CN110082209A - A kind of controllable timber micro mechanics measuring device of moisture content and its measurement method - Google Patents
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Abstract
本发明涉及一种含水率可控木材微力学测量装置,包括升降装置;连接装置,用于连接升降装置和待测木纤维的第一端部,升降装置通过连接装置提拉待测木纤维;称重装置,在称重装置上设置有第一底座,第一底座固定连接待测木纤维的第二端部,第一底座置于称重装置的称重盘上;可调温湿度容器,容器内设置有加热片和加湿器,称重装置和待测木纤维置于可调温湿度容器内,在容器内还设置有用于检测待测木纤维周侧环境温湿度的温湿度探针;待测木纤维竖直设置。该装置可检测不同含水率下木纤维的弹性模量和拉伸长度;解决了木材领域的测量难题且设备简单,成本低廉,测量精度高。
The invention relates to a wood micromechanical measuring device with controllable moisture content, comprising a lifting device; a connecting device is used for connecting the lifting device and the first end of the wood fiber to be tested, and the lifting device pulls the wood fiber to be tested through the connecting device; The weighing device is provided with a first base, the first base is fixedly connected to the second end of the wood fiber to be measured, and the first base is placed on the weighing pan of the weighing device; the temperature and humidity container is adjustable, A heating sheet and a humidifier are arranged in the container, the weighing device and the wood fiber to be measured are placed in an adjustable temperature and humidity container, and a temperature and humidity probe for detecting the ambient temperature and humidity of the wood fiber to be measured is also arranged in the container; The wood fibers to be tested are arranged vertically. The device can detect the elastic modulus and tensile length of wood fibers under different moisture contents; the measurement problem in the field of wood is solved, and the device is simple, the cost is low, and the measurement accuracy is high.
Description
技术领域technical field
本发明涉及一种测量装置,尤其涉及一种含水率可控木材微力学测量装置及其测量方法。The invention relates to a measuring device, in particular to a wood micromechanical measuring device and a measuring method thereof with controllable moisture content.
背景技术Background technique
木材的单根纤维是木材主要的承载单元,纤维细胞壁的力学性能对整个木材有着至关重要的影响,不同含水率下的待测木纤维所呈现的弹性模量和拉伸强度会有较大的差异,在木材加工、制浆造纸、中密度纤维板等实际应用中都需要考虑弹性模量和拉伸强度的问题以确保充分发挥其作用的目的。A single fiber of wood is the main bearing unit of wood, and the mechanical properties of fiber cell walls have a crucial impact on the entire wood. The elastic modulus and tensile strength of the wood fibers to be tested under different moisture contents will be larger. In practical applications such as wood processing, pulp and paper, medium density fiberboard, etc., the elastic modulus and tensile strength need to be considered to ensure that they can fully play their role.
弹性模量是材料重要的性能参数,从宏观角度来说,弹性模量是衡量物体抵抗弹性变形能力大小的尺度,是衡量木材刚度特性的一个重要指标。目前公认的测量技术为静态弯曲法,但该方法测量过程过于繁琐,测试时间较长,并且具有破坏性,已经不能满足现代连续化生产的要求。近几十年来,弹性模量测量的技术在不断的更新升级,现应用较为广泛的测量技术有应力波法、振动检测法,应力波速度检测仪的测试原理:木材的一端受到冲击波的作用,应力波在木材中来回传播,通过测定木材中的应力波传播速度,确定木材的弹性模量值,最终估算出木材的力学强度;振动检测法是基于木材共振频率与弹性模量具有数学关系的原理,利用振动测量得到木材的共振频率进而得到木材的动弹性模量。Elastic modulus is an important performance parameter of materials. From a macroscopic point of view, elastic modulus is a measure of the ability of an object to resist elastic deformation, and an important index to measure the stiffness characteristics of wood. The currently recognized measurement technology is the static bending method, but the measurement process of this method is too cumbersome, the test time is long, and it is destructive, which can no longer meet the requirements of modern continuous production. In recent decades, the measurement technology of elastic modulus has been continuously updated and upgraded. The widely used measurement technologies include stress wave method, vibration detection method, and the testing principle of stress wave velocity detector: one end of the wood is affected by the shock wave, The stress wave propagates back and forth in the wood. By measuring the propagation velocity of the stress wave in the wood, the elastic modulus value of the wood is determined, and the mechanical strength of the wood is finally estimated. The vibration detection method is based on the mathematical relationship between the wood resonance frequency and the elastic modulus. The principle is to use vibration measurement to obtain the resonance frequency of the wood and then obtain the dynamic elastic modulus of the wood.
