CN111303987A - A kind of macadamia nut base oil and preparation method thereof - Google Patents

A kind of macadamia nut base oil and preparation method thereof Download PDF

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CN111303987A
CN111303987A CN202010240952.6A CN202010240952A CN111303987A CN 111303987 A CN111303987 A CN 111303987A CN 202010240952 A CN202010240952 A CN 202010240952A CN 111303987 A CN111303987 A CN 111303987A
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base oil
macadamia nut
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黄欣欣
艾静汶
罗小杰
任二芳
刘功德
苏艳兰
陈根海
何秀珍
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Guangxi Subtropical Crops Research Institute
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    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
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    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
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    • C11B3/00Refining fats or fatty oils
    • C11B3/16Refining fats or fatty oils by mechanical means

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Abstract

本发明属于日用化工中的护肤品技术领域,具体涉及一种澳洲坚果基础油及其制备方法,包括以下步骤:(1)原料前处理(2)粉碎;(3)低温烘干;(4)冷榨;(5)离心;(6)冬化处理;(7)过滤;(8)成品。本发明采用低温压榨的方法,无添加和溶剂残留,加工全程严格控制温度不高于60℃,最大程度地保留澳洲坚果油的天然营养成分。同时,通过冬化处理,提高坚果基础油的稳定性,有效避免其在存放过程中由于低温有悬浮物质析出的质量问题。采用本发明方法制得的澳洲坚果基础油色泽清透明亮,有坚果香气,质地温和不油腻,无刺激性,安全稳定,具有优越的滋润性和肌肤渗透性以及丰富的保湿成分,也可促进其他护肤品营养成分的吸收。

Figure 202010240952

The invention belongs to the technical field of skin care products in the daily chemical industry, and in particular relates to a macadamia nut base oil and a preparation method thereof, comprising the following steps: (1) raw material pretreatment (2) pulverization; (3) low temperature drying; (4) ) cold pressing; (5) centrifugation; (6) winterization treatment; (7) filtration; (8) finished product. The invention adopts the method of low-temperature pressing, without addition and solvent residue, and strictly controls the temperature not higher than 60 DEG C in the whole process of processing, so as to retain the natural nutritional components of the macadamia nut oil to the greatest extent. At the same time, through the winterization treatment, the stability of the nut base oil is improved, and the quality problem of the precipitation of suspended substances due to low temperature during the storage process is effectively avoided. The macadamia nut base oil prepared by the method of the invention is clear and transparent in color, has nutty aroma, mild texture, non-greasy, non-irritating, safe and stable, has superior moisturizing and skin penetration, and is rich in moisturizing ingredients, and can also promote Absorption of nutrients from other skin care products.

Figure 202010240952

Description

一种澳洲坚果基础油及其制备方法A kind of macadamia nut base oil and preparation method thereof

技术领域technical field

本发明属于日用化工中的护肤品技术领域,具体涉及一种澳洲坚果基础油及其制备方法。The invention belongs to the technical field of skin care products in daily chemical industry, and particularly relates to a macadamia nut base oil and a preparation method thereof.

背景技术Background technique

基础油(base oil或是carrier oil),也有人称之为媒介油或是基底油,是从植物的种子、花朵、根茎或果实中萃取的非挥发性油脂。基础油一般性质温和,可润滑肌肤,能直接用于肌肤按摩,也是稀释精油的最佳基底油。常见的有橄榄油、荷荷巴油、甜杏仁油、葡萄籽油、鳄梨油等。单方精油无法直接抹在皮肤上(除薰衣草和茶树可以用棉签小面积点涂外),它们必须在基础油中稀释后,才可以广泛地用在我们人体的肌肤上。很多基础油本身就具有医疗的效果,通过冷压萃取可以将植物中的矿物质、维生素、脂肪酸,保存良好不流失,具有优越的滋润滋养特质。Base oil (base oil or carrier oil), also known as medium oil or carrier oil, is a non-volatile oil extracted from the seeds, flowers, roots or fruits of plants. The base oil is generally mild in nature, can lubricate the skin, can be used directly for skin massage, and is also the best base oil for diluting essential oils. Common ones are olive oil, jojoba oil, sweet almond oil, grapeseed oil, avocado oil, etc. Single essential oils cannot be applied directly to the skin (except for lavender and tea tree, which can be applied to a small area with a cotton swab), they must be diluted in a base oil before they can be widely used on our human skin. Many base oils themselves have medical effects. Through cold-pressed extraction, minerals, vitamins, and fatty acids in plants can be well preserved and not lost, with superior moisturizing and nourishing properties.

澳洲坚果(拉丁学名:Macadamia ternifolia F. Muell.)又名昆士兰栗、夏威夷果、巴布果、澳洲胡桃等,其营养成分非常丰富,含油量高达60-80%。澳洲坚果油中不含胆固醇,饱和脂肪酸含量低,单不饱和脂肪酸含量超过80%,主要是由油酸、棕榈油酸和少量的亚油酸等多不饱和脂肪酸组成。澳洲坚果油中油酸含量高达58%-65%,棕榈油酸含量高达12-15%。实验表明,澳洲坚果的透皮强度和透皮深度优于山茶油,油酸及棕榈油酸的累积渗透量较高,渗透速率较快。澳洲坚果油中不仅不饱和脂肪酸含量丰富,其甾醇含量也非常丰富,因此其对羟自由基、DPPH自由基以及超氧阴离子自由基的清除能力较好,氧化诱导期与橄榄油相比更长,因此其具有良好的抗氧化能力。Macadamia nuts (Latin name: Macadamia ternifolia F. Muell.), also known as Queensland chestnuts, macadamia nuts, baboon nuts, macadamia nuts, etc., are very rich in nutrients, with an oil content of 60-80%. Macadamia nut oil contains no cholesterol, low saturated fatty acid content, and monounsaturated fatty acid content of more than 80%, mainly composed of polyunsaturated fatty acids such as oleic acid, palmitoleic acid and a small amount of linoleic acid. The content of oleic acid in macadamia oil is as high as 58%-65%, and the content of palmitoleic acid is as high as 12-15%. Experiments show that the penetration strength and penetration depth of macadamia nuts are better than those of camellia oil, the cumulative penetration of oleic acid and palmitoleic acid is higher, and the penetration rate is faster. Macadamia nut oil is not only rich in unsaturated fatty acids, but also rich in sterols, so its scavenging ability to hydroxyl radicals, DPPH radicals and superoxide anion radicals is better, and the oxidation induction period is longer than that of olive oil. , so it has good antioxidant capacity.

