CN110721140A - Uterus warming care membrane powder and preparation method thereof - Google Patents
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Abstract
The invention provides uterus warming care membrane powder and a preparation method thereof, and the uterus warming care membrane powder comprises the following components in parts by weight: 15-20 parts of cinnamon extract, 10-18 parts of morinda officinalis extract, 3-6 parts of citronella extract, 1-5 parts of ligusticum wallichii oil and 0.1-0.3 part of moisturizing film-forming agent; the moisture-preserving film forming agent comprises the following components in parts by weight: 5-8 parts of sodium alginate, 0.1-0.5 part of Chinese yam extract, 0.03-0.05 part of ginkgo leaf extract, 0.03-0.05 part of camellia seed extract and 2-3 parts of calcium chloride; the uterus warming care membrane powder provided by the invention can effectively remove cold, diminish inflammation, relieve pain, promote female metabolism, increase female gynecological immunity, effectively recover skin tissue activity, increase drug absorption under heating conditions, accelerate cold removal and improve curative effect.
Description
Technical Field
The invention relates to the technical field of health care and skin care, and particularly relates to uterus warming care membrane powder and a preparation method thereof.
Background
Along with the acceleration of the rhythm of life, more and more women receive the cold problem of palace to arouse the puzzlement of cold hands and feet, obesity, menstrual disorder, metabolism ability decline, women's gynaecology immunity reduction, brought very big influence to women's life.
The existing traditional treatment methods comprise oral administration of Chinese and western medicines or external application of medicines for dispelling cold and conditioning. The existing externally applied medicine has a cold dispelling mode, but the existing externally applied medicine has slow absorption effect and insignificant efficacy; but along with the process of temperature rise, the moisture on the surface of the skin is quickly reduced, so that the surface of the skin of a human body is uncomfortable, even certain damage is caused to the skin after long-time application, and the absorption rate of the medicine is influenced, the curative effect is influenced and the like. Therefore, how to make the external application medicine have obvious curative effect and ensure the absorption of the skin of a human body after long-time application so as to improve the treatment effect of the external application medicine is a problem to be solved urgently.
Disclosure of Invention
In view of the above, the invention provides uterus warming health care membrane powder and a preparation method thereof.
The technical scheme of the invention is realized as follows:
the invention provides uterus warming care membrane powder which comprises the following components in parts by weight: 15-20 parts of cinnamon extract, 10-18 parts of morinda officinalis extract, 3-6 parts of citronella extract, 1-5 parts of ligusticum wallichii oil and 0.1-0.3 part of moisturizing film-forming agent;
the moisture-preserving film forming agent comprises the following components in parts by weight: 5-8 parts of sodium alginate, 0.1-0.5 part of Chinese yam extract, 0.03-0.05 part of ginkgo leaf extract, 0.03-0.05 part of camellia seed extract and 2-3 parts of calcium chloride.
Further explaining, the composition comprises the following components in parts by weight: 18 parts of cinnamon extract, 15 parts of morinda officinalis extract, 4 parts of citronella extract, 3 parts of ligusticum wallichii oil and 0.2 part of moisturizing film-forming agent.
Further explaining, the moisture-preserving film-forming agent comprises the following components in parts by weight: 6 parts of sodium alginate, 0.3 part of Chinese yam extract, 0.04 part of ginkgo leaf extract, 0.04 part of camellia seed extract and 2.5 parts of calcium chloride.
Further, the cinnamon extract, the morinda officinalis extract and the citronella extract are prepared by leaching cinnamon, the morinda officinalis and the citronella in hot water at a material-liquid ratio of 1:35 for 3-4 hours at 70-80 ℃, filtering, concentrating under reduced pressure, drying and sieving to obtain the cinnamon extract, the morinda officinalis extract and the citronella extract respectively, and adopting a water leaching method to improve the yield of the extracts.
Further, the aloe fiber powder is 0.01-0.02 part by weight, and the aloe fiber powder has the effects of moisturizing and repairing skin at high temperature.
