CN110200846A - A kind of oil-control moisturizing mildy wash and preparation method thereof - Google Patents
A kind of oil-control moisturizing mildy wash and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
- A61K8/416—Quaternary ammonium compounds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
- A61K8/442—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/466—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfonic acid derivatives; Salts
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/737—Galactomannans, e.g. guar; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/008—Preparations for oily skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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Abstract
The invention discloses a kind of oil-control moisturizing mildy wash and preparation method thereof, which includes: that water and sodium hydroxyethyl cellulose are uniformly mixed by (1)；When warming while stirring to the first temperature, Cocoamidopropyl betaine, myristoyl-N-methylaminoacetic acid sodium, agar compound stabilizer, melon rubber, NaCl, fatty alkyl dimethyl tertiary amine and 3- chlorine-2-hydroxyl propane sulfonic acid sodium is then added；Warming while stirring is stirred and is spaced under the first mixing speed and be ultrasonically treated to second temperature, cooling, obtains mixing A liquid；(2) lye is added in mixing A liquid and adjusts pH value, 1,2-PD and glycerol is then added, warming while stirring is in the pasty state to reactant, cooling, obtains oil-control moisturizing mildy wash.Oil-control moisturizing mildy wash of the invention has efficient oil removal efficiency and skin clean-up performance, except speed oil is fast, has good oil removing moistening effect.
Description
Technical field
The invention belongs to cosmetic technical fields, more particularly, to a kind of oil-control moisturizing mildy wash and preparation method thereof.
Background technique
Skin is divided into many kinds, can specifically be roughly divided into skin: Oily, dry skin, neutral skin and mixing
The multiple types such as skin.Wherein, the secreting function of Oily person, sebaceous glands are more vigorous, and facial oiliness is not easy to clean, have
Influence the glossy of beauty；Also easily occurs the corresponding skin disease of face, such as acne, seborrhea etc. simultaneously.
In order to preferably cope with Oily, the larger problem of skin ingress of oil amount has abstersive facial cleanser conduct
Facial cleansing agent is gradually received by consumer, but currently, facial cleanser scarce capacity in terms of oil removing, embodies primary
Oil removing is not clean need to be cleaned multiple times oil removing, this is not only larger to facial lesion for user, also wastes time and money；Therefore
In order to better meet Oily Man's Demands, it is necessary to provide a kind of mildy wash, it is made to possess the same of efficient degreasing rate
When, moistening effect is also possessed to skin after oil removing.
Summary of the invention
The purpose of the present invention is overcoming the deficiencies of existing technologies, a kind of efficient oil-control moisturizing mildy wash and its preparation side are provided
Method, except speed oil is fast, also has good moistening effect so that the mildy wash of preparation has efficient oil removal efficiency after oil removing.
To achieve the goals above, an aspect of of the present present invention provides a kind of preparation method of oil-control moisturizing mildy wash, should
Preparation method includes:
(1) water and sodium hydroxyethyl cellulose are uniformly mixed；When warming while stirring to the first temperature, cocounut oil is then added
Amido propyl betaine, myristoyl-N-methylaminoacetic acid sodium, agar compound stabilizer, melon rubber, NaCl, fatty alkyl dimethyl tertiary amine
With 3- chlorine-2-hydroxyl propane sulfonic acid sodium；Warming while stirring stirs under the first mixing speed to second temperature and is spaced progress
Ultrasonic treatment, it is cooling, obtain mixing A liquid；
(2) lye is added in the mixing A liquid and adjusts pH value, 1,2-PD and glycerol is then added, while stirring
Heating, it is in the pasty state to reactant, cooling, obtain the oil-control moisturizing mildy wash.
Another aspect of the present invention provides a kind of oil-control moisturizing mildy wash of above-mentioned preparation method preparation.