总的来说,澳洲坚果油不饱和脂肪酸的组成和比例能较好的促进油脂和营养物质的吸收,在肌肤上形成一层天然的保护膜。不饱和程度很高,其性状如水般,在肌肤上易于流动,可迅速突破皮肤屏障渗入皮下组织。澳洲坚果油的分子结构非常独特,均以小分子团的形式存在,与肌肤具有较好的亲和性与渗透性。此外,分子团里面包埋这天然抗氧化物质如维生素E、甾醇等,能有效对抗自由基,防止皮肤衰老。由于坚果油最大的特点是其与皮肤良好的相容性及亲和性,这是其它大部分植物油无法比拟的,因此非常适宜用作高档化妆品油性原料、按摩基础油、稀释单方精油等。In general, the composition and proportion of unsaturated fatty acids in macadamia oil can better promote the absorption of oils and nutrients, and form a natural protective film on the skin. It has a high degree of unsaturation, and its properties are water-like, easy to flow on the skin, and can quickly penetrate the skin barrier and penetrate into the subcutaneous tissue. The molecular structure of macadamia oil is very unique and exists in the form of small molecular clusters, which has good affinity and permeability with the skin. In addition, the natural antioxidants such as vitamin E and sterols are embedded in the molecular mass, which can effectively fight free radicals and prevent skin aging. Because the biggest feature of argan oil is its good compatibility and affinity with the skin, which is unmatched by most other vegetable oils, so it is very suitable for use as oily raw materials for high-end cosmetics, massage base oils, and diluted unilateral essential oils.

目前市场上澳洲坚果基础油类产品存在诸多问题,一是部分产品以热压榨法制得,焦香味浓郁,颜色深黄,有效成分受到破坏,感官不佳不适宜直接涂抹;另一部分产品虽经冷压榨法制得,但未经冬化处理,产品放置时间长,特别是冬季易出现悬浮物,且由于含有少量饱和脂肪酸,质地黏腻,影响使用感受。因此,目前急需开发一种提取方法简单,成本低,且质地温和清爽,稳定性高的坚果基础油产品,这既能满足消费者对澳洲坚果护肤滋养作用的追求又确保产品稳定性。At present, there are many problems with macadamia nut base oil products on the market. One is that some products are made by hot pressing method, which has a strong coke fragrance, dark yellow color, and damaged active ingredients, which are not suitable for direct application due to poor sensory perception. It is prepared by pressing method, but without winterization treatment, the product is stored for a long time, especially in winter, suspended solids are prone to appear, and because it contains a small amount of saturated fatty acid, the texture is sticky, which affects the feeling of use. Therefore, there is an urgent need to develop a nut base oil product with a simple extraction method, low cost, mild and refreshing texture, and high stability, which can not only satisfy consumers' pursuit of macadamia nut skin care and nourishment, but also ensure product stability.

发明内容SUMMARY OF THE INVENTION

本发明的目的是针对现有澳洲坚果基础油产品感官不佳、质地黏腻、稳定性差等问题,提供一种澳洲坚果基础油及其制备方法。采用本发明方法制得的澳洲坚果基础油色泽清透明亮,有淡淡的坚果香气,质地温和不油腻,无刺激性,安全稳定,具有优越的滋润性和肌肤渗透性以及丰富的保湿成分,也可促进其他护肤品营养成分的吸收;可作为按摩基础油,也可作为稀释其他精油的基础油配合使用。The purpose of the present invention is to provide a macadamia nut base oil and a preparation method thereof for the problems of poor sensory perception, sticky texture and poor stability of the existing macadamia nut base oil products. The macadamia nut base oil prepared by the method of the invention is clear and bright in color, has a light nut aroma, is mild in texture, non-greasy, non-irritating, safe and stable, has excellent moisturizing properties and skin penetration, and is rich in moisturizing ingredients. It can promote the absorption of nutrients in other skin care products; it can be used as a base oil for massage or as a base oil for diluting other essential oils.

为实现上述目的,本发明采用如下技术方案:To achieve the above object, the present invention adopts the following technical solutions:

一方面,本发明提供一种浓澳洲坚果油的制备方法,该制备方法包括如下步骤:On the one hand, the present invention provides a kind of preparation method of concentrated macadamia nut oil, and this preparation method comprises the steps:

(1)原料前处理:选用新鲜采摘、外表无损坏的澳洲坚果作为原料,脱去外层青皮,利用坚果去壳器去除坚果硬壳,剔除发黑、虫蛀及霉烂的果仁;(1) Pre-processing of raw materials: Select freshly picked macadamia nuts with no damage to the appearance as raw materials, remove the outer green skin, use a nut sheller to remove the hard shell of the nuts, and remove the black, moth-eaten and moldy nuts;

(2)粉碎:将脱皮去壳后的果仁进行粉碎处理,得到大小均一的物料;(2) Pulverization: pulverize the peeled and dehulled nuts to obtain materials of uniform size;

(3)低温烘干:将粉碎后的物料送入烘房进行烘干处理,设定干燥温度和时间,最终得到重量含水量≤1.8%的物料;(3) Low-temperature drying: send the pulverized materials to the drying room for drying treatment, set the drying temperature and time, and finally obtain materials with a weight moisture content of ≤1.8%;

(4)冷榨:经低温干燥后的物料送入螺旋压榨机压榨;(4) Cold pressing: the material dried at low temperature is sent to the screw press for pressing;

(5)离心:将压榨得到的油脂混合物送入离心机离心,取上层清油;(5) Centrifugation: the oil mixture obtained by pressing is sent to a centrifuge for centrifugation, and the supernatant oil is taken;

(6)冬化处理:将上层清油置于50℃恒温水浴并不断搅拌,一定时间后将样品转移至冰水浴中降温,缓慢搅拌,待样品冷却至10℃,停止搅拌,放入设定温度的冰箱中,冷却结晶;(6) Winterization treatment: put the supernatant oil in a constant temperature water bath at 50°C and keep stirring. After a certain period of time, transfer the sample to an ice-water bath to cool down and stir slowly. When the sample is cooled to 10°C, stop stirring and put it into the set temperature. in the refrigerator, cooling to crystallize;

(7)过滤:过滤掉样品中析出的悬浮物,恢复至室温,得到成品。(7) Filtration: filter out the suspended matter precipitated in the sample, return to room temperature, and obtain the finished product.

上述的澳洲坚果基础油的制备方法,所述步骤(1)中原料澳洲坚果果仁的重量含水量为12-16%,脂肪含量70-73g/100g,酸价0.15-0.2mgKOH/g,过氧化值0.01-0.016g/100g,油酸含量40-43g/100g,棕榈油酸含量10-12g/100g,要求果仁饱满完整、无瘪仁、无霉变,出仁率为13-15%。要经过严格精选,通过人工或色选机等方式,分离发黑、虫蛀及霉烂的果仁,因为原料未成熟或被微生物侵蚀,易导致澳洲坚果油中酸值升高,有害成分增加,影响成品质量。The preparation method of the above-mentioned macadamia base oil, in the step (1), the weight water content of the raw macadamia nuts is 12-16%, the fat content is 70-73g/100g, the acid value is 0.15-0.2mgKOH/g, The oxidation value is 0.01-0.016g/100g, the oleic acid content is 40-43g/100g, and the palmitoleic acid content is 10-12g/100g. . After strict selection, the blackened, moth-eaten and moldy nuts must be separated manually or by color sorters. Because the raw materials are immature or eroded by microorganisms, it is easy to lead to an increase in the acid value of macadamia nut oil and an increase in harmful components. , affecting the quality of the finished product.