A preparation method of uterus warming care membrane powder comprises the following steps:
(1) preparing a moisturizing film-forming agent: weighing Chinese yam, ginkgo leaf and camellia seed respectively, drying, crushing, sieving with a 60-80-mesh sieve, heating to 90-100 ℃ by using 75-85% ethanol in an amount of 5-10 times, reflux extracting for 2-3 times, each time for 1-2 hours, carrying out suction filtration, taking supernate, concentrating under reduced pressure, and freeze-drying to obtain Chinese yam ethanol extract, ginkgo leaf ethanol extract and camellia seed ethanol extract respectively; uniformly mixing the Chinese yam ethanol extract, the ginkgo leaf ethanol extract and the camellia seed ethanol extract with sodium alginate and calcium chloride according to the weight part ratio to obtain a moisturizing film-forming agent;
(2) weighing the cinnamon extract, the morinda officinalis extract and the citronella extract according to the proportion, adding water, stirring and mixing at the constant temperature of 50-60 ℃ for 20-30 min at the speed of 90-100 r/min to obtain a mixed primary liquid;
(3) adding a moisture-preserving film-forming agent into the mixed primary liquid, stirring at constant temperature of 120-150 r/min for 30-60 min at normal temperature, adding ligusticum wallichii oil, and uniformly stirring at 200-300 r/min to obtain a mixed solution;
(4) and (3) carrying out low-temperature reduced pressure concentration on the mixed solution at the temperature of 30-40 ℃, wherein the concentration rate is 70-80%, and then carrying out freeze drying, crushing and sieving to obtain the uterus warming care membrane powder. Mixing the cinnamon extract, the morinda officinalis extract and the citronella extract at a constant temperature, mixing the cinnamon extract, the morinda officinalis extract and the citronella extract with the moisturizing film-forming agent and the ligusticum oil at a normal temperature so as to ensure the uniformity of the mixture of the components, and finally performing freeze drying after low-temperature reduced pressure concentration to a certain proportion so as to obtain the uterus warming care film powder with uniform particles, which is beneficial to the hot compress absorption of medicaments.
Further, in the step (1), the yam powder, the ginkgo leaf powder and the tea seed powder are respectively heated by 8 times of 80% ethanol and refluxed at 95 ℃ for 3 times, each time for 1.5 hours, and after suction filtration, supernate is taken and concentrated under reduced pressure, and freeze-dried to respectively obtain the yam ethanol extract, the ginkgo leaf ethanol extract and the tea seed ethanol extract.
Further, in the step (2), the cinnamon extract, the morinda officinalis extract and the citronella extract are added with water and stirred and mixed for 25min at the constant temperature of 95r/min and 55 ℃ to obtain a mixed primary liquid.
Further, in the step (3), the moisture-preserving film-forming agent is added into the mixed primary liquid, the mixture is stirred at the constant temperature of 135r/min for 45min at the normal temperature, and then the ligusticum wallichii oil is added and stirred uniformly at the constant temperature of 250r/min to obtain the mixed solution.
Further explaining, in the step (4), before the mixed solution is subjected to low-temperature reduced pressure concentration, the aloe fiber powder is added and uniformly stirred, and the stirring speed is 90-100 r/min.
Compared with the prior art, the invention has the beneficial effects that: the uterus warming care membrane powder provided by the invention has the effects of effectively removing cold, diminishing inflammation, relieving pain, promoting female metabolism and increasing female gynecological immunity mainly by adopting the synergistic compounding of the cinnamon, morinda officinalis and citronella extract and the ligusticum wallichii oil, and meanwhile, by adding the moisturizing film-forming agent, a uniform moisturizing membrane layer is formed in the process of carrying out umbilical hot compress, so that the skin care effect is achieved, the comfort level of human skin is improved, the skin tissue activity is greatly recovered, the drug absorption effect under the heating condition is increased, the cold dispelling is accelerated, and the curative effect is improved.