Technical solution of the present invention has the following beneficial effects:
(1) technical solution of the present invention, during preparing mildy wash, the C-Cl key of 3- chlorine-2-hydroxyl propane sulfonic acid sodium
Fracture regenerates N-Cl key with fatty alkyl dimethyl tertiary amine, and molecule carbon chain increases, and increases surface-active ability, simultaneously
Micella is formed with surfactants other in solution, increases the contact area of lipophilic group and grease in micella, and then effectively
Enhance mildy wash oil removing ability, improves and remove oil mass；The grease of myristoyl-N-methylaminoacetic acid sodium and skin surface can form biggish poly-
Object is closed to adsorb the spot in skin pore, reduces skin tight feeling, optimizes skin face cleaning effect, meanwhile, there is certain guarantor
Wet effect.
(2) the oil-control moisturizing mildy wash that the present invention is prepared has efficient oil removal efficiency and skin clean-up performance, removes
Speed oil is fast, has good oil removing moistening effect.
Other features and advantages of the present invention will then part of the detailed description can be specified.
Specific embodiment
The preferred embodiment of the present invention is described in more detail below.Although the following describe preferred implementations of the invention
Mode, however, it is to be appreciated that may be realized in various forms the present invention without that should be limited by the embodiments set forth herein.Phase
Instead, these embodiments are provided so that the present invention is more thorough and complete, and can be by the scope of the present invention completely
It is communicated to those skilled in the art.
One aspect of the present invention provides a kind of preparation method of oil-control moisturizing mildy wash, which includes:
(1) water and sodium hydroxyethyl cellulose are uniformly mixed；When warming while stirring to the first temperature, cocounut oil is then added
Amido propyl betaine, myristoyl-N-methylaminoacetic acid sodium, agar compound stabilizer, melon rubber, NaCl, fatty alkyl dimethyl tertiary amine
With 3- chlorine-2-hydroxyl propane sulfonic acid sodium；Warming while stirring stirs under the first mixing speed to second temperature and is spaced progress
Ultrasonic treatment, it is cooling, obtain mixing A liquid；
(2) lye is added in the mixing A liquid and adjusts pH value, 1,2-PD and glycerol is then added, while stirring
Heating, it is in the pasty state to reactant, cooling, obtain the oil-control moisturizing mildy wash.
In accordance with the present invention it is preferred that based on parts by weight, the dosage of the water is 40-50 parts, sodium hydroxyethyl cellulose
Dosage is 10-15 parts, the dosage of Cocoamidopropyl betaine is 3-5 parts, the dosage of myristoyl-N-methylaminoacetic acid sodium is 5-10 parts,
The dosage of agar compound stabilizer is 3-8 parts, the dosage of melon rubber is 5-8 parts, the dosage of NaCl is 5-10 parts, fatty alkyl two
The dosage that the dosage of methyl tertiary amine is 10-15 parts, the dosage of 3- chlorine-2-hydroxyl propane sulfonic acid sodium is 10-15 parts, 1,2- propylene glycol
Dosage for 5-10 parts and glycerol is 8-15 parts.
In accordance with the present invention it is preferred that based on parts by weight, the dosage of the water is 43-48 parts, sodium hydroxyethyl cellulose
Dosage is 11-13 parts, the dosage of Cocoamidopropyl betaine is 3-5 parts, the dosage of myristoyl-N-methylaminoacetic acid sodium is newborn 6-9
Part, the dosage of agar compound stabilizer be 4-6 parts, the dosage of melon rubber is 5-7 parts, the dosage of NaCl is 6-9 parts, fatty alkyl
The use that the dosage of dimethyl tertiary amine is 11-13 parts, the dosage of 3- chlorine-2-hydroxyl propane sulfonic acid sodium is 11-13 parts, 1,2- propylene glycol
Amount is 7-9 parts and the dosage of glycerol is 9-12 parts.
In accordance with the present invention it is preferred that first temperature is 65-75 DEG C in step (1)；Second temperature is 85-95 DEG C；
It is described to be stirred under the first mixing speed and be spaced that carry out ultrasonic treatment be low whipping speed be 120-160r/min
Lower stirring 0.5-1h carries out the primary ultrasonic treatment for continuing 4-6min every 8-12min during stirring.