拉伸强度是指试样在拉伸过程中,材料经过屈服阶段后进入强化阶段后随着横向截面尺寸明显缩小在拉断时所承受的最大力,除以试样原横截面积所得的应力,称为抗拉强度或者强度极限,它表示材料在拉力作用下抵抗破坏的最大能力。常用的方法是使用拉伸试验机对材料进行拉伸强度测试。Tensile strength refers to the maximum force that the specimen bears during the tensile process, when the material passes through the yield stage and then enters the strengthening stage as the transverse cross-sectional size is significantly reduced, divided by the stress obtained by dividing the original cross-sectional area of the specimen. , known as tensile strength or strength limit, which represents the maximum ability of a material to resist failure under tension. A common method is to test materials for tensile strength using a tensile testing machine.
虽然对木材等固体材料的力学性能的测试有很多的研究,也总结出了很多的成果,但是对于木材单根纤维不同含水率下的微力学测量的方法相对较少,常规的待测木纤维的测试方法大多数都因为测试纤维非常细小且承受载荷较小易变形而造成测试的困难。由于单根纤维是木材的主要承载结构单元,纤维细胞壁的力学性能的好坏对木材的宏观的力学性能有着至关重要的影响,对木材单根纤维的力学性能的研究其实就是把木材力学研究从宏观研究向微观的研究的过渡。Although there are many studies on the testing of mechanical properties of solid materials such as wood, and many results have been summarized, there are relatively few micromechanical measurement methods for single wood fibers with different moisture contents. Conventional wood fibers to be tested are Most of the test methods are difficult because the test fibers are very small and easily deformed under small loads. Since a single fiber is the main load-bearing structural unit of wood, the mechanical properties of fiber cell walls have a crucial impact on the macroscopic mechanical properties of wood. The study of the mechanical properties of a single fiber of wood is actually the study of wood mechanics. The transition from macro to micro research.
发明内容SUMMARY OF THE INVENTION
本发明的目的在于提供一种可控制木纤维含水率且可测量该含水率下木纤维的微力学性能的装置,该装置可检测木纤维的弹性模量和拉伸长度;解决了木材领域的测量难题且设备简单,成本低廉,测量精度高。The object of the present invention is to provide a device that can control the moisture content of wood fibers and can measure the micromechanical properties of wood fibers under the moisture content, the device can detect the elastic modulus and tensile length of wood fibers; The measurement is difficult, the equipment is simple, the cost is low, and the measurement accuracy is high.
本发明所采取的技术方案为:一种含水率可控木材微力学测量装置,包括升降装置;The technical scheme adopted by the present invention is as follows: a moisture content controllable wood micromechanics measuring device, including a lifting device;
连接装置,用于连接所述升降装置和待测木纤维的第一端部,所述升降装置通过所述连接装置提拉所述待测木纤维;a connecting device for connecting the lifting device and the first end of the wood fiber to be tested, and the lifting device pulls the wood fiber to be tested through the connecting device;
称重装置,在所述称重装置上设置有第一底座,所述第一底座固定连接所述待测木纤维的第二端部,所述第一底座置于所述称重装置的称重盘上;A weighing device, a first base is arranged on the weighing device, the first base is fixedly connected to the second end of the wood fiber to be tested, and the first base is placed on the scale of the weighing device redistribute;
可调温湿度容器,所述容器内设置有加热片和加湿器,所述称重装置和所述待测木纤维置于所述可调温湿度容器内,在所述容器内还设置有用于检测所述待测木纤维周侧环境温湿度的温湿度探针;An adjustable temperature and humidity container, a heating plate and a humidifier are arranged in the container, the weighing device and the wood fiber to be measured are placed in the temperature and humidity container, and a a temperature and humidity probe for detecting the ambient temperature and humidity of the wood fiber to be measured;
所述待测木纤维竖直设置。The wood fibers to be tested are arranged vertically.
进一步的,所述升降装置为滑走式切片机,所述连接装置通过标本固定器固定连接所述滑走式切片机,所述滑走式切片机的步进为微米级。Further, the lifting device is a slide-away microtome, the connecting device is fixedly connected to the slide-away microtome through a specimen holder, and the step of the slide-away microtome is micron level.
进一步的,所述标本固定器包括第二底座、滑板和调节杆,所述第二底座设有立板,所述立板与所述滑板相对设置,所述第二底座上还设有滑槽,所述滑板沿所述滑槽在一维方向上靠近或远离所述立板,所述滑板通过所述调节杆将所述连接装置夹持于所述滑板与所述立板之间。Further, the specimen holder includes a second base, a slide plate and an adjusting rod, the second base is provided with a vertical plate, the vertical plate is arranged opposite to the slide plate, and a chute is also provided on the second base , the sliding plate approaches or moves away from the vertical plate in a one-dimensional direction along the chute, and the sliding plate clamps the connecting device between the sliding plate and the vertical plate through the adjusting rod.
进一步的,在所述第二底座上固定有立柱,所述立柱上设有螺孔,所述螺孔轴向与所述滑板移动方向一致,所述调节杆为螺杆,所述调节杆一端穿过所述螺柱后连接所述滑板,通过旋转所述调节杆调整所述滑板与所述立板对所述连接装置的夹持力。Further, a column is fixed on the second base, and a screw hole is arranged on the column, and the axial direction of the screw hole is consistent with the moving direction of the slide plate. After passing through the stud, the sliding plate is connected, and the clamping force of the sliding plate and the vertical plate on the connecting device is adjusted by rotating the adjusting rod.
