CN110973431A - Sisal hemp pectin solid beverage and preparation method thereof - Google Patents
Sisal hemp pectin solid beverage and preparation method thereof Download PDFInfo
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- 235000010987 pectin Nutrition 0.000 title claims abstract description 101
- 229920001277 pectin Polymers 0.000 title claims abstract description 101
- 244000198134 Agave sisalana Species 0.000 title claims abstract description 75
- 235000011624 Agave sisalana Nutrition 0.000 title claims abstract description 57
- 239000007787 solid Substances 0.000 title claims abstract description 57
- 235000013361 beverage Nutrition 0.000 title claims abstract description 36
- 238000002360 preparation method Methods 0.000 title description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 33
- 239000002253 acid Substances 0.000 claims abstract description 19
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 19
- 239000008213 purified water Substances 0.000 claims abstract description 19
- TVXBFESIOXBWNM-UHFFFAOYSA-N Xylitol Natural products OCCC(O)C(O)C(O)CCO TVXBFESIOXBWNM-UHFFFAOYSA-N 0.000 claims abstract description 14
- HEBKCHPVOIAQTA-UHFFFAOYSA-N meso ribitol Natural products OCC(O)C(O)C(O)CO HEBKCHPVOIAQTA-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000000811 xylitol Substances 0.000 claims abstract description 14
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- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 claims abstract description 14
- 229960002675 xylitol Drugs 0.000 claims abstract description 14
- 229920000858 Cyclodextrin Polymers 0.000 claims abstract description 12
- 229930091371 Fructose Natural products 0.000 claims abstract description 12
- 239000005715 Fructose Substances 0.000 claims abstract description 12
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 claims abstract description 12
- 229920002774 Maltodextrin Polymers 0.000 claims abstract description 12
- 239000005913 Maltodextrin Substances 0.000 claims abstract description 12
- 235000017784 Mespilus germanica Nutrition 0.000 claims abstract description 12
- 235000000560 Mimusops elengi Nutrition 0.000 claims abstract description 12
- UEDUENGHJMELGK-HYDKPPNVSA-N Stevioside Chemical compound O([C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1O[C@]12C(=C)C[C@@]3(C1)CC[C@@H]1[C@@](C)(CCC[C@]1([C@@H]3CC2)C)C(=O)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O UEDUENGHJMELGK-HYDKPPNVSA-N 0.000 claims abstract description 12
- 235000007837 Vangueria infausta Nutrition 0.000 claims abstract description 12
- 229940035034 maltodextrin Drugs 0.000 claims abstract description 12
- 229940013618 stevioside Drugs 0.000 claims abstract description 12
- OHHNJQXIOPOJSC-UHFFFAOYSA-N stevioside Natural products CC1(CCCC2(C)C3(C)CCC4(CC3(CCC12C)CC4=C)OC5OC(CO)C(O)C(O)C5OC6OC(CO)C(O)C(O)C6O)C(=O)OC7OC(CO)C(O)C(O)C7O OHHNJQXIOPOJSC-UHFFFAOYSA-N 0.000 claims abstract description 12
- 235000019202 steviosides Nutrition 0.000 claims abstract description 12
- 239000001116 FEMA 4028 Substances 0.000 claims abstract description 11
- WHGYBXFWUBPSRW-FOUAGVGXSA-N beta-cyclodextrin Chemical compound OC[C@H]([C@H]([C@@H]([C@H]1O)O)O[C@H]2O[C@@H]([C@@H](O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O3)[C@H](O)[C@H]2O)CO)O[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@@H]3O[C@@H]1CO WHGYBXFWUBPSRW-FOUAGVGXSA-N 0.000 claims abstract description 11
- 235000011175 beta-cyclodextrine Nutrition 0.000 claims abstract description 11
- 229960004853 betadex Drugs 0.000 claims abstract description 11
- 239000000706 filtrate Substances 0.000 claims description 35
- 239000011259 mixed solution Substances 0.000 claims description 35
- 239000000243 solution Substances 0.000 claims description 29
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 28
- 239000002244 precipitate Substances 0.000 claims description 28
- 238000003756 stirring Methods 0.000 claims description 28
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 21
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 21
- 239000002245 particle Substances 0.000 claims description 21
- 239000002994 raw material Substances 0.000 claims description 20
- 238000009835 boiling Methods 0.000 claims description 14
- 239000008187 granular material Substances 0.000 claims description 14