In accordance with the present invention it is preferred that the ultrasonic power of ultrasonic treatment described in step (1) is 450-550W.
In accordance with the present invention it is preferred that adjusting pH value is 6-7 in step (2).
In accordance with the present invention it is preferred that the lye is the hydrogen-oxygen that molar concentration is 0.08-0.12mol/L in step (2)
Change aqueous solutions of potassium.
In accordance with the present invention it is preferred that in step (2), warming while stirring be under the mixing speed of 100-120r/min,
85-100 DEG C is warming up to the heating rate of 1-3 DEG C/min.
In accordance with the present invention it is preferred that being cooled to 20-30 DEG C.
It is to be cooled to 20-30 DEG C in step (1) and step (2) in the present invention.
Another aspect of the present invention provides the oil-control moisturizing mildy wash of above-mentioned preparation method preparation.
The present invention is further illustrated by the following examples:
Agar compound stabilizer used in following embodiment comprises the following steps: agar, xanthan gum, carboxymethyl is fine
It ties up plain sodium and water is uniformly mixed, obtain agar compound stabilizer；Relative to the agar compound stabilizer of 1L, agar content 30g,
Xanthans content is 5g, carboxymethylcellulosodium sodium content 20g.
Embodiment 1
The present embodiment provides a kind of oil-control moisturizing mildy wash, are prepared by following raw material in parts by weight: 40 parts of water, hydroxyl
15 parts of ethyl cellulose sodium, 10 parts of 1,2- propylene glycol, 8 parts of glycerol, 3 parts of Cocoamidopropyl betaine, myristoyl-N-methylaminoacetic acid
10 parts of sodium, 8 parts of melon rubber, 10 parts of NaCl, 15 parts of fatty alkyl dimethyl tertiary amine, 10 parts of 3- chlorine-2-hydroxyl propane sulfonic acid sodium,
8 parts of agar compound stabilizer.
Above-mentioned oil-control moisturizing mildy wash, specific preparation process is as follows:
(1) water, sodium hydroxyethyl cellulose, Cocoamidopropyl betaine, myristoyl are weighed respectively according to parts by weight
Sodium sarcosinate, agar compound stabilizer, melon rubber, NaCl, fatty alkyl dimethyl tertiary amine, 3- chlorine-2-hydroxyl propane sulfonic acid sodium；
Water and sodium hydroxyethyl cellulose are mixed evenly at 25 DEG C and are placed in reaction kettle, when warming while stirring is to 65 DEG C,
Then Cocoamidopropyl betaine, myristoyl-N-methylaminoacetic acid sodium, agar compound stabilizer, melon rubber, NaCl, fatty alkane is added
Base dimethyl tertiary amine and 3- chlorine-2-hydroxyl propane sulfonic acid sodium；Warming while stirring is to 95 DEG C, and low whipping speed is 120r/min
Lower stirring 0.5h carries out primary 5min, the power of continuing every 10min during stirring as the ultrasonic treatment of 500W, is cooled to 25 DEG C,
A liquid must be mixed；
(2) 1,2-PD, glycerol are weighed respectively according to parts by weight, the hydrogen-oxygen of 0.1mol/L is added in mixing A liquid
Change aqueous solutions of potassium and adjust pH to 7,1,2-PD and glycerol is added in the mixing A liquid for regulating pH, in stirring for 100r/min
Mix under speed, be warming up to 90 DEG C with the heating rate of 2 DEG C/min, when reactant in the pasty state when be cooled to 25 DEG C, obtain oil-control moisturizing
Mildy wash.
