CN110857877A - Calibration method of natural gas standard flowmeter - Google Patents

Calibration method of natural gas standard flowmeter Download PDF

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Publication number
CN110857877A
CN110857877A CN201810972124.4A CN201810972124A CN110857877A CN 110857877 A CN110857877 A CN 110857877A CN 201810972124 A CN201810972124 A CN 201810972124A CN 110857877 A CN110857877 A CN 110857877A
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China
Prior art keywords
pressure
gas
natural gas
unit
tank
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CN201810972124.4A
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CN110857877B (en
Inventor
宋彬
段继芹
任佳
王强
樊兰蓓
何敏
彭利果
陈荟宇
韦颜
王辉
夏寿华
周芳
周承美
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Petrochina Co Ltd
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Petrochina Co Ltd
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Priority to CN201810972124.4A priority Critical patent/CN110857877B/en
Priority to FR1904200A priority patent/FR3080449B1/en
Priority to RU2019112156A priority patent/RU2712935C1/en
Publication of CN110857877A publication Critical patent/CN110857877A/en
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    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01F—MEASURING VOLUME, VOLUME FLOW, MASS FLOW OR LIQUID LEVEL; METERING BY VOLUME
    • G01F25/00—Testing or calibration of apparatus for measuring volume, volume flow or liquid level or for metering by volume
    • G01F25/10—Testing or calibration of apparatus for measuring volume, volume flow or liquid level or for metering by volume of flowmeters
    • G01F25/15—Testing or calibration of apparatus for measuring volume, volume flow or liquid level or for metering by volume of flowmeters specially adapted for gas meters

Abstract

The invention discloses a calibration method of a natural gas standard flowmeter, which comprises the following steps: conveying the natural gas in the low-pressure gas source to a pressurizing device and a gas path anti-corrosion device, removing sulfur, moisture and solid particles in the natural gas, and pressurizing to a first preset pressure; conveying the natural gas into a high-pressure gas storage device, and conveying the natural gas into a pressure regulating device after the gas pressure is a second preset pressure, so that the pressure of the natural gas is regulated to the working pressure of a natural gas standard flowmeter; conveying natural gas into a constant temperature device, and removing non-inert gas in cooling water flowing into a pressurizing device and the constant temperature device by using a liquid path anticorrosion device; conveying natural gas into a natural gas standard flowmeter to obtain a measured flow value of the natural gas; the method comprises the steps of conveying natural gas into a weighing tank, utilizing a balance and a timer to respectively obtain the inflating mass and the inflating time of the weighing tank, obtaining the actual flow value of the natural gas according to the inflating mass and the inflating time, and calibrating a natural gas standard flowmeter.

Description

Calibration method of natural gas standard flowmeter
Technical Field
The invention relates to the field of natural gas flow detection, in particular to a calibration method of a natural gas standard flowmeter.
Background
In order to ensure the accuracy, reliability and fairness of natural gas trade metering, the measurement accuracy of a natural gas flowmeter for natural gas trade metering is generally evaluated by using a natural gas standard flowmeter. The measurement accuracy of the natural gas standard flowmeter influences the evaluation result of the natural gas flowmeter, so that the natural gas standard flowmeter is required to be carried out.
The prior art provides a calibration method of a natural gas standard flowmeter, and specifically includes that natural gas in a low-pressure gas source is sequentially conveyed to the natural gas standard flowmeter and a weighing device, and a timer is used for acquiring the inflation time of the weighing device. And then, acquiring an actual flow value of the natural gas by using a mass-time method, and comparing the actual flow value with a measured flow value of the natural gas standard flowmeter so as to calibrate the natural gas standard flowmeter.
The inventor finds that the prior art has at least the following problems:
the methods provided by the prior art do not allow for effective calibration of a standard flow meter for natural gas.
Disclosure of Invention
The embodiment of the invention provides a calibration method of a natural gas standard flowmeter, which can solve the problems. The technical scheme is as follows:
a method of calibrating a natural gas standard flow meter, the method of calibrating comprising:
conveying the natural gas in a low-pressure gas source to a pressurizing device and a gas path anti-corrosion device to remove sulfur, moisture and solid particles in the natural gas, and pressurizing to a first preset pressure;
conveying the pressurized and impurity-removed natural gas into a high-pressure gas storage device, and conveying the pressurized and impurity-removed natural gas into a pressure regulating device after the gas pressure of the high-pressure gas storage device is a second preset pressure, so that the pressure of the pressurized and impurity-removed natural gas is regulated to be the same as the working pressure of the natural gas standard flowmeter;
conveying the pressure-regulated natural gas into a constant temperature device, adjusting the temperature of the pressure-regulated natural gas to be the same as the working temperature of the natural gas standard flowmeter, and removing non-inert gas in cooling water flowing into the supercharging device and the constant temperature device by using a liquid path anticorrosion device;
conveying the natural gas subjected to temperature regulation into the natural gas standard flowmeter to obtain a measured flow value of the natural gas subjected to temperature regulation;
conveying the temperature-adjusted natural gas to a low-pressure gas storage device from a second gas outlet of a reversing valve assembly, closing the second gas outlet of the reversing valve assembly after the reading of the natural gas standard flowmeter is stable, opening a first gas outlet of the reversing valve assembly, conveying the temperature-adjusted natural gas to a weighing tank of a weighing device, and simultaneously acquiring the inflation time of the weighing device by using a timer;
acquiring the inflation mass of the weighing tank by using a balance of the weighing device;
calculating to obtain an actual flow value of the natural gas after temperature adjustment according to the inflation quality, the inflation time and a quality-time method;
and comparing the actual flow value with the measured flow value, and calibrating the natural gas standard flowmeter.
In a possible design, the natural gas after the impurity removal by pressurization is conveyed to a high-pressure gas storage device, and after the gas force of the high-pressure gas storage device is a second preset pressure, the natural gas after the impurity removal by pressurization is conveyed to a pressure regulating device, and the method includes:
and conveying the natural gas subjected to the pressurization impurity removal to a first high-pressure gas storage unit or a second high-pressure gas storage unit of the high-pressure gas storage device, and alternately conveying the natural gas subjected to the pressurization impurity removal at a second preset pressure to the pressure regulating device by the first high-pressure gas storage unit and the second high-pressure gas storage unit.
In a possible design, the conveying the natural gas after the impurity removal by pressurization to the first high-pressure gas storage unit or the second high-pressure gas storage unit of the high-pressure gas storage device, and the conveying the natural gas after the impurity removal by pressurization of the second preset pressure in turn from the first high-pressure gas storage unit to the second high-pressure gas storage unit into the pressure regulating device includes:
acquiring gas pressure information of the first high-pressure gas storage unit by using a first pressure sensor, transmitting the gas pressure information to a first gas valve controller, and acquiring gas pressure information of the second high-pressure gas storage unit by using a second pressure sensor, and transmitting the gas pressure information to a second gas valve controller;
if the gas pressure of the first high-pressure gas storage unit is smaller than the second preset pressure and the gas pressure of the second high-pressure gas storage unit is larger than or equal to the second preset pressure, the first gas valve controller is utilized to open the inlet of the first high-pressure gas storage unit and the outlet of the second high-pressure gas storage unit so as to convey the natural gas after the pressurization and impurity removal into the first high-pressure gas storage unit and convey the natural gas after the pressurization and impurity removal into the pressure regulating mechanism,
if the gas pressure of the first high-pressure gas storage unit is larger than or equal to the second preset pressure, the gas pressure of the second high-pressure gas storage unit is smaller than the second preset pressure, the second gas valve controller is utilized to open the outlet of the first high-pressure gas storage unit and the inlet of the second high-pressure gas storage unit, so that the natural gas after the supercharging impurity removal is conveyed into the second high-pressure gas storage unit, and the natural gas after the supercharging impurity removal in the first high-pressure gas storage unit is conveyed into the pressure regulating device.
In a possible design, the step of conveying the pressurized impurity-removed natural gas into a pressure regulating device to adjust the pressure of the pressurized impurity-removed natural gas to be the same as the working pressure of the natural gas standard flowmeter includes:
conveying the pressurized and impurity-removed natural gas in the high-pressure gas storage device to a pressure regulating tank of the pressure regulating device;
acquiring gas pressure information of the pressure regulating tank by using a third pressure sensor, and transmitting the gas pressure information to a third gas valve controller;
if the gas pressure of the pressure regulating tank is larger than the working pressure, the third gas valve controller is utilized to open the vent of the pressure regulating tank so as to discharge the natural gas after the pressurization and impurity removal in the pressure regulating tank until the gas pressure of the pressure regulating tank is equal to the working pressure.
In one possible design, the removing sulfur, moisture, and solid particles from the natural gas includes:
conveying the natural gas to a desulfurization unit of the gas path corrosion prevention device to remove sulfur in the natural gas;
conveying the desulfurized natural gas to a buffer unit of the gas path corrosion prevention device for temporary storage;
enabling the desulfurized natural gas to pass through a dehydration unit of the gas path anticorrosion device from top to bottom so as to adsorb moisture in the desulfurized natural gas;
and conveying the dehydrated natural gas to a filtering unit of the gas path anti-corrosion device, removing solid particles in the dehydrated natural gas, and discharging a part of the natural gas from which the solid particles are removed.
In one possible design, the removing sulfur, moisture, and solid particles from the natural gas further includes:
heating the other part of the natural gas with the solid particles removed to a first preset temperature by using a heating unit of the gas path corrosion prevention device, and enabling the heated natural gas to pass through the dehydration unit from bottom to top so as to analyze the moisture adsorbed by the dehydration unit;
and cooling the moisture generated during the analysis of the dehydration unit by utilizing the condensation unit of the gas path anticorrosion device so as to separate the other part of the natural gas from which the solid particles are removed.
In one possible design, the method for removing non-inert gas in the cooling water flowing into the pressure boosting device and the thermostat device by using the liquid path corrosion prevention device at the same time includes:
conveying the cooling water to a water storage unit of the liquid path corrosion prevention device, and simultaneously sucking the inert gas in an inert gas supply unit of the liquid path corrosion prevention device into the water storage unit by using a suction unit of the liquid path corrosion prevention device;
and under the action of pressure difference, the non-inert gas in the water storage unit is discharged from the exhalation unit of the liquid path corrosion prevention device, so that the non-inert gas in the cooling water in the water storage unit is converted into inert gas.
In one possible embodiment, the weighing tank comprises: the device comprises a first outer tank body and a first inner tank body arranged in the first outer tank body;
a vacuum gap layer is arranged between the first outer tank body and the first inner tank body;
a first inflation port used for being communicated with the reversing valve assembly is arranged on the outer wall of the first outer tank body, and the first inflation port penetrates through the vacuum gap layer to be communicated with the first inner tank body;
the air inflation quality of the weighing tank is calculated by using the following calculation formula:
△m＝m1-m0
wherein the content of the first and second substances,
△ m-the inflated mass of the weighing tank, kg;
m1-the mass of the tank after filling, kg;
m0-the mass of the weighing tank before filling, kg.
In one possible embodiment, the weighing tank comprises: the second outer tank body and the second inner tank body are arranged in the second outer tank body;
a mass compensation gap layer is arranged between the second outer tank body and the second inner tank body, and flowable media are filled in the mass compensation gap layer;
the outer wall of the second outer tank body is provided with a mass compensation pipe which is communicated with the mass compensation gap layer, and the mass compensation pipe is provided with scales and has a standard sectional area;
a second inflation inlet which is used for being communicated with the reversing valve assembly is further arranged on the outer wall of the second outer tank body, and the second inflation inlet penetrates through the mass compensation gap layer to be communicated with the second inner tank body;
the air inflation quality of the weighing tank is calculated by using the following calculation formula:
△m＝m1-m0-ρ×s×(l1-l0)
wherein the content of the first and second substances,
△ m-the inflated mass of the weighing tank, kg;
m1-the mass of the tank after filling, kg;
m0-the mass of the weighing tank before inflation, kg;
rho-density of air surrounding the weighing tank, kg/m3；
s-area of cross section of the mass compensating tube, m2；
l1-the height, m, of the flowable medium in the mass compensation tube after the weighing tank has been inflated;
l0-the height, m, of the flowable medium in the mass compensation tube before the weighing tank is inflated.
In one possible embodiment, the temperature and humidity of the balance chamber of the weighing device are regulated by a temperature and humidity regulating device during the measurement of the filling mass of the weighing tank by the balance.
In one possible embodiment, the composition of the tempered natural gas is analyzed by a gas composition analyzer before the tempered natural gas is supplied to the natural gas standard flowmeter.
In one possible design, the calibration method further includes: and conveying the natural gas with the temperature adjusted in the low-pressure gas storage device to the low-pressure gas source so as to recycle the natural gas with the temperature adjusted.