Detailed Description
In order to better understand the technical content of the invention, specific examples are provided below to further illustrate the invention.
The experimental methods used in the examples of the present invention are all conventional methods unless otherwise specified.
The materials, reagents and the like used in the examples of the present invention can be obtained commercially without specific description.
Example 1-uterus warming care membrane powder, which comprises the following components in parts by weight: 15 parts of cinnamon extract, 10 parts of morinda officinalis extract, 3 parts of citronella extract, 1 part of ligusticum wallichii oil and 0.1 part of moisturizing film-forming agent.
The moisture-preserving film forming agent comprises the following components in parts by weight: 8 parts of sodium alginate, 0.5 part of Chinese yam extract, 0.03 part of ginkgo leaf extract, 0.03 part of camellia seed extract and 3 parts of calcium chloride.
The preparation method of the uterus warming and caring membrane powder comprises the steps of weighing the formula in proportion, respectively mixing the cinnamon extract, the morinda officinalis extract, the citronella extract, the moisturizing film-forming agent and the ligusticum wallichii oil in sequence, concentrating under reduced pressure, drying and sieving to obtain the uterus warming and caring membrane powder.
Embodiment 2-uterus warming care membrane powder, which comprises the following components in parts by weight: 20 parts of cinnamon extract, 18 parts of morinda officinalis extract, 6 parts of citronella extract, 5 parts of ligusticum wallichii oil and 0.3 part of moisturizing film-forming agent.
The moisture-preserving film forming agent comprises the following components in parts by weight: 5 parts of sodium alginate, 0.1 part of Chinese yam extract, 0.05 part of ginkgo leaf extract, 0.05 part of camellia seed extract and 2 parts of calcium chloride.
The preparation method of the uterus warming health care membrane powder comprises the following steps:
(1) preparing a moisturizing film-forming agent: weighing Chinese yam, ginkgo leaf and tea oil seed respectively, drying, crushing, sieving with a 60-mesh sieve, heating to 90 ℃ by adopting 85% ethanol in an amount which is 5 times that of the Chinese yam, ginkgo leaf and tea oil seed respectively, performing reflux extraction for 2-3 times, each time for 1-2 hours, performing suction filtration, taking supernate, performing reduced pressure concentration, and performing freeze drying to obtain Chinese yam ethanol extract, ginkgo leaf ethanol extract and tea oil seed ethanol extract respectively; uniformly mixing the Chinese yam ethanol extract, the ginkgo leaf ethanol extract and the camellia seed ethanol extract with sodium alginate and calcium chloride according to the weight part ratio to obtain a moisturizing film-forming agent;
(2) weighing cortex Cinnamomi extract, radix Morindae officinalis extract and rhizoma Curculiginis extract at a certain proportion, adding water, stirring at constant temperature of 60 deg.C for 30min at 90r/min to obtain mixed primary solution;
(3) adding the moisture-preserving film-forming agent into the mixed primary liquid, stirring at constant temperature for 60min at 120r/min, adding the ligusticum wallichii oil, and uniformly stirring at 300r/min to obtain a mixed solution;
(4) concentrating the mixed solution at 30 deg.C under reduced pressure to a concentration rate of 70%, freeze drying, pulverizing, and sieving to obtain uterus warming caring membrane powder.
Embodiment 3-a uterus warming care membrane powder, comprising the following components in parts by weight: 16 parts of cinnamon extract, 13 parts of morinda officinalis extract, 5 parts of citronella extract, 2 parts of ligusticum wallichii oil, 0.02 part of aloe fiber powder and 0.2 part of moisturizing film-forming agent.
The moisture-preserving film forming agent comprises the following components in parts by weight: 6 parts of sodium alginate, 0.3 part of Chinese yam extract, 0.04 part of ginkgo leaf extract, 0.04 part of camellia seed extract and 2.5 parts of calcium chloride.