上述的澳洲坚果基础油的制备方法,所述步骤(2)中将果仁粉碎至直径为0.3-0.5cm的完整颗粒。由于干燥温度较低,颗粒过大易导致干燥不彻底,水分分布不均匀,颗粒过小易压榨过程机械力不足,影响出油率。因此,将果仁粉碎至0.4cm左右大小十分必要。In the above-mentioned preparation method of macadamia base oil, in the step (2), the nuts are pulverized to complete particles with a diameter of 0.3-0.5 cm. Due to the low drying temperature, too large particles can easily lead to incomplete drying and uneven distribution of moisture. If the particles are too small, the mechanical force during the pressing process will be insufficient, which will affect the oil yield. Therefore, it is necessary to pulverize the nuts to a size of about 0.4 cm.

上述的洲坚果基础油的制备方法,步骤(3)中采用低温干燥处理,具体为:平铺厚度小于0.5cm,45℃下烘干48-56h,直至重量含水量≤1.8%。干燥的温度必须严格控制,全程采用低温(45℃左右)处理,由于温度较低,因此干燥的时间延长,干燥的结束点必须控制好,测量原料的重量含水量低于1.8%时,干燥才完全结束。若干燥不彻底,物料表面与内部水分分布不均,易导致送入螺旋压榨机后由于含水量过高,物料质地仍紧密,水分和油脂难以分离,压榨无法获得油脂,形成粉末状的坚果碎粉。平铺的厚度必须小于0.5cm,并且干燥过程中每隔一定时间翻面,保证干燥达到彻底。In the above-mentioned preparation method of nut base oil, low temperature drying treatment is adopted in step (3), specifically: the thickness of the tile is less than 0.5cm, and drying is carried out at 45°C for 48-56 hours until the weight water content is less than or equal to 1.8%. The drying temperature must be strictly controlled, and the whole process is treated at low temperature (about 45°C). Due to the low temperature, the drying time is prolonged, and the drying end point must be well controlled. When the weight moisture content of the measured raw material is less than 1.8%, drying can be performed. Completely over. If the drying is not complete, the moisture distribution on the surface and the interior of the material will be uneven, which will easily lead to the high moisture content of the material after being sent to the screw press. The texture of the material is still tight, and the moisture and oil are difficult to separate. pink. The thickness of the tile must be less than 0.5cm, and it must be turned over at regular intervals during the drying process to ensure complete drying.

上述的澳洲坚果基础油的制备方法,所述步骤(4)中螺旋压榨机无需预热,进料量50g/min,收集油脂混合物。要注意的是,虽然螺旋压榨机未预热,但在压榨过程中,由于物料与螺旋轴的摩擦易导致温度升高,因此要随时注意观察,当压榨温度升高达到60℃左右,要暂时停止加料,当内部温度降低后再继续加料压榨。In the above-mentioned preparation method of macadamia base oil, in the step (4), the screw press does not need to be preheated, the feed rate is 50 g/min, and the oil mixture is collected. It should be noted that although the screw press is not preheated, during the pressing process, due to the friction between the material and the screw shaft, the temperature is likely to rise, so pay attention to observe at any time. When the pressing temperature rises to about 60 °C, it will be temporarily Stop feeding and continue feeding and pressing when the internal temperature drops.

上述的澳洲坚果基础油的制备方法,所述步骤(5)中离心机转速为4000r/min,离心时间为25-30min。由于物料是经过低温压榨,油相和非油相并未很好的分离,油脂混合物质地粘稠,浑浊,因此离心时间需要适当延长,设定为25-30min,能够很好的分离固液两相,去除油渣得到上层油相样品。In the above-mentioned preparation method of macadamia base oil, in the step (5), the rotating speed of the centrifuge is 4000r/min, and the centrifugation time is 25-30min. Because the material is pressed at low temperature, the oil phase and non-oil phase are not well separated, and the oil mixture is viscous and turbid, so the centrifugation time needs to be appropriately extended, set to 25-30min, which can well separate the solid-liquid two. phase, remove the oil residue to obtain the upper oil phase sample.

上述的澳洲坚果基础油的制备方法,所述步骤(6)中,50℃恒温水浴时间30-40min,冰箱中于4℃下静置24-28h,静置过程中密封。冬化处理指通过将油脂混合物置于低温环境中处理一定时间,油脂中的饱和脂肪酸易析出,从而实现液体油与固体脂的分离。先升温至50℃是为了使固体脂充分溶于油中,若直接进行冬化处理会影响固体脂的析出效果。在4-10℃条件下,随着温度降低,固体脂析出越多,但当温度在2℃时,接近三油酸甘油酯的熔点,油脂中的固体脂和液体油的分离不太容易,因此选择冬化温度为4℃。当冬化时间较短时,冬化不彻底,部分饱和脂肪酸和蜡质未完全析出,当冬化时间增加到24-28h时,结晶较多,且当冬化时间>28h时,结晶量增加已不明显,出于节约能源考虑,4℃处理时间为24-28h。冷却过程中不断搅拌是为了增加析出晶粒之间的碰撞机会,有利于固体脂的析出。In the above-mentioned preparation method of macadamia nut base oil, in the step (6), a constant temperature water bath time of 30-40min at 50°C is placed in a refrigerator at 4°C for 24-28h, and sealed during the standing process. Winterization treatment means that by placing the oil mixture in a low temperature environment for a certain period of time, the saturated fatty acids in the oil are easily precipitated, thereby realizing the separation of liquid oil and solid fat. The purpose of raising the temperature to 50°C is to fully dissolve the solid fat in the oil. If the winterization treatment is carried out directly, the precipitation effect of the solid fat will be affected. Under the condition of 4-10 °C, as the temperature decreases, the more solid fat is precipitated, but when the temperature is at 2 °C, it is close to the melting point of triolein, and the separation of solid fat and liquid oil in oil is not easy. Therefore, the winterization temperature was chosen to be 4°C. When the winterization time is short, the winterization is incomplete, and some saturated fatty acids and waxes are not completely precipitated. When the winterization time increases to 24-28h, the crystallization is more, and when the winterization time is greater than 28h, the amount of crystallization increases. It is not obvious. For the sake of energy saving, the treatment time at 4°C is 24-28h. The continuous stirring during the cooling process is to increase the chance of collision between the precipitated grains, which is beneficial to the precipitation of solid fat.

另一方面,本发明提供一种澳洲坚果基础油,该澳洲坚果基础油通过上述澳洲坚果基础油的制备方法制得。In another aspect, the present invention provides a macadamia nut base oil prepared by the above-mentioned preparation method of a macadamia nut base oil.

