CN110496071A - A kind of amber essence and its extracting method and application - Google Patents
A kind of amber essence and its extracting method and application Download PDFInfo
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- CN110496071A CN110496071A CN201910930835.XA CN201910930835A CN110496071A CN 110496071 A CN110496071 A CN 110496071A CN 201910930835 A CN201910930835 A CN 201910930835A CN 110496071 A CN110496071 A CN 110496071A
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- Prior art keywords
- amber
- solution
- auxiliary material
- essence
- extracts
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/965—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of inanimate origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0261—Solvent extraction of solids comprising vibrating mechanisms, e.g. mechanical, acoustical
- B01D11/0265—Applying ultrasound
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
- B01D61/14—Ultrafiltration; Microfiltration
- B01D61/147—Microfiltration
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Acoustics & Sound (AREA)
- Physics & Mathematics (AREA)
- Dermatology (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Water Supply & Treatment (AREA)
- Mechanical Engineering (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Cosmetics (AREA)
Abstract
Invention provides a kind of amber essence and its extracting method and application, which is characterized in that for the amber essence extracting method the following steps are included: amber extracts medicament stock prepares, amber extracts the modulation of medicament, and amber fine powder prepares, and extracts, filtering.A kind of amber is developed the beneficial effects of the present invention are: the present invention extracting medicament, the very good solution dispersing and dissolving problem of amber improves extraction efficiency and product quality；The amber essence extracting method that the present invention develops has method simple, and extraction effect is good, the excellent feature of product quality, and realizes the efficient recycling of amber leftover bits；Amber essence prepared by the present invention is added in cosmetics according to a certain percentage, is eliminating fatigue, is delaying senescence, body beautification beauty treatment etc. has positive effect.
Description
Technical field
The invention belongs to technical field of natural product extraction, and in particular to a kind of amber essence and its extracting method and answer
With.
Background technique
Amber is a kind of minerals, and value is equivalent to diamond, beautiful, emerald.It is in ground bottom by several hundred million years geology fortune
The dynamic jewellery fossil formed.
With the progress of science and technology, the medical value health value of amber is also more and more important.It can prepare in amber
Patent medicine, amber wine, amber cosmetics etc..Amber is used as medicine, and can calm the nerves and determine gas, body and mind of resting, useful for sleeping.Amber SPA, physical therapy
Fatigue can be eliminated, is delayed senescence, body beautification beauty treatment has important effect.
But due to amber have the characteristics that it is insoluble, so amber processing leftover bits be difficult to be utilized, Jin Erzao
At very big waste.So being badly in need of developing a kind of method that effective amber leftover bits recycle.
Summary of the invention
In order to make up for the deficiencies of the prior art, it the present invention provides a kind of amber essence and its extracting method and application, opens
The amber of hair extracts the difficult technical problem of medicament very good solution amber dissolution, realizes the efficiently sharp again of amber leftover bits
With.
The present invention provides a kind of extracting methods of amber essence, comprising the following steps:
(1) amber extracts medicament stock and prepares: oleic acid solutions is prepared by the mass ratio 5:3 of oleic acid and pure water, by tristearin
The mass ratio 2:1 of acid and pure water prepares stearic acid solution, and it is molten to prepare lauric acid by the mass ratio 2:1 of lauric acid and pure water
Liquid prepares propylene glycol solution by the mass ratio 3:1 of propylene glycol and pure water, prepares by the mass ratio 1:1 of auxiliary material 1 and pure water auxiliary
Expect 1 solution, prepares 2 solution of auxiliary material by the mass ratio 1:1 of auxiliary material 2 and pure water；
(2) amber extracts the modulation of medicament: in stainless steel barrel, pure water is added, is heated up to 70-80 DEG C；It stirs later
Triethanolamine is added, the oleic acid solutions, stearic acid solution, laurel acid solution, propylene glycol solution, 1 solution of auxiliary material and auxiliary material 2 are molten
Liquid, modulation extract medicament into amber；Wherein pure water, triethanolamine, oleic acid solutions, stearic acid solution, laurel acid solution, third
The mass ratio of 2 solution of glycol solution, 1 solution of auxiliary material and auxiliary material is 10:5:4:9:9:10:2:1；
(3) amber fine powder prepares: amber leftover bits being cleaned up, dry milling is to 500 mesh hereinafter, to obtain amber thin
Powder, it is spare；
(4) it extracts: under Ultrasonic Conditions, the amber being added in stainless steel barrel and extracts medicament, and is heated to 80-90
DEG C, it is slowly added to the amber fine powder, keeps ultrasonic wave, heating condition, stirs 1 hour, obtains extracting solution；The amber extracts
The addition mass ratio of medicament and amber fine powder is 5:1；
(5) it filters: the extracting solution is filtered by 3.0-10.0 μm of miillpore filter, filtrate is amber essence
China.
As a preferred solution, the auxiliary material 1 is ethyl alcohol and auxiliary material 2 is ethyl acetate.
It is further preferred that the amber extracts medicament pale yellow, pH 7.5-8.5, specific gravity 1.
The amber essence is prepared using method described in aforementioned any one.