The technical scheme provided by the embodiment of the invention has the beneficial effects that at least:
according to the calibration method of the natural gas standard flowmeter, the pressure of natural gas is increased to be larger than the working pressure of the standard flowmeter by using the supercharging device, and gas with the same pressure as the working pressure of the standard flowmeter can be conveyed into the standard flowmeter by matching the high-pressure gas storage device and the pressure regulating device, so that the calibration precision of the natural gas standard flowmeter can be improved, the natural gas standard flowmeters under different working pressures can be calibrated, and the application range is widened; the gas path anti-corrosion device and the water path anti-corrosion device are matched, so that the natural gas and the cooling water can be subjected to anti-corrosion treatment at the same time, the corrosion of a pressurizing device, a high-pressure gas storage device, a pressure regulating device, a constant temperature device, a natural gas standard flowmeter, a reversing valve assembly and a weighing tank of a weighing device is effectively reduced, the long-term stable operation of the device is ensured, and the calibration precision of the natural gas standard flowmeter can be improved; in addition, through the cooperation of the reversing valve assembly and the timer, the inflation time of the weighing device can be accurately measured, and the calibration precision of the natural gas standard flowmeter can be further improved.
In summary, the calibration method for the natural gas standard flowmeter provided by the embodiment of the invention can improve the calibration precision of the natural gas standard flowmeter and can also expand the application range of the calibration method.
Drawings
In order to more clearly illustrate the technical solutions in the embodiments of the present invention, the drawings needed to be used in the description of the embodiments will be briefly introduced below, and it is obvious that the drawings in the following description are only some embodiments of the present invention, and it is obvious for those skilled in the art to obtain other drawings based on these drawings without creative efforts.
FIG. 1 is a block flow diagram of a method for calibrating a standard flow meter for natural gas according to an embodiment of the invention;
FIG. 2 is a block flow diagram of a method for calibrating another type of standard natural gas flow meter provided by an embodiment of the invention;
fig. 3 is a schematic view illustrating an installation of the high-pressure gas storage device, the pressure boosting device and the pressure regulating device according to the embodiment of the present invention;
FIG. 4 is a schematic structural diagram of a high pressure gas storage device according to an embodiment of the present invention;
FIG. 5 is a schematic structural diagram of a first high pressure gas storage unit and a second high pressure gas storage unit according to an embodiment of the present invention;
fig. 6 is a schematic structural diagram of a pressure regulating device provided in an embodiment of the present invention;
FIG. 7 is a schematic structural diagram of a gas path corrosion prevention device provided in an embodiment of the present invention;
fig. 8 is a schematic structural diagram of a liquid path corrosion prevention device provided in an embodiment of the present invention.
FIG. 9 is a schematic structural diagram of a weighing apparatus according to an embodiment of the present invention;
FIG. 10 is a schematic structural diagram of a support assembly provided by an embodiment of the present invention;
FIG. 11 is a top view of a first sphere and three second spheres provided by an embodiment of the present invention;
FIG. 12 is a schematic diagram illustrating the positions between the centers of three second spheres provided by the embodiment of the present invention;
FIG. 13 is a diagram illustrating the force relationship between a first sphere and three second spheres provided by an embodiment of the present invention;
FIG. 14 is a schematic diagram illustrating the force relationship between three second spheres and three third spheres provided by the embodiment of the present invention;
FIG. 15 is a top view of a mobile docking unit provided in an embodiment of the present invention;
FIG. 16 is a top view of the mobile docking device with the first support unit positioned above the second support unit according to the embodiment of the present invention;
fig. 17 is a front view of a second supporting unit provided in the embodiment of the present invention;
fig. 18 is a plan view of a second supporting unit provided in the embodiment of the present invention;
FIG. 19 is a schematic diagram of a weighing tank of the type provided by embodiments of the present invention;
FIG. 20 is a schematic illustration of another type of weigh tank configuration provided by embodiments of the present invention before and after inflation;
FIG. 21 is a schematic structural view of a reversing valve assembly provided by an embodiment of the present invention.
Wherein the various reference numbers in the drawings are described below:
1-low pressure gas source;
2-a pressure boosting device;
3-high pressure gas storage device;
301-a first high pressure gas storage unit, 3011-a first solenoid valve, 3012-a second solenoid valve, 3013-a first pressure sensor, 301 a-a first inlet trunk line, 301 b-a first outlet trunk line, 301 c-a first gas branch line, 301 d-a first gas storage tank, 302-a second high pressure gas storage unit, 3021-a third solenoid valve, 3022-a fourth solenoid valve, 3023-a second pressure sensor, 302 a-a second inlet trunk line, 302 b-a second outlet trunk line, 302 c-a second gas branch line, 302 d-a second gas storage tank, 303 a first gas valve controller, 304-a second gas valve controller;
4-a pressure regulating device;
401-tank body, 4011-third pressure sensor, 4012-fifth electromagnetic valve, 4013-sixth electromagnetic valve, 402-third air valve controller;
5-a constant temperature device;
6-standard flow meter;
7-a reversing valve assembly;
701-a seventh electromagnetic valve, 702-an eighth electromagnetic valve;
8-a weighing device;
801-balance, 802-support component, 8021-upper support shaft, 8022-vertical force transfer component, 8022 a-housing, 8022 b-first sphere, 8022 c-second sphere, 8022 d-third sphere, 8022 e-top cover, 8023-lower support shaft, 8024-stiffener, 803-first support unit, 8031-limiting groove, 804-transmission unit, 805-second support unit, 8051-support platform, 8051 a-arc groove, 8052-fourth sphere, 806-driving unit, 807-weighing tank, 807 a-first weighing tank, 807 b-second weighing tank, 8071 a-first outer tank, 8071 b-second outer tank, 8072 a-first inner tank, 8072 b-second inner tank, 8073-vacuum gap layer, 8074 a-a first inflation inlet, 8074 b-a second inflation inlet, 8075-a mass compensation gap layer, 8076-a mass compensation pipe, 8077-a first anti-corrosion layer, 8078-a first sealing element, 808 balance chamber, 809 a-a main pipeline, 809 b-a first branch pipeline, 809 c-a second branch pipeline, 809 d-an inclined tee joint and 810-a weight;
9-low pressure gas storage device;
10-gas path anticorrosion device;
1001-desulfurization unit, 1002-buffer unit, 1003-dehydration unit, 1004-filtration unit, 1005-heating unit, 1006-condensation unit, 1007-conveying pipeline;
11-liquid path anticorrosion devices;
1101-a water storage unit, 1102-an inhalation unit, 1102 a-an inhalation pipeline, 1102 b-a first filter, 1102 c-a first valve body, 1102 d-a first check valve, 1103-an exhalation unit, 1103 a-an exhalation pipeline, 1103 b-a second filter, 1103 c-a second valve body, 1103 d-a second check valve, 1104-an inert gas supply unit;
12-a timer;
13-gas component analyzing apparatus.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, embodiments of the present invention will be described in detail with reference to the accompanying drawings.
The embodiment of the invention provides a calibration method of a natural gas standard flowmeter, which comprises the following steps:
step S1, the natural gas in the low-pressure gas source 1 is delivered to the pressurization device 2 and the gas path corrosion prevention device 10 to remove sulfur, moisture and solid particles in the natural gas, and pressurized to a first preset pressure.
And step S2, conveying the pressurized and impurity-removed natural gas to the high-pressure gas storage device 3, and conveying the pressurized and impurity-removed natural gas to the pressure regulating device 4 after the gas pressure of the high-pressure gas storage device 3 is a second preset pressure, so that the pressure of the pressurized and impurity-removed natural gas is regulated to be the same as the working pressure of the natural gas standard flowmeter 6.
And step S3, conveying the pressure-regulated natural gas into the constant temperature device 5, adjusting the temperature of the pressure-regulated natural gas to be the same as the working temperature of the natural gas standard flowmeter 6, and removing the non-inert gas in the cooling water flowing into the pressurizing device 2 and the constant temperature device 5 by using the liquid path anticorrosion device 11.
And step S4, conveying the natural gas after temperature adjustment to the natural gas standard flowmeter 6, and obtaining the measured flow value of the natural gas after temperature adjustment.
And step S5, conveying the temperature-regulated natural gas to the low-pressure gas storage device 9 from the second gas outlet of the reversing valve assembly 7, closing the second gas outlet of the reversing valve assembly 7 after the reading of the natural gas standard flowmeter 6 is stable, and opening the first gas outlet of the reversing valve assembly 7 to convey the temperature-regulated natural gas to the weighing tank 807 of the weighing device 8.
In step S6, the balance 801 of the weighing apparatus 8 acquires the inflation mass of the weighing tank 807, and the timer 12 acquires the inflation time of the weighing apparatus 8.
And step S7, calculating the actual flow value of the natural gas after temperature adjustment according to the inflation quality and the inflation time and by a quality-time method.
And step S8, comparing the actual flow value with the measured flow value, and calibrating the natural gas standard flowmeter 6.
Therefore, according to the calibration method of the natural gas standard flowmeter provided by the embodiment of the invention, the pressure of the natural gas is increased to be greater than the working pressure of the standard flowmeter 6 by using the supercharging device 2, and the gas with the same pressure as the working pressure can be conveyed into the standard flowmeter 6 by matching the high-pressure gas storage device 3 and the pressure regulating device 4, so that the calibration precision of the natural gas standard flowmeter 6 can be improved, the calibration of the natural gas standard flowmeter 6 under different working pressures can be met, and the application range is improved; through the matching of the gas path anticorrosion device 10 and the water path anticorrosion device, the anticorrosion treatment can be simultaneously carried out on the natural gas and the cooling water, the corrosion of the pressurization device 2, the high-pressure gas storage device 3, the pressure regulating device 4, the constant temperature device 5, the natural gas standard flowmeter 6, the reversing valve assembly 7 and the weighing tank 807 of the weighing device 8 is effectively reduced, the long-term stable operation of the devices is ensured, and the calibration precision of the natural gas standard flowmeter 6 can be improved; in addition, through the cooperation of the reversing valve assembly 7 and the timer 12, the inflation time of the weighing device 8 can be accurately measured, and the calibration precision of the natural gas standard flowmeter 6 can be further improved.
In summary, the calibration method for the natural gas standard flowmeter provided in the embodiment of the present invention can improve the calibration accuracy for the natural gas standard flowmeter 6, and can also expand the application range of the calibration method.
The following describes the steps of the calibration method for the natural gas standard flowmeter provided by the embodiment of the invention:
in step S1, the natural gas in the low-pressure gas source 1 may be pressurized to a first preset pressure by the pressurization device 2, and then the sulfur, moisture, and solid particles in the pressurized natural gas may be removed by the gas path corrosion prevention device 10. Or firstly removing sulfur, moisture and solid particles in the natural gas in the low-pressure gas source by using the gas path corrosion prevention device 10, and then pressurizing the natural gas after impurity removal to a first preset pressure by using the pressurizing device 2. Correspondingly, the gas path corrosion prevention device 10 is disposed between the pressurization device 2 and the high-pressure gas storage device 3 (see fig. 1), or disposed between the low-pressure gas source 1 and the pressurization device 2 (see fig. 2).
It should be noted that the first preset pressure is greater than the operating pressure of the natural gas standard flowmeter 6, where the operating pressure of the natural gas standard flowmeter 6 is the ambient pressure in which the natural gas standard flowmeter 6 operates.
Wherein, the low-pressure gas source 1 can be a low-pressure storage tank.
The above-mentioned supercharging device 2 comprises at least one centrifugal gas compressor. In practical application, the discharge capacity of the centrifugal compressor can be calculated according to the volume of the high-pressure gas storage device 3, and the model of the centrifugal gas compressor is selected; in addition, the number of the centrifugal gas compressors can be selected according to the natural gas flow rate detectable by the natural gas standard flow meter 6 so as to meet the requirements of pressurization time and maximum operation cost saving.
In the embodiment of the present invention, sulfur, moisture, and solid particles in the natural gas may be removed by the following method, specifically, the natural gas is conveyed to the desulfurization unit 1001 of the gas path corrosion prevention device 10 to remove sulfur in the natural gas.
And conveying the desulfurized natural gas to the buffer unit 1002 of the gas path corrosion prevention device 10 for temporary storage.
The desulfurized natural gas passes through the dehydration unit 1003 of the gas path corrosion prevention device 10 from top to bottom to adsorb moisture in the desulfurized natural gas.
And conveying the dehydrated natural gas to a filtering unit 1004 of the gas path corrosion prevention device 10, removing solid particles in the dehydrated natural gas, and discharging a part of the natural gas from which the solid particles are removed.
Accordingly, as shown in fig. 7, the gas path corrosion prevention device 10 includes: a desulfurization unit 1001, a buffer unit 1002, a dehydration unit 1003, and a filtration unit 1004 which are sequentially communicated through a pipeline; the desulfurization unit 1001 is communicated with the low-pressure gas source 1 or the supercharging device 2 and is used for removing sulfur in natural gas; the dehydration unit 1003 is used for enabling the desulfurized natural gas to pass through from top to bottom so as to adsorb moisture in the desulfurized natural gas; the filtering unit 1004 is used for removing solid particles from the dehydrated natural gas and conveying a part of the natural gas from which the solid particles are removed to the pressurizing device 2 or the high-pressure gas storage device 3.
Further, in order to prolong the service life and the treatment effect of the gas path corrosion prevention device 10, the method for removing sulfur, moisture and solid particles in the natural gas further comprises: and heating another part of the natural gas with the solid particles removed to a first preset temperature by using the heating unit 1005 of the gas path corrosion prevention device 10, and enabling the heated natural gas to pass through the dehydration unit 1003 from bottom to top so as to analyze the moisture absorbed by the dehydration unit 1003.
