CN110124595B - Lens monomer is high-efficient condensing equipment for reation kettle - Google Patents
Lens monomer is high-efficient condensing equipment for reation kettle Download PDFInfo
- Publication number
- CN110124595B CN110124595B CN201910510735.1A CN201910510735A CN110124595B CN 110124595 B CN110124595 B CN 110124595B CN 201910510735 A CN201910510735 A CN 201910510735A CN 110124595 B CN110124595 B CN 110124595B
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- inner shell
- rotating shaft
- spiral blades
- shell
- storage tank
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- 239000000178 monomer Substances 0.000 title claims abstract description 8
- 239000007788 liquid Substances 0.000 claims abstract description 33
- 238000006243 chemical reaction Methods 0.000 claims abstract description 7
- 239000007921 spray Substances 0.000 claims description 21
- 239000003507 refrigerant Substances 0.000 claims description 8
- 238000011084 recovery Methods 0.000 claims description 7
- 238000005406 washing Methods 0.000 claims description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- 238000009833 condensation Methods 0.000 claims description 5
- 230000005494 condensation Effects 0.000 claims description 4
- 230000000149 penetrating effect Effects 0.000 claims description 2
- 239000012535 impurity Substances 0.000 abstract description 4
- 238000001914 filtration Methods 0.000 abstract description 3
- 239000002245 particle Substances 0.000 abstract description 3
- 239000007787 solid Substances 0.000 abstract description 3
- 238000001816 cooling Methods 0.000 abstract description 2
- 230000010354 integration Effects 0.000 abstract description 2
- 239000011521 glass Substances 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- XXROGKLTLUQVRX-UHFFFAOYSA-N allyl alcohol Chemical compound OCC=C XXROGKLTLUQVRX-UHFFFAOYSA-N 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000004064 recycling Methods 0.000 description 2
- 229920005989 resin Polymers 0.000 description 2
- 239000011347 resin Substances 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000007859 condensation product Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 229920003002 synthetic resin Polymers 0.000 description 1
- 239000000057 synthetic resin Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
- B01D5/0057—Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes
- B01D5/0072—Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes with filtration
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
- B01D5/0078—Condensation of vapours; Recovering volatile solvents by condensation characterised by auxiliary systems or arrangements
- B01D5/009—Collecting, removing and/or treatment of the condensate
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D50/00—Combinations of methods or devices for separating particles from gases or vapours
- B01D50/20—Combinations of devices covered by groups B01D45/00 and B01D46/00
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/002—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by condensation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
- B01D53/1487—Removing organic compounds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00121—Controlling the temperature by direct heating or cooling
- B01J2219/0013—Controlling the temperature by direct heating or cooling by condensation of reactants
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Analytical Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The invention provides a high-efficiency condensing device for a lens monomer reaction kettle, which comprises a condenser body supported by supporting feet in a standing manner; the condenser body consists of a double-layer shell formed by an outer shell and an inner shell, the lower end and the upper end of the inner shell are respectively provided with an air inlet pipe and an air outlet pipe, and the upper end of the air inlet pipe penetrates through the porous plate and is communicated with the treatment section; a rotating shaft vertically extending from the top of the inner shell to the bottom, and spiral blades fixed on the rotating shaft; the two side walls of the inner shell are symmetrically provided with a plurality of layers of filter plates which are inclined upwards, and the end parts of the filter plates are close to but not connected with the spiral blades; the invention adopts the spiral blades arranged on the rotating shaft to form a spiral air passage for the air flow to rise in the condenser, and solid small particles and some liquid drop impurities in the air are adsorbed on the spiral blades and the filter plate, thereby realizing the integration of filtration and cooling.
Description
Technical Field
The invention relates to a high-efficiency condensing device for a lens monomer reaction kettle.
Background
At present, development of glasses lenses on the market using synthetic resins having excellent optical characteristics as lens materials in addition to organic glass is continuously under development; compared with inorganic glass, the resin lens has the characteristics of light weight, high transparency, impact resistance, easiness in processing and the like; in the production process of the existing resin lens synthesis reaction equipment, gasified products such as allyl alcohol and the like or liquid or solid impurity particles wrapped in the gasified products are produced in a reaction kettle, and then condensing equipment is additionally arranged for recycling, but the existing condensing equipment is generally low in condensing efficiency and does not have a filtering function, impurities mixed in the condensed liquid are easy to block an air inlet pipe, and the yield loss of the condensed products is caused, so that the prior art is necessary to be further improved.