进一步的,所述连接装置为L型支架,所述L型支架一端固定连接所述升降装置,另一端连接待测木纤维的第一端部。Further, the connecting device is an L-shaped bracket, one end of the L-shaped bracket is fixedly connected to the lifting device, and the other end is connected to the first end of the wood fiber to be tested.
进一步的,所述待测木纤维与所述连接装置通过紫外光固化胶粘剂进行粘接。Further, the wood fiber to be tested and the connecting device are bonded by a UV-curable adhesive.
进一步的,所述第一底座为铜块,铜块质量为30-100g;第一底座与待测木纤维之间用紫外光固化胶粘剂胶稳固粘结。Further, the first base is a copper block, and the mass of the copper block is 30-100 g; the first base and the wood fiber to be tested are firmly bonded with an ultraviolet light curing adhesive.
进一步的,所述称重装置为电子天平。Further, the weighing device is an electronic balance.
进一步的,所述加湿器为通电即加湿,断电即停止加湿的小型加湿器,喷雾均匀且可调节喷雾量的大小;所述加湿器插在湿度控制器面板上,由温湿度控制器给其通断电。Further, the humidifier is a small humidifier that humidifies when power is turned on, and stops humidifying when power is turned off, and the spray is uniform and the size of the spray volume can be adjusted; the humidifier is inserted on the humidity controller panel, and the temperature and humidity It is switched on and off.
进一步的,所述加热片为通电即加热,断电即停止加热的加热片,其加热温度范围为0~55℃。Further, the heating sheet is a heating sheet that heats when power is turned on, and stops heating when power is turned off, and its heating temperature ranges from 0 to 55°C.
进一步的,所述温湿度控制器上有两个独立插座,分别供加热片和加湿器电源接入。温湿度控制器可检测的温度范围为0~55℃,湿度范围为可将玻璃箱内湿度控制在环境湿度-100%;所述温湿度控制器上设有温度探针和湿度探针。Further, there are two independent sockets on the temperature and humidity controller, which are respectively connected to the power supply of the heating plate and the humidifier. The temperature and humidity controller can detect a temperature range of 0 to 55°C, and the humidity range is such that the humidity in the glass box can be controlled at ambient humidity -100%; the temperature and humidity controller is provided with a temperature probe and a humidity probe.
本发明还提供了一种含水率可控木材微力学测量装置的测量方法,包括以下步骤The invention also provides a measurement method of a wood micromechanics measurement device with controllable moisture content, comprising the following steps
S01读取所述称重装置初始读数;调整所述容器内温湿度至设定值;S01 reads the initial reading of the weighing device; adjusts the temperature and humidity in the container to a set value;
S02通过所述升降装置和所述连接装置提拉所述待测木纤维,记录所述升降装置位移和所述称重装置读数,根据所述称重装置的读数和初始读数得到拉伸载荷,根据所述升降装置位移得到该载荷下的绝对伸长量;S02 pulls the wood fiber to be tested by the lifting device and the connecting device, records the displacement of the lifting device and the reading of the weighing device, and obtains the tensile load according to the reading and the initial reading of the weighing device, Obtain the absolute elongation under the load according to the displacement of the lifting device;
S03根据所述拉伸载荷、断裂载荷和绝对伸长量等得到待测木纤维的弹性模量、拉伸强度。S03 obtains the elastic modulus and tensile strength of the wood fiber to be tested according to the tensile load, breaking load and absolute elongation.