The condensation unit 1006 of the gas path corrosion prevention device 10 cools the moisture generated during the desorption in the dehydration unit 1003 to separate another part of the natural gas from which the solid particles are removed.
Correspondingly, as shown in fig. 7, the gas path corrosion prevention device 10 further includes: a heating unit 1005 disposed between the filtering unit 1004 and the dehydration unit 1003, and a condensation unit 1006 communicating with the dehydration unit 1003; the heating unit 1005 is used for heating another part of the natural gas from which the solid particles are removed to a first preset temperature, and enabling the heated natural gas to pass through the dehydration unit 1003 from bottom to top so as to analyze moisture absorbed by the dehydration unit 1003; the condensing unit 1006 is used for cooling the moisture generated by the desorption of the dehydration unit 1003 to separate another part of the natural gas from which the solid particles are removed.
Through setting up as above, when utilizing gas circuit anticorrosive device 10 to treat the gas that awaits measuring, the gas that awaits measuring flows out by low-pressure gas source 1 or supercharging device 2, flows into in desulfurization unit 1001 to get rid of the sulphur in the natural gas, and the natural gas after the desulfurization flows into in buffer unit 1002, stores temporarily. Then, the desulfurized natural gas passes through the dehydration unit 1003 from top to bottom, so that the dehydration unit 1003 is used to adsorb moisture in the desulfurized natural gas. The dehydrated natural gas then flows into the filtering unit 1004 to remove solid particles in the dehydrated natural gas, such as the dehydrating agent in the dehydrating unit 1003. Wherein, a part of the natural gas from which the solid particles are removed flows into the supercharging device 2 or the high-pressure gas storage unit; the other part of the natural gas from which the solid particles are removed flows into the heating unit 1005 to be heated to a first preset temperature (for example, 200 ℃ to 350 ℃), and the heated natural gas passes through the dehydration unit 1003 from bottom to top to resolve the moisture adsorbed by the dehydration unit 1003, that is, the heated natural gas is used to change the moisture adsorbed by the dehydration unit 1003 into steam, and the steam is mixed with the heated natural gas. Then, the water vapor and the heated natural gas flow into the condensing unit 1006, and the water vapor (i.e., the moisture generated by the analysis in the dehydrating unit 1003) is cooled by the condensing unit 1006 to be condensed into liquid water, thereby realizing the separation of the water vapor and the heated natural gas. Wherein, the condensed steam can be discharged to a sewage pipe, and the heated natural gas can be discharged to a low-pressure pipe network.
As an example, the desulfurization unit 1001 includes: the desulfurizer bed layer is arranged in the shell; the shell is provided with a top opening and a bottom opening, the top opening is communicated with the low-pressure air source 1 or the supercharging device 2, and the bottom opening is communicated with the buffer unit 1002.
It is understood that the desulfurized natural gas can enter the desulfurization unit 1001 through the top opening of the housing and exit through the bottom opening of the housing; similarly, heated natural gas enters the desulfurization unit 1001 through the bottom opening of the housing and exits through the top opening of the housing.
The desulfurizer bed layer is a zinc oxide bed layer, and by the arrangement, sulfur in the natural gas to be detected can be effectively removed, and the operation cost of the natural gas purification device can be reduced.
In addition, in a possible embodiment, as shown in fig. 7, a conveying pipeline 1007 is further provided between the bottom opening of the desulfurization unit 1001 and the heating unit 1005 for conveying a part of the desulfurized natural gas into the heating unit 1005 to resolve moisture adsorbed by the dehydration unit 1003.
By the arrangement, the problem that the flow rate of the natural gas which flows through the heating unit 1005 and is subjected to solid particle removal is too small due to blockage of the pipeline between the heating unit 1005 and the filtering unit 1004, and the water adsorbed by the dehydration unit 1003 cannot be effectively analyzed can be avoided.
In order to analyze the dehydration unit 1003 and not affect the adsorption of the moisture in the desulfurized natural gas, in the embodiment of the present invention, the dehydration unit 1003 includes: a plurality of adsorption columns; the top openings of the adsorption towers are respectively communicated with the buffer unit 1002 and the condensation unit 1006, and the bottom openings of the adsorption towers are respectively communicated with the heating unit 1005 and the filtering unit 1004; and reversing valves are arranged on the top opening and the bottom opening of the adsorption tower.
It can be understood that the above-mentioned reversing valve can control the fluid flow direction in the adsorption tower, and can make the desulfurized natural gas pass through the adsorption tower from top to bottom, or make the heated natural gas pass through the adsorption tower from bottom to top. And the working states of a part of the adsorption towers are opposite to the working states of the rest of the adsorption towers, namely, the part of the adsorption towers are in an adsorption state and the rest of the adsorption towers are in an analysis state by controlling respective reversing valves; after the preset time, a part of the absorption towers are adjusted from the adsorption state to the analysis state, and the rest of the absorption towers are adjusted from the analysis state to the adsorption state.
The number of adsorption towers may be 2 to 4, for example, 2, 3, or 4, and this arrangement makes it possible to efficiently adsorb moisture in the desulfurized natural gas while analyzing the dehydration unit 1003, and also makes it easy to control the flow direction of the fluid in each adsorption tower in the dehydration unit 1003.
In addition, the adsorption tower can be a molecular sieve adsorption tower, and specifically, the molecular sieve of the adsorption tower can be a 4A type molecular sieve.
The molecular sieve adsorption tower has strong adsorption selectivity and higher adsorption capacity, and can prolong the service life of the molecular sieve. In addition, this type of molecular sieve is not easily destroyed by liquid water.
In order to avoid that the temperature of the desorbed dehydration unit 1003 is too high to effectively adsorb the moisture in the desulfurized natural gas of the next round, in the embodiment of the present invention, the heating unit 1005 is further configured to heat the natural gas, from which the solid particles are removed, to the second preset temperature, and make the heated natural gas pass through the dehydration unit 1003 from bottom to top, so as to cool the dehydration unit 1003 after desorption of the moisture.
It should be noted that the natural gas after being treated by the filtering unit 1004 and being subjected to moisture removal is divided into three parts, one part is conveyed to the pressure boosting device 2 or the high-pressure low-pressure gas source 1, the other part is conveyed to the heating unit 1005 until being heated to the first preset temperature, and the rest part is conveyed to the heating unit 1005 until being heated to the second preset temperature.
The first predetermined temperature is 200 to 350 ℃, for example, 200 ℃, 250 ℃, 300 ℃, 350 ℃ and the like, in order to effectively analyze the dehydration unit 1003.
Based on the setting of the first preset temperature, in order to perform effective analysis on the dehydration unit 1003, the analysis time of the dehydration unit 100313 may be set to 2h to 6h, for example, specifically set to 2h, 3h, 4h, 5h, 6h, and the like.
In addition, the second predetermined temperature may be less than or equal to 20 ℃, for example, 20 ℃, 18 ℃, 16 ℃, 14 ℃, 12 ℃, 10 ℃ and the like may be set. By the above arrangement, the temperature of the dehydration unit 1003 after the analysis can be effectively reduced.
Wherein, the heating unit 1005 can be arranged as a tubular heat exchanger, and the heating unit 1005 is easy to obtain and has low price. Specifically, the natural gas from which the solid particles are removed passes through the shell side of the tubular heat exchanger, and the heat source passes through the tube side of the tubular heating unit 1005.
In addition, the filtering unit 1004 may be an apparatus structure provided with a plurality of filtering membranes, and the condensing unit 1006 may be a tube heat exchanger.
In order to effectively analyze the heated natural gas in the dehydration unit 1003 and effectively cool the analyzed dehydration unit 1003, a temperature sensor and a display electrically connected with the temperature sensor are arranged on a pipeline between the dehydration unit 1003 and the heating unit 1005 in the embodiment of the invention; the temperature sensor is used for acquiring the temperature information of the heated natural gas and transmitting the temperature information to the display; the display is used for displaying temperature information. By the above arrangement, the temperature of the heated natural gas entering the dehydration unit 1003 can be effectively adjusted.
In order to further enable the heated natural gas to effectively analyze the dehydration unit 1003 and effectively cool the analyzed dehydration unit 1003, in the embodiment of the present invention, a flow meter is further disposed on the pipeline between the dehydration unit 1003 and the heating unit 1005 for measuring the flow rate of the heated natural gas flowing into the dehydration unit 1003.
Wherein the flow rate of the heated natural gas can be controlled to 500Nm3/h～700Nm3H, preferably 600Nm3H is used as the reference value. The flowmeter can be an orifice plate flowmeter, and the natural gas flow measured by the flowmeter can be uploaded to the flow indicator, so that an operator can observe whether the flow of the regenerated gas is in a proper range.
In the embodiment of the invention, the related pipelines are provided with valves so as to ensure the safety of operation.
After the natural gas to be detected is treated by the gas path corrosion prevention device 10 provided by the embodiment of the invention, H is2S content less than 5.7mg/m3(even not higher than 4 mg/m)3) And the water dew point can be below-60 ℃ (even below-65 ℃).
In step S2, in order to continuously convey the pressurized and impurity-removed natural gas into the high-pressure gas storage device 3, the pressurized and impurity-removed natural gas may be conveyed into the high-pressure gas storage device 3 by the following method, specifically, the pressurized and impurity-removed natural gas is conveyed into the first high-pressure gas storage unit 301 or the second high-pressure gas storage unit 302 of the high-pressure gas storage device 3, and the pressurized and impurity-removed natural gas of the second preset pressure is alternately conveyed into the pressure regulating device 4 by the first high-pressure gas storage unit 301 and the second high-pressure gas storage unit 302.
The pressurized and purified natural gas can be alternately conveyed into the pressure regulating device 4 by a method that the first pressure sensor 3013 is used to obtain the gas pressure information of the first high-pressure gas storage unit 301 and transmit the gas pressure information to the first gas valve controller 303, and the second pressure sensor 3023 is used to obtain the gas pressure information of the second high-pressure gas storage unit 302 and transmit the gas pressure information to the second gas valve controller 304.
If the gas pressure of the first high-pressure gas storage unit 301 is smaller than the second preset pressure and the gas pressure of the second high-pressure gas storage unit 302 is greater than or equal to the second preset pressure, the first gas valve controller 303 is utilized to open the inlet of the first high-pressure gas storage unit 301 and the outlet of the second high-pressure gas storage unit 302 so as to convey the natural gas after the pressurization and impurity removal to the first high-pressure gas storage unit 301 and convey the natural gas after the pressurization and impurity removal in the second high-pressure gas storage unit 302 to the pressure regulating mechanism,
if the gas pressure of the first high-pressure gas storage unit 301 is greater than or equal to the second preset pressure and the gas pressure of the second high-pressure gas storage unit 302 is less than the second preset pressure, the second gas valve controller 304 is used to open the outlet of the first high-pressure gas storage unit 301 and the inlet of the second high-pressure gas storage unit 302 so as to convey the natural gas after the pressurization and impurity removal to the second high-pressure gas storage unit 302 and convey the natural gas after the pressurization and impurity removal in the first high-pressure gas storage unit 301 to the pressure regulating device 4.
In the embodiment of the present invention, a first solenoid valve 3011 may be disposed at the inlet of the first high pressure gas storage unit 301, and a second solenoid valve 3012 may be disposed at the outlet of the first high pressure gas storage unit 301, so as to automatically control the opening and closing of the inlet and outlet of the first high pressure gas storage unit 301; similarly, a third solenoid valve 3021 may be provided at the inlet of the second high pressure gas storage unit 302, and a fourth solenoid valve 3022 may be provided at the outlet thereof, so as to automatically control the opening and closing of the inlet and outlet of the second high pressure gas storage unit 302.
Accordingly, as shown in fig. 3 and fig. 4, the high pressure gas storage apparatus 3 includes: the inlet of the first high-pressure gas storage unit 301 is communicated with the supercharging device 2 or the gas path anticorrosion device 10, the outlet of the first high-pressure gas storage unit 301 is communicated with the pressure regulating device 4, the inlet and the outlet of the first high-pressure gas storage unit 301 are respectively provided with a first electromagnetic valve 3011 and a second electromagnetic valve 3012, and the first high-pressure gas storage unit 301 is also provided with a first pressure sensor 3013; a second high-pressure gas storage unit 302 with an inlet communicated with the supercharging device 2 or the gas path corrosion prevention device 10 and an outlet communicated with the pressure regulating device 4, wherein the inlet and the outlet of the second high-pressure gas storage unit 302 are respectively provided with a third electromagnetic valve 3021 and a fourth electromagnetic valve 3022, and the second high-pressure gas storage unit 302 is also provided with a second pressure sensor 3023; the first air valve controller 303 is electrically connected with the first electromagnetic valve 3011, the fourth electromagnetic valve 3022 and the first pressure sensor 3013, and is configured to receive the gas pressure information of the first high-pressure gas storage unit 301 transmitted by the first pressure sensor 3013, and control the opening and closing of the first electromagnetic valve 3011 and the fourth electromagnetic valve 3022 according to the gas pressure information of the first high-pressure gas storage unit 301; the second gas valve controller 304, which is electrically connected to the second solenoid valve 3012, the third solenoid valve 3021 and the second pressure sensor 3023, is configured to receive the gas pressure information of the second high pressure gas storage unit 302 transmitted by the second pressure sensor 3023, and control the opening and closing of the second solenoid valve 3012 and the third solenoid valve 3021 according to the gas pressure information of the second high pressure gas storage unit 302.
