CN111303987A - A kind of macadamia nut base oil and preparation method thereof - Google Patents
A kind of macadamia nut base oil and preparation method thereof Download PDFInfo
- Publication number
- CN111303987A CN111303987A CN202010240952.6A CN202010240952A CN111303987A CN 111303987 A CN111303987 A CN 111303987A CN 202010240952 A CN202010240952 A CN 202010240952A CN 111303987 A CN111303987 A CN 111303987A
- Authority
- CN
- China
- Prior art keywords
- base oil
- macadamia nut
- nut base
- macadamia
- oil
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000002199 base oil Substances 0.000 title claims abstract description 66
- 235000018330 Macadamia integrifolia Nutrition 0.000 title claims abstract description 47
- 240000000912 Macadamia tetraphylla Species 0.000 title claims abstract description 47
- 235000003800 Macadamia tetraphylla Nutrition 0.000 title claims abstract description 47
- 238000002360 preparation method Methods 0.000 title claims abstract description 28
- 238000001035 drying Methods 0.000 claims abstract description 41
- 238000003825 pressing Methods 0.000 claims abstract description 35
- 238000000034 method Methods 0.000 claims abstract description 25
- 238000005119 centrifugation Methods 0.000 claims abstract description 20
- 239000002994 raw material Substances 0.000 claims abstract description 16
- 238000001914 filtration Methods 0.000 claims abstract description 7
- 238000010298 pulverizing process Methods 0.000 claims abstract description 7
- 239000003921 oil Substances 0.000 claims description 44
- 239000000463 material Substances 0.000 claims description 29
- 239000000047 product Substances 0.000 claims description 25
- SECPZKHBENQXJG-FPLPWBNLSA-N palmitoleic acid Chemical compound CCCCCC\C=C/CCCCCCCC(O)=O SECPZKHBENQXJG-FPLPWBNLSA-N 0.000 claims description 24
- 241000208467 Macadamia Species 0.000 claims description 21
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 21
- 239000000203 mixture Substances 0.000 claims description 16
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 claims description 12
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 claims description 12
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 claims description 12
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 claims description 12
- 239000005642 Oleic acid Substances 0.000 claims description 12
- 235000021319 Palmitoleic acid Nutrition 0.000 claims description 12
- SECPZKHBENQXJG-UHFFFAOYSA-N cis-palmitoleic acid Natural products CCCCCCC=CCCCCCCCC(O)=O SECPZKHBENQXJG-UHFFFAOYSA-N 0.000 claims description 12
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 claims description 12
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 claims description 12
- 239000006228 supernatant Substances 0.000 claims description 12
- 238000003756 stirring Methods 0.000 claims description 11
- 239000002253 acid Substances 0.000 claims description 8
- 239000002245 particle Substances 0.000 claims description 8
- 239000005457 ice water Substances 0.000 claims description 6
- 150000002978 peroxides Chemical class 0.000 claims description 6
- 238000012546 transfer Methods 0.000 claims description 6
- 238000007781 pre-processing Methods 0.000 claims description 2
- 230000008569 process Effects 0.000 abstract description 14
- 230000003020 moisturizing effect Effects 0.000 abstract description 10
- 239000000126 substance Substances 0.000 abstract description 9
- 235000015097 nutrients Nutrition 0.000 abstract description 8
- 238000010521 absorption reaction Methods 0.000 abstract description 7
- 239000010466 nut oil Substances 0.000 abstract description 7
- 230000035515 penetration Effects 0.000 abstract description 7
- 239000004615 ingredient Substances 0.000 abstract description 4
- 231100000344 non-irritating Toxicity 0.000 abstract description 4
- 238000001556 precipitation Methods 0.000 abstract description 4
- 238000012545 processing Methods 0.000 abstract description 2
- 239000002904 solvent Substances 0.000 abstract description 2
- 238000003860 storage Methods 0.000 abstract description 2
- 235000012041 food component Nutrition 0.000 abstract 1
- 235000014571 nuts Nutrition 0.000 description 42
- 235000019198 oils Nutrition 0.000 description 40
- 235000021313 oleic acid Nutrition 0.000 description 11
- 239000007787 solid Substances 0.000 description 8
- 239000002537 cosmetic Substances 0.000 description 7
- 235000019197 fats Nutrition 0.000 description 7
- 239000004006 olive oil Substances 0.000 description 6
- 235000008390 olive oil Nutrition 0.000 description 6
- 150000004671 saturated fatty acids Chemical class 0.000 description 6
- 239000000341 volatile oil Substances 0.000 description 6
- PRAKJMSDJKAYCZ-UHFFFAOYSA-N squalane Chemical compound CC(C)CCCC(C)CCCC(C)CCCCC(C)CCCC(C)CCCC(C)C PRAKJMSDJKAYCZ-UHFFFAOYSA-N 0.000 description 5
- 235000019493 Macadamia oil Nutrition 0.000 description 4
- 239000010495 camellia oil Substances 0.000 description 4
- 238000001816 cooling Methods 0.000 description 4
- 238000001514 detection method Methods 0.000 description 4
- 238000007865 diluting Methods 0.000 description 4
- 239000010469 macadamia oil Substances 0.000 description 4
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 4
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 4
- YYGNTYWPHWGJRM-UHFFFAOYSA-N (6E,10E,14E,18E)-2,6,10,15,19,23-hexamethyltetracosa-2,6,10,14,18,22-hexaene Chemical compound CC(C)=CCCC(C)=CCCC(C)=CCCC=C(C)CCC=C(C)CCC=C(C)C YYGNTYWPHWGJRM-UHFFFAOYSA-N 0.000 description 3
- BHEOSNUKNHRBNM-UHFFFAOYSA-N Tetramethylsqualene Natural products CC(=C)C(C)CCC(=C)C(C)CCC(C)=CCCC=C(C)CCC(C)C(=C)CCC(C)C(C)=C BHEOSNUKNHRBNM-UHFFFAOYSA-N 0.000 description 3
- 229910052785 arsenic Inorganic materials 0.000 description 3
- 238000002425 crystallisation Methods 0.000 description 3
- 230000008025 crystallization Effects 0.000 description 3
- 235000014113 dietary fatty acids Nutrition 0.000 description 3
- 238000000605 extraction Methods 0.000 description 3
- 229930195729 fatty acid Natural products 0.000 description 3
- 239000000194 fatty acid Substances 0.000 description 3
- 150000004665 fatty acids Chemical class 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 3
- 229910052753 mercury Inorganic materials 0.000 description 3
- 235000003441 saturated fatty acids Nutrition 0.000 description 3
- 230000001953 sensory effect Effects 0.000 description 3
- 230000021317 sensory perception Effects 0.000 description 3
- 229940031439 squalene Drugs 0.000 description 3
- TUHBEKDERLKLEC-UHFFFAOYSA-N squalene Natural products CC(=CCCC(=CCCC(=CCCC=C(/C)CCC=C(/C)CC=C(C)C)C)C)C TUHBEKDERLKLEC-UHFFFAOYSA-N 0.000 description 3
- 238000007655 standard test method Methods 0.000 description 3
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- OYHQOLUKZRVURQ-HZJYTTRNSA-N Linoleic acid Chemical compound CCCCC\C=C/C\C=C/CCCCCCCC(O)=O OYHQOLUKZRVURQ-HZJYTTRNSA-N 0.000 description 2
- 229930182558 Sterol Natural products 0.000 description 2
- 239000004480 active ingredient Substances 0.000 description 2
- 239000003963 antioxidant agent Substances 0.000 description 2
- 235000006708 antioxidants Nutrition 0.000 description 2
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 description 2
- 230000004888 barrier function Effects 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 2
- 239000000571 coke Substances 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- 238000007731 hot pressing Methods 0.000 description 2
- 229910052500 inorganic mineral Inorganic materials 0.000 description 2
- 235000020778 linoleic acid Nutrition 0.000 description 2
- OYHQOLUKZRVURQ-IXWMQOLASA-N linoleic acid Natural products CCCCC\C=C/C\C=C\CCCCCCCC(O)=O OYHQOLUKZRVURQ-IXWMQOLASA-N 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 239000011707 mineral Substances 0.000 description 2
- 235000010755 mineral Nutrition 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 206010033675 panniculitis Diseases 0.000 description 2
- 230000037368 penetrate the skin Effects 0.000 description 2
- 230000035699 permeability Effects 0.000 description 2
- 230000001681 protective effect Effects 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 235000003702 sterols Nutrition 0.000 description 2