本发明的有益效果为:The beneficial effects of the present invention are:

目前市场上澳洲坚果基础油类产品存在诸多问题,一是部分产品以热压榨法制得,焦香味浓郁,颜色深黄,有效成分受到破坏,感官不佳不适宜直接涂抹;另一部分产品虽经冷压榨法制得,但未经冬化处理,产品放置时间长,特别是冬季易出现悬浮物,且由于含有少量饱和脂肪酸,质地黏腻,影响使用感受,影响产品档次和竞争力。At present, there are many problems with macadamia nut base oil products on the market. One is that some products are made by hot pressing method, which has a strong coke fragrance, dark yellow color, and damaged active ingredients, which are not suitable for direct application due to poor sensory perception. It is prepared by pressing method, but without winterization treatment, the product is stored for a long time, especially in winter, suspended solids are prone to occur, and because it contains a small amount of saturated fatty acid, the texture is sticky, which affects the feeling of use, and affects the grade and competitiveness of the product.

针对上述问题,一方面,本发明采用新鲜澳洲坚果低温压榨的方法,无添加和溶剂残留,加工全程严格控制温度不高于60℃,最大程度地保留澳洲坚果油的天然营养成分,富含多种不饱和脂肪酸、氨基酸、矿物质等。同时,通过冬化处理,提高坚果基础油的稳定性,有效避免其在存放过程中由于低温有悬浮物质析出的质量问题。另一方面,采用本发明方法制得的澳洲坚果基础油色泽清透明亮,有淡淡的坚果香气,质地温和不油腻,无刺激性,安全稳定,具有优越的滋润性和肌肤渗透性以及丰富的保湿成分,也可促进其他护肤品营养成分的吸收。可作为按摩基础油,也可作为稀释其他精油的基础油配合使用。In view of the above problems, on the one hand, the present invention adopts the method of low-temperature pressing of fresh macadamia nuts, without addition and solvent residues, and the temperature is strictly controlled not to be higher than 60°C in the whole process of processing, so as to retain the natural nutrients of macadamia nut oil to the greatest extent, and is rich in more unsaturated fatty acids, amino acids, minerals, etc. At the same time, through the winterization treatment, the stability of the nut base oil is improved, and the quality problem of the precipitation of suspended substances due to low temperature during the storage process is effectively avoided. On the other hand, the macadamia nut base oil prepared by the method of the present invention is clear and bright in color, has a light nut aroma, mild texture, non-greasy, non-irritating, safe and stable, and has excellent moisturizing and skin permeability and rich Moisturizing ingredients, can also promote the absorption of other skin care products nutrients. Can be used as a base oil for massage or as a base oil for diluting other essential oils.

附图说明Description of drawings

图1为本发明澳洲坚果基础油的制备方法的制备工艺路线图;Fig. 1 is the preparation process route diagram of the preparation method of macadamia base oil of the present invention;

图2 为本发明实施例1-3制备得到的澳洲坚果基础油与市售山茶油、橄榄油的黏度对比图。Figure 2 is a viscosity comparison diagram of the macadamia nut base oil prepared in Examples 1-3 of the present invention, and commercially available camellia oil and olive oil.

具体实施方式Detailed ways

为了使本发明的目的、技术方案及优点更加清楚明白,以下结合具体实施例,对本发明进行进一步详细说明。应当理解,此处所描述的具体实施例仅用以解释本发明,并不用于限定本发明。In order to make the objectives, technical solutions and advantages of the present invention clearer, the present invention will be further described in detail below with reference to specific embodiments. It should be understood that the specific embodiments described herein are only used to explain the present invention, but not to limit the present invention.

一种澳洲坚果基础油的制备方法,包括如下步骤:A preparation method of macadamia nut base oil, comprising the following steps:

(1)原料前处理:选用新鲜采摘、外表无损坏的澳洲坚果作为原料,脱去外层青皮,利用坚果去壳器去除坚果硬壳,剔除发黑、虫蛀及霉烂的果仁;所述的原料澳洲坚果果仁的重量含水量为12-16%,脂肪含量70-73g/100g,酸价0.15-0.2mgKOH/g,过氧化值0.01-0.016g/100g,油酸含量40-43g/100g,棕榈油酸含量10-12g/100g,要求果仁饱满完整、无瘪仁、无霉变,出仁率为13-15%;(1) Pretreatment of raw materials: choose freshly picked macadamia nuts with no damage to the appearance as raw materials, remove the outer green skin, use a nut sheller to remove the hard shell of the nuts, and remove the black, moth-eaten and moldy nuts; The raw macadamia nuts have a weight water content of 12-16%, a fat content of 70-73g/100g, an acid value of 0.15-0.2mgKOH/g, a peroxide value of 0.01-0.016g/100g, and an oleic acid content of 40-43g/g. 100g, the palmitoleic acid content is 10-12g/100g, the kernels are required to be full and complete, no shriveled kernels, no mildew, and the kernel rate is 13-15%;

(2)粉碎:将脱皮去壳后的果仁进行粉碎处理,粉碎至直径为0.3-0.5cm的完整颗粒,得到大小均一的物料;(2) Pulverization: The peeled and dehulled nuts are pulverized to complete particles with a diameter of 0.3-0.5 cm to obtain materials of uniform size;

(3)低温烘干:将粉碎后的物料送入烘房进行烘干处理,设定干燥温度和时间,最终得到重量含水量≤1.8%的物料;具体为:平铺厚度小于0.5cm,45℃下烘干48-56h,直至重量含水量≤1.8%;(3) Low-temperature drying: send the pulverized materials to the drying room for drying treatment, set the drying temperature and time, and finally obtain materials with a weight moisture content of ≤1.8%; specifically: the tile thickness is less than 0.5cm, 45 Dry at ℃ for 48-56h until the water content by weight is less than or equal to 1.8%;

(4)冷榨:经低温干燥后的物料送入螺旋压榨机压榨;螺旋压榨机无需预热,进料量50g/min,收集油脂混合物;过程中随时观察压榨温度,若温度升高,停止压榨,待温度下降至<60℃,继续压榨;(4) Cold pressing: the material dried at low temperature is sent to the screw press for pressing; the screw press does not need to be preheated, the feed rate is 50g/min, and the oil mixture is collected; the pressing temperature is observed at any time during the process, and if the temperature rises, stop Press, and continue pressing when the temperature drops to <60°C;

(5)离心:将压榨得到的油脂混合物送入离心机离心,离心机转速为4000r/min,离心时间为25-30min,取上层清油;(5) Centrifugation: send the oil mixture obtained by pressing into a centrifuge for centrifugation, the centrifuge speed is 4000r/min, the centrifugation time is 25-30min, and the supernatant oil is taken;

(6)冬化处理:将上层清油置于50℃恒温水浴并不断搅拌,30-40min后将样品转移至冰水浴中降温;待样品冷却至10℃,放入4℃冰箱中静置24-28h冷却结晶,静置过程中密封;(6) Winterization treatment: put the supernatant oil in a constant temperature water bath at 50°C and keep stirring. After 30-40min, transfer the sample to an ice-water bath to cool down; when the sample is cooled to 10°C, put it in a 4°C refrigerator and let it stand for 24-40 minutes. 28h cooling and crystallization, and sealing during standing;

(7)过滤:过滤掉样品中析出的悬浮物,恢复至室温,得到成品。(7) Filtration: filter out the suspended matter precipitated in the sample, return to room temperature, and obtain the finished product.

