CN110328980A - A kind of printing layer and preparation method thereof of radium-shine composite water transfer film - Google Patents

A kind of printing layer and preparation method thereof of radium-shine composite water transfer film Download PDF

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Publication number
CN110328980A
CN110328980A CN201910787700.2A CN201910787700A CN110328980A CN 110328980 A CN110328980 A CN 110328980A CN 201910787700 A CN201910787700 A CN 201910787700A CN 110328980 A CN110328980 A CN 110328980A
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China
Prior art keywords
polyvinyl alcohol
radium
film
paraffin
shine
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Pending
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CN201910787700.2A
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Chinese (zh)
Inventor
陈垂连
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Quanzhou Yingcai Color Printing Co Ltd
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Quanzhou Yingcai Color Printing Co Ltd
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Priority to CN201910787700.2A priority Critical patent/CN110328980A/en
Publication of CN110328980A publication Critical patent/CN110328980A/en
Pending legal-status Critical Current

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B27/00—Layered products comprising a layer of synthetic resin
    • B32B27/06—Layered products comprising a layer of synthetic resin as the main or only constituent of a layer, which is next to another layer of the same or of a different material
    • B32B27/08—Layered products comprising a layer of synthetic resin as the main or only constituent of a layer, which is next to another layer of the same or of a different material of synthetic resin
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B27/00—Layered products comprising a layer of synthetic resin
    • B32B27/30—Layered products comprising a layer of synthetic resin comprising vinyl (co)polymers; comprising acrylic (co)polymers
    • B32B27/306—Layered products comprising a layer of synthetic resin comprising vinyl (co)polymers; comprising acrylic (co)polymers comprising vinyl acetate or vinyl alcohol (co)polymers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B27/00—Layered products comprising a layer of synthetic resin
    • B32B27/30—Layered products comprising a layer of synthetic resin comprising vinyl (co)polymers; comprising acrylic (co)polymers
    • B32B27/308—Layered products comprising a layer of synthetic resin comprising vinyl (co)polymers; comprising acrylic (co)polymers comprising acrylic (co)polymers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B27/00—Layered products comprising a layer of synthetic resin
    • B32B27/40—Layered products comprising a layer of synthetic resin comprising polyurethanes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B7/00—Layered products characterised by the relation between layers; Layered products characterised by the relative orientation of features between layers, or by the relative values of a measurable parameter between layers, i.e. products comprising layers having different physical, chemical or physicochemical properties; Layered products characterised by the interconnection of layers
    • B32B7/04—Interconnection of layers
    • B32B7/12—Interconnection of layers using interposed adhesives or interposed materials with bonding properties
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
    • B41M—PRINTING, DUPLICATING, MARKING, OR COPYING PROCESSES; COLOUR PRINTING
    • B41M5/00—Duplicating or marking methods; Sheet materials for use therein
    • B41M5/025—Duplicating or marking methods; Sheet materials for use therein by transferring ink from the master sheet
    • B41M5/0253—Duplicating or marking methods; Sheet materials for use therein by transferring ink from the master sheet using a chemical colour-forming ink, e.g. chemical hectography
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
    • B41M—PRINTING, DUPLICATING, MARKING, OR COPYING PROCESSES; COLOUR PRINTING
    • B41M5/00—Duplicating or marking methods; Sheet materials for use therein
    • B41M5/025—Duplicating or marking methods; Sheet materials for use therein by transferring ink from the master sheet
    • B41M5/03—Duplicating or marking methods; Sheet materials for use therein by transferring ink from the master sheet by pressure
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
    • C08J5/18—Manufacture of films or sheets
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00—Inks
    • C09D11/02—Printing inks
    • C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00—Inks
    • C09D11/02—Printing inks
    • C09D11/10—Printing inks based on artificial resins
    • C09D11/102—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions other than those only involving unsaturated carbon-to-carbon bonds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00—Inks
    • C09D11/02—Printing inks
    • C09D11/10—Printing inks based on artificial resins
    • C09D11/106—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C09D11/107—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds from unsaturated acids or derivatives thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2307/00—Properties of the layers or laminate
    • B32B2307/50—Properties of the layers or laminate having particular mechanical properties
    • B32B2307/54—Yield strength; Tensile strength
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2307/00—Properties of the layers or laminate
    • B32B2307/50—Properties of the layers or laminate having particular mechanical properties
    • B32B2307/554—Wear resistance
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2329/00—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal, or ketal radical; Hydrolysed polymers of esters of unsaturated alcohols with saturated carboxylic acids; Derivatives of such polymer
    • C08J2329/02—Homopolymers or copolymers of unsaturated alcohols
    • C08J2329/04—Polyvinyl alcohol; Partially hydrolysed homopolymers or copolymers of esters of unsaturated alcohols with saturated carboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2403/00—Characterised by the use of starch, amylose or amylopectin or of their derivatives or degradation products
    • C08J2403/02—Starch; Degradation products thereof, e.g. dextrin
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2491/00—Characterised by the use of oils, fats or waxes; Derivatives thereof
    • C08J2491/06—Waxes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00—Use of organic ingredients
    • C08K5/04—Oxygen-containing compounds
    • C08K5/05—Alcohols; Metal alcoholates
    • C08K5/053—Polyhydroxylic alcohols