- 238000002156 mixing Methods 0.000 claims description 13
- 244000182216 Mimusops elengi Species 0.000 claims description 11
- 238000000034 method Methods 0.000 claims description 10
- 238000010298 pulverizing process Methods 0.000 claims description 9
- BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 claims description 7
- BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 claims description 7
- 238000001816 cooling Methods 0.000 claims description 7
- 239000008367 deionised water Substances 0.000 claims description 7
- 229910021641 deionized water Inorganic materials 0.000 claims description 7
- 238000001035 drying Methods 0.000 claims description 7
- 238000001914 filtration Methods 0.000 claims description 7
- 238000010438 heat treatment Methods 0.000 claims description 7
- 239000007788 liquid Substances 0.000 claims description 7
- 239000001630 malic acid Substances 0.000 claims description 7
- 235000011090 malic acid Nutrition 0.000 claims description 7
- 238000000926 separation method Methods 0.000 claims description 7
- 238000002791 soaking Methods 0.000 claims description 7
- 235000013305 food Nutrition 0.000 claims description 6
- 238000007873 sieving Methods 0.000 claims description 5
- 244000241838 Lycium barbarum Species 0.000 claims description 2
- 235000015459 Lycium barbarum Nutrition 0.000 claims description 2
- 235000015468 Lycium chinense Nutrition 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims 1
- HFHDHCJBZVLPGP-UHFFFAOYSA-N schardinger α-dextrin Chemical compound O1C(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(O)C2O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC2C(O)C(O)C1OC2CO HFHDHCJBZVLPGP-UHFFFAOYSA-N 0.000 claims 1
- 240000002624 Mespilus germanica Species 0.000 abstract 1
- 230000000052 comparative effect Effects 0.000 description 4
- 230000000694 effects Effects 0.000 description 3
- 239000008280 blood Substances 0.000 description 2
- 210000004369 blood Anatomy 0.000 description 2
- 230000035622 drinking Effects 0.000 description 2
- 201000006549 dyspepsia Diseases 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 210000004072 lung Anatomy 0.000 description 2
- 235000016709 nutrition Nutrition 0.000 description 2
- 230000035764 nutrition Effects 0.000 description 2
- 238000012216 screening Methods 0.000 description 2
- 241000746976 Agavaceae Species 0.000 description 1
- 244000099147 Ananas comosus Species 0.000 description 1
- 235000007119 Ananas comosus Nutrition 0.000 description 1
- 244000025254 Cannabis sativa Species 0.000 description 1
- 235000012766 Cannabis sativa ssp. sativa var. sativa Nutrition 0.000 description 1
- 235000012765 Cannabis sativa ssp. sativa var. spontanea Nutrition 0.000 description 1
- 206010010774 Constipation Diseases 0.000 description 1
- AEMOLEFTQBMNLQ-YMDCURPLSA-N D-galactopyranuronic acid Chemical compound OC1O[C@H](C(O)=O)[C@H](O)[C@H](O)[C@H]1O AEMOLEFTQBMNLQ-YMDCURPLSA-N 0.000 description 1
- IAJILQKETJEXLJ-UHFFFAOYSA-N Galacturonsaeure Natural products O=CC(O)C(O)C(O)C(O)C(O)=O IAJILQKETJEXLJ-UHFFFAOYSA-N 0.000 description 1
- 244000193174 agave Species 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 210000004204 blood vessel Anatomy 0.000 description 1
- 235000009120 camo Nutrition 0.000 description 1
- 235000005607 chanvre indien Nutrition 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000032050 esterification Effects 0.000 description 1
- 238000005886 esterification reaction Methods 0.000 description 1
- 235000013373 food additive Nutrition 0.000 description 1
- 239000002778 food additive Substances 0.000 description 1
- 230000020169 heat generation Effects 0.000 description 1
- 239000011487 hemp Substances 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof
- A23L2/385—Concentrates of non-alcoholic beverages
- A23L2/39—Dry compositions
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Mycology (AREA)
- Non-Alcoholic Beverages (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
The invention discloses a sisal hemp pectin solid beverage which comprises, by weight, 20-30 parts of sisal hemp pectin, 2-5 parts of fructose, 0.2-0.5 part of stevioside, 3-5 parts of medlar, 3-6 parts of maltodextrin, 4-6 parts of β -cyclodextrin, 8-10 parts of xylitol, 2-4 parts of an acid agent and 20-30 parts of purified water.