The cinnamon extract, the morinda officinalis extract and the citronella extract are prepared by leaching cinnamon, the morinda officinalis and the citronella in hot water at 70-80 ℃ for 3-4 h according to a material-liquid ratio of 1:35 respectively, filtering, concentrating under reduced pressure, drying and sieving to obtain the cinnamon extract, the morinda officinalis extract and the citronella extract respectively.
The preparation method of the uterus warming care membrane powder comprises the following steps:
(1) preparing a moisturizing film-forming agent: weighing Chinese yam, ginkgo leaf and tea oil seed respectively, drying, crushing, sieving with a 80-mesh sieve, heating to 100 ℃ by using 10 times of 75% ethanol respectively, reflux-extracting for 2-3 times, each time for 1-2 hours, carrying out suction filtration, taking supernate, concentrating under reduced pressure, and freeze-drying to obtain Chinese yam ethanol extract, ginkgo leaf ethanol extract and tea oil seed ethanol extract respectively; uniformly mixing the Chinese yam ethanol extract, the ginkgo leaf ethanol extract and the camellia seed ethanol extract with sodium alginate and calcium chloride according to the weight part ratio to obtain a moisturizing film-forming agent;
(2) weighing cortex Cinnamomi extract, radix Morindae officinalis extract and rhizoma Curculiginis extract at a certain ratio, adding water, stirring at constant temperature of 50 deg.C at 100r/min for 20min to obtain primary mixed solution;
(3) adding the moisture-keeping film-forming agent into the mixed primary liquid, stirring at constant temperature of 150r/min for 30min, adding rhizoma Ligustici Chuanxiong oil, stirring at 200r/min, adding Aloe fiber powder, and stirring at 90r/min to obtain mixed solution;
(4) concentrating the mixed solution at 40 deg.C under reduced pressure to obtain concentrated solution with concentration rate of 80%, freeze drying, pulverizing, and sieving to obtain uterus warming caring membrane powder.
Example 4-a uterus warming care membrane powder, comprising the following components in parts by weight: 18 parts of cinnamon extract, 15 parts of morinda officinalis extract, 4 parts of citronella extract, 3 parts of ligusticum wallichii oil, 0.01 part of aloe fiber powder and 0.2 part of moisturizing film-forming agent.
The moisture-preserving film forming agent comprises the following components in parts by weight: 6 parts of sodium alginate, 0.3 part of Chinese yam extract, 0.04 part of ginkgo leaf extract, 0.04 part of camellia seed extract and 2.5 parts of calcium chloride.
The preparation method of the uterus warming care membrane powder comprises the following steps:
(1) preparing a moisturizing film-forming agent: weighing rhizoma Dioscoreae, folium Ginkgo and semen Camelliae sinensis, oven drying, pulverizing, sieving with 60 mesh sieve, reflux extracting with 8 times of 80% ethanol at 95 deg.C for 3 times, 1.5 times each time, vacuum filtering, concentrating the supernatant under reduced pressure, and freeze drying to obtain rhizoma Dioscoreae ethanol extract, folium Ginkgo ethanol extract and semen Camelliae sinensis ethanol extract; uniformly mixing the Chinese yam ethanol extract, the ginkgo leaf ethanol extract and the camellia seed ethanol extract with sodium alginate and calcium chloride according to the weight part ratio to obtain a moisturizing film-forming agent;
(2) weighing cortex Cinnamomi extract, radix Morindae officinalis extract and rhizoma Curculiginis extract at a certain ratio, adding water, stirring at constant temperature of 95r/min and 55 deg.C for 25min to obtain primary mixed solution;
(3) adding the moisture-preserving film-forming agent into the mixed primary liquid, stirring at constant temperature for 45min at 135r/min, adding the ligusticum oil, stirring uniformly at 250r/min, adding the aloe fiber powder, and stirring uniformly at the stirring speed of 100r/min to obtain a mixed solution;
(4) concentrating the mixed solution at 30 deg.C under reduced pressure to a concentration rate of 70%, freeze drying, pulverizing, and sieving to obtain uterus warming caring membrane powder.