A kind of application of the amber essence in cosmetics.
The beneficial effects of the present invention are: a kind of amber essence and its extracting method provided by the invention and application have with
Lower advantage:
1. the present invention develops a kind of amber and extract medicament, the very good solution dispersing and dissolving problem of amber is improved
Extraction efficiency and product quality；
2. the amber essence extracting method that the present invention develops has method simple, extraction effect is good, the excellent spy of product quality
Point；
3. the amber essence extracting method that the present invention develops realizes the efficient recycling of amber leftover bits；
4. amber essence prepared by the present invention is added in cosmetics according to a certain percentage, fatigue is being eliminated, is delaying to decline
Always, body beautification beauty treatment etc., there is positive effect.
Specific embodiment
In order to make the object, technical scheme and advantages of the embodiment of the invention clearer, to the technology in the embodiment of the present invention
Scheme is clearly and completely described, it is clear that and described embodiments are some of the embodiments of the present invention, rather than whole
Embodiment.
Embodiment 1
A kind of extracting method of amber essence, comprising the following steps:
(1) amber extracts medicament stock and prepares: oleic acid solutions is prepared by the mass ratio 5:3 of oleic acid and pure water, by tristearin
The mass ratio 2:1 of acid and pure water prepares stearic acid solution, and it is molten to prepare lauric acid by the mass ratio 2:1 of lauric acid and pure water
Liquid prepares propylene glycol solution by the mass ratio 3:1 of propylene glycol and pure water, prepares by the mass ratio 1:1 of ethyl alcohol and pure water auxiliary
Expect 1 solution, prepares 2 solution of auxiliary material by the mass ratio 1:1 of ethyl acetate and pure water；
(2) amber extracts the modulation of medicament: in stainless steel barrel, 20kg pure water is added, is heated up to 70-80 DEG C；Later
10kg triethanolamine is added in stirring, and 8kg oleic acid solutions, 18kg tristearin acid solution, 18kg laurel acid solution, 20kg propylene glycol are molten
2 solution of liquid, 1 solution of 6kg auxiliary material and auxiliary material, modulation extract medicament (pale yellow, pH 7.5-8.5, specific gravity 1) into amber；
(3) amber fine powder prepares: amber leftover bits being cleaned up, dry milling is to 500 mesh hereinafter, to obtain amber thin
Powder, it is spare；
(4) it extracts: under Ultrasonic Conditions, the amber being added in stainless steel barrel and extracts medicament, and is heated to 80-90
DEG C, it is slowly added to the amber fine powder, keeps ultrasonic wave, heating condition, stirs 1 hour, obtains extracting solution；The amber extracts
The addition mass ratio of medicament and amber fine powder is 5:1；
(5) it filters: the extracting solution is filtered by 3.0-10.0 μm of miillpore filter, filtrate is amber essence
China.
Embodiment 2
The amber essential oil that embodiment 1 is prepared carries out quality testing, detection method and the results are shown in Table 1.
1 amber essential oil quality testing data of table
| Project | Index |
| Appearance | Weak yellow liquid |
| Taste | Light Chinese herbal medicine taste |
| Texture | Uniformly |
| Density (20 DEG C) | 0.93 |
| Shading index (20 DEG C) | 1.54 |
| Amber oil concentration | 58% |
| Total plate count (CFU/g) | 23 |
Embodiment 3
The amber essence that embodiment 1 is prepared, according to 5-10% ratio be added facial mask essence in, and with not plus
The facial mask essence of amber essence compares test, and experimental result is shown, the facial mask water lock capability improving of amber essence is added
8-12% illustrates that amber essence prepared by the present invention in cosmetic applications, is eliminating fatigue, delaying senescence, the side such as body beautification beauty treatment
There is positive effect in face.
It should be appreciated that described above, the specific embodiments are only for explaining the present invention, is not intended to limit the present invention.By
Spiritual changes and variations that derived from of the invention are still in the protection scope of this invention.
Claims (5)
1. a kind of extracting method of amber essence, which is characterized in that the described method comprises the following steps:
(1) amber extracts medicament stock and prepares: prepare oleic acid solutions by the mass ratio 5:3 of oleic acid and pure water, by stearic acid and
The mass ratio 2:1 of pure water prepares stearic acid solution, prepares laurel acid solution by the mass ratio 2:1 of lauric acid and pure water, presses
The mass ratio 3:1 of propylene glycol and pure water prepares propylene glycol solution, and it is molten to prepare auxiliary material 1 by the mass ratio 1:1 of auxiliary material 1 and pure water
Liquid prepares 2 solution of auxiliary material by the mass ratio 1:1 of auxiliary material 2 and pure water；
(2) amber extracts the modulation of medicament: in stainless steel barrel, pure water is added, is heated up to 70-80 DEG C；Stirring is added later
Triethanolamine, the oleic acid solutions, stearic acid solution, laurel acid solution, 2 solution of propylene glycol solution, 1 solution of auxiliary material and auxiliary material,
Modulation extracts medicament into amber；Wherein pure water, triethanolamine, oleic acid solutions, stearic acid solution, laurel acid solution, the third two
The mass ratio of 2 solution of alcoholic solution, 1 solution of auxiliary material and auxiliary material is 10:5:4:9:9:10:2:1；
(3) amber fine powder prepares: amber leftover bits are cleaned up, dry milling to 500 mesh hereinafter, obtain amber fine powder,
It is spare；
(4) it extracts: under Ultrasonic Conditions, the amber being added in stainless steel barrel and extracts medicament, and is heated to 80-90 DEG C, delays
Slowly the amber fine powder is added, keeps ultrasonic wave, heating condition, stirs 1 hour, obtains extracting solution；The amber extracts medicament
Addition mass ratio with amber fine powder is 5:1；
(5) it filters: the extracting solution being filtered by 3.0-10.0 μm of miillpore filter, filtrate is amber essence.