Description
Technical Field
The invention relates to the technical field of food, in particular to a sisal hemp pectin solid beverage.
Background
The pectin is linked by galacturonic acid with different esterification degrees and α -1, 4 glycosidic bond, and can be used as natural food additive, and has effects of significantly reducing blood lipid and blood sugar, dredging blood vessel, and treating constipation.
Sisal hemp is also called pineapple hemp, belonging to agave genus of agave family, and is a perennial heat generation crop with hard leaf fiber, which is originally produced in mexico, is mainly planted in africa, latin america, asia and the like, and is a hard fiber with the largest amount and the widest range in the world; the content of pectin in sisal hemp is high, and the quality of sisal hemp can completely meet the requirements of food. The existing market lacks solid beverage prepared by taking sisal pectin as a raw material, and sisal resources are not fully utilized.
Disclosure of Invention
The invention aims to provide a sisal pectin solid beverage to solve the problems in the background technology.
In order to achieve the purpose, the invention provides the following technical scheme:
a sisal hemp pectin solid beverage comprises, by weight, 20-30 parts of sisal hemp pectin, 2-5 parts of fructose, 0.2-0.5 part of stevioside, 3-5 parts of medlar, 3-6 parts of maltodextrin, 4-6 parts of β -cyclodextrin, 8-10 parts of xylitol, 2-4 parts of an acid agent and 20-30 parts of purified water.
The health-care food comprises the following raw materials, by weight, 22-28 parts of sisal hemp pectin, 3-4 parts of fructose, 0.3-0.4 part of stevioside, 3.5-4.5 parts of medlar, 4-5 parts of maltodextrin, 4.5-5.5 parts of β -cyclodextrin, 8.5-9.5 parts of xylitol, 2.5-3.5 parts of an acid agent and 22-28 parts of purified water.
The health-care food is characterized by comprising the following raw materials of, by weight, 25 parts of sisal pectin, 3.5 parts of fructose, 0.4 part of stevioside, 4 parts of medlar, 4.5 parts of maltodextrin, 5 parts of β -cyclodextrin, 9 parts of xylitol, 3 parts of an acid agent and 25 parts of purified water.
As a still further scheme of the invention: the sisal hemp pectin is extracted by the following method: 1) crushing sisal hemp, soaking in an ethanol solution for 10min, draining, adding deionized water 10 times the weight of the sisal hemp, stirring and mixing uniformly, boiling for 8min, and cooling to obtain a mixed solution I; 2) adjusting the pH value of the mixed solution I obtained in the step 1) to 2, heating to 60 ℃, and reacting for 20min to obtain a mixed solution II; 3) dripping glycerol into the mixed solution II obtained in the step 2), uniformly stirring, refrigerating for 2 hours after the stirring is finished, and performing centrifugal separation to obtain pectin crude filtrate; 4) clarifying the pectin crude filtrate obtained in the step 3) to obtain pectin clarified liquid; 5) concentrating the pectin crude filtrate obtained in the step 4) in a vacuum environment, wherein the concentration temperature is 40 ℃ until the weight of the pectin clear solution reaches 1/8 before concentration; 6) adding an ethanol solution into the pectin concentrated solution obtained in the step 5), and standing for 20min to obtain flocculent precipitate; 7) drying the flocculent precipitate obtained in the step 6) until the water content of the precipitate is not more than 10%, and crushing the precipitate to obtain the sisal hemp pectin.
As a still further scheme of the invention: the acid agent is prepared by mixing citric acid and malic acid according to the weight ratio of 1: 3.