- 150000003432 sterols Chemical class 0.000 description 2
- 210000004304 subcutaneous tissue Anatomy 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- OYHQOLUKZRVURQ-NTGFUMLPSA-N (9Z,12Z)-9,10,12,13-tetratritiooctadeca-9,12-dienoic acid Chemical compound C(CCCCCCC\C(=C(/C\C(=C(/CCCCC)\[3H])\[3H])\[3H])\[3H])(=O)O OYHQOLUKZRVURQ-NTGFUMLPSA-N 0.000 description 1
- 244000144725 Amygdalus communis Species 0.000 description 1
- 235000011437 Amygdalus communis Nutrition 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 240000001548 Camellia japonica Species 0.000 description 1
- 235000014036 Castanea Nutrition 0.000 description 1
- 241001070941 Castanea Species 0.000 description 1
- 235000009024 Ceanothus sanguineus Nutrition 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- 244000178870 Lavandula angustifolia Species 0.000 description 1
- 235000010663 Lavandula angustifolia Nutrition 0.000 description 1
- 240000003553 Leptospermum scoparium Species 0.000 description 1
- 235000015459 Lycium barbarum Nutrition 0.000 description 1
- 241000208473 Macadamia ternifolia Species 0.000 description 1
- NIPNSKYNPDTRPC-UHFFFAOYSA-N N-[2-oxo-2-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 NIPNSKYNPDTRPC-UHFFFAOYSA-N 0.000 description 1
- 241001504519 Papio ursinus Species 0.000 description 1
- BAECOWNUKCLBPZ-HIUWNOOHSA-N Triolein Natural products O([C@H](OCC(=O)CCCCCCC/C=C\CCCCCCCC)COC(=O)CCCCCCC/C=C\CCCCCCCC)C(=O)CCCCCCC/C=C\CCCCCCCC BAECOWNUKCLBPZ-HIUWNOOHSA-N 0.000 description 1
- PHYFQTYBJUILEZ-UHFFFAOYSA-N Trioleoylglycerol Natural products CCCCCCCCC=CCCCCCCCC(=O)OCC(OC(=O)CCCCCCCC=CCCCCCCCC)COC(=O)CCCCCCCC=CCCCCCCCC PHYFQTYBJUILEZ-UHFFFAOYSA-N 0.000 description 1
- 229930003427 Vitamin E Natural products 0.000 description 1
- 239000008168 almond oil Substances 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 239000010478 argan oil Substances 0.000 description 1
- 235000021302 avocado oil Nutrition 0.000 description 1
- 239000008163 avocado oil Substances 0.000 description 1
- 238000003965 capillary gas chromatography Methods 0.000 description 1
- 235000012000 cholesterol Nutrition 0.000 description 1
- 235000018597 common camellia Nutrition 0.000 description 1
- 230000001186 cumulative effect Effects 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N diethyl ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 239000003974 emollient agent Substances 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 235000019387 fatty acid methyl ester Nutrition 0.000 description 1
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 description 1
- 239000008169 grapeseed oil Substances 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 230000006698 induction Effects 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 229940119170 jojoba wax Drugs 0.000 description 1
- 239000001102 lavandula vera Substances 0.000 description 1
- 235000018219 lavender Nutrition 0.000 description 1
- 230000001050 lubricating effect Effects 0.000 description 1
- 230000007721 medicinal effect Effects 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 235000021281 monounsaturated fatty acids Nutrition 0.000 description 1
- JXTPJDDICSTXJX-UHFFFAOYSA-N n-Triacontane Natural products CCCCCCCCCCCCCCCCCCCCCCCCCCCCCC JXTPJDDICSTXJX-UHFFFAOYSA-N 0.000 description 1
- 239000000346 nonvolatile oil Substances 0.000 description 1
- 238000010606 normalization Methods 0.000 description 1
- 235000020777 polyunsaturated fatty acids Nutrition 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 230000002000 scavenging effect Effects 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 230000009759 skin aging Effects 0.000 description 1
- 208000017520 skin disease Diseases 0.000 description 1
- 231100000245 skin permeability Toxicity 0.000 description 1
- 229940032094 squalane Drugs 0.000 description 1
- PHYFQTYBJUILEZ-IUPFWZBJSA-N triolein Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OCC(OC(=O)CCCCCCC\C=C/CCCCCCCC)COC(=O)CCCCCCC\C=C/CCCCCCCC PHYFQTYBJUILEZ-IUPFWZBJSA-N 0.000 description 1
- 229940117972 triolein Drugs 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 235000019165 vitamin E Nutrition 0.000 description 1
- 229940046009 vitamin E Drugs 0.000 description 1
- 239000011709 vitamin E Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 239000001993 wax Substances 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
- C11B1/04—Pretreatment of vegetable raw material
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/06—Production of fats or fatty oils from raw materials by pressing
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/001—Refining fats or fatty oils by a combination of two or more of the means hereafter
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/008—Refining fats or fatty oils by filtration, e.g. including ultra filtration, dialysis
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/16—Refining fats or fatty oils by mechanical means
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Microbiology (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- Animal Behavior & Ethology (AREA)
- Mechanical Engineering (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
- Fats And Perfumes (AREA)
Abstract
本发明属于日用化工中的护肤品技术领域,具体涉及一种澳洲坚果基础油及其制备方法,包括以下步骤:(1)原料前处理(2)粉碎;(3)低温烘干;(4)冷榨;(5)离心;(6)冬化处理;(7)过滤;(8)成品。本发明采用低温压榨的方法,无添加和溶剂残留,加工全程严格控制温度不高于60℃,最大程度地保留澳洲坚果油的天然营养成分。同时,通过冬化处理,提高坚果基础油的稳定性,有效避免其在存放过程中由于低温有悬浮物质析出的质量问题。采用本发明方法制得的澳洲坚果基础油色泽清透明亮,有坚果香气,质地温和不油腻,无刺激性,安全稳定,具有优越的滋润性和肌肤渗透性以及丰富的保湿成分,也可促进其他护肤品营养成分的吸收。
The invention belongs to the technical field of skin care products in the daily chemical industry, and in particular relates to a macadamia nut base oil and a preparation method thereof, comprising the following steps: (1) raw material pretreatment (2) pulverization; (3) low temperature drying; (4) ) cold pressing; (5) centrifugation; (6) winterization treatment; (7) filtration; (8) finished product. The invention adopts the method of low-temperature pressing, without addition and solvent residue, and strictly controls the temperature not higher than 60 DEG C in the whole process of processing, so as to retain the natural nutritional components of the macadamia nut oil to the greatest extent. At the same time, through the winterization treatment, the stability of the nut base oil is improved, and the quality problem of the precipitation of suspended substances due to low temperature during the storage process is effectively avoided. The macadamia nut base oil prepared by the method of the invention is clear and transparent in color, has nutty aroma, mild texture, non-greasy, non-irritating, safe and stable, has superior moisturizing and skin penetration, and is rich in moisturizing ingredients, and can also promote Absorption of nutrients from other skin care products.
Description
技术领域technical field
本发明属于日用化工中的护肤品技术领域,具体涉及一种澳洲坚果基础油及其制备方法。The invention belongs to the technical field of skin care products in daily chemical industry, and particularly relates to a macadamia nut base oil and a preparation method thereof.
背景技术Background technique
基础油(base oil或是carrier oil),也有人称之为媒介油或是基底油,是从植物的种子、花朵、根茎或果实中萃取的非挥发性油脂。基础油一般性质温和,可润滑肌肤,能直接用于肌肤按摩,也是稀释精油的最佳基底油。常见的有橄榄油、荷荷巴油、甜杏仁油、葡萄籽油、鳄梨油等。单方精油无法直接抹在皮肤上(除薰衣草和茶树可以用棉签小面积点涂外),它们必须在基础油中稀释后,才可以广泛地用在我们人体的肌肤上。很多基础油本身就具有医疗的效果,通过冷压萃取可以将植物中的矿物质、维生素、脂肪酸,保存良好不流失,具有优越的滋润滋养特质。Base oil (base oil or carrier oil), also known as medium oil or carrier oil, is a non-volatile oil extracted from the seeds, flowers, roots or fruits of plants. The base oil is generally mild in nature, can lubricate the skin, can be used directly for skin massage, and is also the best base oil for diluting essential oils. Common ones are olive oil, jojoba oil, sweet almond oil, grapeseed oil, avocado oil, etc. Single essential oils cannot be applied directly to the skin (except for lavender and tea tree, which can be applied to a small area with a cotton swab), they must be diluted in a base oil before they can be widely used on our human skin. Many base oils themselves have medical effects. Through cold-pressed extraction, minerals, vitamins, and fatty acids in plants can be well preserved and not lost, with superior moisturizing and nourishing properties.