以下结合具体实施例进一步说明。The following is further described in conjunction with specific embodiments.

实施例1Example 1

一种澳洲坚果基础油的制备方法,包括如下步骤:A preparation method of macadamia nut base oil, comprising the following steps:

(1)原料前处理:选用新鲜采摘、外表无损坏的澳洲坚果作为原料,脱去外层青皮,利用坚果去壳器去除坚果硬壳,剔除发黑、虫蛀及霉烂的果仁;果仁的重量含水量为14.2%,脂肪含量71.2g/100g,酸价0.17mgKOH/g,过氧化值0.012g/100g,油酸含量40.1g/100g,棕榈油酸含量10.3g/100g,要求果仁饱满完整、无瘪仁、无霉变,出仁率为13.8%;(1) Pretreatment of raw materials: Select freshly picked macadamia nuts with no damage to the appearance as raw materials, remove the outer green skin, use a nut sheller to remove the hard shell of the nuts, and remove the black, moth-eaten and moldy nuts; The weight of the water content is 14.2%, the fat content is 71.2g/100g, the acid value is 0.17mgKOH/g, the peroxide value is 0.012g/100g, the oleic acid content is 40.1g/100g, and the palmitoleic acid content is 10.3g/100g. Full and complete, no shriveled kernels, no mildew, the kernel rate is 13.8%;

(2)粉碎:将脱皮去壳后的果仁进行粉碎处理,粉碎至直径为0.3-0.5cm的完整颗粒,得到大小均一的物料;(2) Pulverization: The peeled and dehulled nuts are pulverized to complete particles with a diameter of 0.3-0.5 cm to obtain materials of uniform size;

(3)低温烘干:将粉碎后的物料送入烘房进行烘干处理,平铺的厚度小于0.5cm,45℃干燥52h,干燥过程中每隔一定时间翻面,保证干燥达到彻底,最终得到重量含水量1.71%的物料;(3) Low-temperature drying: The pulverized material is sent to the drying room for drying treatment. The thickness of the tile is less than 0.5cm, and it is dried at 45 °C for 52 hours. During the drying process, it is turned over at regular intervals to ensure complete drying. A material with a water content of 1.71% by weight was obtained;

(4)冷榨:经低温干燥后的物料送入螺旋压榨机压榨;螺旋压榨机无需预热,进料量50g/min,收集油脂混合物;过程中随时观察压榨温度,若温度升高,停止压榨,待温度下降至<60℃,继续压榨;(4) Cold pressing: the material dried at low temperature is sent to the screw press for pressing; the screw press does not need to be preheated, the feed rate is 50g/min, and the oil mixture is collected; the pressing temperature is observed at any time during the process, and if the temperature rises, stop Press, and continue pressing when the temperature drops to <60°C;

(5)离心:将压榨得到的油脂混合物送入离心机离心,离心机转速为4000r/min,离心时间为30min,取上层清油;(5) Centrifugation: send the oil mixture obtained by pressing into a centrifuge for centrifugation, the centrifuge speed is 4000r/min, the centrifugation time is 30min, and the supernatant oil is taken;

(6)冬化处理:将上层清油置于50℃恒温水浴并不断搅拌,30min后将样品转移至冰水浴中降温,待样品冷却至10℃,放入4℃冰箱中静置25h冷却结晶,静置过程中密封;(6) Winterization treatment: put the supernatant oil in a 50°C constant temperature water bath and keep stirring. After 30 minutes, transfer the sample to an ice-water bath to cool down. When the sample is cooled to 10°C, put it in a 4°C refrigerator for 25 hours to cool and crystallize. Sealed during standing;

(7)过滤:过滤掉样品中析出的悬浮物,恢复至室温,得到成品。(7) Filtration: filter out the suspended matter precipitated in the sample, return to room temperature, and obtain the finished product.

实施例2Example 2

一种澳洲坚果基础油的制备方法,包括如下步骤:A preparation method of macadamia nut base oil, comprising the following steps:

(1)原料前处理:选用新鲜采摘、外表无损坏的澳洲坚果作为原料,脱去外层青皮,利用坚果去壳器去除坚果硬壳,剔除发黑、虫蛀及霉烂的果仁;果仁的重量含水量为12.5%,脂肪含量72.4g/100g,酸价0.2mgKOH/g,过氧化值0.016g/100g,油酸含量43.0g/100g,棕榈油酸含量10.6g/100g,要求果仁饱满完整、无瘪仁、无霉变,出仁率为14.7%;(1) Pretreatment of raw materials: Select freshly picked macadamia nuts with no damage to the appearance as raw materials, remove the outer green skin, use a nut sheller to remove the hard shell of the nuts, and remove the black, moth-eaten and moldy nuts; The weight of the water content is 12.5%, the fat content is 72.4g/100g, the acid value is 0.2mgKOH/g, the peroxide value is 0.016g/100g, the oleic acid content is 43.0g/100g, and the palmitoleic acid content is 10.6g/100g. Full and complete, no shriveled kernels, no mildew, the kernel rate is 14.7%;

(2)粉碎:将脱皮去壳后的果仁进行粉碎处理,粉碎至直径为0.3-0.5cm的完整颗粒,得到大小均一的物料;(2) Pulverization: The peeled and dehulled nuts are pulverized to complete particles with a diameter of 0.3-0.5 cm to obtain materials of uniform size;

(3)低温烘干:将粉碎后的物料送入烘房进行烘干处理,平铺的厚度小于0.5cm,45℃干燥48h,干燥过程中每隔一定时间翻面,保证干燥达到彻底,最终得到重量含水量1.62%的物料;(3) Low-temperature drying: send the pulverized material to the drying room for drying treatment. The thickness of the tile is less than 0.5cm, and it is dried at 45 °C for 48 hours. During the drying process, it is turned over at regular intervals to ensure complete drying. A material with a water content of 1.62% by weight was obtained;

(4)冷榨:经低温干燥后的物料送入螺旋压榨机压榨;螺旋压榨机无需预热,进料量50g/min,收集油脂混合物;过程中随时观察压榨温度,若温度升高,停止压榨,待温度下降至<60℃,继续压榨;(4) Cold pressing: the material dried at low temperature is sent to the screw press for pressing; the screw press does not need to be preheated, the feed rate is 50g/min, and the oil mixture is collected; the pressing temperature is observed at any time during the process, and if the temperature rises, stop Press, and continue pressing when the temperature drops to <60°C;

(5)离心:将压榨得到的油脂混合物送入离心机离心,离心机转速为4000r/min,离心时间为25min,取上层清油;(5) Centrifugation: send the oil mixture obtained by pressing into a centrifuge for centrifugation, the centrifuge speed is 4000r/min, the centrifugation time is 25min, and the supernatant oil is taken;

(6)冬化处理:将上层清油置于50℃恒温水浴并不断搅拌,30min后将样品转移至冰水浴中降温。待样品冷却至10℃,放入4℃冰箱中静置24h冷却结晶,静置过程中密封;(6) Winterization treatment: put the supernatant oil in a constant temperature water bath at 50°C and keep stirring, and transfer the sample to an ice water bath for cooling after 30 min. After the sample is cooled to 10°C, put it in a 4°C refrigerator for 24 hours to cool and crystallize, and seal it during the standing process;

(7)过滤:过滤掉样品中析出的悬浮物,恢复至室温,得到成品。(7) Filtration: filter out the suspended matter precipitated in the sample, return to room temperature, and obtain the finished product.