The preparation method of the sisal hemp pectin solid beverage comprises the following steps:
1) pulverizing fructus Lycii to obtain fructus Lycii granule, adding purified water into fructus Lycii granule, boiling for 5-10min, and filtering to obtain filtrate;
2) adding other raw materials into the filtrate obtained in the step 1), stirring for 30-50min at the rotating speed of 400-600r/min, and standing for 10-15min to obtain a mixed solution;
3) distilling the mixed liquor obtained in the step 2) to obtain solid particles;
4) crushing the solid particles obtained in the step 3), and sieving the crushed solid particles with a 100-mesh and 150-mesh sieve to obtain the sisal hemp pectin solid beverage.
The solid beverage is applied to the field of food.
Compared with the prior art, the invention has the beneficial effects that:
under the combined action of various raw materials, the solid beverage prepared by the invention is rich in nutrition and good in taste, has the effects of clearing heat, moistening lung and relieving dyspepsia, and is suitable for drinking.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
A sisal hemp pectin solid beverage comprises the following raw materials, by weight, 20 parts of sisal hemp pectin, 2 parts of fructose, 0.2 part of stevioside, 3 parts of medlar, 3 parts of maltodextrin, 4 parts of β -cyclodextrin, 8 parts of xylitol, 2 parts of an acid agent and 20 parts of purified water.
Wherein, the sisal pectin is extracted by the following method: 1) crushing sisal hemp, soaking in an ethanol solution for 10min, draining, adding deionized water 10 times the weight of the sisal hemp, stirring and mixing uniformly, boiling for 8min, and cooling to obtain a mixed solution I; 2) Adjusting the pH value of the mixed solution I obtained in the step 1) to 2, heating to 60 ℃, and reacting for 20min to obtain a mixed solution II; 3) Dripping glycerol into the mixed solution II obtained in the step 2), uniformly stirring, refrigerating for 2 hours after the stirring is finished, and performing centrifugal separation to obtain pectin crude filtrate; 4) clarifying the pectin crude filtrate obtained in the step 3) to obtain pectin clarified liquid; 5) concentrating the pectin crude filtrate obtained in the step 4) in a vacuum environment, wherein the concentration temperature is 40 ℃ until the weight of the pectin clear solution reaches 1/8 before concentration; 6) adding an ethanol solution into the pectin concentrated solution obtained in the step 5), and standing for 20min to obtain flocculent precipitate; 7) drying the flocculent precipitate obtained in the step 6) until the water content of the precipitate is not more than 10%, and crushing the precipitate to obtain the sisal hemp pectin.
Wherein the acid agent is prepared by mixing citric acid and malic acid according to the weight ratio of 1: 3.
In this embodiment, the preparation method of the sisal pectin solid beverage includes the following steps:
1) pulverizing fructus Lycii to obtain fructus Lycii granule, adding purified water into fructus Lycii granule, boiling for 5min, and filtering to obtain filtrate;
2) adding other raw materials into the filtrate obtained in the step 1), stirring for 30min at the rotating speed of 400r/min, and standing for 10min to obtain a mixed solution;
3) distilling the mixed liquor obtained in the step 2) to obtain solid particles;
4) crushing the solid particles obtained in the step 3), and screening the solid particles through a 100-mesh screen to obtain the sisal hemp pectin solid beverage.
Example 2
A sisal hemp pectin solid beverage comprises the following raw materials, by weight, 28 parts of sisal hemp pectin, 4 parts of fructose, 0.4 part of stevioside, 4.5 parts of medlar, 4 parts of maltodextrin, 4.5 parts of β -cyclodextrin, 8.5 parts of xylitol, 2.5 parts of an acid agent and 22 parts of purified water.