It can be understood that the inlet of the first high-pressure gas storage unit 301 is communicated with the supercharging device 2, and the outlet of the first high-pressure gas storage unit 301 is communicated with the pressure regulating device 4; the inlet of the second high-pressure gas storage unit 302 is communicated with the supercharging device 2, and the outlet of the second high-pressure gas storage unit 302 is communicated with the pressure regulating device 4. A first electromagnetic valve 3011 is arranged at the inlet of the first high-pressure gas storage unit 301, and a second electromagnetic valve 3012 is arranged at the outlet of the first high-pressure gas storage unit 301; a third electromagnetic valve 3021 is disposed at an inlet of the second high pressure gas storage unit 302, and a fourth electromagnetic valve 3022 is disposed at an outlet of the second high pressure gas storage unit 302.
Further, in order to meet the measurement and calibration requirements of the standard flow meter 6 with different detectable flow ranges, in the embodiment of the present invention, as shown in fig. 5, the first high pressure gas storage unit 301 includes: a first inlet trunk line 301a, a first outlet trunk line 301b, a plurality of first gas branch lines 301c, a plurality of first gas tanks 301 d; the first air intake trunk line 301a is communicated with the supercharging device 2, and the first air intake trunk line 301a is also provided with a first electromagnetic valve 3011; the first air outlet trunk line 301b is communicated with the pressure regulating device 4, and the first air outlet trunk line 301b is also provided with a second electromagnetic valve 3012; a plurality of first gas branch lines 301c are arranged in parallel between the first inlet trunk line 301a and the first outlet trunk line 301 b; the inlet and outlet of the first air storage tank 301d are communicated with the corresponding first gas branch line 301c, and the inlet and outlet of the first air storage tank 301d are respectively provided with a manual valve; and, a first pressure sensor 3013 is disposed on at least one first air tank 301 d.
Through the arrangement, the number of the first air storage tanks 301d which run on line, namely the number of the first air storage tanks 301d with the inlets communicated with the supercharging device 2 and the outlets communicated with the pressure regulating device 4 can be determined according to the flow range detectable by the natural gas standard flow meter 6, so that the volume of the first high-pressure air storage unit 301 can be changed.
It should be noted that the inlet and outlet of each first air tank 301d are in the same working state, for example, in the open state at the same time, or in the closed state at the same time. Moreover, the inlet and outlet of each first air storage tank 301d are only communicated with the same first air branch line 301 c.
The number of the first air tanks 301d may be 3 to 10, for example, 3, 4, 5, 6, 7, 8, 9, or 10.
In addition, at least one first air tank 301d may be provided with the first pressure sensor 3013, for example, one first air tank 301d may be provided with the first pressure sensor 3013, or each first air tank 301d may be provided with the first pressure sensor 3013, or the like. Note that the pressure of the natural gas in each first storage tank 301d is the same.
Similarly, in order to meet the measurement and calibration requirements of the standard natural gas flow meter 6 with different detectable flow ranges, in the embodiment of the present invention, as shown in fig. 5, the second high pressure gas storage unit 302 includes: a second inlet trunk line 302a, a second outlet trunk line 302b, a plurality of second gas branch lines 302c, a plurality of second gas tanks 302 d; the second intake trunk line 302a is communicated with the supercharging device 2, and the second intake trunk line 302a is also provided with a third electromagnetic valve 3021; the second air outlet trunk line 302b is communicated with the pressure regulating device 4, and a fourth electromagnetic valve 3022 is further arranged on the second air outlet trunk line 302 b; a plurality of second gas branch lines 302c are disposed in parallel between second inlet trunk line 302a and second outlet trunk line 302 b; the inlet and outlet of the second gas storage tank 302d are communicated with the corresponding second gas branch line 302c, and the inlet and outlet of the second gas storage tank 302d are respectively provided with a manual valve; and, a second pressure sensor 3023 is provided to at least one second air tank 302 d.
Through the arrangement, the number of the second air storage tanks 302d which are operated online, namely the number of the second air storage tanks 302d with the inlets communicated with the supercharging device 2 and the outlets communicated with the pressure regulating device 4, can be determined according to the flow range detectable by the standard flow meter 6, so that the volume of the second high-pressure air storage unit 302 can be changed.
It should be noted that the inlet and outlet of each second air tank 302d are in the same working state, for example, in the open state at the same time, or in the closed state at the same time. And, the inlet and outlet of each second air container 302d are connected to the same second gas branch line 302 c.
The number of the second air tanks 302d may be 3 to 10, for example, 3, 4, 5, 6, 7, 8, 9, or 10.
In addition, a second pressure sensor 3023 may be provided in at least one of the second air tanks 302d, for example, a second pressure sensor 3023 may be provided in one of the second air tanks 302d, or a second pressure sensor 3023 may be provided in each of the second air tanks 302 d. Note that the pressure of the natural gas in each second gas tank 302d is the same.
According to the embodiment of the invention, the pressure of the natural gas after pressurization and impurity removal is adjusted to the working pressure of the natural gas standard flowmeter 6 by the following method, specifically, the natural gas after pressurization and impurity removal in the high-pressure gas storage device 3 is conveyed into the pressure regulating tank 401 of the pressure regulating device 4.
The third pressure sensor 4011 is used to obtain information on the gas pressure in the surge tank 401, and transmit the information to the third gas valve controller 402.
If the gas pressure of the pressure regulating tank 401 is higher than the working pressure, the vent of the pressure regulating tank 401 is opened by using the third gas valve controller 402 to discharge the pressurized and impurity-removed natural gas in the pressure regulating tank 401 until the gas pressure of the pressure regulating tank 401 is equal to the working pressure.
A fifth electromagnetic valve 4012 can be arranged at the vent of the pressure regulating tank 401, so that the third air valve controller 402 controls the opening and closing of the vent; in addition, a sixth solenoid valve 4013 may be provided at an outlet of the pressure regulating tank 401, so that the third gas valve controller 32 controls whether the pressure regulating mechanism 3 delivers the pressure-regulated natural gas into the natural gas standard flowmeter 6.
Correspondingly, as shown in fig. 6, the pressure regulating device 4 includes: a tank 401 with an inlet communicated with the high-pressure gas storage device 3 and an outlet communicated with the constant temperature device 5; a third pressure sensor 4011 provided on can 401; the fifth electromagnetic valve 4012 is arranged at the emptying port of the tank body 401, and the fifth electromagnetic valve 4012 is used for discharging the pressurized gas to be detected in the tank body 401; a sixth solenoid valve 4013 disposed at an outlet of the tank 401; and the third gas valve controller 402 is respectively connected with the third pressure sensor 4011, the fifth solenoid valve 4012 and the sixth solenoid valve 4013, and is configured to receive the gas pressure information of the tank 401 transmitted by the third pressure sensor 4011, and control the opening and closing of the fifth solenoid valve 4012 and the sixth solenoid valve 4013 according to the gas pressure information of the tank 401.
Wherein, the bottom of the tank 401 is provided with an evacuation port, and a fifth electromagnetic valve 4012 is installed at the evacuation port.
Based on pressure regulating device 4 of above-mentioned structure, in order to improve and carry out cyclic utilization to the gas that discharges out, as shown in figure 6, the evacuation mouth of jar body 4011 accessible pipeline communicates with the import of low pressure gas storage device 9.
For step S3, the thermostat 5 may be a shell-and-tube heat exchanger. Wherein, the tube pass inlet of the constant temperature device 5 is connected with the air outlet of the pressure regulating device 4, and the tube pass outlet is communicated with the standard flowmeter 6; and a shell pass inlet of the constant temperature device 5 is communicated with a cooling water source, and a shell pass outlet is used for discharging cooling water.
It should be noted that the operating temperature of the natural gas standard flowmeter 6 refers to the temperature of the environment in which the natural gas standard flowmeter 6 operates.
In the embodiment of the present invention, the non-inert gas in the cooling water flowing into the pressure boosting device 2 and the thermostat device 5 may be removed by, specifically, feeding the cooling water to the water storage unit 1101 of the liquid path corrosion prevention device 11, and simultaneously sucking the inert gas in the inert gas supply unit 1104 of the liquid path corrosion prevention device 11 into the water storage unit 1101 by the suction unit 1102 of the liquid path corrosion prevention device 11.
Under the action of the pressure difference, the non-inert gas in the water storage unit 1101 is discharged from the exhalation unit 1103 of the liquid path corrosion prevention device 11, so as to convert the non-inert gas in the cooling water in the water storage unit 1101 into an inert gas.
Correspondingly, as shown in fig. 8, the liquid path corrosion prevention device 11 includes: a water storage unit 1101, an inhalation unit 1102, an exhalation unit 1103, an inert gas supply unit 1104; a water inlet and a water outlet are formed in the water storage unit 1101, and the water outlet of the water storage unit 1101 is communicated with the pressurization device 2 and the constant temperature device 5 at the same time; the inhalation unit 1102 and the exhalation unit 1103 are both communicated with the top wall of the water storage unit 1101, and the inhalation unit 1102 is communicated with the inert gas supply unit 1104; the non-inert gas in the water storage unit 1101 is exhausted by the exhalation unit 1103.
With the above arrangement, when the coolant for cooling the pressurizer 2 and the thermostat 5 is treated by the waterway preservative device, the coolant is first supplied through the water inlet of the water storage unit 1101, and at the same time, the inert gas (e.g., nitrogen gas or argon gas) supply unit is controlled to supply the inert gas into the water storage unit 1101 through the air suction unit 1102. Under the action of the pressure difference, the non-inert gas in the water storage unit 1101 is discharged from the exhalation unit 1103, so that the non-inert gas in the cooling water in the water storage unit 1101 is converted into inert gas. The cooling water treated by the non-inert gas is conveyed into the supercharging device 2 (such as a centrifugal gas compressor) and the thermostatic device 5 (such as a heat exchange device) through the water outlet of the water storage unit 1101, so that the cooling water can be favorably used in a natural gas flow primary standard device, the cooling water cannot cause corrosion of pipelines or equipment, and an anti-corrosion effect is achieved.
As an example, as shown in fig. 8, the water inlet of the water storage unit 1101 is higher than the water outlet of the water storage unit 1101; and, the water inlet of the water storage unit 1101 and the water outlet of the water storage unit 1101 are located at both sides of the water storage unit 1101.
By such an arrangement, a difference exists between the cooling water input into the water storage unit 1101 and the cooling water output from the water storage unit 1101, which is beneficial for the non-inert gas (non-inert gas) in the cooling water to be exhausted from the exhalation unit 1103 under the action of air pressure.
The water storage unit 1101 may be a water storage tank.
In addition, the water storage unit 1101 may perform non-inert gas treatment on the cooling water, and may also perform treatment on other water bodies, such as soft water, oil well produced water, domestic water, and the like.
Considering that the pressure difference may cause the cooling water in the water storage unit 1101 to be output by the air suction unit 1102 and even damage the inert gas supply unit 1104, as shown in fig. 8, the air suction unit 1102 includes: an intake pipe 1102a, a first check valve 1102 d; a first end of the air suction pipe line 1102a communicates with the water storage unit 1101, and a second end communicates with the inert gas supply unit 1104; a first check valve 1102d is disposed on the suction line 1102 a.
The first check valve 1102d allows the suction unit 1102 to introduce the inert gas from the inert gas supply unit 1104 into the water storage unit 1101 through the suction line 1102a without causing a fluid such as gas or liquid to flow in the reverse direction.
The inert gas supply unit 1104 may be an inert gas tank, for example, a tank filled with an inert gas such as nitrogen and/or argon.
In order to efficiently input the inert gas into the cooling water, the gas suction pipe 1102a may extend into the inner cavity of the water storage unit 1101, or even into the cooling water, so as to blow the inert gas into the cooling water, and further to discharge the non-inert gas (such as oxygen) in the cooling water, thereby preventing the non-inert gas in the cooling water from reacting with other pipes or devices to cause corrosion.
The first end of the gas suction line 1102a may be provided with a first filter 1102b in consideration that solid impurities in the water storage unit 1101 may enter the inert gas supply unit 1104, or solid impurities and the like in the inert gas supply unit 1104 may enter the water storage unit 1101.
In order to facilitate the control of the frequency of the inert gas supply unit 1104 inputting the inert gas into the water storage unit 1101, as shown in fig. 8, the gas suction pipe 1102a may be further provided with a first valve 1102 c.
Under the action of the pressure difference, the phenomenon of air suction of the exhalation unit 1103 inevitably occurs, and the treatment effect of the corrosion prevention device for detecting the natural gas flow on the cooling water is influenced. To solve this problem, as shown in fig. 8, the exhalation unit 1103 includes: an expiration pipeline 1103a with one end communicated with the water storage unit 1101, and a second check valve 1103d arranged on the expiration pipeline 1103 a.
The second check valve 1103d allows the exhalation unit 1103 to output the non-inert gas from the water storage unit 1101, and prevents the fluid such as gas or liquid from flowing backward into the water storage unit 1101.
Further, in order to prevent external solid impurities from entering the water storage unit 1101 through the exhalation line 1103a, as shown in fig. 8, a second filter 1103b is disposed at one end of the exhalation line 1103 a.