Disclosure of Invention
The invention aims to solve the defects in the prior art and provides a high-efficiency condensing device for a lens monomer reaction kettle, which comprises a condenser body supported in a standing way through supporting feet; the condenser body consists of a double-layer shell formed by an outer shell and an inner shell, and a condensation treatment area is arranged in the inner shell; the condensing treatment zone comprises an upper treatment zone and a lower conical liquid recovery zone separated by a perforated plate;
the lower end and the upper end of the inner shell are respectively provided with an air inlet pipe and an air outlet pipe, and the upper end of the air inlet pipe penetrates through the porous plate to be communicated with the treatment section; a rotating shaft vertically penetrating into the bottom from the top of the inner shell, wherein spiral blades are fixed on the rotating shaft;
The two side walls of the inner shell are symmetrically provided with a plurality of layers of filter plates which are inclined upwards, and the end parts of the filter plates are close to but not connected with the spiral blades; the upper end and the lower end of the outer shell are respectively provided with a refrigerant outlet and a refrigerant inlet;
The condensing device also comprises a washing spray circulation system, wherein the washing spray circulation system comprises a liquid storage tank, a circulating water pump and spray heads which extend into the inner shell from the upper end of the inner shell and are respectively positioned at two sides of the rotating shaft; the conical liquid recovery area is communicated with a liquid storage tank through a liquid outlet pipe, and the liquid storage tank is communicated with the spray header through the circulating water pump;
Preferably, the spray head is a rotary spray head.
Preferably, the filter plate is provided with 3-5 layers.
Preferably, the inclination angle of the filter plate is 30-45 degrees.
Preferably, the bottom of the liquid storage tank is provided with a liquid discharge valve.
The beneficial effects are that: the invention adopts the rotating shaft and the spiral blades arranged on the rotating shaft to form the spiral air passage for the air flow to rise in the condenser, and solid small particles and some liquid drop impurities in the air are adsorbed on the rotating blades and the filter plate, thereby realizing the integration of filtration and cooling, simultaneously increasing the contact time of the air, the spiral blades and the filter plate, and effectively improving the yield of condensation products; in addition, the liquid after pre-condensation is utilized to spray and further condense and enrich the gas, so that the recycling of the organic gas in the system is realized, and the production efficiency is high.
Drawings
FIG. 1 is a schematic structural diagram of a high-efficiency condensing device for a lens monomer reaction kettle.
In the figure, a 1-condenser body, an 11-outer shell, a 12-inner shell, a 13-condensation treatment area, a 131-treatment area, a 132-conical liquid recovery area, a 14-porous plate, a 15-air inlet pipe, a 16-air outlet pipe, a 17-rotating shaft, 18-supporting feet, a 19-filter plate, 171-spiral blades, a 2-washing spray circulation system, a 21-liquid storage tank, a 22-circulating water pump, a 23-spray head, a 24-liquid outlet pipe, a 25-liquid discharge valve, a 3-refrigerant outlet and a 4-refrigerant inlet.
Detailed Description
As shown in fig. 1, the present embodiment provides a high-efficiency condensing device for a lens monomer reaction kettle, which comprises a condenser body 1 standing and supported by supporting legs 18; the condenser body 1 consists of a double-layer shell formed by an outer shell 11 and an inner shell 12, wherein a condensation treatment area 13 is arranged in the inner shell 12; the condensing treatment zone 13 comprises an upper treatment zone 131 and a lower conical liquid recovery zone 132 separated by a perforated plate 14;
The lower end and the upper end of the inner shell 12 are respectively provided with an air inlet pipe 15 and an air outlet pipe 16, and the upper end of the air inlet pipe 15 passes through the porous plate 14 to be communicated with the treatment area 131; a rotation shaft 17 extending vertically from the top of the inner shell 12 to the bottom, wherein spiral blades 171 are fixed on the rotation shaft 17;
The two side walls of the inner shell 12 are symmetrically provided with a plurality of layers of filter plates 19 which are inclined upwards, and the end parts of the filter plates 19 are close to but not connected with the spiral blades 171; the upper and lower ends of the outer shell 11 are respectively provided with a refrigerant outlet 3 and a refrigerant inlet 4.