Wherein, the sisal pectin is extracted by the following method: 1) crushing sisal hemp, soaking in an ethanol solution for 12min, draining, adding deionized water 13 times the weight of the sisal hemp, stirring and mixing uniformly, boiling for 9min, and cooling to obtain a mixed solution I; 2) Adjusting the pH value of the mixed solution I obtained in the step 1) to 4, heating to 75 ℃, and reacting for 22min to obtain a mixed solution II; 3) Dripping glycerol into the mixed solution II obtained in the step 2), uniformly stirring, refrigerating for 2.2 hours after the stirring is finished, and performing centrifugal separation to obtain pectin crude filtrate; 4) clarifying the pectin crude filtrate obtained in the step 3) to obtain pectin clarified liquid; 5) concentrating the pectin crude filtrate obtained in the step 4) in a vacuum environment, wherein the concentration temperature is 45 ℃ until the weight of the pectin clear solution reaches 1/7 before concentration; 6) adding an ethanol solution into the pectin concentrated solution obtained in the step 5), and standing for 28min to obtain flocculent precipitate; 7) drying the flocculent precipitate obtained in the step 6) until the water content of the precipitate is not more than 10%, and crushing the precipitate to obtain the sisal hemp pectin.
Wherein the acid agent is prepared by mixing citric acid and malic acid according to the weight ratio of 1: 3.
In this embodiment, the preparation method of the sisal pectin solid beverage includes the following steps:
1) pulverizing fructus Lycii to obtain fructus Lycii granule, adding purified water into fructus Lycii granule, boiling for 8min, and filtering to obtain filtrate;
2) adding other raw materials into the filtrate obtained in the step 1), stirring for 40 minutes at the rotating speed of 500r/min, and standing for 12 minutes to obtain a mixed solution;
3) distilling the mixed liquor obtained in the step 2) to obtain solid particles;
4) crushing the solid particles obtained in the step 3), and sieving the crushed solid particles with a 120-mesh sieve to obtain the sisal hemp pectin solid beverage.
Example 3
A sisal hemp pectin solid beverage comprises the following raw materials, by weight, 25 parts of sisal hemp pectin, 3.5 parts of fructose, 0.4 part of stevioside, 4 parts of medlar, 4.5 parts of maltodextrin, 5 parts of β -cyclodextrin, 9 parts of xylitol, 3 parts of an acid agent and 25 parts of purified water.
Wherein, the sisal pectin is extracted by the following method: 1) pulverizing sisal hemp, soaking in ethanol solution for 12min, draining, adding deionized water 12 times of sisal hemp, stirring, mixing, boiling for 9min, and cooling to obtain mixed solution I; 2) Adjusting the pH value of the mixed solution I obtained in the step 1) to 3, heating to 70 ℃, and reacting for 25min to obtain a mixed solution II; 3) dripping glycerol into the mixed solution II obtained in the step 2), uniformly stirring, refrigerating for 2.5 hours after the stirring is finished, and performing centrifugal separation to obtain pectin crude filtrate; 4) clarifying the pectin crude filtrate obtained in the step 3) to obtain pectin clarified liquid; 5) concentrating the pectin crude filtrate obtained in the step 4) in a vacuum environment, wherein the concentration temperature is 50 ℃ until the weight of the pectin clear solution reaches 1/6 before concentration; 6) adding an ethanol solution into the pectin concentrated solution obtained in the step 5), and standing for 25min to obtain flocculent precipitate; 7) drying the flocculent precipitate obtained in the step 6) until the water content of the precipitate is not more than 10%, and crushing the precipitate to obtain the sisal hemp pectin.
Wherein the acid agent is prepared by mixing citric acid and malic acid according to the weight ratio of 1: 3.
In this embodiment, the preparation method of the sisal pectin solid beverage includes the following steps:
1) pulverizing fructus Lycii to obtain fructus Lycii granule, adding purified water into fructus Lycii granule, boiling for 8min, and filtering to obtain filtrate;
2) adding other raw materials into the filtrate obtained in the step 1), stirring for 40 minutes at the rotating speed of 500r/min, and standing for 12 minutes to obtain a mixed solution;
3) distilling the mixed liquor obtained in the step 2) to obtain solid particles;
4) crushing the solid particles obtained in the step 3), and sieving the crushed solid particles with a 120-mesh sieve to obtain the sisal hemp pectin solid beverage.
Example 4
A sisal hemp pectin solid beverage comprises the following raw materials, by weight, 22 parts of sisal hemp pectin, 3 parts of fructose, 0.3 part of stevioside, 3.5 parts of medlar, 5 parts of maltodextrin, 5.5 parts of β -cyclodextrin, 9.5 parts of xylitol, 3.5 parts of an acid agent and 28 parts of purified water.