进一步的,本发明利用温湿度探针检测玻璃箱内的温湿度并实时反映在温湿度控制器上,设置温湿度控制器的上下限值,一旦低于或高于设定值时温湿度控制器便相应地接通或断开加热片和加湿器的电源,调节箱内的温度和湿度,从而控制木材的含水率。在一定的温湿度条件下,利用精密电子天平测量施力大小,具体包括以下步骤Further, the present invention uses the temperature and humidity probe to detect the temperature and humidity in the glass box and reflects it on the temperature and humidity controller in real time, and sets the upper and lower limit values of the temperature and humidity controller. Once the temperature and humidity are lower than or higher than the set value, the temperature and humidity control The device will turn on or off the power of the heating plate and humidifier accordingly, adjust the temperature and humidity in the box, and thus control the moisture content of the wood. Under certain temperature and humidity conditions, use a precision electronic balance to measure the force, which includes the following steps
(1)用高倍显微镜测量待测木纤维的横截面尺寸,得到待测木纤维横截面面积S;(1) measure the cross-sectional size of the wood fiber to be tested with a high-power microscope to obtain the cross-sectional area S of the wood fiber to be tested;
(2)将称重装置置于穿过容器的连接装置下方,所述连接装置为L型支架,L型支架一端正对所述称重装置;(2) placing the weighing device under the connecting device passing through the container, the connecting device is an L-shaped bracket, and one end of the L-shaped bracket is facing the weighing device;
(3)将待测木纤维通过第一底座放置于称重装置上,通过升降装置使L型支架降落至与所述第一底座接触,并调整使第一底座的中心点与L型支架一端的中心点完全重合,竖直方向上提升所述L型支架与所述第一底座分离;(3) The wood fiber to be tested is placed on the weighing device through the first base, the L-shaped bracket is lowered to contact with the first base through the lifting device, and the center point of the first base is adjusted so that the center point of the first base is connected to one end of the L-shaped bracket The center points of the two are completely coincident, and the L-shaped bracket is vertically lifted to separate from the first base;
(4)采用紫外光固化胶粘剂将待测木纤维的一端先与第一底座粘连好,待测木纤维固定在第一底座中心点上;(4) Adhere one end of the wood fiber to be tested to the first base by using an ultraviolet curing adhesive, and fix the wood fiber to be tested on the center point of the first base;
(5)调节升降装置使L型支架下移至与待测木纤维另一端刚好触碰为止,用紫外光固化胶粘剂将二者粘连,将称重装置的读数归零;(5) Adjust the lifting device so that the L-shaped bracket is moved down until it just touches the other end of the wood fiber to be tested, and the two are adhered with ultraviolet curing adhesive, and the reading of the weighing device is reset to zero;
(6)调整容器内温湿度至设定值;(6) Adjust the temperature and humidity in the container to the set value;
(7)在待测木纤维线弹性范围内,通过控制升降装置对待测木纤维进行拉伸,产生拉伸载荷F,记录升降装置的升高位移即为单根待测木纤维在该载荷下的绝对伸长量dL,同时记录该伸长量下的电子天平读数m,计算拉伸载荷F=-mg;根据式(1)计算单根待测木纤维的弹性模量E,(7) Within the linear elasticity range of the wood fiber to be tested, the wood fiber to be tested is stretched by controlling the lifting device to generate a tensile load F, and the lifting displacement of the recording lifting device is the single wood fiber to be tested under the load. The absolute elongation dL is recorded, and the electronic balance reading m under the elongation is recorded at the same time, and the tensile load F=-mg is calculated; according to the formula (1), the elastic modulus E of a single wood fiber to be tested is calculated,
其中:F为拉伸载荷,S为纤维的截面积,L为纤维的初始长度,测量方法见步骤(11),dL为纤维的伸长量;Wherein: F is the tensile load, S is the cross-sectional area of the fiber, L is the initial length of the fiber, see step (11) for the measurement method, and dL is the elongation of the fiber;
(8)继续移动L型支架对待测木纤维进行拉伸至设定距离,再次记录待测木纤维的绝对伸长量dL及电子天平读数m,并根据式(1)计算待测木纤维的弹性模量E;至少做5组数据取平均值作为弹性模量的测试数据;(8) Continue to move the L-shaped bracket to stretch the wood fiber to be tested to the set distance, record the absolute elongation dL of the wood fiber to be tested and the reading m of the electronic balance, and calculate the wood fiber to be tested according to formula (1). Elastic modulus E; do at least 5 sets of data and take the average value as the elastic modulus test data;
(9)控制升降装置进一步对待测木纤维进行拉伸直至待测木纤维在长度方向发生断裂,记录断裂发生时的电子天平的读数mc,计算临界载荷Fc=-mcg;(9) Control the lifting device to further stretch the wood fiber to be tested until the wood fiber to be tested breaks in the length direction, record the reading m c of the electronic balance when the break occurs, and calculate the critical load F c =-m c g;
(10)根据式(2)计算待测木纤维的拉伸强度σ,(10) Calculate the tensile strength σ of the wood fiber to be tested according to formula (2),
其中,Fc为纤维断裂时的临界载荷,S为纤维的截面积。Among them, F c is the critical load when the fiber breaks, and S is the cross-sectional area of the fiber.
进一步的,所述升降装置为滑走式切片机,所述待测木纤维的初长测量方法为:Further, the lifting device is a slide-away slicer, and the initial length measurement method of the wood fiber to be measured is:
待测木纤维端部与所述L型支架粘结且所述待测木纤维所受拉伸载荷为零时,所述滑走式切片机的步进为零;When the end of the wood fiber to be tested is bonded to the L-shaped bracket and the tensile load of the wood fiber to be tested is zero, the step of the slide-away slicer is zero;
待测木纤维断裂后,天平示数自动归零,操作滑走式切片机下移L型支架直至L型支架上的紫外固化胶与底座上的紫外固化胶正好触碰为止,此时天平示数刚好为正,记录此时的步进长度,该长度即为单根木材纤维的初始长度L。After the wood fiber to be tested is broken, the balance indication will automatically return to zero. Operate the slide-away slicer to move the L-shaped bracket down until the UV-curable glue on the L-shaped bracket just touches the UV-curable glue on the base. At this time, the balance indicates the number. If it is just positive, record the step length at this time, which is the initial length L of a single wood fiber.