Embodiment 2
The present embodiment provides a kind of oil-control moisturizing mildy wash, are prepared by following raw material in parts by weight: 50 parts of water, hydroxyl
13 parts of ethyl cellulose sodium, 7 parts of 1,2- propylene glycol, 15 parts of glycerol, 5 parts of Cocoamidopropyl betaine, myristoyl-N-methylaminoacetic acid
7 parts of sodium, 5 parts of melon rubber, 5 parts of NaCl, 11 parts of fatty alkyl dimethyl tertiary amine, 15 parts of 3- chlorine-2-hydroxyl propane sulfonic acid sodium, fine jade
6 parts of rouge compound stabilizer.
Above-mentioned oil-control moisturizing mildy wash, specific preparation process is as follows:
(1) water, sodium hydroxyethyl cellulose, Cocoamidopropyl betaine, myristoyl are weighed respectively according to parts by weight
Sodium sarcosinate, agar compound stabilizer, melon rubber, NaCl, fatty alkyl dimethyl tertiary amine, 3- chlorine-2-hydroxyl propane sulfonic acid sodium；
Water and sodium hydroxyethyl cellulose are mixed evenly at 25 DEG C and are placed in reaction kettle, when warming while stirring is to 70 DEG C,
Then Cocoamidopropyl betaine, myristoyl-N-methylaminoacetic acid sodium, agar compound stabilizer, melon rubber, NaCl, fatty alkane is added
Base dimethyl tertiary amine and 3- chlorine-2-hydroxyl propane sulfonic acid sodium；Warming while stirring is to 87 DEG C, and low whipping speed is 145r/min
Lower stirring 0.8h carries out primary 5min, the power of continuing every 10min during stirring as the ultrasonic treatment of 500W, is cooled to 25 DEG C,
A liquid must be mixed；
(2) 1,2-PD, glycerol are weighed respectively according to parts by weight, the hydrogen-oxygen of 0.1mol/L is added in mixing A liquid
Change aqueous solutions of potassium and adjust pH to 6.5,1,2-PD and glycerol is added in the mixing A liquid for regulating pH, 120r/min's
Under mixing speed, be warming up to 96 DEG C with the heating rate of 2 DEG C/min, when reactant in the pasty state when be cooled to 25 DEG C, obtain oil-control guarantor
Wet mildy wash.
Embodiment 3
The present embodiment provides a kind of oil-control moisturizing mildy wash, are prepared by following raw material in parts by weight: 42 parts of water, hydroxyl
10 parts of ethyl cellulose sodium, 5 parts of 1,2- propylene glycol, 13 parts of glycerol, 4 parts of Cocoamidopropyl betaine, myristoyl-N-methylaminoacetic acid
5 parts of sodium, 6 parts of melon rubber, 7 parts of NaCl, 10 parts of fatty alkyl dimethyl tertiary amine, 11 parts of 3- chlorine-2-hydroxyl propane sulfonic acid sodium, fine jade
3 parts of rouge compound stabilizer.
Above-mentioned oil-control moisturizing mildy wash, specific preparation process is as follows:
(1) water, sodium hydroxyethyl cellulose, Cocoamidopropyl betaine, myristoyl are weighed respectively according to parts by weight
Sodium sarcosinate, agar compound stabilizer, melon rubber, NaCl, fatty alkyl dimethyl tertiary amine, 3- chlorine-2-hydroxyl propane sulfonic acid sodium；
Water and sodium hydroxyethyl cellulose are mixed evenly at 25 DEG C and are placed in reaction kettle, when warming while stirring is to 70 DEG C,
Then Cocoamidopropyl betaine, myristoyl-N-methylaminoacetic acid sodium, agar compound stabilizer, melon rubber, NaCl, fatty alkane is added
Base dimethyl tertiary amine and 3- chlorine-2-hydroxyl propane sulfonic acid sodium；Warming while stirring is to 88 DEG C, and low whipping speed is 160r/min
Lower stirring 1h carries out primary 5min, the power of continuing every 10min during stirring as the ultrasonic treatment of 500W, is cooled to 25 DEG C, obtains
Mix A liquid；
(2) 1,2-PD, glycerol are weighed respectively according to parts by weight, the hydrogen-oxygen of 0.1mol/L is added in mixing A liquid
Change aqueous solutions of potassium and adjust pH to 6,1,2-PD and glycerol is added in the mixing A liquid for regulating pH, in stirring for 110r/min
Mix under speed, be warming up to 85 DEG C with the heating rate of 2 DEG C/min, when reactant in the pasty state when be cooled to 25 DEG C, obtain oil-control moisturizing
Mildy wash.
