization and bacteriostasis effects and decontamination effects, does not hurt hands, is prepared from pure natural substances, has a hand protection function, can powerfully sterilize, avoids bacteria from invading skin, protects skin, has strong cleaning power, and protects human bodies by one more layer.
The foregoing is only a preferred embodiment of the present invention, and it should be noted that those skilled in the art can make various improvements and modifications without departing from the principle of the present invention, and these improvements and modifications should also be construed as the protection scope of the present invention.
Claims (9)
1. A laundry detergent containing silk hydrolase and plant components is characterized in that: the composition comprises the following components in parts by weight: 1-3 parts of silk protein hydrolysate, 3-12 parts of essential oil, 3-20 parts of traditional Chinese medicine extract, 0.1-1 part of enzyme preparation, 0.1-1 part of aromatic, 0.05-1 part of emulsifier and a proper amount of water.
2. The liquid laundry detergent according to claim 1, comprising silk hydrolase and a plant component, wherein: the preparation method of the laundry detergent comprises the steps of adding essential oil and an emulsifier into the silk protein hydrolysate, adding a small amount of water, mixing and stirring for emulsification, sequentially adding the traditional Chinese medicine extract, the enzyme preparation and the aromatic agent after emulsification, uniformly mixing, and adding water for dilution to obtain a finished product.
3. The liquid laundry detergent according to claim 2, comprising silk hydrolase and a plant component, wherein: the emulsification is carried out by high-speed stirring, and the emulsification time is 20-40 min.
4. The liquid laundry detergent according to claim 2, comprising silk hydrolase and a plant component, wherein: the method for hydrolyzing the fibroin comprises the following steps: removing silk, adding into enamel reactor, adding lemon juice, heating for hydrolysis, fermenting, cooling to room temperature, adjusting pH to neutral, decolorizing, removing impurities, filtering, concentrating, and sterilizing to obtain silk protein hydrolysate colloid.
5. The liquid laundry detergent according to claim 4, comprising silk hydrolase and a plant component, wherein: the lemon juice is obtained by directly squeezing lemon, the hydrolysis temperature is 90-120 ℃, the hydrolysis time is 24-48 hours, the fermentation time is 1-5 days, and the fermentation temperature is 70-90 ℃.
6. The liquid laundry detergent according to claim 2, comprising silk hydrolase and a plant component, wherein: the plant extract comprises the following raw materials of fructus cnidii, scutellaria baicalensis, honeysuckle, tea trees and dianthus chinensis, and the weight ratio of the components is (10-20): (10-20): (15-30): (5-13): (12-20).
7. The liquid laundry detergent according to claim 6, comprising silk hydrolase and a plant component, wherein: the preparation method of the plant extract comprises the steps of weighing the raw materials according to the weight ratio, mixing, adding fermentation strains, heating for fermentation, stirring simultaneously in the fermentation process, filtering out the fermentation liquor after fermentation is finished, sterilizing and inactivating, and further filtering the strains to obtain viscous fermentation liquor, namely the plant extract.
8. The liquid laundry detergent according to claim 7, comprising silk hydrolase and a plant component, wherein: the fermentation time is 12-48h, the fermentation temperature is 40-60 ℃, and the sterilization adopts ultraviolet sterilization.
9. The liquid laundry detergent according to claim 2, comprising silk hydrolase and a plant component, wherein: the aromatic is prepared by mixing lemon peel and lotus according to the weight ratio of 1:1, fermenting, filtering, and extracting with alcohol.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN202010396654.6A CN111548869A (en) | 2020-05-12 | 2020-05-12 | Laundry detergent containing silk hydrolase and plant components |
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| Application Number | Priority Date | Filing Date | Title |
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| CN202010396654.6A CN111548869A (en) | 2020-05-12 | 2020-05-12 | Laundry detergent containing silk hydrolase and plant components |
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| CN111548869A true CN111548869A (en) | 2020-08-18 |
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| CN202010396654.6A Pending CN111548869A (en) | 2020-05-12 | 2020-05-12 | Laundry detergent containing silk hydrolase and plant components |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106800980A (en) * | 2016-12-22 | 2017-06-06 | 韩思越 | A kind of liquid detergent and preparation method thereof |
| CN107513474A (en) * | 2017-09-18 | 2017-12-26 | 贵州南风日化有限公司 | A kind of ferment antimicrobial laundry liquid |
| CN108048238A (en) * | 2017-12-27 | 2018-05-18 | 库柏（天津）科技有限公司 | A kind of plant formula liquid detergent containing ferment and preparation method thereof |
| CN110951554A (en) * | 2019-11-06 | 2020-04-03 | 高万东 | Deoiling plant laundry detergent and preparation method thereof |
-
2020
- 2020-05-12 CN CN202010396654.6A patent/CN111548869A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106800980A (en) * | 2016-12-22 | 2017-06-06 | 韩思越 | A kind of liquid detergent and preparation method thereof |
| CN107513474A (en) * | 2017-09-18 | 2017-12-26 | 贵州南风日化有限公司 | A kind of ferment antimicrobial laundry liquid |
| CN108048238A (en) * | 2017-12-27 | 2018-05-18 | 库柏（天津）科技有限公司 | A kind of plant formula liquid detergent containing ferment and preparation method thereof |
| CN110951554A (en) * | 2019-11-06 | 2020-04-03 | 高万东 | Deoiling plant laundry detergent and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 山东省农业科学院 等主编: "《山东蚕桑》", 31 May 2002, 中国农业出版社 * |
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