Abstract

The present invention relates to a kind of printing layers of radium-shine composite water transfer film, above-mentioned printing layer includes polyvinyl alcohol film layer and ink layer, and polyvinyl alcohol film layer includes the following each component of percentage: 10~13wt% of polyvinyl alcohol powder, 2.5~3.2wt% of starch, 0.8~1.2wt% of paraffin, 1.9~2.3wt% of glycerol, 0.9~1.1wt% of plasticizer, 78~86wt% of 0.42~0.52wt% of defoaming agent, 0.45~0.55wt% of stabilizer and water；Ink layer includes the following each component of percentage: 21.5~24.5wt% of acrylic resin, 7.1~8.0wt% of polyurethane resin, 8.5~9.2wt% of butyl acetate, 8.7~9.5wt% of ethyl acetate, 4.5~6.0wt% of 18.6~20.6wt% of ethyl acetate, 30~35wt% of toner and paraffin.Radium-shine layer is compounded in by glue after the polyvinyl alcohol material film forming of the printing layer of radium-shine composite water transfer film of the invention, polyvinyl alcohol film is tightly compounded on radium-shine layer, and printing layer is wear-resisting, stretch-proof, good transferring effect, it is both artistic and practical, it closes and is promoted the use of in radium-shine water transfer printing film technical field.