In view of being able to conveniently control the exhalation unit 1103 and the inhalation unit 1102 to work alternately to efficiently discharge the non-inert gas in the water storage unit 1101, as shown in fig. 8, the exhalation line 1103a is provided with a second valve body 1103 c.
In view of being able to easily control the exhalation unit 1103 and the inhalation unit 1102 to alternately operate, the first valve body 1102c and the second valve body 1103c may be manual valves to facilitate the operation.
In the embodiment of the present invention, the first filter member 1102b and the second filter member 1103b may be configured in various structures, and both the first filter member 1102b and the second filter member 1103b are filter nets based on simple structure and easy access.
In step S4, the components of the temperature-adjusted natural gas may be analyzed by the gas component analyzing device 13 before the temperature-adjusted natural gas is sent to the natural gas standard flowmeter 6.
Through so setting up, the content (for example) of the harmful substance in the measurable quantity gas of waiting to detect, and then can judge the treatment effect of gas circuit anticorrosive device 10, can in time change, maintain gas circuit anticorrosive device 10.
The gas component analyzing device 13 may be a natural gas chromatograph.
In addition, the natural gas standard flowmeter 6 can be a venturi flowmeter, and the flowmeter has the characteristics of high measurement accuracy and high stability.
With respect to step S5, the calibration method further includes: and conveying the temperature-regulated natural gas in the low-pressure gas storage device 9 to the low-pressure gas source 1 so as to recycle the temperature-regulated natural gas.
It can be understood that the air outlet of the low-pressure air storage device 9 is communicated with the air inlet of the low-pressure air source 1 through a conveying pipeline.
An example is given in the embodiment of the present invention with respect to the structure of a weighing apparatus 8, as shown in fig. 9, the weighing apparatus 8 including: a balance 801, a support assembly 802, a first support unit 803, a transfer unit 804, a second support unit 805, a drive unit 806, weights 810, a weighing tank 807, and a balance chamber 808; balance 801, support assembly 802, weight 810, and weigh tank 807 are located within balance chamber 808; the support assembly 802 includes: an upper support shaft 8021, a vertical force transmission member 8022, and a lower support shaft 8023 (see fig. 10) connected in sequence from top to bottom; the upper support shaft 8021 is connected with the lower end of the balance 801, and the upper end and the lower end of the vertical force transmission piece 8022 are respectively movably connected with the lower end of the upper support shaft 8021 and the upper end of the lower support shaft 8023; the weight 810 is used for matching with the balance 801 to weigh the weighing tank 807; the first supporting unit 803 and the second supporting unit 805 are respectively arranged at the first end and the second end of the transmission unit 804, the first end of the transmission unit 804 is close to the balance 801, and the second end of the transmission unit 804 is close to the reversing valve assembly 7; the first supporting unit 803 is used for bearing a weighing tank 807, the transmission unit 804 is used for transmitting the first supporting unit 803 and the weighing tank 807 to the upper end of the second supporting unit 805, and the second supporting unit 805 is used for supporting the first supporting unit 803 and the weighing tank 807; the driving unit 806 is used for driving the second supporting unit 805 to move up and down and rotate until the weighing tank 807 is in stress-free butt joint with the first air outlet of the reversing valve assembly 7.
With the above arrangement, when the weighing tank 807 is inflated, the weighing tank 807 is fixed to the first supporting unit 803, and the first supporting unit 803 is transferred above the second supporting unit 805 by the transferring unit 804. The second supporting unit 805 is driven to ascend by the driving unit 806 to support the first supporting unit 803 and the weighing pot 807. The second supporting unit 805 is driven to rotate by the driving unit 806 until the weighing tank 807 is in stress-free abutment with the first air outlet of the reversing valve assembly 7 and is connected by a flange. And when the weighing tank 807 starts to be inflated, the timer 12 is started to count time, and when the weighing tank 807 stops being inflated, the timer 12 is stopped to count time.
After the air inflation is finished, the second supporting unit 805 is driven to move by the driving unit 806, so that the weighing tank 807 is separated from the first air outlet of the reversing valve assembly 7. The second supporting unit 805 is driven to descend by the driving unit 806, so that the first supporting unit 803 is positioned on the transferring unit 804. The first supporting unit 803 is transferred to the first end of the transfer unit 804 through the transfer unit 804, the weighing tank 807 and the first supporting unit 803 are placed on the balance 801, and the natural gas in the weighing tank 807 is weighed by adjusting the weight 810.
In the weighing process, after the weighing tank 807 and the first supporting unit 803 are placed on the balance 801, the balance 801 sequentially transfers the force to the upper supporting shaft 8021, the vertical force transfer member 8022, and the lower supporting shaft 8023. Because the upper supporting shaft 8021, the vertical force transmission piece 8022 and the lower supporting shaft 8023 are movably connected from top to bottom in sequence, the gravity of the balance 801 is favorably enabled to fall on the same supporting point on the supporting component 802, the pressure direction of the balance 801 on the supporting point is favorably kept parallel to the gravity center line of the weight 810, accurate weighing is favorably realized, and the uncertainty of mass measurement is reduced.
In the embodiment of the present invention, the balance 801 may be an equiarm balance 801, and the working principle of the balance 801 is weighing by using an alternative method.
In embodiments of the present invention, the vertical force transfer member 8022202 may be provided in a variety of forms. Given the constant position of the vertical force transfer member 8022202 on the support point of balance 8011, and the simplicity of construction, the following examples are given:
as an example, as shown in fig. 10, the vertical force transfer member 8022 includes: a housing 8022a, and a first sphere 8022b, three second spheres 8022c, and a third sphere 8022d of equal diameter; the first sphere 8022b, the second sphere 8022c and the third sphere 8022d2024 are rotatably but non-rollably disposed in the housing 8022 a; the three second spheres 8022c are arranged on the same horizontal plane; the first sphere 8022b and the third sphere 8022d are disposed above and below the three second spheres 8022c, respectively, and an included angle formed by a connection line between the center of the first sphere 8022b and the centers of the three second spheres 8022c is 120 ° (see fig. 11). The lower end of the upper support shaft 8021 is provided with a first concave surface, and the first sphere 8022b is rotatably limited in the first concave surface; the upper end of the lower support shaft 8023 is provided with a second concave surface, and the third sphere 8022d is rotatably limited in the second concave surface.
It can be understood that, since the centers of the first spheres 8022b and the connecting lines between the centers of the three second spheres 8022c form an included angle of 120 °, the first sphere 8022b is located right above the center between the three second spheres 8022c, and the third sphere 8022d is located right below the center between the three second spheres 8022 c.
It should be noted that the centers of gravity of the upper support shaft 8021, the first sphere 8022b, the third sphere 8022d, and the lower support shaft 8023 are on the same vertical line.
In fig. 12, Q1, Q2, and Q3 respectively indicate the spherical centers (gravity centers) of the three second spheres 8022 d. The three sphere centers are connected to form a triangle, and since the diameters of the three second spheres 8022d are equal and are arranged in a tangent manner on the same horizontal plane, the included angle formed by the centers of the three second spheres 8022d and the connecting line of the three sphere centers is 120 degrees.
With the above arrangement, when the weighing pot 807 is carried on the balance 801, the weighing pot 807 transmits force to the balance 801, and the balance 801 transmits force F to the upper support shaft 8021. Since the first ball 8022b can rotate but does not roll and is limited in the first concave surface of the lower end of the upper support shaft 8021, the upper support shaft 8021 can stably and vertically transmit force to the first ball 8022 b. Analysis of the force between the first sphere 8022b and the three second spheres 8022c as shown in fig. 13, when the first sphere 8022b is pressed vertically downward by the balance 801, the three second spheres 8022c will be pressed by forces F1, F2 and F3 with the same magnitude. Through the force transmission among the three second spheres 8022c, as shown in fig. 14, the three second spheres 8022c transmit forces F1, F2 and F3 with the same magnitude to the third sphere 8022d, and the third sphere 8022d also receives a downward force F. Since the third ball 8022d can rotate but does not roll and is restrained in the second concave surface of the upper end of the lower support shaft 8023, the third ball 8022d can stably and vertically transfer the force F to the third ball 8022 d. Since the first, second and third spheres 8022b, 8022c, 8022d can rotate but do not roll, and the forces transmitted to the upper and lower support shafts 8021, 8023 are all in the vertical direction, the support point of the balance 801 by the support assembly 802 remains unchanged. The support assembly 802 is simple in structure and easy to install.
As an example, the first sphere 8022b, the second sphere 8022c, and the third sphere 8022d can be limited in the housing 8022a by a limiting member, so as to avoid displacement caused by rolling. Specifically, the limiting member may be a limiting rod, one end of the limiting rod rotatably penetrates into the first sphere 8022b, the second sphere 8022c, or the third sphere 8022d, and the other end of the limiting rod is fixed in the housing 8022 a.
With the above arrangement, the first, second, and third spheres 8022b, 8022c, 8022d can be rotated without being displaced.
The diameters of the first sphere 8022b, the second sphere 8022c, and the third sphere 8022d may also be different. In addition, the first sphere 8022b, the second sphere 8022c, and the third sphere 8022d are rigid spheres and are not deformed by collision.
As described above, the upper end of the upper support shaft 8021 is connected to the lower end of the balance 801. For example, when the upper end of the upper support shaft 8021 is connected to the middle of the lower end of the balance 801, the balance 801 is an equiarm balance 801. When the upper end of the upper support shaft 8021 is connected to both sides of the lower end of the balance 801, the balance 801 is an unequal arm balance 801. The upper support shaft 8021 may also be connected to the lower end of the balance 801 by a living connection.
Considering that the force transfer effect between the upper support shaft 8021 and the first sphere 8022b is good, and the force transfer effect between the lower support shaft 8023 and the third sphere 8022d is good, as an example, the volume of the first sphere 8022b limited in the first concave surface is smaller than the volume of 1/3 of the first sphere 8022 b; the volume of the third sphere 8022d retained in the second concave surface is less than the 1/3 volume of the third sphere 8022 d.
In order to increase the supporting effect of the lower supporting shaft 8023, as shown in fig. 10, the weighing apparatus 8 according to the embodiment of the present invention further includes: a stiffener 8024; one end of the reinforcing member 8024 is movably connected to the lower end of the housing 8022a, and the other end is connected to the side wall of the lower support shaft 8023.
The reinforcing member 8024 can function to support the housing 8022a, the first sphere 8022b, the second sphere 8022c, and the third sphere 8022 d. By movably connecting one end of the reinforcing member 8024 to the lower end of the housing 8022a, a cushioning effect can be exerted. Specifically, one end of the reinforcing member 8024 may be movably connected to the lower end of the housing 8022a by a ball stud.
As an example, the number of the reinforcing members 8024 may be provided in plural, for example, three, and uniformly provided along the circumferential direction of the lower support shaft 8023.
The reinforcing member 8024 may be in the form of a rod-like structure, which is readily available for the reinforcing member 8024.
In view of being able to easily dispose the first, second and third spheres 8022b, 8022c, 8022d in the housing 8022a, as shown in fig. 8, the upper end of the housing 8022a is detachably provided with a top cover 8022e through which the upper support shaft 8021 passes 8022 e. Wherein the top 8022e may be a flange.
The structure of the housing 8022a can be various, for example, the outer contour of the housing 8022a can be a column, a square, a hexagonal prism, or the like. Similarly, the outer contours of the upper support shaft 8021 and the lower support shaft 8023 may be in the shape of a column, a square, a hexagonal prism, or the like.
In order to prevent the balance 801 from tilting over a large angle or even falling over on the support assembly 802, the weighing device 8 further comprises: and the limiting part is used for limiting the balance 801. In particular, the limiting member may be a limit switch.
As an example, the support assembly 802 may be free to lift. Before gas weighing, the balance 801 is first adjusted so that the balance 801 is in a normal operating state, i.e., when no weight is being weighed, the balance 801 is adjusted. During adjustment of balance 801, balance 801 may not be in contact with support assembly 802. The balance 801 can be limited by the limiting part, so that the balance 801 does not incline greatly. The balance 801 is balanced by adding a weight 810 or by the action of an electromagnetic force, and after the balance 801 is balanced, the support assembly 802 is lifted to support the balance 801 to achieve a weighing state of the balance 801. When the balance 801 is used for weighing, the balance 801 is favorably placed on the same supporting point of the gravity center of the supporting assembly 802, the pressure direction of the supporting point by the balance 801 is favorably kept parallel to the gravity center line of the hook of the balance 801, the weighing device 8 is favorably accurate and reliable, and the uncertainty of mass-time method measurement is reduced.
In embodiments of the present invention, the support assembly 802 may be suitable for accurate weighing of gases, particularly natural gas weighing. The support assembly 802 may support an isometric balance 801 and is particularly suitable for supporting a dual tank isometric electromagnetic balance 801.
As an example, in the weighing apparatus 8 for a natural gas primary standard apparatus, when the support assembly 802 is used to support the double-tank equiarm electromagnetic balance 801 for measurement, the uncertainty can reach 1g, the minimum resolution can reach 0.1g, and the measurement uncertainty can be favorably reduced.
In the embodiment of the present invention, the first supporting unit 803 may be provided in various structures, for example, it may be provided in a platform structure to facilitate the weighing tank 807 to be fixed on the top surface thereof.