Wherein, the sisal pectin is extracted by the following method: 1) crushing sisal hemp, soaking in an ethanol solution for 14min, draining, adding deionized water 14 times the weight of the sisal hemp, stirring and mixing uniformly, boiling for 10min, and cooling to obtain a mixed solution I; 2) Adjusting the pH value of the mixed solution I obtained in the step 1) to 4, heating to 75 ℃, and reacting for 28min to obtain a mixed solution II; 3) Dripping glycerol into the mixed solution II obtained in the step 2), uniformly stirring, refrigerating for 2.7 hours after the stirring is finished, and performing centrifugal separation to obtain pectin crude filtrate; 4) clarifying the pectin crude filtrate obtained in the step 3) to obtain pectin clarified liquid; 5) concentrating the pectin crude filtrate obtained in the step 4) in a vacuum environment, wherein the concentration temperature is 55 ℃, until the weight of the pectin clear solution reaches 1/5 before concentration; 6) adding an ethanol solution into the pectin concentrated solution obtained in the step 5), and standing for 22min to obtain flocculent precipitate; 7) drying the flocculent precipitate obtained in the step 6) until the water content of the precipitate is not more than 10%, and crushing the precipitate to obtain the sisal hemp pectin.
Wherein the acid agent is prepared by mixing citric acid and malic acid according to the weight ratio of 1: 3.
In this embodiment, the preparation method of the sisal pectin solid beverage includes the following steps:
1) pulverizing fructus Lycii to obtain fructus Lycii granule, adding purified water into fructus Lycii granule, boiling for 8min, and filtering to obtain filtrate;
2) adding other raw materials into the filtrate obtained in the step 1), stirring for 40 minutes at the rotating speed of 500r/min, and standing for 12 minutes to obtain a mixed solution;
3) distilling the mixed liquor obtained in the step 2) to obtain solid particles;
4) crushing the solid particles obtained in the step 3), and sieving the crushed solid particles with a 120-mesh sieve to obtain the sisal hemp pectin solid beverage.
Example 5
A sisal hemp pectin solid beverage comprises the following raw materials, by weight, 30 parts of sisal hemp pectin, 5 parts of fructose, 0.5 part of stevioside, 5 parts of medlar, 6 parts of maltodextrin, 6 parts of β -cyclodextrin, 10 parts of xylitol, 4 parts of an acid agent and 30 parts of purified water.
Wherein, the sisal pectin is extracted by the following method: 1) crushing sisal hemp, soaking in an ethanol solution for 15min, draining, adding deionized water 15 times the weight of the sisal hemp, stirring and mixing uniformly, boiling for 10min, and cooling to obtain a mixed solution I; 2) Adjusting the pH value of the mixed solution I obtained in the step 1) to 4, heating to 80 ℃, and reacting for 30min to obtain a mixed solution II; 3) Dripping glycerol into the mixed solution II obtained in the step 2), uniformly stirring, refrigerating for 3 hours after the stirring is finished, and performing centrifugal separation to obtain pectin crude filtrate; 4) clarifying the pectin crude filtrate obtained in the step 3) to obtain pectin clarified liquid; 5) concentrating the pectin crude filtrate obtained in the step 4) in a vacuum environment at the concentration temperature of 60 ℃ until the weight of the pectin clear solution reaches 1/4 before concentration; 6) adding an ethanol solution into the pectin concentrated solution obtained in the step 5), and standing for 30min to obtain flocculent precipitate; 7) drying the flocculent precipitate obtained in the step 6) until the water content of the precipitate is not more than 10%, and crushing the precipitate to obtain the sisal hemp pectin.
Wherein the acid agent is prepared by mixing citric acid and malic acid according to the weight ratio of 1: 3.