实施例3Example 3

一种澳洲坚果基础油的制备方法,包括如下步骤:A preparation method of macadamia nut base oil, comprising the following steps:

(1)原料前处理:选用新鲜采摘、外表无损坏的澳洲坚果作为原料,脱去外层青皮,利用坚果去壳器去除坚果硬壳,剔除发黑、虫蛀及霉烂的果仁;果仁的重量含水量为15.1%,脂肪含量70.1g/100g,酸价0.15mgKOH/g,过氧化值0.010g/100g,油酸含量43.0g/100g,棕榈油酸含量10.6g/100g,要求果仁饱满完整、无瘪仁、无霉变,出仁率为13.1%;(1) Pretreatment of raw materials: Select freshly picked macadamia nuts with no damage to the appearance as raw materials, remove the outer green skin, use a nut sheller to remove the hard shell of the nuts, and remove the black, moth-eaten and moldy nuts; The weight of the water content is 15.1%, the fat content is 70.1g/100g, the acid value is 0.15mgKOH/g, the peroxide value is 0.010g/100g, the oleic acid content is 43.0g/100g, and the palmitoleic acid content is 10.6g/100g. Full and complete, no shriveled kernels, no mildew, the kernel rate is 13.1%;

(2)粉碎:将脱皮去壳后的果仁进行粉碎处理,粉碎至直径为0.3-0.5cm的完整颗粒,得到大小均一的物料;(2) Pulverization: The peeled and dehulled nuts are pulverized to complete particles with a diameter of 0.3-0.5 cm to obtain materials of uniform size;

(3)低温烘干:将粉碎后的物料送入烘房进行烘干处理,平铺的厚度小于0.5cm,45℃干燥56h,干燥过程中每隔一定时间翻面,保证干燥达到彻底,最终得到重量含水量1.75%的物料;(3) Low-temperature drying: The pulverized material is sent to the drying room for drying treatment. The thickness of the tile is less than 0.5cm, and it is dried at 45 °C for 56 hours. During the drying process, it is turned over at regular intervals to ensure complete drying. A material with a water content of 1.75% by weight was obtained;

(4)冷榨:经低温干燥后的物料送入螺旋压榨机压榨;螺旋压榨机无需预热,进料量50g/min,收集油脂混合物;过程中随时观察压榨温度,若温度升高,停止压榨,待温度下降至<60℃,继续压榨;(4) Cold pressing: the material dried at low temperature is sent to the screw press for pressing; the screw press does not need to be preheated, the feed rate is 50g/min, and the oil mixture is collected; the pressing temperature is observed at any time during the process, and if the temperature rises, stop Press, and continue pressing when the temperature drops to <60°C;

(5)离心:将压榨得到的油脂混合物送入离心机离心,离心机转速为4000r/min,离心时间为30min,取上层清油;(5) Centrifugation: send the oil mixture obtained by pressing into a centrifuge for centrifugation, the centrifuge speed is 4000r/min, the centrifugation time is 30min, and the supernatant oil is taken;

(6)冬化处理:将上层清油置于50℃恒温水浴并不断搅拌,30min后将样品转移至冰水浴中降温,待样品冷却至10℃,放入4℃冰箱中静置28h冷却结晶,静置过程中密封;(6) Winterization treatment: Put the supernatant oil in a constant temperature water bath at 50°C and keep stirring. After 30 minutes, transfer the sample to an ice-water bath to cool down. After the sample is cooled to 10°C, put it in a 4°C refrigerator for 28 hours to cool and crystallize. Sealed during standing;

(7)过滤:过滤掉样品中析出的悬浮物,恢复至室温,得到成品。(7) Filtration: filter out the suspended matter precipitated in the sample, return to room temperature, and obtain the finished product.

理化指标及卫生指标检测Physical and chemical indicators and health indicators detection

针对实施例1-3中制得的澳洲坚果基础油,分别测定理化指标和卫生指标,具体各指标的检测方法如下:For the macadamia nut base oil prepared in the embodiment 1-3, measure the physicochemical index and the hygienic index respectively, and the detection method of each specific index is as follows:

QBT4079-2010按摩基础油、按摩油QBT4079-2010 Massage base oil, massage oil

GB/T 7917.1-1987 化妆品卫生化学标准检验方法 汞GB/T 7917.1-1987 Standard Test Method for Hygienic Chemistry of Cosmetics Mercury

GB/T 7917.2-1987 化妆品卫生化学标准检验方法 砷GB/T 7917.2-1987 Standard Test Method for Hygienic Chemistry of Cosmetics - Arsenic

GB/T 7917.3-1987 化妆品卫生化学标准检验方法 铅GB/T 7917.3-1987 Standard test method for cosmetic hygiene chemical lead

实施例1-3中制得的澳洲坚果基础油理化指标和卫生指标的检测结果如表1所示。The test results of the physical and chemical indexes and hygienic indexes of the macadamia nut base oil prepared in Examples 1-3 are shown in Table 1.

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Figure 197942DEST_PATH_IMAGE001

功效成分检测Efficacy component detection

针对实施例1-3中制得的澳洲坚果基础油分别测定油酸、棕榈油酸、亚油酸、角鲨烷含量,具体成分的检测方法如下:The contents of oleic acid, palmitoleic acid, linoleic acid, and squalane were determined for the macadamia nut base oil obtained in Examples 1-3, and the detection method of the specific components was as follows:

脂肪酸的测定采用水解-提取法,试样经水解-乙醚溶液提取其中的脂肪后,在碱性条件下皂化和甲酯化,生成脂肪酸甲酯,经毛细管柱气相色谱分析,面积归一化法定量测定脂肪酸百分含量。The determination of fatty acid adopts hydrolysis-extraction method. After the sample is extracted by hydrolysis-diethyl ether solution, the fat is saponified and methyl esterified under alkaline conditions to generate fatty acid methyl ester, which is analyzed by capillary column gas chromatography and area normalization method. Quantitative determination of the percentage of fatty acids.

角鲨烯的测定参考标准LS/T 6120-2017。The reference standard for the determination of squalene is LS/T 6120-2017.

实施例1-3中制得的澳洲坚果基础油部分功效成分的检测结果如表2所示。The test results of some functional components of the macadamia nut base oil prepared in Examples 1-3 are shown in Table 2.