As an example, the first support unit 803 is a movable cart. This is provided to facilitate the first support unit 803 to be movable on the transfer unit 804. The trolley can be provided with a motor for driving the trolley to move.
The transmission unit 804 may be provided in various forms, and on the premise of simple structure and convenient transmission, the following example is given, as shown in fig. 15 and 16, the transmission unit 804 includes: two opposite slide rails, the second supporting unit 805 is disposed between the two slide rails; the bottom surface of the first supporting unit 803 is provided with two sliding grooves; the sliding groove is slidably sleeved on the sliding rail.
The sliding of the first support unit 803 on the transmission unit 804 can be achieved by sliding the sliding grooves on the sliding rails. When the first supporting unit 803 is transferred from the first end to the second end of the transfer unit 804, the driving unit 806 controls the second supporting unit 805 to move up, so that the first supporting unit 803 and the weighing tank 807 can be positioned on the second supporting unit 805, and the first supporting unit 803 and the weighing tank 807 can be supported.
In consideration of the fact that the first support unit 803 can easily slide on a slide rail, a plurality of pulleys may be provided at intervals along the sliding direction of the first support unit 803 on the slide rail.
The transfer unit 804 has a simple structure, and the first support unit 803 can easily slide on the transfer unit 8044.
Specifically, the first support unit 803 may be given a power to slide forward by an external force.
Further, considering that the first supporting unit 803 can easily slide on the transferring unit 804, the transferring unit 804 is gradually inclined downward from the first end to the second end thereof to facilitate the first supporting unit 803 to slide on the transferring unit 804 under its own weight.
As mentioned above, the second supporting unit 805 can move up and down under the driving action of the driving unit 806. The second supporting unit 805 may be provided in various structures, and the following examples are given based on the structural simplicity and in consideration that the second supporting unit 805 can finely adjust the positions of the first supporting unit 803 and the weighing pot 807 located thereon:
as shown in fig. 17 and 18, the second supporting unit 805 includes: a support platform 8051 and a plurality of fourth spheres 8052; a plurality of arc grooves 8051a are arranged on the top surface of the supporting platform 8051, a limiting groove 8031 is arranged on the bottom surface of the first supporting unit 803, and the fourth sphere 8052 can be simultaneously positioned in the arc grooves 8051a and the limiting groove 8031 in a rolling manner.
With the above arrangement, when the second supporting unit 805 rotates under the driving action of the driving unit 806, the force applied to the fourth sphere 8052 changes due to the gravity of the first supporting unit 803 and the weighing tank 807, and the fourth sphere 8052 rolls to a proper position in the arc-shaped groove 8051 a. And because the bottom surface of the first supporting unit 803 is provided with the limiting groove 8031, the position of the limiting groove 8031 is adjusted along with the rolling of the fourth sphere 8052, thereby realizing the fine adjustment of the first supporting unit 803 and the weighing tank 807.
For example, the second supporting unit 805 includes at least three equal-diameter fourth spheres 8052, and the three fourth spheres 8052 are arranged on the supporting platform 8051 in a triangular arrangement. Accordingly, the limiting groove 8031 on the bottom surface of the first supporting unit 803 may be a triangular limiting groove 8031 capable of accommodating three fourth spheres 8052, or may be a limiting groove 8031 having the same structure as the arc-shaped groove 8051 a.
Or, the supporting platform 8051 is a square structure, and four corners of the top surface of the supporting platform 8051 are respectively provided with an arc-shaped groove 8051 a. Accordingly, the limiting groove 8031 on the bottom surface of the first supporting unit 803 may be a quadrilateral limiting groove 8031 capable of accommodating four fourth spheres 8052, or may be a limiting groove 8031 having the same structure as the arc-shaped groove 8051 a. When the weighing tank 807 is unbalanced and needs to be adjusted in space, the position of the fourth sphere 8052 in the arc groove 8051a can be adjusted.
As an example, the fourth sphere 8052 can be a rigid sphere.
The positions of the first supporting unit 803 and the weighing tank 807 are adjusted by the cooperation of the driving unit 806 and the fourth ball 8052, so that the weighing tank 807 can be accurately and seamlessly butted with the reversing valve assembly 7 without stress.
As an example, the depth of the cambered groove 8051a is 1/3-2/3 times the diameter of the fourth sphere 8052. For example, the depth of the cambered groove 8051a is 1/3 times, 1/2 times, 2/3 times, etc. the diameter of the fourth sphere 8052. The arc of the arc groove 8051a may be 1 ° to 10 °, for example, 1 °, 2 °, 3 °, 4 °, 5 °, 6 °, 7 °, 8 °, 9 °, 10 °, and the like.
With this arrangement, not only the fourth spherical body 8052 can be disengaged from the arc-shaped groove 8051a, but also the positions of the first supporting unit 803 and the weighing pot 807 can be accurately adjusted.
As mentioned above, the driving unit 806 drives the second supporting unit 805 to move up and down and rotate. Among them, the driving unit 806 may be provided in various forms, and on the premise of easy setting, the following example is given: the driving unit 806 includes: the driving device comprises a first driving module, a second driving module and a third driving module; the first driving module is used for driving the second supporting unit 805 to move up and down; the second driving module is configured to drive the second supporting unit 805 to rotate along a first direction, where the first direction is: the direction in which the first supporting unit 803 is transmitted by the transmitting unit 804; the third driving module is configured to drive the second supporting unit 805 to rotate along a second direction, where the second direction is: a direction perpendicular to the first direction.
The first driving module can drive the second supporting unit 805 to move up and down, and the second driving module and the third driving module can drive the second supporting unit 805 to rotate along the front-back direction and the left-right direction.
The first driving module, the second driving module and the third driving module may be electric push rods, so as to realize the pushing and pulling of the second supporting unit 805. The first driving module, the second driving module and the third driving module may further include a top pull rod capable of enabling the first supporting unit 803 to be pulled by twisting, so that the second supporting unit 805 can rotate 360 ° in the horizontal plane.
As an example, the second supporting unit 805 has a rectangular structure, and four corners of the lower end thereof are respectively provided with an electric push-pull rod. The rotation of the second support unit 805 may be achieved by having two opposing motorized push-pull rods push against the second support unit 805 and the remaining two motorized push-pull rods pull on the second support unit 805. The second supporting unit 805 is lifted by controlling the four electric push-pull rods to simultaneously push against the second supporting unit 805. The second support unit 805 is lowered by controlling the four electric push-pull rods to pull the second support unit 805 at the same time.
As an example, the angle of rotation of the second support unit 805 in the vertical direction is 0 ° to 7.5 °, and may be, for example, 0 °, 1 °, 2 °, 3 °, 4 °, 5 °, 6 °, 7.5 °, and the like.
With this arrangement, the first supporting unit 803 and the weighing tank 807 which are located on the second supporting unit 805 can be prevented from being separated from the second supporting unit 805 by their own weight when they are tilted.
In view of being able to easily place the first supporting unit 803 and the weighing pot 807 above the second supporting unit 805, the weighing apparatus 8 according to the embodiment of the present invention further includes: an auxiliary driving unit for driving the first supporting unit 803 to move up and down (not shown in the drawing).
The auxiliary driving unit may be an electric push-pull rod, and the first supporting unit 803 is pushed and pulled by the electric push-pull rod, so that the first supporting unit 803 can move up and down.
The auxiliary driving unit may be disposed on the first supporting unit 803, or may be disposed at a first end of the transferring unit 804.
Because the volume of the weighing tank 807 is slightly changed due to changes in gas pressure and temperature in the tank body before and after the weighing tank 807 is inflated, the air buoyancy borne by the weighing tank 807 before and after the inflation changes, which affects the weighing result of the gas mass, and in order to avoid this situation, two examples are given for the structure of the weighing tank 807 in the embodiment of the present invention:
in example (1), as shown in fig. 19, a weighing pot 807 includes: a first outer tank 8071a, a first inner tank 8072a arranged in the first outer tank 8071 a; a vacuum gap layer 8073 is arranged between the first outer tank 8071a and the first inner tank 8072 a; the outer wall of the first outer tank 8071a is also provided with a first inflation port 8074a for communicating with the reversing valve assembly 7, and the first inflation port 8074a passes through the vacuum gap layer 8073 to communicate with the first inner tank 8072 a; the first outer tank 8071a is further provided with a first hanger for hanging the weighing tank 807 on the balance 801.
With the above arrangement, during the process of filling the weighing tank 8 with gas, the first inner tank 8072a expands due to the internal inflation, causing a change in volume of the first inner tank 8072 a. Because the vacuum gap layer 8073 is arranged between the first outer tank 8071a and the first inner tank 8072a, the vacuum gap layer 8073 can prevent the first outer tank 8071a from being subjected to pressure and temperature changes caused by the expansion of the first inner tank 8072a, so that the volume of the first outer tank 8071a cannot be changed due to the inflation of the first inner tank 8072a, further the air buoyancy force of the gas weighing tank 8 before and after inflation can be prevented from being changed, and the accuracy of gas mass weighing is ensured.
In addition, after the gas flow rate flowing into the weighing tank 8 is obtained through calculation, the gas in the weighing tank 8 needs to be emptied, so as to obtain the mass of the gas filled into the weighing tank 8 in the next round. With the weighing tank 8 provided in the prior art, after the gas is exhausted, the temperature inside the weighing tank 8 is suddenly reduced, and small water drops are generated on the outer wall of the weighing tank 8. Then, when the next round of gas is filled into the weighing tank 8, small water droplets on the outer wall of the weighing tank 8 evaporate, which results in the balance 801 not being able to accurately measure the mass of the actually filled gas. In the weighing tank 8 provided in the embodiment of the present invention, since the vacuum gap layer 8073 is disposed between the first outer tank 8071a and the first inner tank 8072a, the vacuum gap layer 8073 does not contain moisture, and can prevent small water droplets from being generated on the outer wall of the first inner tank 8072a, and also has a heat insulation effect, so that a large temperature difference between the inside and the outside of the first outer tank 8071a can be prevented, and further, the small water droplets can be prevented from being generated on the outer wall of the first outer tank 8071a, and the balance 801 can be ensured to accurately measure the quality of the charged gas.
It can be seen that, by arranging the weighing tank 8 into a structure comprising the first inner tank 8072a, the vacuum gap layer 8073 and the first outer tank 8071a in sequence from inside to outside, not only can the air buoyancy force borne by the gas weighing tank 8 before and after inflation be prevented from changing, but also small water drops can be prevented from being generated on the outer wall of the first outer tank 8071a, the balance 801 can be ensured to accurately measure the mass of the inflation gas, and the accuracy of the gas flow primary standard device in gas flow calibration can be further improved; in addition, the weighing tank 8 can be conveniently hung on the beam of the balance 801 by arranging the hanging piece on the first outer tank body 8071 a.
Correspondingly, the inflation mass of the weighing tank 807 is calculated using the following calculation formula:
△m＝m1-m0
wherein the content of the first and second substances,
△ m-weigh the inflated mass, kg, of tank 807;
m1-weighing the inflated mass of tank 807 in kg;
m0weigh the mass of tank 807 in kg before inflation.
In order to avoid the influence of the moisture in the air on the life of the weighing tank 807 due to the corrosion of the first outer tank 8071a, in the embodiment of the present invention, the outer wall of the first outer tank 8071a is coated with a first anticorrosive layer 8077.
By the above arrangement, not only the moisture in the air can be prevented from corroding the first outer tank 8071a, but also the air can be prevented from entering the vacuum gap layer 8073.
The first anticorrosive layer 8077 may be of various types, and may be, for example, a polyethylene coating. The first anticorrosive layer 8077 is not only convenient to obtain, but also low in price.
Regarding the connection manner of the first outer tank 8071a and the first inflation port 8074a, various manners may be provided, for example, the first inflation port 8074a may be welded to the first outer tank 8071a, which not only facilitates production and manufacture, but also prevents external air from entering into the vacuum gap 8073.
It should be noted that the first inflation port 8074a is a tubular structure with two ports.
Based on the first inflation port 8074a with the above structure, the first inflation port 8074a is flanged with the reversing valve assembly 7, so that the weighing tank 807 or the reversing valve assembly 7 can be conveniently assembled and disassembled.
Wherein, the first inflation inlet 8074a and the reversing valve assembly 7 are provided with adaptive flanges.
Similarly, in order to prevent the air in the first inner tank 8072a from entering the vacuum gap 8073, in the embodiment of the present invention, as shown in fig. 19, a first sealing member 8078 is disposed between the first inflation inlet 8074a and the first inner tank 8072 a.
The first sealing element 8078 can be a rubber sealing ring.
In addition, with respect to the manner of mounting the first seal 8078, the first seal 8078 may be adhered to the first inflation port 8074 a. For example, an annular groove may be provided on the outer wall of the first inflation port 8074a, and the first seal 8078 may be adhered within the annular groove.
As described above, in order to facilitate the suspension of the weighing tank 807 on the balance 801, in the embodiment of the present invention, the first upper body of the first outer tank 8071a is provided with a first hanger for suspending the weighing tank 807 on the balance 801.
Wherein, the first hanging piece can be an arc-shaped rod, an arch-shaped rod and other structures.
In addition, for convenience of production and manufacture, the first suspension member is welded to the first outer tank 8071 a.