Description

A kind of printing layer and preparation method thereof of radium-shine composite water transfer film
Technical field
The present invention relates to radium-shine composite water transfer film, a kind of printing layer and its preparation of radium-shine composite water transfer film Method.
Background technique
Water transfer is one kind of specialty printing, it is acted on using the pressure of water and is transferred to the picture and text layer of ink on medium film It is a kind of novel printing mode by printing process and coating technology perfect combination on stock.The transfer of ordinary circumstance water can be with Be divided into water gauge transfer with water coating transfer, the two the difference is that transfer materials difference, water gauge transfer rely on transfer paper Realize the transfer of picture and text, and what water coating transfer relied on is flexible fabulous transfer film.There is transfer effect in existing water transfer printing film Fruit difference and problem at high cost, can not meet demand of the people to water transfer printing film.
Summary of the invention
The present invention provides a kind of printing layer and preparation method thereof of radium-shine composite water transfer film, to overcome above-mentioned existing water Transfer film there are the problem of.
The present invention adopts the following technical scheme:
A kind of printing layer of radium-shine composite water transfer film, which is characterized in that the printing layer includes polyvinyl alcohol film layer and oil Layer of ink,
Polyvinyl alcohol film layer includes the following each component of percentage: 10~13wt% of polyvinyl alcohol powder, starch 2.5~ 3.2wt%, 0.8~1.2wt% of paraffin, 1.9~2.3wt% of glycerol, 0.9~1.1wt% of plasticizer, 0.42~0.52wt% of defoaming agent, 75~86wt% of 0.45~0.55wt% of stabilizer and water；
Ink layer includes the following each component of percentage: 21.5~24.5wt% of acrylic resin, polyurethane resin 7.1~8.0wt%, 8.5~9.2wt% of butyl acetate, 8.7~9.5wt% of ethyl acetate, 18.6~20.6wt% of ethyl acetate, color 4.5~6.0wt% of 30~35wt% of powder and paraffin.
It is further improved ground, above-mentioned polyvinyl alcohol film layer includes the following each component of percentage: polyvinyl alcohol Powder 11wt%, starch 3.0wt%, paraffin 1.0wt%, glycerol 2.1wt%, plasticizer 1.0wt%, defoaming agent 0.48wt%, stabilizer 0.51wt% and water 80wt%；
Above-mentioned ink layer includes the following each component of percentage: acrylic resin 21.5wt%, polyurethane resin 7.6wt%, butyl acetate 8.9wt%, ethyl acetate 7.2wt%, ethyl acetate 19.2wt%, toner 30wt% and paraffin 5.6wt%.
A kind of preparation method of the printing layer of radium-shine composite water transfer film as described in claim 1, including walk as follows It is rapid:
(1), by polyvinyl alcohol powder, starch, paraffin, glycerol, plasticizer, defoaming agent, stabilizer and water pour into reaction kettle stirring it is molten Solution, heating pressurization dissolve it sufficiently, generate polyvinyl alcohol membrane material；
(2), acrylic resin, polyurethane resin, butyl acetate, ethyl acetate and ethyl acetate are poured into reaction kettle stir it is molten Solution, heating pressurization dissolve it sufficiently, generate modified colloidal resin；
(3), toner and paraffin will be added in colloidal resin modified in step (2), carries out being ground into ink.
By the above-mentioned description of this invention it is found that compared to the prior art, the present invention has the advantage that radium of the invention It penetrates after the polyvinyl alcohol material film forming of the printing layer of composite water transfer film and radium-shine layer is compounded in by glue, polyvinyl alcohol film is tight It is tightly compounded on radium-shine layer, printing layer is wear-resisting, stretch-proof, and good transferring effect is both artistic and practical, closes and leads in radium-shine water transfer printing film technology It promotes the use of in domain.
Specific embodiment
Embodiment 1:
A kind of printing layer of radium-shine composite water transfer film, above-mentioned printing layer include polyvinyl alcohol film layer and ink layer,
Above-mentioned polyvinyl alcohol film layer includes the following each component of percentage: polyvinyl alcohol powder 11wt%, starch 3.0wt%, paraffin 1.0wt%, glycerol 2.1wt%, plasticizer 1.0wt%, defoaming agent 0.48wt%, stabilizer 0.51wt% and water 80wt%；
Above-mentioned ink layer includes the following each component of percentage: acrylic resin 21.5wt%, polyurethane resin 7.6wt%, butyl acetate 8.9wt%, ethyl acetate 7.2wt%, ethyl acetate 19.2wt%, toner 30wt% and paraffin 5.6wt%.
A kind of preparation method of the printing layer of radium-shine composite water transfer film as described in claim 1, including walk as follows It is rapid:
(1), by polyvinyl alcohol powder, starch, paraffin, glycerol, plasticizer, defoaming agent, stabilizer and water pour into reaction kettle stirring it is molten Solution, heating pressurization dissolve it sufficiently, generate polyvinyl alcohol membrane material；
(2), acrylic resin, polyurethane resin, butyl acetate, ethyl acetate and ethyl acetate are poured into reaction kettle stir it is molten Solution, heating pressurization dissolve it sufficiently, generate modified colloidal resin；
(3), toner and paraffin will be added in colloidal resin modified in step (2), carries out being ground into ink.
Embodiment 2:
A kind of printing layer of radium-shine composite water transfer film, above-mentioned printing layer include polyvinyl alcohol film layer and ink layer,
Polyvinyl alcohol film layer includes the following each component of percentage: polyvinyl alcohol powder 10wt%, starch 2.5wt%, stone Wax 0.8wt%, glycerol 1.9wt%, plasticizer 0.9wt%, defoaming agent 0.42wt%, stabilizer 0.45wt% and water 83wt%；
Ink layer includes the following each component of percentage: acrylic resin 21.5wt%, polyurethane resin 7.1wt%, Butyl acetate 8.5wt%, ethyl acetate 8.7wt%, ethyl acetate 17.6wt%, toner 31wt% and paraffin 4.5wt%.
The preparation method of the printing layer of radium-shine composite water transfer film is same as Example 1.
Embodiment 3:
A kind of printing layer of radium-shine composite water transfer film, above-mentioned printing layer include polyvinyl alcohol film layer and ink layer,
Polyvinyl alcohol film layer includes the following each component of percentage: polyvinyl alcohol powder 13wt%, starch 3.2wt%, stone Wax 1.2wt%, glycerol 2.3wt%, plasticizer 1.1wt%, defoaming agent 0.52wt%, stabilizer 0.55wt% and water 78wt%；
Ink layer includes the following each component of percentage: acrylic resin 21.5wt%, polyurethane resin 7.1wt%, Butyl acetate 9.2wt%, ethyl acetate 9.5wt%, ethyl acetate 20.6wt%, toner 27wt% and paraffin 6.0wt%.
The preparation method of the printing layer of radium-shine composite water transfer film is same as Example 1.
It is compounded in after the polyvinyl alcohol material film forming of the printing layer of radium-shine composite water transfer film of the invention by glue Radium-shine layer, polyvinyl alcohol film are tightly compounded on radium-shine layer, and printing layer is wear-resisting, stretch-proof, and good transferring effect is both artistic and practical, are closed It is promoted the use of in radium-shine water transfer printing film technical field.
The above is only a specific embodiment of the present invention, but the design concept of the present invention is not limited to this, all to utilize this Design makes a non-material change to the present invention, and should all belong to behavior that violates the scope of protection of the present invention.