Figure 921047DEST_PATH_IMAGE002
Figure 921047DEST_PATH_IMAGE002

从表1中可以看出,本发明的制备方法制得的澳洲坚果基础油品质良好、安全,酸值、过氧化值远低于国家标准,并且无铅、砷、汞等重金属有害物质,也没有有害菌,符合化妆品卫生标准;从表2中可以看出,本发明的制备方法制得的澳洲坚果基础油中油酸、棕榈油酸、亚油酸和角鲨烯等功效成分含量丰富且得到很好的保留。As can be seen from Table 1, the macadamia nut base oil obtained by the preparation method of the present invention is of good quality and safety, and its acid value and peroxide value are far lower than the national standard, and it is free of heavy metal harmful substances such as lead, arsenic and mercury, and is also free from harmful substances such as lead, arsenic and mercury. There is no harmful bacteria and meets the cosmetic hygiene standard; as can be seen from Table 2, the functional components such as oleic acid, palmitoleic acid, linoleic acid and squalene in the macadamia nut base oil obtained by the preparation method of the present invention are rich in content and obtained Well reserved.

黏度测定Viscosity determination

对实施例1-3中制得的澳洲坚果基础油测定其黏度,方法如下:使用旋转黏度计测定,选择转子,20℃下,在50mL烧杯中放人约40mL样品,以浸没转子圆盘为标准,测3次取平均值。同时测定市售某品牌山茶润肤油、橄榄油的黏度进行对比参考。黏度测定结果如图2所示。The viscosity of the macadamia nut base oil prepared in Examples 1-3 was measured, and the method was as follows: use a rotational viscometer to measure, select a rotor, put about 40 mL of sample in a 50 mL beaker at 20 ° C, and use the immersed rotor disc as Standard, measured 3 times and averaged. At the same time, the viscosity of a certain brand of camellia emollient oil and olive oil in the market was measured for comparison and reference. The viscosity measurement results are shown in Figure 2.

感官评价Sensory evaluation

选取志愿者共计20人,男女各半,年龄在22~55岁之间,无皮肤病。待洗净双手揩拭干净后,分别在左手背上手背滴0.5mL实施例1-3制备的澳洲坚果基础油,摩擦至皮肤吸收,不涂抹其他化妆品。以颜色、滋润度、吸收性、油腻感和气味为考察指标,感官评分标准见表3所列。A total of 20 volunteers were selected, half male and half, aged between 22 and 55 years old, without skin diseases. After washing hands and wiping clean, drop 0.5 mL of the macadamia nut base oil prepared in Examples 1-3 on the back of the left hand respectively, rub it until the skin absorbs, and do not apply other cosmetics. Taking color, moisture, absorbency, greasy feeling and odor as the inspection indicators, the sensory scoring standards are listed in Table 3.

Figure 532157DEST_PATH_IMAGE003
Figure 532157DEST_PATH_IMAGE003

将实施例1-3制备的澳洲坚果基础油与市售某品牌山茶油、橄榄油进行对比,根据使用感受进行评分,评分结果为五种产品的相对值,非绝对值,感官评价结果如表4所示。The macadamia nut base oil prepared in Example 1-3 was compared with the commercially available camellia oil and olive oil of a certain brand, and the scores were scored according to the experience of use. The scoring results were the relative values of five products, not absolute values, and the sensory evaluation results were as shown in the table. 4 shown.

Figure 885778DEST_PATH_IMAGE004
Figure 885778DEST_PATH_IMAGE004

由图2可以看出,通过黏度计测量实施例1-3制备的澳洲坚果基础油黏度分别为47.8mPa·s、49.6 mPa·s、46.3 mPa·s,黏度均低于市售某品牌山茶油(52.8 mPa·s)和橄榄油(54.2 mPa·s)。由表4可以看出,这几种产品的颜色和气味评分一致,均为透明有光泽、无杂质,并且无刺激性气味酸败味,符合国家化妆品的卫生标准。评分差异较大的是产品的滋润度、吸收性和油腻感。实施例1-3均表现出良好的滋润度和吸收性,志愿者反映涂抹澳洲坚果基础油吸收速度较快,2min后手背皮肤几乎无粘性和油光,但皮肤变得滋润光滑,涂抹24h后,皮肤仍能保持较好的润滑感,未有发干、起皮现象,即表现出良好的保湿特性。油腻感是大多数志愿者比较关注的指标,实施例1-3流动性较好,易铺展,特别是实施例3制备的基础油,不干不涩,流动性最佳,这与黏度计测量的结果是一致的,实施例3的黏度最低。结合功效成分含量测定结果,澳洲坚果基础油中油酸、棕榈油酸含量较高,并且含有角鲨烯等成分,澳洲坚果油不饱和脂肪酸的组成和比例能较好的促进油脂和营养物质的吸收,在肌肤上形成一层天然的保护膜。而且通过冬化处理,使得油中大部分饱和脂肪酸析出,因此不饱和程度很高,其性状如水般,在肌肤上易于流动,可迅速突破皮肤屏障渗入皮下组织。澳洲坚果油的分子结构非常独特,均以小分子团的形式存在,与肌肤具有较好的亲和性与渗透性。As can be seen from Figure 2, the viscosity of the macadamia base oil prepared in Examples 1-3 was measured by viscometer to be 47.8 mPa s, 49.6 mPa s, and 46.3 mPa s, respectively, and the viscosities were lower than those of a certain brand of commercial camellia oil. (52.8 mPa s) and olive oil (54.2 mPa s). As can be seen from Table 4, the color and odor scores of these products are consistent, and they are all transparent and glossy, without impurities, and without irritating odor and rancidity, which meet the national cosmetic hygiene standards. The biggest differences in ratings were the product's moisturization, absorbency and greasy feel. Examples 1-3 all showed good moisturization and absorption. The volunteers reported that the application of macadamia nut base oil absorbed faster, and the skin on the back of the hand was almost non-sticky and shiny after 2 minutes, but the skin became moist and smooth. After 24 hours of application, The skin can still maintain a good lubricating feeling without dryness and peeling, that is, it shows good moisturizing properties. The greasy feeling is an indicator that most volunteers are concerned about. Examples 1-3 have better fluidity and are easy to spread. Especially the base oil prepared in Example 3 is not dry or astringent, and has the best fluidity, which is similar to the viscometer measurement. The results are consistent, Example 3 has the lowest viscosity. Combined with the results of the content determination of functional components, the content of oleic acid and palmitoleic acid in macadamia nut base oil is relatively high, and it contains squalene and other components. The composition and proportion of unsaturated fatty acids in macadamia nut oil can better promote the absorption of oil and nutrients. , forms a natural protective film on the skin. Moreover, through the winterization treatment, most of the saturated fatty acids in the oil are precipitated, so the degree of unsaturation is very high, its properties are like water, it is easy to flow on the skin, and it can quickly penetrate the skin barrier and penetrate into the subcutaneous tissue. The molecular structure of macadamia oil is very unique and exists in the form of small molecular clusters, which has good affinity and permeability with the skin.