附图说明Description of drawings
图1本发明含水率可控木材微力学测量装置示意图;Fig. 1 is the schematic diagram of the wood micromechanics measuring device with controllable moisture content of the present invention;
图2本发明中标本固定器的主视图;Figure 2 is a front view of the specimen holder in the present invention;
图3本发明中标本固定器的左视图;Figure 3 is a left side view of the specimen holder in the present invention;
图4本发明中标本固定器的俯视图;Figure 4 is a plan view of the specimen holder in the present invention;
图5本发明中不同含水率木材微力学测量方法中木材纤维固定示意图;Fig. 5 is a schematic diagram of the fixation of wood fibers in the micromechanical measurement method of wood with different moisture contents in the present invention;
图6利用本发明对杉木测量的应力增量—应变增量数据拟合图。Fig. 6 is a fitting diagram of the stress increment-strain increment data measured on Chinese fir using the present invention.
具体实施方式Detailed ways
下面结合附图对本发明作进一步描述。以下实施例仅用于更加清楚地说明本发明的技术方案,而不能以此来限制本发明的保护范围。The present invention will be further described below in conjunction with the accompanying drawings. The following examples are only used to illustrate the technical solutions of the present invention more clearly, and cannot be used to limit the protection scope of the present invention.
本发明提供了使用温湿度控制器控制木材含水率,并在竖直方向上直接向不同含水率的待测木纤维施加拉伸载荷来测试微米级的含水率可控木材微力学测量方法及装置。The invention provides a micromechanical measurement method and device for testing micron-level moisture content controllable wood by using a temperature and humidity controller to control the moisture content of wood, and directly applying a tensile load in the vertical direction to wood fibers with different moisture contents to be tested. .
本发明中,在设定的温度湿度范围内,由温湿度控制器控制加热片和加湿器的接通或断开,由精密电子天平测量载荷大小,设计一种在竖直方向上直接向待测木纤维施加拉伸载荷的L型支架,利用滑走式切片机带动L型支架在竖直方向上移,使纤维在线弹性范围内发生拉伸变形,由切片机的控制面板显示的距离直接作为纤维变形伸长量,根据应力增量应变增量关系计算出单根待测木纤维的弹性模量,进一步对待测木纤维进行拉伸,直至待测木纤维发生断裂,根据发生断裂时的临界载荷值和纤维尺寸可计算出纤维的拉伸强度。In the present invention, within the set temperature and humidity range, the temperature and humidity controller controls the connection or disconnection of the heating plate and the humidifier, the precision electronic balance measures the load size, and designs a vertical The L-shaped bracket that measures the tensile load of the wood fiber is used to drive the L-shaped bracket to move up in the vertical direction, so that the fiber is stretched and deformed within the linear elastic range, and the distance displayed by the control panel of the slicing machine is directly used as The amount of fiber deformation and elongation, the elastic modulus of a single wood fiber to be tested is calculated according to the relationship of stress increment and strain increment, and the wood fiber to be tested is further stretched until the wood fiber to be tested breaks. The load value and fiber size can calculate the tensile strength of the fiber.
弹性模量由应力增量—应变增量关系测试,为了解决载荷精密测量的问题,设计一种直接作用于待测木纤维拉伸载荷的L型支架,用精密电子天平测量载荷,纤维上面承受单向拉伸应力,显微镜下该纤维长度为L,通过操作滑走式切片机带动L型支架移动从而使待测木纤维发生长度方向的位移,然后按照弹性模量的定义来计算其弹性模量。当拉伸载荷进一步增加,直至待测木纤维发生断裂,由断裂的临界载荷值和待测木纤维的截面积可以计算出其拉伸强度。The elastic modulus is measured by the relationship between the stress increment and the strain increment. In order to solve the problem of precise measurement of the load, an L-shaped bracket is designed that directly acts on the tensile load of the wood fiber to be measured. Uniaxial tensile stress, the fiber length is L under the microscope, and the L-shaped bracket is moved by operating the slide-away slicer, so that the wood fiber to be tested is displaced in the length direction, and then its elastic modulus is calculated according to the definition of elastic modulus. . When the tensile load is further increased until the wood fiber to be tested breaks, the tensile strength can be calculated from the critical load value of breaking and the cross-sectional area of the wood fiber to be tested.