Comparative example 1-uterus warming caring membrane powder formulation and preparation method according to example 4, with the difference that: the film forming agent comprises 6 parts of sodium alginate, 2.5 parts of calcium chloride and 1 part of glycerin by weight, and the rest formula and steps are the same as those in example 4.
Comparative example 2-formula and preparation of uterus warming caring membrane powder according to example 4, with the difference that: the formulation was identical to example 4 except that no film former was added.
Data of clinical trials
300 clinically recorded female patients are randomly selected for treatment effect statistics, 300 female patients have symptoms of cold hands and feet, obesity, waist soreness, menstrual disorder, menstrual pain, frequent micturition, enuresis, hyposexuality, abortion and the like caused by cold womb, the symptoms are averagely divided into 5 groups, each group respectively uses the uterus warming care membrane powder of the invention examples 1, 2 and 4 and the comparative examples 1 and 2, hot compress is carried out according to a conventional traditional Chinese medicine navel hot compress method, hot compress is carried out for 1 time every 2 days, hot compress is carried out for 1h every time, 10 days are a treatment course, the effect of treating 300 patients for 1 month is respectively observed, and the somatosensory effect of the patients in the hot compress process is recorded.
Criteria for efficacy assessment
And (3) curing: the symptoms of the patient disappear and the patient returns to normal;
the effect is shown: the patient's symptoms have substantially or mostly disappeared;
the method has the following advantages: the symptoms of the patients are obviously improved;
and (4) invalidation: the patient had no improvement in symptoms.
The statistical results are shown in table 1:
as can be seen from the above table, the uterus warming and caring membrane powder prepared by the present invention can be effectively used for treating the uterus, removing cold qi, diminishing inflammation, relieving pain, promoting female metabolism, and increasing female gynecological immunity, and as can be seen from the comparison of examples 1, 2, and 4, the aloe fiber powder with a certain amount is added in example 4, so that the curative effect is further improved. Meanwhile, as can be seen from the example 4 and the comparative examples 1 to 2, by adding the moisturizing film-forming agent, a uniform moisturizing film layer is formed in the umbilical hot compress process, so that the skin care effect is achieved, the comfort level of human skin is improved, the skin tissue activity is greatly recovered by using the combination of the Chinese yam, the ginkgo leaves, the tea oil seed extract and the ligusticum wallichii oil, the drug absorption effect under the heating condition is increased, the cold dispelling is accelerated, the treatment effect is quick, and the curative effect is remarkable.
The inventor also provides a use method of the herbal heat energy body beautifying film powder, which specifically comprises the following steps: referring to the conventional traditional Chinese medicine navel hot compress method, the membrane powder is filled into a breathable thin cloth and is tightly attached to the navel, and hot compress is carried out through a weight-reducing pad. In addition, the membrane powder can also be processed with suitable membrane forming material to make into membrane, which is tightly adhered to navel, and hot-compressed by weight reducing pad.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like that fall within the spirit and principle of the present invention are intended to be included therein.
Claims (10)
1. The uterus warming care membrane powder is characterized in that: the coating comprises the following components in parts by weight: 15-20 parts of cinnamon extract, 10-18 parts of morinda officinalis extract, 3-6 parts of citronella extract, 1-5 parts of ligusticum wallichii oil and 0.1-0.3 part of moisturizing film-forming agent;
the moisture-preserving film forming agent comprises the following components in parts by weight: 5-8 parts of sodium alginate, 0.1-0.5 part of Chinese yam extract, 0.03-0.05 part of ginkgo leaf extract, 0.03-0.05 part of camellia seed extract and 2-3 parts of calcium chloride.
2. The uterus warming care membrane powder according to claim 1, characterized in that: the coating comprises the following components in parts by weight: 18 parts of cinnamon extract, 15 parts of morinda officinalis extract, 4 parts of citronella extract, 3 parts of ligusticum wallichii oil and 0.2 part of moisturizing film-forming agent.