澳洲坚果(拉丁学名:Macadamia ternifolia F. Muell.)又名昆士兰栗、夏威夷果、巴布果、澳洲胡桃等,其营养成分非常丰富,含油量高达60-80%。澳洲坚果油中不含胆固醇,饱和脂肪酸含量低,单不饱和脂肪酸含量超过80%,主要是由油酸、棕榈油酸和少量的亚油酸等多不饱和脂肪酸组成。澳洲坚果油中油酸含量高达58%-65%,棕榈油酸含量高达12-15%。实验表明,澳洲坚果的透皮强度和透皮深度优于山茶油,油酸及棕榈油酸的累积渗透量较高,渗透速率较快。澳洲坚果油中不仅不饱和脂肪酸含量丰富,其甾醇含量也非常丰富,因此其对羟自由基、DPPH自由基以及超氧阴离子自由基的清除能力较好,氧化诱导期与橄榄油相比更长,因此其具有良好的抗氧化能力。Macadamia nuts (Latin name: Macadamia ternifolia F. Muell.), also known as Queensland chestnuts, macadamia nuts, baboon nuts, macadamia nuts, etc., are very rich in nutrients, with an oil content of 60-80%. Macadamia nut oil contains no cholesterol, low saturated fatty acid content, and monounsaturated fatty acid content of more than 80%, mainly composed of polyunsaturated fatty acids such as oleic acid, palmitoleic acid and a small amount of linoleic acid. The content of oleic acid in macadamia oil is as high as 58%-65%, and the content of palmitoleic acid is as high as 12-15%. Experiments show that the penetration strength and penetration depth of macadamia nuts are better than those of camellia oil, the cumulative penetration of oleic acid and palmitoleic acid is higher, and the penetration rate is faster. Macadamia nut oil is not only rich in unsaturated fatty acids, but also rich in sterols, so its scavenging ability to hydroxyl radicals, DPPH radicals and superoxide anion radicals is better, and the oxidation induction period is longer than that of olive oil. , so it has good antioxidant capacity.
总的来说,澳洲坚果油不饱和脂肪酸的组成和比例能较好的促进油脂和营养物质的吸收,在肌肤上形成一层天然的保护膜。不饱和程度很高,其性状如水般,在肌肤上易于流动,可迅速突破皮肤屏障渗入皮下组织。澳洲坚果油的分子结构非常独特,均以小分子团的形式存在,与肌肤具有较好的亲和性与渗透性。此外,分子团里面包埋这天然抗氧化物质如维生素E、甾醇等,能有效对抗自由基,防止皮肤衰老。由于坚果油最大的特点是其与皮肤良好的相容性及亲和性,这是其它大部分植物油无法比拟的,因此非常适宜用作高档化妆品油性原料、按摩基础油、稀释单方精油等。In general, the composition and proportion of unsaturated fatty acids in macadamia oil can better promote the absorption of oils and nutrients, and form a natural protective film on the skin. It has a high degree of unsaturation, and its properties are water-like, easy to flow on the skin, and can quickly penetrate the skin barrier and penetrate into the subcutaneous tissue. The molecular structure of macadamia oil is very unique and exists in the form of small molecular clusters, which has good affinity and permeability with the skin. In addition, the natural antioxidants such as vitamin E and sterols are embedded in the molecular mass, which can effectively fight free radicals and prevent skin aging. Because the biggest feature of argan oil is its good compatibility and affinity with the skin, which is unmatched by most other vegetable oils, so it is very suitable for use as oily raw materials for high-end cosmetics, massage base oils, and diluted unilateral essential oils.
目前市场上澳洲坚果基础油类产品存在诸多问题,一是部分产品以热压榨法制得,焦香味浓郁,颜色深黄,有效成分受到破坏,感官不佳不适宜直接涂抹;另一部分产品虽经冷压榨法制得,但未经冬化处理,产品放置时间长,特别是冬季易出现悬浮物,且由于含有少量饱和脂肪酸,质地黏腻,影响使用感受。因此,目前急需开发一种提取方法简单,成本低,且质地温和清爽,稳定性高的坚果基础油产品,这既能满足消费者对澳洲坚果护肤滋养作用的追求又确保产品稳定性。At present, there are many problems with macadamia nut base oil products on the market. One is that some products are made by hot pressing method, which has a strong coke fragrance, dark yellow color, and damaged active ingredients, which are not suitable for direct application due to poor sensory perception. It is prepared by pressing method, but without winterization treatment, the product is stored for a long time, especially in winter, suspended solids are prone to appear, and because it contains a small amount of saturated fatty acid, the texture is sticky, which affects the feeling of use. Therefore, there is an urgent need to develop a nut base oil product with a simple extraction method, low cost, mild and refreshing texture, and high stability, which can not only satisfy consumers' pursuit of macadamia nut skin care and nourishment, but also ensure product stability.
发明内容SUMMARY OF THE INVENTION
本发明的目的是针对现有澳洲坚果基础油产品感官不佳、质地黏腻、稳定性差等问题,提供一种澳洲坚果基础油及其制备方法。采用本发明方法制得的澳洲坚果基础油色泽清透明亮,有淡淡的坚果香气,质地温和不油腻,无刺激性,安全稳定,具有优越的滋润性和肌肤渗透性以及丰富的保湿成分,也可促进其他护肤品营养成分的吸收;可作为按摩基础油,也可作为稀释其他精油的基础油配合使用。The purpose of the present invention is to provide a macadamia nut base oil and a preparation method thereof for the problems of poor sensory perception, sticky texture and poor stability of the existing macadamia nut base oil products. The macadamia nut base oil prepared by the method of the invention is clear and bright in color, has a light nut aroma, is mild in texture, non-greasy, non-irritating, safe and stable, has excellent moisturizing properties and skin penetration, and is rich in moisturizing ingredients. It can promote the absorption of nutrients in other skin care products; it can be used as a base oil for massage or as a base oil for diluting other essential oils.
为实现上述目的,本发明采用如下技术方案:To achieve the above object, the present invention adopts the following technical solutions:
一方面,本发明提供一种浓澳洲坚果油的制备方法,该制备方法包括如下步骤:On the one hand, the present invention provides a kind of preparation method of concentrated macadamia nut oil, and this preparation method comprises the steps:
(1)原料前处理:选用新鲜采摘、外表无损坏的澳洲坚果作为原料,脱去外层青皮,利用坚果去壳器去除坚果硬壳,剔除发黑、虫蛀及霉烂的果仁;(1) Pre-processing of raw materials: Select freshly picked macadamia nuts with no damage to the appearance as raw materials, remove the outer green skin, use a nut sheller to remove the hard shell of the nuts, and remove the black, moth-eaten and moldy nuts;
(2)粉碎:将脱皮去壳后的果仁进行粉碎处理,得到大小均一的物料;(2) Pulverization: pulverize the peeled and dehulled nuts to obtain materials of uniform size;
(3)低温烘干:将粉碎后的物料送入烘房进行烘干处理,设定干燥温度和时间,最终得到重量含水量≤1.8%的物料;(3) Low-temperature drying: send the pulverized materials to the drying room for drying treatment, set the drying temperature and time, and finally obtain materials with a weight moisture content of ≤1.8%;
(4)冷榨:经低温干燥后的物料送入螺旋压榨机压榨;(4) Cold pressing: the material dried at low temperature is sent to the screw press for pressing;
(5)离心:将压榨得到的油脂混合物送入离心机离心,取上层清油;(5) Centrifugation: the oil mixture obtained by pressing is sent to a centrifuge for centrifugation, and the supernatant oil is taken;
(6)冬化处理:将上层清油置于50℃恒温水浴并不断搅拌,一定时间后将样品转移至冰水浴中降温,缓慢搅拌,待样品冷却至10℃,停止搅拌,放入设定温度的冰箱中,冷却结晶;(6) Winterization treatment: put the supernatant oil in a constant temperature water bath at 50°C and keep stirring. After a certain period of time, transfer the sample to an ice-water bath to cool down and stir slowly. When the sample is cooled to 10°C, stop stirring and put it into the set temperature. in the refrigerator, cooling to crystallize;
(7)过滤:过滤掉样品中析出的悬浮物,恢复至室温,得到成品。(7) Filtration: filter out the suspended matter precipitated in the sample, return to room temperature, and obtain the finished product.