为此,本发明特别设计一种含水率可控木材微力学测量装置。参见图1所示,测量装置主要包括滑走式切片机1、L型支架2、电子天平3及待测木纤维第一底座4、容器、加热片15、加湿器12、温湿度控制器13等部分。本实施例中容器为玻璃箱,滑走式切片机1的标本固定器6上固定有L型支架2,L型支架2的另一端的中心与待测木纤维5相连;电子天平3、加热片15贴在玻璃箱14的内壁上,加湿器12、探针11和L型支架2的一部分置于亚克力玻璃箱14内,加热片15、加湿器12、湿度探针11与温度探针16通过置于玻璃箱之外的湿度控制器13来控制启闭,湿度探针11和温度探针16置于待测木纤维5的附近且远离加湿器12;电子天平3置于L型支架2的下部,待测木纤维第一底座4放置于电子天平3之上,待测木纤维5安装于第一底座4的中心点上,第一底座放置的电子天平3上,两者无连接件连接;滑走式切片机1还设有将标本固定器6上移或下降的调节旋钮10、控制面板8和步进按钮9。Therefore, the present invention specially designs a wood micromechanics measuring device with controllable moisture content. Referring to FIG. 1, the measuring device mainly includes a slide-away slicer 1, an L-shaped bracket 2, an electronic balance 3, a first base 4 of the wood fiber to be measured, a container, a heating sheet 15, a humidifier 12, a temperature and humidity controller 13, etc. part. In this embodiment, the container is a glass box, an L-shaped bracket 2 is fixed on the specimen holder 6 of the slide-away microtome 1, and the center of the other end of the L-shaped bracket 2 is connected to the wood fiber 5 to be tested; the electronic balance 3, the heating plate 15 is attached to the inner wall of the glass box 14, the humidifier 12, the probe 11 and a part of the L-shaped bracket 2 are placed in the acrylic glass box 14, the heating sheet 15, the humidifier 12, the humidity probe 11 and the temperature probe 16 pass through The humidity controller 13 placed outside the glass box controls the opening and closing, the humidity probe 11 and the temperature probe 16 are placed near the wood fiber 5 to be tested and away from the humidifier 12; the electronic balance 3 is placed on the L-shaped bracket 2 In the lower part, the first base 4 of the wood fiber to be tested is placed on the electronic balance 3, the wood fiber 5 to be tested is installed on the center point of the first base 4, and the electronic balance 3 placed on the first base is connected without a connector. ; The slide-away microtome 1 is also provided with an adjustment knob 10, a control panel 8 and a step button 9 for moving the specimen holder 6 up or down.
其中,滑走式切片机1的步进范围为0~120μm,最小步进为0.25μm,通过控制面板8上的步进按钮9进行设定。为保证精确性,选取最小步进0.25μm作为标准尺度。标本固定器6可垂直移动距离为40mm,本发明中使用该标本固定器固定L型支架2的一端,见图1所示。切片机左侧调节旋钮10,每上抬一次,L型支架2上升相应步进,待测木纤维5产生相应的伸长量,从控制面板8可以得到待测木纤维移动至任意竖直位置产生的位移。Among them, the step range of the slide-away microtome 1 is 0-120 μm, and the minimum step is 0.25 μm, which is set by the step button 9 on the control panel 8 . To ensure accuracy, the minimum step of 0.25 μm is selected as the standard scale. The vertical moving distance of the specimen holder 6 is 40 mm, and the specimen holder 6 is used to fix one end of the L-shaped bracket 2 in the present invention, as shown in FIG. 1 . The adjustment knob 10 on the left side of the slicer, each time it is lifted up, the L-shaped bracket 2 rises correspondingly, and the wood fiber 5 to be tested produces a corresponding elongation. From the control panel 8, it can be obtained that the wood fiber to be tested moves to any vertical position resulting displacement.
其中,标本固定器6由轻质铝合金制成,其构成参见图2、图3和图4所示,包括调节杆7、滑槽17、立柱18、第二底座19、滑板20、滑动脚21等部件。第二底座19的一端设有立板,立板与滑板相对,另一端设有立柱18,立柱18为第二底座19的一部分,立柱18与第二底座19一体成型,且与滑板相对,在立柱18上设有螺纹孔,其作用是为调节杆7控制滑板20的前后移动提供支撑;第二底座19上开有滑槽17,滑动脚21的顶部与滑板20相连接。滑动脚21为滑板20的一部分,调节杆7为长形螺丝,穿过立柱18的螺纹孔固定连接滑板20,通过转动调节杆7,可使其自身前后移动,即调节杆7、滑板20和滑动脚21三者同步移动。将L型支架2放入第二底座19与滑板20之间,顺时针转动调节杆7推动滑板20直至无法转动为止,将L型支架2夹紧。Among them, the specimen holder 6 is made of light aluminum alloy, and its structure is shown in Fig. 2, Fig. 3 and Fig. 4, including an adjusting rod 7, a chute 17, a column 18, a second base 19, a sliding plate 20, and sliding feet 21 and other components. One end of the second base 19 is provided with a vertical plate, the vertical plate is opposite to the slide plate, and the other end is provided with a column 18. The column 18 is a part of the second base 19. The column 18 is integrally formed with the second base 19 and is opposite to the slide plate. The upright column 18 is provided with a threaded hole, which is used to provide support for the adjustment rod 7 to control the front and rear movement of the sliding plate 20 ; The sliding foot 21 is a part of the sliding plate 20, and the adjusting rod 7 is an elongated screw, which is fixedly connected to the sliding plate 20 through the threaded hole of the upright column 18. The three sliding feet 21 move synchronously. Put the L-shaped bracket 2 between the second base 19 and the sliding plate 20 , turn the adjusting rod 7 clockwise to push the sliding plate 20 until it cannot rotate, and clamp the L-shaped bracket 2 .