2. a kind of extracting method of amber essence according to claim 1, which is characterized in that the auxiliary material 1 is ethyl alcohol, and
Auxiliary material 2 is ethyl acetate.
3. a kind of extracting method of amber essence according to claim 1, which is characterized in that the amber extracts medicament color
Yellowish, the pH 7.5-8.5 in pool, specific gravity 1.
4. a kind of amber essence, which is characterized in that the amber essence be using claim 1-3 any one method preparation
It obtains.
5. a kind of application of the amber essence according to claim 1 in cosmetics.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910930835.XA CN110496071A (en) | 2019-09-29 | 2019-09-29 | A kind of amber essence and its extracting method and application |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910930835.XA CN110496071A (en) | 2019-09-29 | 2019-09-29 | A kind of amber essence and its extracting method and application |
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| Publication Number | Publication Date |
|---|---|
| CN110496071A true CN110496071A (en) | 2019-11-26 |
Family
ID=68593016
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910930835.XA Pending CN110496071A (en) | 2019-09-29 | 2019-09-29 | A kind of amber essence and its extracting method and application |
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Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1325678A (en) * | 2000-05-26 | 2001-12-12 | 天津市化妆品科学技术研究所 | Amber cosmetics |
| FR2911779A1 (en) * | 2007-01-30 | 2008-08-01 | Lvmh Rech | Cosmetic composition containing extract of amber as active ingredient plus other active ingredients, e.g. plant extracts or vegetable glycolipid, used e.g. in gels, lotions or creams for skin care |
| JP2008266260A (en) * | 2007-04-24 | 2008-11-06 | Institute Of Physical & Chemical Research | Composition containing hyaluronic acid generation promoting factor obtainable from amber, and its use |
| JP2011256164A (en) * | 2010-05-11 | 2011-12-22 | Institute Of Physical & Chemical Research | Amber-derived vegf production promoter and formulation or cosmetic or hair and scalp cosmetic including the amber-derived vegf production promoter |
| JP2012240967A (en) * | 2011-05-19 | 2012-12-10 | Institute Of Physical & Chemical Research | Endothelin-1 production inhibitor, scf production inhibitor, and melanin production inhibitor obtained from amber, and use thereof |
| CN104666214A (en) * | 2013-11-30 | 2015-06-03 | 烟台巨先药业有限公司 | Foundation cream containing amber extract |
| CN106580800A (en) * | 2016-10-18 | 2017-04-26 | 张涛 | Amber mask |
| CN108949362A (en) * | 2018-08-07 | 2018-12-07 | 大连民族大学 | A method of extracting amber oil from amber |
-
2019
- 2019-09-29 CN CN201910930835.XA patent/CN110496071A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1325678A (en) * | 2000-05-26 | 2001-12-12 | 天津市化妆品科学技术研究所 | Amber cosmetics |
| FR2911779A1 (en) * | 2007-01-30 | 2008-08-01 | Lvmh Rech | Cosmetic composition containing extract of amber as active ingredient plus other active ingredients, e.g. plant extracts or vegetable glycolipid, used e.g. in gels, lotions or creams for skin care |
| JP2008266260A (en) * | 2007-04-24 | 2008-11-06 | Institute Of Physical & Chemical Research | Composition containing hyaluronic acid generation promoting factor obtainable from amber, and its use |
| JP2011256164A (en) * | 2010-05-11 | 2011-12-22 | Institute Of Physical & Chemical Research | Amber-derived vegf production promoter and formulation or cosmetic or hair and scalp cosmetic including the amber-derived vegf production promoter |
| JP2012240967A (en) * | 2011-05-19 | 2012-12-10 | Institute Of Physical & Chemical Research | Endothelin-1 production inhibitor, scf production inhibitor, and melanin production inhibitor obtained from amber, and use thereof |
| CN104666214A (en) * | 2013-11-30 | 2015-06-03 | 烟台巨先药业有限公司 | Foundation cream containing amber extract |
| CN106580800A (en) * | 2016-10-18 | 2017-04-26 | 张涛 | Amber mask |
| CN108949362A (en) * | 2018-08-07 | 2018-12-07 | 大连民族大学 | A method of extracting amber oil from amber |
Non-Patent Citations (1)
| Title |
|---|
| 黄文等: "《食品添加剂（第二版）》", 31 March 2013, 中国质检出版社 * |
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Application publication date: 20191126 |
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