上述的澳洲坚果基础油的制备方法,所述步骤(1)中原料澳洲坚果果仁的重量含水量为12-16%,脂肪含量70-73g/100g,酸价0.15-0.2mgKOH/g,过氧化值0.01-0.016g/100g,油酸含量40-43g/100g,棕榈油酸含量10-12g/100g,要求果仁饱满完整、无瘪仁、无霉变,出仁率为13-15%。要经过严格精选,通过人工或色选机等方式,分离发黑、虫蛀及霉烂的果仁,因为原料未成熟或被微生物侵蚀,易导致澳洲坚果油中酸值升高,有害成分增加,影响成品质量。The preparation method of the above-mentioned macadamia base oil, in the step (1), the weight water content of the raw macadamia nuts is 12-16%, the fat content is 70-73g/100g, the acid value is 0.15-0.2mgKOH/g, The oxidation value is 0.01-0.016g/100g, the oleic acid content is 40-43g/100g, and the palmitoleic acid content is 10-12g/100g. . After strict selection, the blackened, moth-eaten and moldy nuts must be separated manually or by color sorters. Because the raw materials are immature or eroded by microorganisms, it is easy to lead to an increase in the acid value of macadamia nut oil and an increase in harmful components. , affecting the quality of the finished product.
上述的澳洲坚果基础油的制备方法,所述步骤(2)中将果仁粉碎至直径为0.3-0.5cm的完整颗粒。由于干燥温度较低,颗粒过大易导致干燥不彻底,水分分布不均匀,颗粒过小易压榨过程机械力不足,影响出油率。因此,将果仁粉碎至0.4cm左右大小十分必要。In the above-mentioned preparation method of macadamia base oil, in the step (2), the nuts are pulverized to complete particles with a diameter of 0.3-0.5 cm. Due to the low drying temperature, too large particles can easily lead to incomplete drying and uneven distribution of moisture. If the particles are too small, the mechanical force during the pressing process will be insufficient, which will affect the oil yield. Therefore, it is necessary to pulverize the nuts to a size of about 0.4 cm.
上述的洲坚果基础油的制备方法,步骤(3)中采用低温干燥处理,具体为:平铺厚度小于0.5cm,45℃下烘干48-56h,直至重量含水量≤1.8%。干燥的温度必须严格控制,全程采用低温(45℃左右)处理,由于温度较低,因此干燥的时间延长,干燥的结束点必须控制好,测量原料的重量含水量低于1.8%时,干燥才完全结束。若干燥不彻底,物料表面与内部水分分布不均,易导致送入螺旋压榨机后由于含水量过高,物料质地仍紧密,水分和油脂难以分离,压榨无法获得油脂,形成粉末状的坚果碎粉。平铺的厚度必须小于0.5cm,并且干燥过程中每隔一定时间翻面,保证干燥达到彻底。In the above-mentioned preparation method of nut base oil, low temperature drying treatment is adopted in step (3), specifically: the thickness of the tile is less than 0.5cm, and drying is carried out at 45°C for 48-56 hours until the weight water content is less than or equal to 1.8%. The drying temperature must be strictly controlled, and the whole process is treated at low temperature (about 45°C). Due to the low temperature, the drying time is prolonged, and the drying end point must be well controlled. When the weight moisture content of the measured raw material is less than 1.8%, drying can be performed. Completely over. If the drying is not complete, the moisture distribution on the surface and the interior of the material will be uneven, which will easily lead to the high moisture content of the material after being sent to the screw press. The texture of the material is still tight, and the moisture and oil are difficult to separate. pink. The thickness of the tile must be less than 0.5cm, and it must be turned over at regular intervals during the drying process to ensure complete drying.
上述的澳洲坚果基础油的制备方法,所述步骤(4)中螺旋压榨机无需预热,进料量50g/min,收集油脂混合物。要注意的是,虽然螺旋压榨机未预热,但在压榨过程中,由于物料与螺旋轴的摩擦易导致温度升高,因此要随时注意观察,当压榨温度升高达到60℃左右,要暂时停止加料,当内部温度降低后再继续加料压榨。In the above-mentioned preparation method of macadamia base oil, in the step (4), the screw press does not need to be preheated, the feed rate is 50 g/min, and the oil mixture is collected. It should be noted that although the screw press is not preheated, during the pressing process, due to the friction between the material and the screw shaft, the temperature is likely to rise, so pay attention to observe at any time. When the pressing temperature rises to about 60 °C, it will be temporarily Stop feeding and continue feeding and pressing when the internal temperature drops.
上述的澳洲坚果基础油的制备方法,所述步骤(5)中离心机转速为4000r/min,离心时间为25-30min。由于物料是经过低温压榨,油相和非油相并未很好的分离,油脂混合物质地粘稠,浑浊,因此离心时间需要适当延长,设定为25-30min,能够很好的分离固液两相,去除油渣得到上层油相样品。In the above-mentioned preparation method of macadamia base oil, in the step (5), the rotating speed of the centrifuge is 4000r/min, and the centrifugation time is 25-30min. Because the material is pressed at low temperature, the oil phase and non-oil phase are not well separated, and the oil mixture is viscous and turbid, so the centrifugation time needs to be appropriately extended, set to 25-30min, which can well separate the solid-liquid two. phase, remove the oil residue to obtain the upper oil phase sample.
上述的澳洲坚果基础油的制备方法,所述步骤(6)中,50℃恒温水浴时间30-40min,冰箱中于4℃下静置24-28h,静置过程中密封。冬化处理指通过将油脂混合物置于低温环境中处理一定时间,油脂中的饱和脂肪酸易析出,从而实现液体油与固体脂的分离。先升温至50℃是为了使固体脂充分溶于油中,若直接进行冬化处理会影响固体脂的析出效果。在4-10℃条件下,随着温度降低,固体脂析出越多,但当温度在2℃时,接近三油酸甘油酯的熔点,油脂中的固体脂和液体油的分离不太容易,因此选择冬化温度为4℃。当冬化时间较短时,冬化不彻底,部分饱和脂肪酸和蜡质未完全析出,当冬化时间增加到24-28h时,结晶较多,且当冬化时间>28h时,结晶量增加已不明显,出于节约能源考虑,4℃处理时间为24-28h。冷却过程中不断搅拌是为了增加析出晶粒之间的碰撞机会,有利于固体脂的析出。In the above-mentioned preparation method of macadamia nut base oil, in the step (6), a constant temperature water bath time of 30-40min at 50°C is placed in a refrigerator at 4°C for 24-28h, and sealed during the standing process. Winterization treatment means that by placing the oil mixture in a low temperature environment for a certain period of time, the saturated fatty acids in the oil are easily precipitated, thereby realizing the separation of liquid oil and solid fat. The purpose of raising the temperature to 50°C is to fully dissolve the solid fat in the oil. If the winterization treatment is carried out directly, the precipitation effect of the solid fat will be affected. Under the condition of 4-10 °C, as the temperature decreases, the more solid fat is precipitated, but when the temperature is at 2 °C, it is close to the melting point of triolein, and the separation of solid fat and liquid oil in oil is not easy. Therefore, the winterization temperature was chosen to be 4°C. When the winterization time is short, the winterization is incomplete, and some saturated fatty acids and waxes are not completely precipitated. When the winterization time increases to 24-28h, the crystallization is more, and when the winterization time is greater than 28h, the amount of crystallization increases. It is not obvious. For the sake of energy saving, the treatment time at 4°C is 24-28h. The continuous stirring during the cooling process is to increase the chance of collision between the precipitated grains, which is beneficial to the precipitation of solid fat.
另一方面,本发明提供一种澳洲坚果基础油,该澳洲坚果基础油通过上述澳洲坚果基础油的制备方法制得。In another aspect, the present invention provides a macadamia nut base oil prepared by the above-mentioned preparation method of a macadamia nut base oil.
本发明的有益效果为:The beneficial effects of the present invention are:
目前市场上澳洲坚果基础油类产品存在诸多问题,一是部分产品以热压榨法制得,焦香味浓郁,颜色深黄,有效成分受到破坏,感官不佳不适宜直接涂抹;另一部分产品虽经冷压榨法制得,但未经冬化处理,产品放置时间长,特别是冬季易出现悬浮物,且由于含有少量饱和脂肪酸,质地黏腻,影响使用感受,影响产品档次和竞争力。At present, there are many problems with macadamia nut base oil products on the market. One is that some products are made by hot pressing method, which has a strong coke fragrance, dark yellow color, and damaged active ingredients, which are not suitable for direct application due to poor sensory perception. It is prepared by pressing method, but without winterization treatment, the product is stored for a long time, especially in winter, suspended solids are prone to occur, and because it contains a small amount of saturated fatty acid, the texture is sticky, which affects the feeling of use, and affects the grade and competitiveness of the product.