The condensing device also comprises a washing spray circulation system 2, wherein the washing spray circulation system comprises a liquid storage tank 21, a circulating water pump 22 and spray heads 23 which extend into the inner-layer shell 12 from the upper end of the inner-layer shell 12 and are respectively positioned at two sides of the rotating shaft 17; the conical liquid recovery area 132 is communicated with a liquid storage tank 21 through a liquid outlet pipe 24, and the liquid storage tank 21 is communicated with the spray header 23 through the circulating water pump 22;
in the above technical solution, the spray header 23 is a rotary spray header.
In the above technical solution, the filter plate 19 is provided with 3-5 layers.
In the above technical scheme, the inclination angle of the filter plate 19 is 30-45 degrees.
In the above technical solution, the bottom of the liquid storage tank 21 is provided with a liquid discharge valve 25.
The foregoing description of the preferred embodiments of the invention is not intended to be limiting, but rather is intended to cover all modifications, equivalents, alternatives, and improvements that fall within the spirit and scope of the invention.
Claims (1)
1. The efficient condensing device for the lens monomer reaction kettle is characterized by comprising a condenser body which is supported in a standing manner through supporting feet; the condenser body consists of a double-layer shell formed by an outer shell and an inner shell, and a condensation treatment area is arranged in the inner shell; the condensing treatment area is divided into an upper treatment area and a conical liquid recovery area positioned at the lower part by a porous plate;
the lower end and the upper end of the inner shell are respectively provided with an air inlet pipe and an air outlet pipe, and the upper end of the air inlet pipe penetrates through the porous plate to be communicated with the treatment section; a rotating shaft vertically penetrating into the bottom from the top of the inner shell, wherein spiral blades are fixed on the rotating shaft;
The two side walls of the inner shell are symmetrically provided with a plurality of layers of filter plates which are inclined upwards, and the end parts of the filter plates are close to but not connected with the spiral blades; the upper end and the lower end of the outer shell are respectively provided with a refrigerant outlet and a refrigerant inlet;
the condensing device also comprises a washing spray circulation system, wherein the washing spray circulation system comprises a liquid storage tank, a circulating water pump and spray heads which extend into the inner shell from the upper end of the inner shell and are respectively positioned at two sides of the rotating shaft; the conical liquid recovery area is communicated with the liquid storage tank through a liquid outlet pipe, the liquid storage tank is communicated with the spray header through the circulating water pump, the spray header is a rotary spray head, the filter plate is provided with 3-5 layers, the inclination angle of the filter plate is 30-45 degrees, and the bottom of the liquid storage tank is provided with a liquid discharge valve.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910510735.1A CN110124595B (en) | 2019-06-13 | 2019-06-13 | Lens monomer is high-efficient condensing equipment for reation kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910510735.1A CN110124595B (en) | 2019-06-13 | 2019-06-13 | Lens monomer is high-efficient condensing equipment for reation kettle |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN110124595A CN110124595A (en) | 2019-08-16 |
| CN110124595B true CN110124595B (en) | 2024-04-30 |
Family
ID=67581529
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910510735.1A Active CN110124595B (en) | 2019-06-13 | 2019-06-13 | Lens monomer is high-efficient condensing equipment for reation kettle |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN110124595B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111391171A (en) * | 2020-05-11 | 2020-07-10 | 江苏可奥熙光学材料科技有限公司 | A dry recovery unit of monomer for lens resin production |
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| CN208465226U (en) * | 2018-04-26 | 2019-02-05 | 浙江龙安环保工程有限公司 | A kind of waste gas condensation device in sewage disposal process |
| CN208959593U (en) * | 2018-09-28 | 2019-06-11 | 王钰淇 | A kind of environment-friendly type industrial waste-gas purifier |
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2019
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| SU704641A1 (en) * | 1977-03-05 | 1979-12-25 | Казанский Химико-Технологический Институт Им. С.М.Кирова | Mass-exchange apparatus |
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| CN205699538U (en) * | 2016-04-29 | 2016-11-23 | 淮安市赛利化工有限公司 | A kind of glycol recovery device |
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| CN208959593U (en) * | 2018-09-28 | 2019-06-11 | 王钰淇 | A kind of environment-friendly type industrial waste-gas purifier |
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| Publication number | Publication date |
|---|---|
| CN110124595A (en) | 2019-08-16 |
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