其中,通过操作调节旋钮10,滑走式切片机1内置电脑控制标本固定器6进行上下移动。Among them, by operating the adjustment knob 10 , the computer built in the slide-away microtome 1 controls the specimen holder 6 to move up and down.
其中,L型支架2,由轻质铝合金制成,一端固定于滑走式切片机1的标本固定器6中,另一端与待测木纤维5相连,该端口对角线交点为支架2与待测木纤维5的连接点,连接点处用紫外光固化胶粘剂胶稳固粘结。通过该L型支架2的上下位移用于对待测木纤维5在竖直方向进行拉伸。Among them, the L-shaped bracket 2 is made of lightweight aluminum alloy, one end is fixed in the specimen holder 6 of the slide-away microtome 1, and the other end is connected with the wood fiber 5 to be tested. The diagonal intersection of the port is the bracket 2 and the The connection points of the wood fibers 5 to be tested are firmly bonded with UV-curable adhesive. The vertical displacement of the L-shaped bracket 2 is used to stretch the wood fiber 5 to be tested in the vertical direction.
其中,电子天平3与滑走式切片机1均放置于同一水平工作台上;待测木纤维固定系统的组成如图5所示,包括待测木纤维5、L型支架2和待测木纤维第一底座4。使用铜块作为待测木纤维第一底座4,置于电子天平3之上,待测木纤维第一底座4的中心点为待测木纤维5与第一底座4的连接点,第一底座4与待测木纤维5之间用紫外光固化胶粘剂胶稳固粘结。Among them, the electronic balance 3 and the slide-away slicer 1 are placed on the same horizontal workbench; the composition of the wood fiber fixing system to be tested is shown in Figure 5, including the wood fiber to be tested 5, the L-shaped bracket 2 and the wood fiber to be tested. The first base 4 . A copper block is used as the first base 4 of the wood fiber to be tested and placed on the electronic balance 3. The center point of the first base 4 of the wood fiber to be tested is the connection point of the wood fiber 5 to be tested and the first base 4. The first base 4 and the wood fiber 5 to be tested are firmly bonded with UV-curable adhesive.
本发明的检测基本步骤包括测量待测木纤维的自身长度和横截面尺寸,固定待测木纤维,调节玻璃箱内湿度,然后在待测木纤维的线弹性范围内对其进行长度方向的拉伸,记录待测木纤维相应的伸长量,并读取相应伸长量下电子天平的读数以此计算待测木纤维在相应含水率下受到的拉力载荷。根据获得的载荷增量和对应的伸长量以及待测木纤维横截面积计算出相应含水率下待测木纤维的弹性模量。对待测木纤维继续拉伸直至纤维断裂,计算出临界载荷,通过临界载荷和待测木纤维横截面积计算其强度。测试方法如下:The basic detection steps of the present invention include measuring the length and cross-sectional size of the wood fiber to be tested, fixing the wood fiber to be tested, adjusting the humidity in the glass box, and then pulling the wood fiber in the length direction within the linear elasticity range of the wood fiber to be tested. Elongation, record the corresponding elongation of the wood fiber to be tested, and read the reading of the electronic balance under the corresponding elongation to calculate the tensile load of the wood fiber to be tested under the corresponding moisture content. According to the obtained load increment and corresponding elongation and the cross-sectional area of the wood fiber to be tested, the elastic modulus of the wood fiber to be tested under the corresponding moisture content is calculated. The wood fiber to be tested continues to stretch until the fiber breaks, and the critical load is calculated, and its strength is calculated from the critical load and the cross-sectional area of the wood fiber to be tested. The test method is as follows:
(1)用高倍显微镜测量待测木纤维的横截面尺寸,得到待测木纤维横截面面积S;(1) measure the cross-sectional size of the wood fiber to be tested with a high-power microscope to obtain the cross-sectional area S of the wood fiber to be tested;
(2)将电子天平置于穿过玻璃箱的L型支架下部,L型支架一端固定在滑走式切片机的标本控制器上;(2) Place the electronic balance at the lower part of the L-shaped bracket passing through the glass box, and one end of the L-shaped bracket is fixed on the specimen controller of the slide-away microtome;
(3)将待测木纤维第一底座放置于电子天平之上,调整待测木纤维第一底座的位置并通过标本控制器上下移动L型支架,使待测木纤维第一底座的中心点与L型支架一端截面对角线交点完全重合,再通过移动标本控制器使L型支架仅在竖直方向发生位移,待测木纤维第一底座中心点与支架截面对角线交点处于同一条竖直线上;(3) Place the first base of the wood fiber to be tested on the electronic balance, adjust the position of the first base of the wood fiber to be tested and move the L-shaped bracket up and down through the specimen controller to make the center point of the first base of the wood fiber to be tested It is completely coincident with the diagonal intersection of one end of the L-shaped bracket, and then the L-shaped bracket is only displaced in the vertical direction by moving the specimen controller. The center point of the first base of the wood fiber to be tested and the diagonal intersection of the bracket section are in the same line vertical line;