针对上述问题,一方面,本发明采用新鲜澳洲坚果低温压榨的方法,无添加和溶剂残留,加工全程严格控制温度不高于60℃,最大程度地保留澳洲坚果油的天然营养成分,富含多种不饱和脂肪酸、氨基酸、矿物质等。同时,通过冬化处理,提高坚果基础油的稳定性,有效避免其在存放过程中由于低温有悬浮物质析出的质量问题。另一方面,采用本发明方法制得的澳洲坚果基础油色泽清透明亮,有淡淡的坚果香气,质地温和不油腻,无刺激性,安全稳定,具有优越的滋润性和肌肤渗透性以及丰富的保湿成分,也可促进其他护肤品营养成分的吸收。可作为按摩基础油,也可作为稀释其他精油的基础油配合使用。In view of the above problems, on the one hand, the present invention adopts the method of low-temperature pressing of fresh macadamia nuts, without addition and solvent residues, and the temperature is strictly controlled not to be higher than 60°C in the whole process of processing, so as to retain the natural nutrients of macadamia nut oil to the greatest extent, and is rich in more unsaturated fatty acids, amino acids, minerals, etc. At the same time, through the winterization treatment, the stability of the nut base oil is improved, and the quality problem of the precipitation of suspended substances due to low temperature during the storage process is effectively avoided. On the other hand, the macadamia nut base oil prepared by the method of the present invention is clear and bright in color, has a light nut aroma, mild texture, non-greasy, non-irritating, safe and stable, and has excellent moisturizing and skin permeability and rich Moisturizing ingredients, can also promote the absorption of other skin care products nutrients. Can be used as a base oil for massage or as a base oil for diluting other essential oils.
附图说明Description of drawings
图1为本发明澳洲坚果基础油的制备方法的制备工艺路线图;Fig. 1 is the preparation process route diagram of the preparation method of macadamia base oil of the present invention;
图2 为本发明实施例1-3制备得到的澳洲坚果基础油与市售山茶油、橄榄油的黏度对比图。Figure 2 is a viscosity comparison diagram of the macadamia nut base oil prepared in Examples 1-3 of the present invention, and commercially available camellia oil and olive oil.
具体实施方式Detailed ways
为了使本发明的目的、技术方案及优点更加清楚明白,以下结合具体实施例,对本发明进行进一步详细说明。应当理解,此处所描述的具体实施例仅用以解释本发明,并不用于限定本发明。In order to make the objectives, technical solutions and advantages of the present invention clearer, the present invention will be further described in detail below with reference to specific embodiments. It should be understood that the specific embodiments described herein are only used to explain the present invention, but not to limit the present invention.
一种澳洲坚果基础油的制备方法,包括如下步骤:A preparation method of macadamia nut base oil, comprising the following steps:
(1)原料前处理:选用新鲜采摘、外表无损坏的澳洲坚果作为原料,脱去外层青皮,利用坚果去壳器去除坚果硬壳,剔除发黑、虫蛀及霉烂的果仁;所述的原料澳洲坚果果仁的重量含水量为12-16%,脂肪含量70-73g/100g,酸价0.15-0.2mgKOH/g,过氧化值0.01-0.016g/100g,油酸含量40-43g/100g,棕榈油酸含量10-12g/100g,要求果仁饱满完整、无瘪仁、无霉变,出仁率为13-15%;(1) Pretreatment of raw materials: choose freshly picked macadamia nuts with no damage to the appearance as raw materials, remove the outer green skin, use a nut sheller to remove the hard shell of the nuts, and remove the black, moth-eaten and moldy nuts; The raw macadamia nuts have a weight water content of 12-16%, a fat content of 70-73g/100g, an acid value of 0.15-0.2mgKOH/g, a peroxide value of 0.01-0.016g/100g, and an oleic acid content of 40-43g/g. 100g, the palmitoleic acid content is 10-12g/100g, the kernels are required to be full and complete, no shriveled kernels, no mildew, and the kernel rate is 13-15%;
(2)粉碎:将脱皮去壳后的果仁进行粉碎处理,粉碎至直径为0.3-0.5cm的完整颗粒,得到大小均一的物料;(2) Pulverization: The peeled and dehulled nuts are pulverized to complete particles with a diameter of 0.3-0.5 cm to obtain materials of uniform size;
(3)低温烘干:将粉碎后的物料送入烘房进行烘干处理,设定干燥温度和时间,最终得到重量含水量≤1.8%的物料;具体为:平铺厚度小于0.5cm,45℃下烘干48-56h,直至重量含水量≤1.8%;(3) Low-temperature drying: send the pulverized materials to the drying room for drying treatment, set the drying temperature and time, and finally obtain materials with a weight moisture content of ≤1.8%; specifically: the tile thickness is less than 0.5cm, 45 Dry at ℃ for 48-56h until the water content by weight is less than or equal to 1.8%;
(4)冷榨:经低温干燥后的物料送入螺旋压榨机压榨;螺旋压榨机无需预热,进料量50g/min,收集油脂混合物;过程中随时观察压榨温度,若温度升高,停止压榨,待温度下降至<60℃,继续压榨;(4) Cold pressing: the material dried at low temperature is sent to the screw press for pressing; the screw press does not need to be preheated, the feed rate is 50g/min, and the oil mixture is collected; the pressing temperature is observed at any time during the process, and if the temperature rises, stop Press, and continue pressing when the temperature drops to <60°C;
(5)离心:将压榨得到的油脂混合物送入离心机离心,离心机转速为4000r/min,离心时间为25-30min,取上层清油;(5) Centrifugation: send the oil mixture obtained by pressing into a centrifuge for centrifugation, the centrifuge speed is 4000r/min, the centrifugation time is 25-30min, and the supernatant oil is taken;
(6)冬化处理:将上层清油置于50℃恒温水浴并不断搅拌,30-40min后将样品转移至冰水浴中降温;待样品冷却至10℃,放入4℃冰箱中静置24-28h冷却结晶,静置过程中密封;(6) Winterization treatment: put the supernatant oil in a constant temperature water bath at 50°C and keep stirring. After 30-40min, transfer the sample to an ice-water bath to cool down; when the sample is cooled to 10°C, put it in a 4°C refrigerator and let it stand for 24-40 minutes. 28h cooling and crystallization, and sealing during standing;
(7)过滤:过滤掉样品中析出的悬浮物,恢复至室温,得到成品。(7) Filtration: filter out the suspended matter precipitated in the sample, return to room temperature, and obtain the finished product.
以下结合具体实施例进一步说明。The following is further described in conjunction with specific embodiments.
实施例1Example 1
一种澳洲坚果基础油的制备方法,包括如下步骤:A preparation method of macadamia nut base oil, comprising the following steps:
(1)原料前处理:选用新鲜采摘、外表无损坏的澳洲坚果作为原料,脱去外层青皮,利用坚果去壳器去除坚果硬壳,剔除发黑、虫蛀及霉烂的果仁;果仁的重量含水量为14.2%,脂肪含量71.2g/100g,酸价0.17mgKOH/g,过氧化值0.012g/100g,油酸含量40.1g/100g,棕榈油酸含量10.3g/100g,要求果仁饱满完整、无瘪仁、无霉变,出仁率为13.8%;(1) Pretreatment of raw materials: Select freshly picked macadamia nuts with no damage to the appearance as raw materials, remove the outer green skin, use a nut sheller to remove the hard shell of the nuts, and remove the black, moth-eaten and moldy nuts; The weight of the water content is 14.2%, the fat content is 71.2g/100g, the acid value is 0.17mgKOH/g, the peroxide value is 0.012g/100g, the oleic acid content is 40.1g/100g, and the palmitoleic acid content is 10.3g/100g. Full and complete, no shriveled kernels, no mildew, the kernel rate is 13.8%;
(2)粉碎:将脱皮去壳后的果仁进行粉碎处理,粉碎至直径为0.3-0.5cm的完整颗粒,得到大小均一的物料;(2) Pulverization: The peeled and dehulled nuts are pulverized to complete particles with a diameter of 0.3-0.5 cm to obtain materials of uniform size;
(3)低温烘干:将粉碎后的物料送入烘房进行烘干处理,平铺的厚度小于0.5cm,45℃干燥52h,干燥过程中每隔一定时间翻面,保证干燥达到彻底,最终得到重量含水量1.71%的物料;(3) Low-temperature drying: The pulverized material is sent to the drying room for drying treatment. The thickness of the tile is less than 0.5cm, and it is dried at 45 °C for 52 hours. During the drying process, it is turned over at regular intervals to ensure complete drying. A material with a water content of 1.71% by weight was obtained;
(4)冷榨:经低温干燥后的物料送入螺旋压榨机压榨;螺旋压榨机无需预热,进料量50g/min,收集油脂混合物;过程中随时观察压榨温度,若温度升高,停止压榨,待温度下降至<60℃,继续压榨;(4) Cold pressing: the material dried at low temperature is sent to the screw press for pressing; the screw press does not need to be preheated, the feed rate is 50g/min, and the oil mixture is collected; the pressing temperature is observed at any time during the process, and if the temperature rises, stop Press, and continue pressing when the temperature drops to <60°C;
(5)离心:将压榨得到的油脂混合物送入离心机离心,离心机转速为4000r/min,离心时间为30min,取上层清油;(5) Centrifugation: send the oil mixture obtained by pressing into a centrifuge for centrifugation, the centrifuge speed is 4000r/min, the centrifugation time is 30min, and the supernatant oil is taken;
(6)冬化处理:将上层清油置于50℃恒温水浴并不断搅拌,30min后将样品转移至冰水浴中降温,待样品冷却至10℃,放入4℃冰箱中静置25h冷却结晶,静置过程中密封;(6) Winterization treatment: put the supernatant oil in a 50°C constant temperature water bath and keep stirring. After 30 minutes, transfer the sample to an ice-water bath to cool down. When the sample is cooled to 10°C, put it in a 4°C refrigerator for 25 hours to cool and crystallize. Sealed during standing;
(7)过滤:过滤掉样品中析出的悬浮物,恢复至室温,得到成品。(7) Filtration: filter out the suspended matter precipitated in the sample, return to room temperature, and obtain the finished product.