Claims (3)

1. a kind of printing layer of radium-shine composite water transfer film, which is characterized in that the printing layer include polyvinyl alcohol film layer and Ink layer,
Polyvinyl alcohol film layer includes the following each component of percentage: 10~13wt% of polyvinyl alcohol powder, starch 2.5~ 3.2wt%, 0.8~1.2wt% of paraffin, 1.9~2.3wt% of glycerol, 0.9~1.1wt% of plasticizer, 0.42~0.52wt% of defoaming agent, 75~86wt% of 0.45~0.55wt% of stabilizer and water；
Ink layer includes the following each component of percentage: 21.5~24.5wt% of acrylic resin, polyurethane resin 7.1~8.0wt%, 8.5~9.2wt% of butyl acetate, 8.7~9.5wt% of ethyl acetate, 18.6~20.6wt% of ethyl acetate, color 4.5~6.0wt% of 30~35wt% of powder and paraffin.
2. a kind of printing layer of radium-shine composite water transfer film as described in claim 1, which is characterized in that
The polyvinyl alcohol film layer includes the following each component of percentage: polyvinyl alcohol powder 11wt%, starch 3.0wt%, paraffin 1.0wt%, glycerol 2.1wt%, plasticizer 1.0wt%, defoaming agent 0.48wt%, stabilizer 0.51wt% and water 80wt%；
The ink layer includes the following each component of percentage: acrylic resin 21.5wt%, polyurethane resin 7.6wt%, butyl acetate 8.9wt%, ethyl acetate 7.2wt%, ethyl acetate 19.2wt%, toner 30wt% and paraffin 5.6wt%.
3. a kind of preparation method of the printing layer of radium-shine composite water transfer film as described in claim 1, which is characterized in that packet Include following steps:
(1), by polyvinyl alcohol powder, starch, paraffin, glycerol, plasticizer, defoaming agent, stabilizer and water pour into reaction kettle stirring it is molten Solution, heating pressurization dissolve it sufficiently, are machined by coating and generate polyvinyl alcohol thin-film material；
(2), acrylic resin, polyurethane resin, butyl acetate, ethyl acetate and ethyl acetate are poured into reaction kettle stir it is molten Solution, heating pressurization dissolve it sufficiently, generate modified colloidal resin；
(3), toner and paraffin will be added in colloidal resin modified in step (2), carries out being ground into ink.
CN201910787700.2A 2019-08-26 2019-08-26 A kind of printing layer and preparation method thereof of radium-shine composite water transfer film Pending CN110328980A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111890830A (en) * 2020-01-17 2020-11-06 英狮科技(东莞)有限公司 Preparation method of magnetic 3D water transfer film
CN115058045A (en) * 2022-07-21 2022-09-16 石狮市锦源体育用品有限公司 Radium-shine pva water transfer printing membrane of stable form

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111890830A (en) * 2020-01-17 2020-11-06 英狮科技(东莞)有限公司 Preparation method of magnetic 3D water transfer film
CN115058045A (en) * 2022-07-21 2022-09-16 石狮市锦源体育用品有限公司 Radium-shine pva water transfer printing membrane of stable form

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