Example (2), as shown in fig. 20, a weighing pot 807 includes: a second outer tank 8071b, a second inner tank 8072b arranged inside the second outer tank 8071 b; a mass compensation gap layer 8075 is arranged between the second outer tank 8071b and the second inner tank 8072b, and flowable media are filled in the mass compensation gap layer 8075; a mass compensation pipe 8076 which is communicated with the mass compensation gap layer 8075 is arranged on the outer wall of the second outer tank body 8071b, and the mass compensation pipe 8076 is provided with scales and has a standard sectional area; a second inflation port 8074b used for being communicated with the reversing valve assembly 7 is further arranged on the outer wall of the second outer tank 8071b, and the second inflation port 8074b penetrates through the mass compensation gap layer 8075 to be communicated with the second inner tank 8072 b; the second outer tank 8071b is also provided with a hanger for hanging the weighing tank 807 on the balance 801.
In the embodiment of the present invention, since the mass compensation gap layer 8075 is formed between the second outer tank 8071b and the second inner tank 8072b, and the mass compensation gap layer 8075 is filled with the flowable medium, the flowable medium separates the second outer tank 8071b from the second inner tank 8072 b. When the second inner tank 8072b expands due to the influence of the pressure and temperature of the inflation gas, the flowable medium in the mass compensation gap layer 8075 is squeezed by the second inner tank 8072b, and the flowable medium enters the mass compensation tube 8076 due to the squeezing, so that the liquid level of the flowable medium inside the mass compensation tube 8076 rises. Therefore, the second outer tank 8071b can be prevented from being affected when the second inner tank 8072b is expanded, that is, the pressure and the temperature of the second outer tank 8071b do not change due to the inflation of the second inner tank 8072b, and the volume of the corresponding second outer tank 8071b does not change due to the inflation of the second inner tank 8072 b.
Therefore, the final liquid level of the flowable medium inside the mass compensating pipe 8076 can be determined according to the length scale on the pipe wall of the mass compensating pipe 8076 after the inflation. Then, the difference between the initial liquid level height and the final liquid level height of the flowable medium inside the mass compensation pipe 8076 after the second inner tank 8072b is inflated is calculated, and the volume change amount of the second inner tank 8072b is determined according to the product of the difference and the standard sectional area of the mass compensation pipe 8076. Then, the sum of the product and the standard volume of the second inner tank 8072b is calculated, and the calculated sum is determined as the compensated volume of the second inner tank 8072b to realize the volume compensation of the symmetrical measuring tank 807, so that the compensated volume can be used for gas flow measurement, and the accuracy of the gas flow measurement is improved.
Wherein, the inflation quality of the weighing tank 807 can be calculated by the following formula:
△m＝m1-m0-ρ×s×(l1-l0)
in the above formula:
△ m-weigh the inflated mass, kg, of tank 807;
m1-weighing the inflated mass of tank 807 in kg;
m0weigh tank 807 mass before inflation, kg;
rho-density of air in kg/m around the weighing tank 8073；
s-area of cross section of Mass compensating tube 8076, m2；
l1-the height of the medium, m, in the mass compensation tube 8076 after the tank 807 has been inflated;
l0the media height, m, in the mass compensation tube 8076 before the weighing tank 807 is inflated.
For example, if the cross-sectional area of the mass-compensating tube 8076 is 0.02m2And is weighedThe tank 807 is inflated before and after, and the internal media height is 0mm, 370mm respectively. The mass of the weighing tank 807 before and after inflation was 3102.6543kg and 3172.4252kg, respectively, and the air density outside the weighing tank 807 was 1.145kg/m3Then, the charge mass of the weighing tank 807 is obtained from the above calculation formula as △ m-3172.4252-3102.6543-1.145 × 0.02 × (0.37-0) — 69.7709-0.0085-69.762 kg.
The mass compensation tube 8076 may be a cylindrical thin tube with a standard cross-sectional area, which is a cross-sectional area with a standard specification and a fixed value, but may also be other shapes in practical applications, such as a thin tube with a square column with a standard cross-sectional area. Wherein, the mass compensating pipe 8076 has a length L and an upper port.
In addition, the flow medium in the mass compensating tube 8076 may be water.
In order to prevent the moisture in the air from corroding the second outer tank 8071b and affecting the service life of the weighing tank 807, in the embodiment of the present invention, the outer wall of the second outer tank 8071b is coated with a second anticorrosive layer (not shown in the drawings).
By the above arrangement, not only the moisture in the air can be prevented from corroding the second outer can body 8071b, but also the air can be prevented from entering the gap layer 8073.
The second anticorrosive layer may be a polyethylene coating, for example. The second anticorrosive coating is convenient to obtain and low in price.
The connection between the second outer tank 8071b and the second inflation port 8074b can be set in various ways, for example, the second inflation port 8074b can be welded to the second outer tank 8071b, which not only facilitates the production and manufacture, but also prevents the external air from entering into the gap layer 8073.
It should be noted that the second inflation port 8074b is a tubular structure with two ports.
Based on the second inflation port 8074b with the above structure, the second inflation port 8074b is flanged with the reversing valve assembly 7, so that the weighing tank 807 or the reversing valve assembly 7 can be conveniently disassembled and assembled.
Wherein, the second inflation inlet 8074b and the reversing valve assembly 7 are provided with adaptive flanges.
Similarly, in order to prevent the air in the inner tank 8072 from entering the gap layer 8073, in the embodiment of the present invention, a second sealing member (not shown in the drawings) is disposed between the inflation inlet and the inner tank 8072.
Wherein, the second sealing element can be a rubber sealing ring.
In addition, with respect to the manner of installation of the second seal, the second seal can be adhered to the second inflation port 8074 b. For example, an annular groove may be provided on the outer wall of the second inflation port 8074b, and the second seal may be adhered within the annular groove.
As described above, in order to facilitate hanging the weighing tank 807 on the balance 801, in the embodiment of the present invention, the second outer tank body 8071b is provided with a second hanger for hanging the weighing tank 807 on the balance 801.
Wherein, the second hanging piece can be an arc-shaped rod, an arch-shaped rod and other structures.
In addition, for convenience of production and manufacture, the second suspension member is welded to the second outer tank 8071 b.
Further, in the embodiment of the present invention, as shown in fig. 21, the weighing tank 807 includes: a first weighing tank 807a, a second weighing tank 807 b; the weighing device 8 further comprises: main conduit 809a, first branch conduit 809b, second branch conduit 809 c; the air outlets of the first branch pipe 809b and the second branch pipe 809c are respectively connected with the first weighing tank 807a and the second weighing tank 807 b; a first valve is arranged on the first branch pipeline 809b, and a second valve is arranged on the second branch pipeline 809 c; the reversing valve assembly 7 is arranged on the main pipeline 809 a; further, the weighing device 8 further includes: the inclined tee 809 d; the air inlets of the first branch pipe 809b and the second branch pipe 809c are connected with the air outlet of the main pipe 809a through a slant tee 809 d.
Therefore, the working efficiency of the primary standard system of the gas flow can be improved by arranging the first weighing tank 807a and the second weighing tank 807b in the embodiment of the invention; in addition, by arranging the inclined tee joint 809d and connecting the air inlets of the first branch pipeline 809b and the second branch pipeline 809c with the air outlet of the main pipeline 809a through the inclined tee joint 809d, the path of the gas flowing into the first weighing tank 807a and the second weighing tank 807b is shortened, the mass change of the gas in the additional pipeline is further reduced, and the uncertainty of the weighing result is reduced.
An expansion joint can be arranged on the first branch pipeline 809b and the second branch pipeline 809c, and rails are arranged at the bottom ends of the first weighing tank 807a and the second weighing tank 807b, so that the distance between the first weighing tank 807a and the second weighing tank 807b and the inclined tee 809d can be adjusted at any time, the path of the additional pipeline is shortened, and the uncertainty of the subsequent gas weighing result is further reduced.
In order to further reduce the mass change of the gas in the additional pipeline and reduce the uncertainty of the weighing result, the main pipeline 809a and the first branch pipeline 809b are connected to form a first included angle, and the first included angle is 100-170 degrees (such as 120 degrees, 127.5 degrees, 150 degrees and the like). The main pipeline 809a and the second branch pipeline 809c form a second included angle after being connected, and the second included angle is 100-170 degrees (such as 120 degrees, 127.5 degrees, 150 degrees and the like).
It should be noted that an included angle between a first pipe orifice in the inclined tee 809d, which is communicated with the main pipeline 809a, and a second pipe orifice in the inclined tee 809d, which is communicated with the first branch pipeline 809b, is the same as the first included angle; in addition, the included angle between the first pipe orifice of the inclined tee 809d, which is communicated with the main pipeline 809a, and the third pipe orifice of the inclined tee 809d, which is communicated with the second branch pipeline 809c, is the same as that of the second included angle.
Wherein, the degree of the first included angle and the second included angle can be kept consistent.
In order to facilitate weighing of the first weighing tank 807a and the second weighing tank 807b after being inflated, as shown in fig. 21, in the embodiment of the present invention, a third valve detachably connected is disposed on the first branch pipe 809b, and a fourth valve detachably connected is disposed on the second branch pipe 809 c.
Specifically, after the first weighing tank 807a is inflated, the first valve and the third valve are closed, and the first valve and the third valve are separated, so that the first weighing tank 807a can be detached while the inlet of the first weighing tank 807a and the outlet of the first branch pipe 809b are kept in a sealed state. Similarly, after the second weighing tank 807b is inflated, the second valve and the fourth valve are closed, and the second valve and the fourth valve are separated, so that the second weighing tank 807b can be detached, and the inlet of the second weighing tank 807b and the outlet of the second branch pipe 809c are kept in a sealed state.
The first valve and the third valve can be connected through a flange, and the second valve and the fourth valve can be connected through a flange. In addition, the first valve, the second valve, the third valve and the fourth valve can be ball valves.
In an embodiment of the present invention, as shown in fig. 21, the reversing valve assembly 7 comprises: a seventh electromagnetic valve 701, an inlet of which is communicated with the standard gas flowmeter, and an outlet of which is communicated with an inlet of a main pipeline 809 a; an eighth electromagnetic valve 702 with an air inlet communicated with the standard gas flowmeter and an outlet communicated with the low-pressure gas storage device 9; a third controller electrically connected to the seventh solenoid valve 701 and the eighth solenoid valve 702, the third controller being configured to control the seventh solenoid valve 701 and the eighth solenoid valve 702 to open and close; and a timer 12 electrically connected to the seventh solenoid valve 701 for acquiring a communication time of the seventh solenoid valve 701.
It can be understood that the air outlet of the seventh electromagnetic valve 701 is a first air outlet of the reversing valve assembly 7, and the air outlet of the second electromagnetic valve 3012 is a second air outlet of the reversing valve assembly 7.
With the above arrangement, when the flow rate of the gas to be detected flowing through the standard flowmeter 6 is stabilized, the eighth solenoid valve 702 is closed by the third controller, and the seventh solenoid valve 701 is opened, so that the gas to be detected flows into the first weighing tank 807a or the second weighing tank 807b, and at the same time, the timer 12 is used to start timing. After the first weighing tank 807a or the second weighing tank 807b is completely inflated, the eighth solenoid valve 702 is opened by the third controller, the seventh solenoid valve 701 is closed, and the timer 12 is stopped to count time, so as to obtain the communication time of the seventh solenoid valve 701. Then, the first weighing tank 807a or the second weighing tank 807b after the inflation is moved to the balance 801 of the weighing apparatus 8, the mass of the first weighing tank 807a or the second weighing tank 807b is weighed, and the actual gas flow rate flowing through the standard flowmeter 6 is calculated based on the communication time of the seventh electromagnetic valve 701 acquired by the timer 12.
Wherein, the third controller can be a PLC control cabinet (programmable control cabinet).
In step S6, the temperature and humidity of the balance chamber 808 of the weighing apparatus 8 are adjusted by the temperature and humidity adjusting apparatus while the air charge mass of the weighing tank 807 is measured by the balance 801.
By the above arrangement, the measurement accuracy of the weighing device 8 can be improved.
With regard to the structure of the temperature and humidity adjustment device, an example is given in an embodiment of the present invention, and in an embodiment of the present invention, the temperature and humidity adjustment device includes: the device comprises a temperature adjusting unit, a humidity adjusting unit, an air supply unit, a rectifying unit and an air exhaust unit; the temperature adjusting unit is used for adjusting the temperature in the balance chamber 808; the humidity adjusting unit is used for adjusting the humidity in the balance chamber 808; the rectifying units are arranged on the side wall or/and the top wall of the balance chamber 808; the air supply unit inputs air into the balance chamber 808 through the rectifying unit; the air exhaust unit is disposed on the bottom wall of the balance chamber 808, and the air exhaust unit is configured to exhaust air in the balance chamber 808.
The temperature adjusting unit may include: a temperature sensor disposed within the balance chamber 808; a first controller electrically connected to the temperature sensor; the heater and the refrigerator are electrically connected with the controller; the temperature sensor is used for acquiring temperature information in the balance chamber 808 and transmitting the temperature information to the first controller; the first controller controls the on and off of the heater and the refrigerator according to the temperature information.