采用本发明方法制得的澳洲坚果基础油色泽清透明亮,有淡淡的坚果香气,质地温和不油腻,无刺激性,安全稳定,具有优越的滋润性和肌肤渗透性以及丰富的保湿成分,也可促进其他护肤品营养成分的吸收。可作为按摩基础油,也可作为稀释其他精油的基础油配合使用。这既能满足消费者对澳洲坚果护肤滋养作用的追求又确保产品稳定性,提升产品档次和市场竞争力。The macadamia nut base oil prepared by the method of the invention is clear and bright in color, has a light nut aroma, is mild in texture, non-greasy, non-irritating, safe and stable, has excellent moisturizing properties and skin penetration, and is rich in moisturizing ingredients. It can promote the absorption of other skin care nutrients. Can be used as a base oil for massage or as a base oil for diluting other essential oils. This can not only satisfy consumers' pursuit of macadamia nut skin care and nourishing effect, but also ensure product stability, improve product quality and market competitiveness.

以上所述本发明的具体实施方式,并不构成对本发明保护范围的限定。任何根据本发明的技术构思所作出的各种其他相应的改变与变形,均应包含在本发明权利要求的保护范围内。The specific embodiments of the present invention described above do not limit the protection scope of the present invention. Any other corresponding changes and modifications made according to the technical concept of the present invention shall be included in the protection scope of the claims of the present invention.

Claims (8)

1.一种澳洲坚果基础油的制备方法,其特征在于,包括如下步骤:1. a preparation method of macadamia base oil, is characterized in that, comprises the steps: (1)原料前处理:选用新鲜采摘、外表无损坏的澳洲坚果作为原料,脱去外层青皮,利用坚果去壳器去除坚果硬壳,剔除发黑、虫蛀及霉烂的果仁;(1) Pre-processing of raw materials: Select freshly picked macadamia nuts with no damage to the appearance as raw materials, remove the outer green skin, use a nut sheller to remove the hard shell of the nuts, and remove the black, moth-eaten and moldy nuts; (2)粉碎:将脱皮去壳后的果仁进行粉碎处理,得到大小均一的物料;(2) Pulverization: pulverize the peeled and dehulled nuts to obtain materials of uniform size; (3)低温烘干:将粉碎后的物料送入烘房进行烘干处理,设定干燥温度和时间,最终得到重量含水量≤1.8%的物料;(3) Low-temperature drying: send the pulverized materials to the drying room for drying treatment, set the drying temperature and time, and finally obtain materials with a weight moisture content of ≤1.8%; (4)冷榨:经低温干燥后的物料送入螺旋压榨机压榨;(4) Cold pressing: the material dried at low temperature is sent to the screw press for pressing; (5)离心:将压榨得到的油脂混合物送入离心机离心,取上层清油;(5) Centrifugation: the oil mixture obtained by pressing is sent to a centrifuge for centrifugation, and the supernatant oil is taken; (6)冬化处理:将上层清油置于50℃恒温水浴并不断搅拌,一定时间后将样品转移至冰水浴中降温,缓慢搅拌,待样品冷却至10℃,停止搅拌,放入设定温度的冰箱中,冷却结晶;(6) Winterization treatment: put the supernatant oil in a constant temperature water bath at 50°C and keep stirring. After a certain period of time, transfer the sample to an ice-water bath to cool down and stir slowly. When the sample is cooled to 10°C, stop stirring and put it into the set temperature. In the refrigerator, cool and crystallize; (7)过滤:过滤掉样品中析出的悬浮物,恢复至室温,得到成品。(7) Filtration: filter out the suspended matter precipitated in the sample, return to room temperature, and obtain the finished product. 2.根据权利要求1所述的澳洲坚果基础油的制备方法,其特征在于,所述步骤(1)中原料澳洲坚果果仁的重量含水量为12-16%,脂肪含量70-73g/100g,酸价0.15-0.2mgKOH/g,过氧化值0.01-0.016g/100g,油酸含量40-43g/100g,棕榈油酸含量10-12g/100g,要求果仁饱满完整、无瘪仁、无霉变,出仁率为13-15%。2. The preparation method of macadamia nut base oil according to claim 1, characterized in that, in the step (1), the weight water content of the raw macadamia nuts is 12-16%, and the fat content is 70-73g/100g , the acid value is 0.15-0.2mgKOH/g, the peroxide value is 0.01-0.016g/100g, the oleic acid content is 40-43g/100g, and the palmitoleic acid content is 10-12g/100g. Mildew, the kernel rate is 13-15%. 3.根据权利要求1所述的澳洲坚果基础油的制备方法,其特征在于,所述步骤(2)中将果仁粉碎至直径为0.3-0.5cm的完整颗粒。3 . The method for preparing macadamia nut base oil according to claim 1 , wherein in the step (2), the nuts are pulverized to complete particles with a diameter of 0.3-0.5 cm. 4 . 4.根据权利要求1所述的澳洲坚果基础油的制备方法,其特征在于,所述步骤(3)中采用低温干燥处理,具体为:平铺厚度小于0.5cm,45℃下烘干48-56h,直至重量含水量≤1.8%。4. The preparation method of macadamia nut base oil according to claim 1, characterized in that, in the step (3), a low-temperature drying treatment is adopted, specifically: the thickness of the tiling is less than 0.5cm, and drying at 45°C for 48- 56h, until the water content by weight is less than or equal to 1.8%. 5.根据权利要求1所述的澳洲坚果基础油的制备方法,其特征在于,所述步骤(4)中螺旋压榨机无需预热,进料量50g/min,收集油脂混合物。5 . The preparation method of macadamia nut base oil according to claim 1 , wherein in the step (4), the screw press does not need to be preheated, and the feed rate is 50 g/min to collect the oil mixture. 6 . 6.根据权利要求1所述的澳洲坚果基础油的制备方法,其特征在于,所述步骤(5)中离心机转速为4000r/min,离心时间为25-30min。6 . The preparation method of macadamia nut base oil according to claim 1 , wherein in the step (5), the rotating speed of the centrifuge is 4000 r/min, and the centrifugation time is 25-30 min. 7 . 7.根据权利要求1所述的澳洲坚果基础油的制备方法,其特征在于,所述步骤(6)中,50℃恒温水浴时间30-40min,冰箱中于4℃下静置24-28h,静置过程中密封。7. The preparation method of macadamia nut base oil according to claim 1, characterized in that, in the step (6), the time in a constant temperature water bath at 50°C is 30-40min, and in a refrigerator, it is left to stand at 4°C for 24-28h, Seal while standing. 8.一种澳洲坚果基础油,其特征在于,所述澳洲坚果基础油按照权利要求1-8中任一项的制备方法制得。8. A macadamia nut base oil, characterized in that, the macadamia nut base oil is obtained according to the preparation method of any one of claims 1-8.
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CN113413342A (en) * 2021-06-25 2021-09-21 西南林业大学 Method for extracting palmitoleic acid from macadamia nut and application of palmitoleic acid
CN115678663A (en) * 2022-11-28 2023-02-03 合肥工业大学 A kind of pecan oil and preparation method thereof

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Application publication date: 20200619