Embodiment 4
The present embodiment provides a kind of oil-control moisturizing mildy wash, are prepared by following raw material in parts by weight: 45 parts of water, hydroxyl
12 parts of ethyl cellulose sodium, 8 parts of 1,2- propylene glycol, 10 parts of glycerol, 4 parts of Cocoamidopropyl betaine, myristoyl-N-methylaminoacetic acid
8 parts of sodium, 6 parts of melon rubber, 8 parts of NaCl, 12 parts of fatty alkyl dimethyl tertiary amine, 12 parts of 3- chlorine-2-hydroxyl propane sulfonic acid sodium, fine jade
5 parts of rouge compound stabilizer.
Wherein, the preparation method is the same as that of Example 1 for the oil-control moisturizing mildy wash.
Embodiment 5
The present embodiment provides a kind of oil-control moisturizing mildy wash, are prepared by following raw material in parts by weight: 47 parts of water, hydroxyl
11 parts of ethyl cellulose sodium, 6 parts of 1,2- propylene glycol, 12 parts of glycerol, 3 parts of Cocoamidopropyl betaine, myristoyl-N-methylaminoacetic acid
9 parts of sodium, 7 parts of melon rubber, 8 parts of NaCl, 13 parts of fatty alkyl dimethyl tertiary amine, 14 parts of 3- chlorine-2-hydroxyl propane sulfonic acid sodium, fine jade
7 parts of rouge compound stabilizer.
Wherein, the oil-control moisturizing mildy wash preparation method is the same as embodiment 2.
Test case
1-5 of the embodiment of the present invention and commercially available Oily mildy wash are tested for the property, wherein foaming capacity and foam
Stability improves the test of Ross-Miles method using GB/T7462-94.Specific test result is as shown in table 1；
Wherein, skin oil and fat contains before oil removal rate=(skin oil and fat content after skin oil and fat content-oil removing before oil removing)/oil removing
Amount × 100%.
1 oil-control moisturizing mildy wash the performance test results of table
As shown in Table 1, oil-control moisturizing mildy wash of the invention, improves mildy wash degreasing ability, has good remove
Oily moistening effect.
Various embodiments of the present invention are described above, above description is exemplary, and non-exclusive, and
It is not limited to disclosed each embodiment.Without departing from the scope and spirit of illustrated each embodiment, for this skill
Many modifications and changes are obvious for the those of ordinary skill in art field.
Claims (10)
1. a kind of preparation method of oil-control moisturizing mildy wash, which is characterized in that the preparation method includes:
(1) water and sodium hydroxyethyl cellulose are uniformly mixed；When warming while stirring to the first temperature, coconut oleoyl amine is then added
Propyl betaine, myristoyl-N-methylaminoacetic acid sodium, agar compound stabilizer, melon rubber, NaCl, fatty alkyl dimethyl tertiary amine and 3-
Chlorine-2-hydroxyl propane sulfonic acid sodium；Warming while stirring stirs under the first mixing speed to second temperature and is spaced progress ultrasound
Processing, it is cooling, obtain mixing A liquid；
(2) lye is added in the mixing A liquid and adjusts pH value, then addition 1,2-PD and glycerol, warming while stirring,
In the pasty state to reactant, cooling, obtain the oil-control moisturizing mildy wash.