The electric heaters may include coarse tuned primary electric heaters and fine tuned secondary electric heaters that allow for precise control of the temperature within the balance chamber 808.
In addition, the first controller may be a PLC control cabinet (programmable control cabinet).
The humidity adjustment unit may include: a humidity sensor disposed within the balance chamber 808; a second controller electrically connected to the humidity sensor; the humidifier and the filter are electrically connected with the second controller; the humidity sensor is used for acquiring humidity information in the balance chamber 808 and transmitting the humidity information to the second controller; the second controller controls the on and off of the humidifier according to the temperature information; the filter is used for impurities in water used by the humidifier.
Wherein, the humidifier can be an electric heating humidifier.
In addition, the second controller may be a PLC control cabinet (programmable control cabinet).
Two examples are given for the configuration of the rectification unit according to embodiments of the present invention, which may include a plurality of micro-porous pipes uniformly distributed on the side wall or/and the top wall of the balance chamber 808, or be provided in a plate-like configuration having a plurality of rectification holes uniformly distributed. By so doing, air can be made to enter the balance chamber 808 uniformly.
The air supply unit may be a positive pressure blower.
In addition, the exhaust unit includes a plurality of exhaust ports.
In addition, the temperature and humidity adjusting device may further include a fresh air unit disposed between the air supply unit and the rectification unit so as to be able to supply fresh gas (e.g., air) into the balance chamber 808.
In step S6, the actual flow rate value of the temperature-adjusted natural gas, that is, the actual flow rate value is calculated by the mass-time method from the charge mass and the charge time, and is equal to the charge mass of the weighing tank 807 and the charge time of the weighing tank 807.
In step S7, if the absolute value of the (measured flow value-actual flow value)/actual flow value is within the preset threshold, it can be determined that the measurement accuracy of the natural gas standard flowmeter 6 is high, and the measurement accuracy of the natural gas standard flowmeter can be evaluated with the measurement accuracy of the natural gas flowmeter for natural gas trade measurement, so as to ensure the accuracy, reliability and fairness of the natural gas trade measurement.
Wherein, the preset threshold value can be set to be 0.001-0.005.
All the above optional technical solutions may be combined arbitrarily to form the optional embodiments of the present disclosure, and are not described herein again.
The above description is only an illustrative embodiment of the present invention, and should not be taken as limiting the scope of the invention, and any modifications, equivalents, improvements and the like that are within the spirit and principle of the present invention should be included in the scope of the present invention.

Claims (12)

1. A method of calibrating a natural gas standard flow meter, the method comprising:
conveying the natural gas in the low-pressure gas source (1) to a pressurizing device (2) and a gas path anti-corrosion device (10) to remove sulfur, moisture and solid particles in the natural gas, and pressurizing to a first preset pressure;
conveying the pressurized and impurity-removed natural gas into a high-pressure gas storage device (3), and conveying the pressurized and impurity-removed natural gas into a pressure regulating device (4) after the gas pressure of the high-pressure gas storage device (3) is a second preset pressure, so that the pressure of the pressurized and impurity-removed natural gas is regulated to be the same as the working pressure of a natural gas standard flowmeter (6);
conveying the pressure-regulated natural gas into a constant temperature device (5), adjusting the temperature of the pressure-regulated natural gas to be the same as the working temperature of the natural gas standard flowmeter (6), and removing non-inert gas in cooling water flowing into the supercharging device (2) and the constant temperature device (5) by using a liquid path anticorrosion device (11);
conveying the natural gas subjected to temperature regulation into the natural gas standard flowmeter (6) to obtain a measured flow value of the natural gas subjected to temperature regulation;
conveying the temperature-regulated natural gas to a low-pressure gas storage device (9) from a second gas outlet of a reversing valve assembly (7), after the reading of the natural gas standard flowmeter (6) is stable, closing the second gas outlet of the reversing valve assembly (7), opening a first gas outlet of the reversing valve assembly (7), conveying the temperature-regulated natural gas to a weighing tank (807) of a weighing device (8), and simultaneously acquiring the charging time of the weighing device (8) by using a timer (12);
-acquiring the aerated mass of the weighing tank (807) by means of the balance (801) of the weighing device (8);
calculating to obtain an actual flow value of the natural gas after temperature adjustment according to the inflation quality, the inflation time and a quality-time method;
and comparing the actual flow value with the measured flow value, and calibrating the natural gas standard flowmeter (6).
2. The calibration method according to claim 1, wherein the step of conveying the pressurized and purified natural gas to the high-pressure gas storage device (3) and conveying the pressurized and purified natural gas to the pressure regulating device (4) after the gas force of the high-pressure gas storage device (3) is the second preset pressure comprises:
and conveying the natural gas after the pressurization impurity removal to the inside of a first high-pressure gas storage unit (301) or a second high-pressure gas storage unit (302) of the high-pressure gas storage device (3), and alternately conveying the natural gas after the pressurization impurity removal of the second preset pressure to the inside of the pressure regulating device (4) by the first high-pressure gas storage unit (301) and the second high-pressure gas storage unit (302).
3. The calibration method according to claim 2, wherein the step of conveying the pressurized and purified natural gas into the first high-pressure gas storage unit (301) or the second high-pressure gas storage unit (302) of the high-pressure gas storage device (3) and alternately conveying the pressurized and purified natural gas at the second preset pressure into the pressure regulating device (4) by the first high-pressure gas storage unit (301) and the second high-pressure gas storage unit (302) comprises:
acquiring gas pressure information of the first high-pressure gas storage unit (301) by using a first pressure sensor (3013) and transmitting the gas pressure information to a first gas valve controller (303), and acquiring gas pressure information of the second high-pressure gas storage unit (302) by using a second pressure sensor (3023) and transmitting the gas pressure information to a second gas valve controller (304);
if the gas pressure of the first high-pressure gas storage unit (301) is smaller than the second preset pressure, the gas pressure of the second high-pressure gas storage unit (302) is larger than or equal to the second preset pressure, the inlet of the first high-pressure gas storage unit (301) and the outlet of the second high-pressure gas storage unit (302) are opened by utilizing the first gas valve controller (303) so as to convey the natural gas after the pressurization and impurity removal to the first high-pressure gas storage unit (301) and convey the natural gas after the pressurization and impurity removal in the second high-pressure gas storage unit (302) to the pressure regulating mechanism,
if the gas pressure of first high pressure gas storage unit (301) is greater than or equal to the second pressure of predetermineeing, the gas pressure of second high pressure gas storage unit (302) is less than the second pressure of predetermineeing, utilizes second pneumatic valve controller (304) are opened the export of first high pressure gas storage unit (301) and the import of second high pressure gas storage unit (302), in order to carry in the second high pressure gas storage unit (302) natural gas after the pressure boost edulcoration, and will natural gas after the pressure boost edulcoration in the first high pressure gas storage unit (301) is carried to in pressure regulating device (4).
4. The calibration method according to claim 3, wherein the step of conveying the pressurized and purified natural gas into a pressure regulating device (4) to adjust the pressure of the pressurized and purified natural gas to be the same as the working pressure of the natural gas standard flowmeter (6) comprises the following steps:
conveying the natural gas subjected to pressurization and impurity removal in the high-pressure gas storage device (3) into a pressure regulating tank (401) of the pressure regulating device (4);
acquiring gas pressure information of the pressure regulating tank (401) by using a third pressure sensor (4011), and transmitting the information to a third gas valve controller (402);
if the gas pressure of pressure regulating jar (401) is greater than operating pressure, utilize third pneumatic valve controller (402), open the drain of pressure regulating jar (401) is in order to discharge natural gas after the pressure boost edulcoration in pressure regulating jar (401) until the gas pressure of pressure regulating jar (401) equals operating pressure.
5. The calibration method of claim 1, wherein said removing sulfur, moisture, and solid particles from said natural gas comprises:
conveying the natural gas to a desulfurization unit (1001) of the gas path corrosion prevention device (10) to remove sulfur in the natural gas;
conveying the desulfurized natural gas to a buffer unit (1002) of the gas path corrosion prevention device (10) for temporary storage;
enabling the desulfurized natural gas to pass through a dehydration unit (1003) of the gas path anticorrosion device (10) from top to bottom so as to adsorb moisture in the desulfurized natural gas;
and conveying the dehydrated natural gas to a filtering unit (1004) of the gas path anticorrosion device (10), removing solid particles in the dehydrated natural gas, and discharging a part of the natural gas from which the solid particles are removed.
6. The calibration method of claim 5, wherein said removing sulfur, moisture, and solid particles from said natural gas further comprises:
heating another part of the natural gas with the solid particles removed to a first preset temperature by using a heating unit (1005) of the gas path anticorrosion device (10), and enabling the heated natural gas to pass through the dehydration unit (1003) from bottom to top so as to analyze the moisture adsorbed by the dehydration unit (1003);
and cooling the moisture generated in the analysis of the dehydration unit (1003) by using a condensation unit (1006) of the gas path corrosion prevention device (10) so as to separate the other part of the natural gas from which the solid particles are removed.
7. The calibration method according to claim 1, wherein the removing of the non-inert gas in the cooling water flowing into the pressure boosting device (2) and the thermostatic device (5) by means of the liquid path corrosion prevention device (11) comprises:
the cooling water is conveyed to a water storage unit (1101) of the liquid path corrosion prevention device (11), and meanwhile, an inert gas in an inert gas supply unit (1104) of the liquid path corrosion prevention device (11) is sucked into the water storage unit (1101) by a suction unit (1102) of the liquid path corrosion prevention device (11);
and under the action of the pressure difference, discharging the non-inert gas in the water storage unit (1101) from the exhalation unit (1103) of the liquid path corrosion prevention device (11) so as to convert the non-inert gas in the cooling water in the water storage unit (1101) into the inert gas.
8. Calibration method according to claim 1, characterized in that said weighing tank (807) comprises: a first outer tank (8071a), a first inner tank (8072a) disposed within the first outer tank (8071 a);
a vacuum gap layer (8073) is arranged between the first outer tank (8071a) and the first inner tank (8072 a);
a first inflation port (8074a) used for communicating with the reversing valve assembly (7) is arranged on the outer wall of the first outer tank body (8071a), and the first inflation port (8074a) passes through the vacuum gap layer (8073) to be communicated with the first inner tank body (8072 a);
the inflation quality of the weighing tank (807) is calculated by using the following calculation formula:
△m＝m1-m0
wherein the content of the first and second substances,
△ m — the mass of the charge, kg, of the weighing tank (807);
m1-the mass, kg, of the tank (807) after inflation;
m0-the mass, kg, of the weighing tank (807) before inflation.
9. Calibration method according to claim 1, characterized in that said weighing tank (807) comprises: a second outer tank (8071b), a second inner tank (8072b) disposed within the second outer tank (8071 b);
a mass compensation gap layer (8075) is arranged between the second outer tank body (8071b) and the second inner tank body (8072b), and flowable media are filled in the mass compensation gap layer (8075);
a mass compensation pipe (8076) which is communicated with the mass compensation clearance layer (8075) is arranged on the outer wall of the second outer tank body (8071b), and scales are arranged on the mass compensation pipe (8076) and have a standard sectional area;
a second inflation port (8074b) used for being communicated with the reversing valve assembly (7) is further arranged on the outer wall of the second outer tank body (8071b), and the second inflation port (8074b) penetrates through the mass compensation gap layer (8075) to be communicated with the second inner tank body (8072 b);
the inflation quality of the weighing tank (807) is calculated by using the following calculation formula:
△m＝m1-m0-ρ×s×(l1-l0)
wherein the content of the first and second substances,
△ m — the mass of the charge, kg, of the weighing tank (807);
m1-the mass, kg, of the tank (807) after inflation;
m0-the mass of the tank (807) before inflation, kg;
ρ -density of air around the weighing tank (807), kg/m3；
s-cross-sectional area of the mass compensating tube (8076), m2；
l1-the height, m, of the flowable medium in the mass compensation pipe (8076) after inflation of the weighing tank (807);
l0-the height, m, of the flowable medium in the mass compensation pipe (8076) before the weighing tank (807) is inflated.
10. Calibration method according to claim 1, characterized in that the temperature and humidity of the balance chamber (808) of the weighing device (8) are adjusted by means of a temperature and humidity adjusting device during the measurement of the aerated mass of the weighing tank (807) by means of the balance (801).
11. Calibration method according to claim 1, characterized in that the composition of the tempered natural gas is analyzed with a gas composition analysis device (13) before being fed to the natural gas standard flow meter (6).
12. The calibration method according to claim 1, further comprising: and conveying the natural gas with the temperature adjusted in the low-pressure gas storage device (9) to the low-pressure gas source (1) so as to recycle the natural gas with the temperature adjusted.
CN201810972124.4A 2018-04-23 2018-08-23 Calibration method of natural gas standard flowmeter Active CN110857877B (en)

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CN201810972124.4A CN110857877B (en) 2018-08-23 2018-08-23 Calibration method of natural gas standard flowmeter
FR1904200A FR3080449B1 (en) 2018-04-23 2019-04-19 PRIMARY PROCESS AND INSTALLATION IN MASS-TIME OF NATURAL GAS FLOW MEASUREMENT
RU2019112156A RU2712935C1 (en) 2018-04-23 2019-04-22 Primary plant and method for measuring parameters of mass-time of natural gas flow

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