In this embodiment, the preparation method of the sisal pectin solid beverage includes the following steps:
1) pulverizing fructus Lycii to obtain fructus Lycii granule, adding purified water into fructus Lycii granule, boiling for 10min, and filtering to obtain filtrate;
2) adding other raw materials into the filtrate obtained in the step 1), stirring for 50 minutes at the rotating speed of 600r/min, and standing for 15 minutes to obtain a mixed solution;
3) distilling the mixed liquor obtained in the step 2) to obtain solid particles;
4) crushing the solid particles obtained in the step 3), and screening the crushed solid particles through a 150-mesh screen to obtain the sisal hemp pectin solid beverage.
Comparative example 1
Compared with example 3, the method does not contain medlar, and the other steps are the same as example 3.
Comparative example 2
Compared with example 3, the method does not contain xylitol, and the other steps are the same as example 3.
Comparative example 3
Compared with example 3, the wolfberry fruit and xylitol are not contained, and the rest is the same as example 3.
The solid beverages prepared in examples 1 to 5 and comparative examples 1 to 3 were tested, and the test results are shown in table 1.
TABLE 1
The results show that the solid beverage prepared by the invention has rich nutrition and good taste under the combined action of various raw materials, has the effects of clearing heat, moistening lung and relieving dyspepsia, and is suitable for drinking.
It will be evident to those skilled in the art that the invention is not limited to the details of the foregoing illustrative embodiments, and that the present invention may be embodied in other specific forms without departing from the spirit or essential attributes thereof. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein. Any reference sign in a claim should not be construed as limiting the claim concerned.
Furthermore, it should be understood that although the present description refers to embodiments, not every embodiment may contain only a single embodiment, and such description is for clarity only, and those skilled in the art should integrate the description, and the embodiments may be combined as appropriate to form other embodiments understood by those skilled in the art.
Claims (7)
1. The sisal hemp pectin solid beverage is characterized by comprising the following raw materials, by weight, 20-30 parts of sisal hemp pectin, 2-5 parts of fructose, 0.2-0.5 part of stevioside, 3-5 parts of wolfberry, 3-6 parts of maltodextrin, β -4-6 parts of cyclodextrin, 8-10 parts of xylitol, 2-4 parts of an acid agent and 20-30 parts of purified water.
2. The sisal hemp pectin solid beverage according to claim 1, which comprises the following raw materials, by weight, 22-28 parts of sisal hemp pectin, 3-4 parts of fructose, 0.3-0.4 part of stevioside, 3.5-4.5 parts of medlar, 4-5 parts of maltodextrin, 4.5-5.5 parts of β -cyclodextrin, 8.5-9.5 parts of xylitol, 2.5-3.5 parts of an acid agent, and 22-28 parts of purified water.
3. The sisal hemp pectin solid beverage according to claim 2, which comprises the following raw materials, by weight, 25 parts of sisal hemp pectin, 3.5 parts of fructose, 0.4 part of stevioside, 4 parts of medlar, 4.5 parts of maltodextrin, 5 parts of β -cyclodextrin, 9 parts of xylitol, 3 parts of an acid agent and 25 parts of purified water.
4. The sisal pectin solid beverage according to claim 1, wherein the sisal pectin is extracted by the following method: 1) pulverizing sisal hemp, soaking in ethanol solution for 10-15min, draining, adding deionized water 10-15 times of sisal hemp, stirring, mixing, boiling for 8-10min, and cooling to obtain mixed solution I; 2) adjusting the pH value of the mixed solution I obtained in the step 1) to 2-4, heating to 60-80 ℃, and reacting for 20-30min to obtain a mixed solution II; 3) dripping glycerol into the mixed solution II obtained in the step 2), uniformly stirring, refrigerating for 2-3h after the stirring is finished, and performing centrifugal separation to obtain pectin crude filtrate; 4) clarifying the pectin crude filtrate obtained in the step 3) to obtain pectin clarified liquid; 5) concentrating the pectin crude filtrate obtained in step 4) in vacuum at 40-60 deg.C until the weight of pectin clear solution reaches 1/8-1/4 before concentration; 6) adding an ethanol solution into the pectin concentrated solution obtained in the step 5), and standing for 20-30min to obtain flocculent precipitate; 7) drying the flocculent precipitate obtained in the step 6) until the water content of the precipitate is not more than 10%, and crushing the precipitate to obtain the sisal hemp pectin.