实施例2Example 2
一种澳洲坚果基础油的制备方法,包括如下步骤:A preparation method of macadamia nut base oil, comprising the following steps:
(1)原料前处理:选用新鲜采摘、外表无损坏的澳洲坚果作为原料,脱去外层青皮,利用坚果去壳器去除坚果硬壳,剔除发黑、虫蛀及霉烂的果仁;果仁的重量含水量为12.5%,脂肪含量72.4g/100g,酸价0.2mgKOH/g,过氧化值0.016g/100g,油酸含量43.0g/100g,棕榈油酸含量10.6g/100g,要求果仁饱满完整、无瘪仁、无霉变,出仁率为14.7%;(1) Pretreatment of raw materials: Select freshly picked macadamia nuts with no damage to the appearance as raw materials, remove the outer green skin, use a nut sheller to remove the hard shell of the nuts, and remove the black, moth-eaten and moldy nuts; The weight of the water content is 12.5%, the fat content is 72.4g/100g, the acid value is 0.2mgKOH/g, the peroxide value is 0.016g/100g, the oleic acid content is 43.0g/100g, and the palmitoleic acid content is 10.6g/100g. Full and complete, no shriveled kernels, no mildew, the kernel rate is 14.7%;
(2)粉碎:将脱皮去壳后的果仁进行粉碎处理,粉碎至直径为0.3-0.5cm的完整颗粒,得到大小均一的物料;(2) Pulverization: The peeled and dehulled nuts are pulverized to complete particles with a diameter of 0.3-0.5 cm to obtain materials of uniform size;
(3)低温烘干:将粉碎后的物料送入烘房进行烘干处理,平铺的厚度小于0.5cm,45℃干燥48h,干燥过程中每隔一定时间翻面,保证干燥达到彻底,最终得到重量含水量1.62%的物料;(3) Low-temperature drying: send the pulverized material to the drying room for drying treatment. The thickness of the tile is less than 0.5cm, and it is dried at 45 °C for 48 hours. During the drying process, it is turned over at regular intervals to ensure complete drying. A material with a water content of 1.62% by weight was obtained;
(4)冷榨:经低温干燥后的物料送入螺旋压榨机压榨;螺旋压榨机无需预热,进料量50g/min,收集油脂混合物;过程中随时观察压榨温度,若温度升高,停止压榨,待温度下降至<60℃,继续压榨;(4) Cold pressing: the material dried at low temperature is sent to the screw press for pressing; the screw press does not need to be preheated, the feed rate is 50g/min, and the oil mixture is collected; the pressing temperature is observed at any time during the process, and if the temperature rises, stop Press, and continue pressing when the temperature drops to <60°C;
(5)离心:将压榨得到的油脂混合物送入离心机离心,离心机转速为4000r/min,离心时间为25min,取上层清油;(5) Centrifugation: send the oil mixture obtained by pressing into a centrifuge for centrifugation, the centrifuge speed is 4000r/min, the centrifugation time is 25min, and the supernatant oil is taken;
(6)冬化处理:将上层清油置于50℃恒温水浴并不断搅拌,30min后将样品转移至冰水浴中降温。待样品冷却至10℃,放入4℃冰箱中静置24h冷却结晶,静置过程中密封;(6) Winterization treatment: put the supernatant oil in a constant temperature water bath at 50°C and keep stirring, and transfer the sample to an ice water bath for cooling after 30 min. After the sample is cooled to 10°C, put it in a 4°C refrigerator for 24 hours to cool and crystallize, and seal it during the standing process;
(7)过滤:过滤掉样品中析出的悬浮物,恢复至室温,得到成品。(7) Filtration: filter out the suspended matter precipitated in the sample, return to room temperature, and obtain the finished product.
实施例3Example 3
一种澳洲坚果基础油的制备方法,包括如下步骤:A preparation method of macadamia nut base oil, comprising the following steps:
(1)原料前处理:选用新鲜采摘、外表无损坏的澳洲坚果作为原料,脱去外层青皮,利用坚果去壳器去除坚果硬壳,剔除发黑、虫蛀及霉烂的果仁;果仁的重量含水量为15.1%,脂肪含量70.1g/100g,酸价0.15mgKOH/g,过氧化值0.010g/100g,油酸含量43.0g/100g,棕榈油酸含量10.6g/100g,要求果仁饱满完整、无瘪仁、无霉变,出仁率为13.1%;(1) Pretreatment of raw materials: Select freshly picked macadamia nuts with no damage to the appearance as raw materials, remove the outer green skin, use a nut sheller to remove the hard shell of the nuts, and remove the black, moth-eaten and moldy nuts; The weight of the water content is 15.1%, the fat content is 70.1g/100g, the acid value is 0.15mgKOH/g, the peroxide value is 0.010g/100g, the oleic acid content is 43.0g/100g, and the palmitoleic acid content is 10.6g/100g. Full and complete, no shriveled kernels, no mildew, the kernel rate is 13.1%;
(2)粉碎:将脱皮去壳后的果仁进行粉碎处理,粉碎至直径为0.3-0.5cm的完整颗粒,得到大小均一的物料;(2) Pulverization: The peeled and dehulled nuts are pulverized to complete particles with a diameter of 0.3-0.5 cm to obtain materials of uniform size;
(3)低温烘干:将粉碎后的物料送入烘房进行烘干处理,平铺的厚度小于0.5cm,45℃干燥56h,干燥过程中每隔一定时间翻面,保证干燥达到彻底,最终得到重量含水量1.75%的物料;(3) Low-temperature drying: The pulverized material is sent to the drying room for drying treatment. The thickness of the tile is less than 0.5cm, and it is dried at 45 °C for 56 hours. During the drying process, it is turned over at regular intervals to ensure complete drying. A material with a water content of 1.75% by weight was obtained;
(4)冷榨:经低温干燥后的物料送入螺旋压榨机压榨;螺旋压榨机无需预热,进料量50g/min,收集油脂混合物;过程中随时观察压榨温度,若温度升高,停止压榨,待温度下降至<60℃,继续压榨;(4) Cold pressing: the material dried at low temperature is sent to the screw press for pressing; the screw press does not need to be preheated, the feed rate is 50g/min, and the oil mixture is collected; the pressing temperature is observed at any time during the process, and if the temperature rises, stop Press, and continue pressing when the temperature drops to <60°C;
(5)离心:将压榨得到的油脂混合物送入离心机离心,离心机转速为4000r/min,离心时间为30min,取上层清油;(5) Centrifugation: send the oil mixture obtained by pressing into a centrifuge for centrifugation, the centrifuge speed is 4000r/min, the centrifugation time is 30min, and the supernatant oil is taken;
(6)冬化处理:将上层清油置于50℃恒温水浴并不断搅拌,30min后将样品转移至冰水浴中降温,待样品冷却至10℃,放入4℃冰箱中静置28h冷却结晶,静置过程中密封;(6) Winterization treatment: Put the supernatant oil in a constant temperature water bath at 50°C and keep stirring. After 30 minutes, transfer the sample to an ice-water bath to cool down. After the sample is cooled to 10°C, put it in a 4°C refrigerator for 28 hours to cool and crystallize. Sealed during standing;
(7)过滤:过滤掉样品中析出的悬浮物,恢复至室温,得到成品。(7) Filtration: filter out the suspended matter precipitated in the sample, return to room temperature, and obtain the finished product.