3. The uterus warming care membrane powder according to claim 1, characterized in that: the moisture-preserving film forming agent comprises the following components in parts by weight: 6 parts of sodium alginate, 0.3 part of Chinese yam extract, 0.04 part of ginkgo leaf extract, 0.04 part of camellia seed extract and 2.5 parts of calcium chloride.
4. The uterus warming care membrane powder according to claim 3, characterized in that: the cinnamon extract, the morinda officinalis extract and the citronella extract are prepared by leaching cinnamon, the morinda officinalis and the citronella in hot water at 70-80 ℃ for 3-4 h according to a material-liquid ratio of 1:35 respectively, filtering, concentrating under reduced pressure, drying and sieving to obtain the cinnamon extract, the morinda officinalis extract and the citronella extract respectively.
5. The uterus warming care membrane powder according to claim 1, characterized in that: the aloe fiber powder also comprises 0.01-0.02 parts by weight of aloe fiber powder.
6. A preparation method of the uterus warming caring membrane powder according to any one of claims 1 to 5, characterized by comprising the following steps: the method comprises the following steps:
(1) preparing a moisturizing film-forming agent: weighing Chinese yam, ginkgo leaf and camellia seed respectively, drying, crushing, sieving with a 60-80-mesh sieve, heating to 90-100 ℃ by using 75-85% ethanol in an amount of 5-10 times, reflux extracting for 2-3 times, each time for 1-2 hours, carrying out suction filtration, taking supernate, concentrating under reduced pressure, and freeze-drying to obtain Chinese yam ethanol extract, ginkgo leaf ethanol extract and camellia seed ethanol extract respectively; uniformly mixing the Chinese yam ethanol extract, the ginkgo leaf ethanol extract and the camellia seed ethanol extract with sodium alginate and calcium chloride according to the weight part ratio to obtain a moisturizing film-forming agent;
(2) weighing the cinnamon extract, the morinda officinalis extract and the citronella extract according to the proportion, adding water, stirring and mixing at the constant temperature of 50-60 ℃ for 20-30 min at the speed of 90-100 r/min to obtain a mixed primary liquid;
(3) adding a moisture-preserving film-forming agent into the mixed primary liquid, stirring at constant temperature of 120-150 r/min for 30-60 min at normal temperature, adding ligusticum wallichii oil, and uniformly stirring at 200-300 r/min to obtain a mixed solution;
(4) and (3) carrying out low-temperature reduced pressure concentration on the mixed solution at the temperature of 30-40 ℃, wherein the concentration rate is 70-80%, and then carrying out freeze drying, crushing and sieving to obtain the uterus warming care membrane powder.
7. The preparation method of uterus warming care membrane powder according to claim 6, characterized in that: in the step (1), the yam powder, the ginkgo leaf powder and the tea seed powder are respectively heated by 8 times of 80% ethanol and refluxed at 95 ℃ for 3 times, each time for 1.5 hours, and after suction filtration, supernate is taken and concentrated under reduced pressure, and freeze-dried to respectively obtain a yam ethanol extract, a ginkgo leaf ethanol extract and a tea seed ethanol extract.
8. The preparation method of uterus warming care membrane powder according to claim 6, characterized in that: in the step (2), the cinnamon extract, the morinda officinalis extract and the citronella extract are added with water and stirred and mixed for 25min at the constant temperature of 95r/min and 55 ℃ to obtain mixed primary liquid.
9. The preparation method of uterus warming care membrane powder according to claim 6, characterized in that: and (3) adding the moisture-preserving film-forming agent into the mixed primary liquid, stirring at a constant temperature of 135r/min for 45min at normal temperature, adding the ligusticum wallichii oil, and uniformly stirring at 250r/min to obtain a mixed solution.
10. The preparation method of uterus warming care membrane powder according to claim 6, characterized in that: and (4) adding the aloe fiber powder into the mixed solution before low-temperature reduced pressure concentration, and uniformly stirring at the stirring speed of 90-100 r/min.
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