5. The sisal pectin solid beverage of claim 1, wherein said acid agent is a mixture of citric acid and malic acid at a weight ratio of 1: 3.
6. A method for preparing the sisal pectin solid beverage according to any one of claims 1-5, wherein the steps are as follows:
1) pulverizing fructus Lycii to obtain fructus Lycii granule, adding purified water into fructus Lycii granule, boiling for 5-10min, and filtering to obtain filtrate;
2) adding other raw materials into the filtrate obtained in the step 1), stirring for 30-50min at the rotating speed of 400-600r/min, and standing for 10-15min to obtain a mixed solution;
3) distilling the mixed liquor obtained in the step 2) to obtain solid particles;
4) crushing the solid particles obtained in the step 3), and sieving the crushed solid particles with a 100-mesh and 150-mesh sieve to obtain the sisal hemp pectin solid beverage.
7. Use of a solid beverage according to any one of claims 1 to 5 in the field of food.
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Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101864000A (en) * | 2010-06-25 | 2010-10-20 | 彭胜良 | Pectin extraction method from waste sisal dregs |
| CN103284265A (en) * | 2013-06-03 | 2013-09-11 | 赛珂睿德生物医药科技(上海)有限公司 | Solid beverage with effects of improving intestinal flora and relaxing bowels |
| CN105254778A (en) * | 2015-11-23 | 2016-01-20 | 吴莹 | Extracting method of sisal hemp pectin |
| CN105418791A (en) * | 2015-11-23 | 2016-03-23 | 吴莹 | Preparing method for sisal hemp pectin |
| CN107518217A (en) * | 2016-06-22 | 2017-12-29 | 唐逸 | A kind of pectin diet fiber drink and preparation method thereof |
| CN108219027A (en) * | 2016-12-14 | 2018-06-29 | 杭州垚信生物科技有限公司 | A kind of method that sisal hemp pectin is prepared using sisal hemp waste residue |
| CN108740161A (en) * | 2018-06-06 | 2018-11-06 | 山西华欣久泰信息技术有限公司 | A kind of solid tea beverage and preparation method thereof |
| CN108822225A (en) * | 2018-06-20 | 2018-11-16 | 山东神州翔宇科技集团有限公司 | A kind of preparation method of sweet potato carboxymethyl modified starch |
| CN109170456A (en) * | 2018-08-22 | 2019-01-11 | 湖南米笠农业科技有限公司 | A kind of fruits and vegetables mixing infusing potable and preparation method thereof |
-
2019
- 2019-08-03 CN CN201910714929.3A patent/CN110973431A/en active Pending
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101864000A (en) * | 2010-06-25 | 2010-10-20 | 彭胜良 | Pectin extraction method from waste sisal dregs |
| CN103284265A (en) * | 2013-06-03 | 2013-09-11 | 赛珂睿德生物医药科技(上海)有限公司 | Solid beverage with effects of improving intestinal flora and relaxing bowels |
| CN105254778A (en) * | 2015-11-23 | 2016-01-20 | 吴莹 | Extracting method of sisal hemp pectin |
| CN105418791A (en) * | 2015-11-23 | 2016-03-23 | 吴莹 | Preparing method for sisal hemp pectin |
| CN107518217A (en) * | 2016-06-22 | 2017-12-29 | 唐逸 | A kind of pectin diet fiber drink and preparation method thereof |
| CN108219027A (en) * | 2016-12-14 | 2018-06-29 | 杭州垚信生物科技有限公司 | A kind of method that sisal hemp pectin is prepared using sisal hemp waste residue |
| CN108740161A (en) * | 2018-06-06 | 2018-11-06 | 山西华欣久泰信息技术有限公司 | A kind of solid tea beverage and preparation method thereof |
| CN108822225A (en) * | 2018-06-20 | 2018-11-16 | 山东神州翔宇科技集团有限公司 | A kind of preparation method of sweet potato carboxymethyl modified starch |
| CN109170456A (en) * | 2018-08-22 | 2019-01-11 | 湖南米笠农业科技有限公司 | A kind of fruits and vegetables mixing infusing potable and preparation method thereof |
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