理化指标及卫生指标检测Physical and chemical indicators and health indicators detection
针对实施例1-3中制得的澳洲坚果基础油,分别测定理化指标和卫生指标,具体各指标的检测方法如下:For the macadamia nut base oil prepared in the embodiment 1-3, measure the physicochemical index and the hygienic index respectively, and the detection method of each specific index is as follows:
QBT4079-2010按摩基础油、按摩油QBT4079-2010 Massage base oil, massage oil
GB/T 7917.1-1987 化妆品卫生化学标准检验方法 汞GB/T 7917.1-1987 Standard Test Method for Hygienic Chemistry of Cosmetics Mercury
GB/T 7917.2-1987 化妆品卫生化学标准检验方法 砷GB/T 7917.2-1987 Standard Test Method for Hygienic Chemistry of Cosmetics - Arsenic
GB/T 7917.3-1987 化妆品卫生化学标准检验方法 铅GB/T 7917.3-1987 Standard test method for cosmetic hygiene chemical lead
实施例1-3中制得的澳洲坚果基础油理化指标和卫生指标的检测结果如表1所示。The test results of the physical and chemical indexes and hygienic indexes of the macadamia nut base oil prepared in Examples 1-3 are shown in Table 1.
功效成分检测Efficacy component detection
针对实施例1-3中制得的澳洲坚果基础油分别测定油酸、棕榈油酸、亚油酸、角鲨烷含量,具体成分的检测方法如下:The contents of oleic acid, palmitoleic acid, linoleic acid, and squalane were determined for the macadamia nut base oil obtained in Examples 1-3, and the detection method of the specific components was as follows:
脂肪酸的测定采用水解-提取法,试样经水解-乙醚溶液提取其中的脂肪后,在碱性条件下皂化和甲酯化,生成脂肪酸甲酯,经毛细管柱气相色谱分析,面积归一化法定量测定脂肪酸百分含量。The determination of fatty acid adopts hydrolysis-extraction method. After the sample is extracted by hydrolysis-diethyl ether solution, the fat is saponified and methyl esterified under alkaline conditions to generate fatty acid methyl ester, which is analyzed by capillary column gas chromatography and area normalization method. Quantitative determination of the percentage of fatty acids.
角鲨烯的测定参考标准LS/T 6120-2017。The reference standard for the determination of squalene is LS/T 6120-2017.
实施例1-3中制得的澳洲坚果基础油部分功效成分的检测结果如表2所示。The test results of some functional components of the macadamia nut base oil prepared in Examples 1-3 are shown in Table 2.
从表1中可以看出,本发明的制备方法制得的澳洲坚果基础油品质良好、安全,酸值、过氧化值远低于国家标准,并且无铅、砷、汞等重金属有害物质,也没有有害菌,符合化妆品卫生标准;从表2中可以看出,本发明的制备方法制得的澳洲坚果基础油中油酸、棕榈油酸、亚油酸和角鲨烯等功效成分含量丰富且得到很好的保留。As can be seen from Table 1, the macadamia nut base oil obtained by the preparation method of the present invention is of good quality and safety, and its acid value and peroxide value are far lower than the national standard, and it is free of heavy metal harmful substances such as lead, arsenic and mercury, and is also free from harmful substances such as lead, arsenic and mercury. There is no harmful bacteria and meets the cosmetic hygiene standard; as can be seen from Table 2, the functional components such as oleic acid, palmitoleic acid, linoleic acid and squalene in the macadamia nut base oil obtained by the preparation method of the present invention are rich in content and obtained Well reserved.
黏度测定Viscosity determination
对实施例1-3中制得的澳洲坚果基础油测定其黏度,方法如下:使用旋转黏度计测定,选择转子,20℃下,在50mL烧杯中放人约40mL样品,以浸没转子圆盘为标准,测3次取平均值。同时测定市售某品牌山茶润肤油、橄榄油的黏度进行对比参考。黏度测定结果如图2所示。The viscosity of the macadamia nut base oil prepared in Examples 1-3 was measured, and the method was as follows: use a rotational viscometer to measure, select a rotor, put about 40 mL of sample in a 50 mL beaker at 20 ° C, and use the immersed rotor disc as Standard, measured 3 times and averaged. At the same time, the viscosity of a certain brand of camellia emollient oil and olive oil in the market was measured for comparison and reference. The viscosity measurement results are shown in Figure 2.
感官评价Sensory evaluation
选取志愿者共计20人,男女各半,年龄在22~55岁之间,无皮肤病。待洗净双手揩拭干净后,分别在左手背上手背滴0.5mL实施例1-3制备的澳洲坚果基础油,摩擦至皮肤吸收,不涂抹其他化妆品。以颜色、滋润度、吸收性、油腻感和气味为考察指标,感官评分标准见表3所列。A total of 20 volunteers were selected, half male and half, aged between 22 and 55 years old, without skin diseases. After washing hands and wiping clean, drop 0.5 mL of the macadamia nut base oil prepared in Examples 1-3 on the back of the left hand respectively, rub it until the skin absorbs, and do not apply other cosmetics. Taking color, moisture, absorbency, greasy feeling and odor as the inspection indicators, the sensory scoring standards are listed in Table 3.
将实施例1-3制备的澳洲坚果基础油与市售某品牌山茶油、橄榄油进行对比,根据使用感受进行评分,评分结果为五种产品的相对值,非绝对值,感官评价结果如表4所示。The macadamia nut base oil prepared in Example 1-3 was compared with the commercially available camellia oil and olive oil of a certain brand, and the scores were scored according to the experience of use. The scoring results were the relative values of five products, not absolute values, and the sensory evaluation results were as shown in the table. 4 shown.
由图2可以看出,通过黏度计测量实施例1-3制备的澳洲坚果基础油黏度分别为47.8mPa·s、49.6 mPa·s、46.3 mPa·s,黏度均低于市售某品牌山茶油(52.8 mPa·s)和橄榄油(54.2 mPa·s)。由表4可以看出,这几种产品的颜色和气味评分一致,均为透明有光泽、无杂质,并且无刺激性气味酸败味,符合国家化妆品的卫生标准。评分差异较大的是产品的滋润度、吸收性和油腻感。实施例1-3均表现出良好的滋润度和吸收性,志愿者反映涂抹澳洲坚果基础油吸收速度较快,2min后手背皮肤几乎无粘性和油光,但皮肤变得滋润光滑,涂抹24h后,皮肤仍能保持较好的润滑感,未有发干、起皮现象,即表现出良好的保湿特性。油腻感是大多数志愿者比较关注的指标,实施例1-3流动性较好,易铺展,特别是实施例3制备的基础油,不干不涩,流动性最佳,这与黏度计测量的结果是一致的,实施例3的黏度最低。结合功效成分含量测定结果,澳洲坚果基础油中油酸、棕榈油酸含量较高,并且含有角鲨烯等成分,澳洲坚果油不饱和脂肪酸的组成和比例能较好的促进油脂和营养物质的吸收,在肌肤上形成一层天然的保护膜。而且通过冬化处理,使得油中大部分饱和脂肪酸析出,因此不饱和程度很高,其性状如水般,在肌肤上易于流动,可迅速突破皮肤屏障渗入皮下组织。澳洲坚果油的分子结构非常独特,均以小分子团的形式存在,与肌肤具有较好的亲和性与渗透性。As can be seen from Figure 2, the viscosity of the macadamia base oil prepared in Examples 1-3 was measured by viscometer to be 47.8 mPa s, 49.6 mPa s, and 46.3 mPa s, respectively, and the viscosities were lower than those of a certain brand of commercial camellia oil. (52.8 mPa s) and olive oil (54.2 mPa s). As can be seen from Table 4, the color and odor scores of these products are consistent, and they are all transparent and glossy, without impurities, and without irritating odor and rancidity, which meet the national cosmetic hygiene standards. The biggest differences in ratings were the product's moisturization, absorbency and greasy feel. Examples 1-3 all showed good moisturization and absorption. The volunteers reported that the application of macadamia nut base oil absorbed faster, and the skin on the back of the hand was almost non-sticky and shiny after 2 minutes, but the skin became moist and smooth. After 24 hours of application, The skin can still maintain a good lubricating feeling without dryness and peeling, that is, it shows good moisturizing properties. The greasy feeling is an indicator that most volunteers are concerned about. Examples 1-3 have better fluidity and are easy to spread. Especially the base oil prepared in Example 3 is not dry or astringent, and has the best fluidity, which is similar to the viscometer measurement. The results are consistent, Example 3 has the lowest viscosity. Combined with the results of the content determination of functional components, the content of oleic acid and palmitoleic acid in macadamia nut base oil is relatively high, and it contains squalene and other components. The composition and proportion of unsaturated fatty acids in macadamia nut oil can better promote the absorption of oil and nutrients. , forms a natural protective film on the skin. Moreover, through the winterization treatment, most of the saturated fatty acids in the oil are precipitated, so the degree of unsaturation is very high, its properties are like water, it is easy to flow on the skin, and it can quickly penetrate the skin barrier and penetrate into the subcutaneous tissue. The molecular structure of macadamia oil is very unique and exists in the form of small molecular clusters, which has good affinity and permeability with the skin.