2. preparation method according to claim 1, wherein based on parts by weight, the dosage of the water is 40-50 parts, hydroxyl
The dosage of ethyl cellulose sodium is 10-15 parts, the dosage of Cocoamidopropyl betaine is 3-5 parts, myristoyl-N-methylaminoacetic acid sodium
Dosage be 5-10 parts, the dosage of agar compound stabilizer is 3-8 parts, the dosage of melon rubber is 5-8 parts, the dosage of NaCl is 5-
10 parts, the dosage of fatty alkyl dimethyl tertiary amine be 10-15 parts, the dosage of 3- chlorine-2-hydroxyl propane sulfonic acid sodium is 10-15 parts,
The dosage of 1,2- propylene glycol is 5-10 parts and the dosage of glycerol is 8-15 parts.
3. preparation method according to claim 2, wherein based on parts by weight, the dosage of the water is 43-48 parts, hydroxyl
The dosage of ethyl cellulose sodium is 11-13 parts, the dosage of Cocoamidopropyl betaine is 3-5 parts, myristoyl-N-methylaminoacetic acid sodium
Dosage be 6-9 parts newborn, agar compound stabilizer dosage be 4-6 parts, the dosage of melon rubber is 5-7 parts, the dosage of NaCl is
6-9 parts, the dosage of fatty alkyl dimethyl tertiary amine be 11-13 parts, the dosage of 3- chlorine-2-hydroxyl propane sulfonic acid sodium is 11-13 parts,
The dosage of 1,2- propylene glycol is 7-9 parts and the dosage of glycerol is 9-12 parts.
4. preparation method according to claim 1, wherein in step (1), first temperature is 65-75 DEG C；Second temperature
Degree is 85-95 DEG C；
It is described stirred under the first mixing speed and be spaced carry out ultrasonic treatment be to be stirred under low whipping speed is 120-160r/min
0.5-1h is mixed, carries out the primary ultrasonic treatment for continuing 4-6min every 8-12min during stirring.
5. preparation method according to claim 1, wherein the ultrasonic power of ultrasonic treatment described in step (1) is 450-
550W。
6. preparation method according to claim 1, wherein in step (2), adjusting pH value is 6-7.
7. preparation method according to claim 1, wherein in step (2), the lye is that molar concentration is 0.08-
The potassium hydroxide aqueous solution of 0.12mol/L.
8. preparation method according to claim 1, wherein in step (2), warming while stirring is in 100-120r/min
Mixing speed under, be warming up to 85-100 DEG C with the heating rate of 1-3 DEG C/min.
9. preparation method according to claim 1, wherein be cooled to 20-30 DEG C.
10. the oil-control moisturizing mildy wash of the preparation of preparation method described in any one of claim 1-9.
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| CN106431995A (en) * | 2016-09-09 | 2017-02-22 | 江南大学 | Synthetic method of aryl sulphobetaine in solvent-free system |
| CN107496183A (en) * | 2017-08-17 | 2017-12-22 | 张艺峰 | Clean replenishing water and preserving moisture mildy wash |
| CN107754854A (en) * | 2017-11-12 | 2018-03-06 | 闽江学院 | The preparation and its application of hydroxyl/sulfonic group difunctionality vanadium doping heteropoly acid ion hybrid |
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2019
- 2019-07-11 CN CN201910625092.5A patent/CN110200846A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106038352A (en) * | 2016-06-01 | 2016-10-26 | 茗燕生物科技(上海)有限公司 | Environment-friendly super-concentrated hand washing slices/granules and manufacturing method thereof |
| CN106431995A (en) * | 2016-09-09 | 2017-02-22 | 江南大学 | Synthetic method of aryl sulphobetaine in solvent-free system |
| CN107496183A (en) * | 2017-08-17 | 2017-12-22 | 张艺峰 | Clean replenishing water and preserving moisture mildy wash |
| CN107754854A (en) * | 2017-11-12 | 2018-03-06 | 闽江学院 | The preparation and its application of hydroxyl/sulfonic group difunctionality vanadium doping heteropoly acid ion hybrid |
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Application publication date: 20190906 |
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