采用本发明方法制得的澳洲坚果基础油色泽清透明亮,有淡淡的坚果香气,质地温和不油腻,无刺激性,安全稳定,具有优越的滋润性和肌肤渗透性以及丰富的保湿成分,也可促进其他护肤品营养成分的吸收。可作为按摩基础油,也可作为稀释其他精油的基础油配合使用。这既能满足消费者对澳洲坚果护肤滋养作用的追求又确保产品稳定性,提升产品档次和市场竞争力。The macadamia nut base oil prepared by the method of the invention is clear and bright in color, has a light nut aroma, is mild in texture, non-greasy, non-irritating, safe and stable, has excellent moisturizing properties and skin penetration, and is rich in moisturizing ingredients. It can promote the absorption of other skin care nutrients. Can be used as a base oil for massage or as a base oil for diluting other essential oils. This can not only satisfy consumers' pursuit of macadamia nut skin care and nourishing effect, but also ensure product stability, improve product quality and market competitiveness.
以上所述本发明的具体实施方式,并不构成对本发明保护范围的限定。任何根据本发明的技术构思所作出的各种其他相应的改变与变形,均应包含在本发明权利要求的保护范围内。The specific embodiments of the present invention described above do not limit the protection scope of the present invention. Any other corresponding changes and modifications made according to the technical concept of the present invention shall be included in the protection scope of the claims of the present invention.
Claims (8)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202010240952.6A CN111303987A (en) | 2020-03-31 | 2020-03-31 | A kind of macadamia nut base oil and preparation method thereof |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202010240952.6A CN111303987A (en) | 2020-03-31 | 2020-03-31 | A kind of macadamia nut base oil and preparation method thereof |
Publications (1)
Publication Number | Publication Date |
---|---|
CN111303987A true CN111303987A (en) | 2020-06-19 |
Family
ID=71150340
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN202010240952.6A Pending CN111303987A (en) | 2020-03-31 | 2020-03-31 | A kind of macadamia nut base oil and preparation method thereof |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN111303987A (en) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112206190A (en) * | 2020-10-26 | 2021-01-12 | 云南省热带作物科学研究所 | A kind of high-quality macadamia nut skin cream and preparation method thereof |
CN113416599A (en) * | 2021-06-29 | 2021-09-21 | 广西壮族自治区亚热带作物研究所(广西亚热带农产品加工研究所) | Passion fruit seed oil and preparation method thereof |
CN113413342A (en) * | 2021-06-25 | 2021-09-21 | 西南林业大学 | Method for extracting palmitoleic acid from macadamia nut and application of palmitoleic acid |
CN115678663A (en) * | 2022-11-28 | 2023-02-03 | 合肥工业大学 | A kind of pecan oil and preparation method thereof |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101942356A (en) * | 2010-08-18 | 2011-01-12 | 云南大地石业集团有限公司 | Walnut kernel cold pressing oil production method and walnut kernel cold pressing and cake-making devices specific therefor |
CN106867655A (en) * | 2017-02-08 | 2017-06-20 | 浙江佰帆农业开发有限公司 | A kind of production method of cold pressing Chinese torreya oil |
US20180079991A1 (en) * | 2016-09-22 | 2018-03-22 | Sonoita Pecan Company, LLC | Nut oil separation system and method and products resulting therefrom |
CN108559620A (en) * | 2018-04-09 | 2018-09-21 | 浙江省农业科学院 | A kind of production method of Chinese torreya refined oil |
CN110041993A (en) * | 2019-03-28 | 2019-07-23 | 宋超 | A kind of tiger nut oil extract and its application in cosmetics edible oil |
-
2020
- 2020-03-31 CN CN202010240952.6A patent/CN111303987A/en active Pending
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101942356A (en) * | 2010-08-18 | 2011-01-12 | 云南大地石业集团有限公司 | Walnut kernel cold pressing oil production method and walnut kernel cold pressing and cake-making devices specific therefor |
US20180079991A1 (en) * | 2016-09-22 | 2018-03-22 | Sonoita Pecan Company, LLC | Nut oil separation system and method and products resulting therefrom |
CN106867655A (en) * | 2017-02-08 | 2017-06-20 | 浙江佰帆农业开发有限公司 | A kind of production method of cold pressing Chinese torreya oil |
CN108559620A (en) * | 2018-04-09 | 2018-09-21 | 浙江省农业科学院 | A kind of production method of Chinese torreya refined oil |
CN110041993A (en) * | 2019-03-28 | 2019-07-23 | 宋超 | A kind of tiger nut oil extract and its application in cosmetics edible oil |
Non-Patent Citations (2)
Title |
---|
梁燕理 等: ""澳洲坚果油脂肪酸组成及氧化稳定性分析"", 《粮油食品科技》 * |
郭刚军 等: ""不同压榨方式澳洲坚果油品质及抗氧化活性比较"", 《食品工程》 * |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112206190A (en) * | 2020-10-26 | 2021-01-12 | 云南省热带作物科学研究所 | A kind of high-quality macadamia nut skin cream and preparation method thereof |
CN112206190B (en) * | 2020-10-26 | 2023-03-17 | 云南省热带作物科学研究所 | High-quality macadimia nut skin cream and preparation method thereof |
CN113413342A (en) * | 2021-06-25 | 2021-09-21 | 西南林业大学 | Method for extracting palmitoleic acid from macadamia nut and application of palmitoleic acid |
CN113416599A (en) * | 2021-06-29 | 2021-09-21 | 广西壮族自治区亚热带作物研究所(广西亚热带农产品加工研究所) | Passion fruit seed oil and preparation method thereof |
CN115678663A (en) * | 2022-11-28 | 2023-02-03 | 合肥工业大学 | A kind of pecan oil and preparation method thereof |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN111303987A (en) | A kind of macadamia nut base oil and preparation method thereof | |
CN106109274B (en) | Application of rubber tree seed oil and preparation method thereof | |
US4938984A (en) | Nutritive compositions containing fatty substances | |
CN108743474A (en) | A kind of ointment shape baby's diaper ointment and preparation method thereof | |
CN106085659A (en) | A kind of high skin-moisturizing, skin handmade soap and preparation method thereof | |
JP3635081B2 (en) | Whitening agents, antioxidants, collagenase activity inhibitors, hyaluronidase activity inhibitors, anti-aging agents, external preparations for skin, cosmetics and foods | |
CN104398460B (en) | Skin care product containing winter honey sugar and preparation method of skin care product | |
CN112206190B (en) | High-quality macadimia nut skin cream and preparation method thereof | |
Pandey et al. | Physicochemical evaluation of Prinsepia utilis seed oil (PUSO) and its utilization as a base in pharmaceutical soap formulation | |
CN112877153A (en) | Perfumed soap with moisturizing and sterilizing functions and preparation method thereof | |
CN107502490A (en) | One breeding ass oil soap and preparation method thereof | |
CN104069048A (en) | Lip protector and preparation method thereof | |
WO2016051412A1 (en) | Compositions for reducing acidity | |
JP2013501512A (en) | Method for producing whole olive juice, composition obtained by the method, and use of the composition in cosmetics and nutritional foods | |
CN111631998A (en) | Composition with coconut fragrance and lip moistening effects and preparation method and application thereof | |
CN111773148B (en) | Smooth-peel papaya seed oil cleansing oil and preparation method thereof | |
Ajogun et al. | Comparative Assessment of the Physicochemical Properties and Fatty Acid Profile OF Virgin coconut Oil with Some Commercial Vegetable Oils in Rivers State, Nigeria | |
JP2012039890A (en) | Method for producing olive extracted oil obtained from olive fruit and olive leaf, olive extracted oil produced by the method, and method for reducing grassy smell derived from olive leaf in olive extracted oil obtained from olive fruit and olive leaf | |
JPH0641570A (en) | Grease-like oil and fat composition for food machinery | |
KR20180057906A (en) | Earthworm fermented extracts and method for manuracturing thereof and natural cosmetics and functional health food comprising same | |
CN107550817A (en) | A kind of toilet cream rich in fruits and vegetables and preparation method thereof | |
JP6072202B2 (en) | Defatted seeds | |
CN110478280A (en) | Scrub cream and its manufacturing method | |
CN109699759A (en) | A kind of compound lard and its processing method and application containing rose hip oil | |
US20220023375A1 (en) | Plant based emollient |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
RJ01 | Rejection of invention patent application after publication | ||
RJ01 | Rejection of invention patent application after publication |
Application publication date: 20200619 |