(4)采用紫外光固化胶粘剂将待测木纤维的一端先与待测木纤维第一底座粘连好,待测木纤维固定在第一底座中心点上;(4) Adhere one end of the wood fiber to be tested to the first base of the wood fiber to be tested by using an ultraviolet curing adhesive, and the wood fiber to be tested is fixed on the center point of the first base;
(5)调节滑走式切片机的调节旋钮使L型支架下移至与待测木纤维另一端刚好触碰为止,此时电子天平读数不发生变化;用紫外光固化胶粘剂将二者粘连,随即再将电子天平的读数归零;(5) Adjust the adjustment knob of the slide-away slicer so that the L-shaped bracket moves down until it just touches the other end of the wood fiber to be tested, and the electronic balance reading does not change at this time; the two are adhered with ultraviolet curing adhesive, and then Then reset the reading of the electronic balance to zero;
(6)分别设置温湿度控制器的温度和湿度上下限,将加热片和加湿器的电源接在温湿度控制器上,在设定值范围内由温湿度控制器自动地接通或断开加热片和加湿器的电源;将温湿度探针置于待测木纤维的附近;(6) Set the temperature and humidity upper and lower limits of the temperature and humidity controller respectively, connect the power supply of the heating sheet and the humidifier to the temperature and humidity controller, and the temperature and humidity controller will automatically turn on or off within the set value range Power supply for heating sheet and humidifier; place the temperature and humidity probe near the wood fiber to be tested;
(7)在待测木纤维线弹性范围内,通过控制滑走式切片机的升降对待测木纤维进行拉伸,产生拉伸载荷F,此时滑走式切片机控制面板显示的位移变化即为单根待测木纤维在该载荷下的绝对伸长量dL,同时记录该伸长量下的电子天平读数m,计算拉伸载荷F=-mg;根据式(1)计算单根待测木纤维的弹性模量E,(7) Within the linear elasticity range of the wood fiber to be tested, the wood fiber to be tested is stretched by controlling the lifting and lowering of the slide-away slicer to generate a tensile load F. At this time, the displacement change displayed on the control panel of the slide-away slicer is a single The absolute elongation dL of the wood fiber to be tested under the load, and the electronic balance reading m under the elongation is recorded at the same time, and the tensile load F=-mg is calculated; according to the formula (1), calculate the single wood fiber to be tested. The elastic modulus E,
其中:F为拉伸载荷,S为纤维的截面积,L为纤维的初始长度,测量方法见步骤(11),dL为纤维的伸长量;Wherein: F is the tensile load, S is the cross-sectional area of the fiber, L is the initial length of the fiber, see step (11) for the measurement method, and dL is the elongation of the fiber;
(8)继续移动L型支架对待测木纤维进行拉伸至一定距离,再次记录待测木纤维的绝对伸长量dL及电子天平读数m,并根据式(1)计算待测木纤维的弹性模量E;至少做5组数据取平均值作为弹性模量的测试数据;(8) Continue to move the L-shaped bracket to stretch the wood fiber to be tested to a certain distance, record the absolute elongation dL of the wood fiber to be tested and the reading m of the electronic balance, and calculate the elasticity of the wood fiber to be tested according to formula (1). Modulus E; do at least 5 sets of data and take the average value as the test data of elastic modulus;
(9)控制滑走式切片机进一步对待测木纤维进行拉伸直至待测木纤维在长度方向发生断裂,记录断裂发生时的电子天平的读数mc,计算临界载荷Fc=-mcg;(9) Control the slide-away slicer to further stretch the wood fiber to be tested until the wood fiber to be tested breaks in the length direction, record the reading m c of the electronic balance when the break occurs, and calculate the critical load F c =-m c g;
(10)根据式(2)计算待测木纤维的拉伸强度σ,(10) Calculate the tensile strength σ of the wood fiber to be tested according to formula (2),
其中,Fc为纤维断裂时的临界载荷,S为纤维的截面积;Among them, Fc is the critical load when the fiber breaks, and S is the cross-sectional area of the fiber;
(11)待测木纤维断裂后,天平示数自动归零,操作滑走式切片机下移L型支架直至L型支架上的紫外固化胶与第一底座上的紫外固化胶正好触碰为止,此时天平示数刚好为正,记录此时的步进长度,该长度即为单根待测木纤维的初始长度L。(11) After the wood fiber to be tested is broken, the balance indication is automatically reset to zero, and the slide-away slicer is operated to move the L-shaped bracket down until the UV-curable glue on the L-shaped bracket just touches the UV-curable glue on the first base. At this time, the balance indication is just positive, record the step length at this time, which is the initial length L of a single wood fiber to be tested.
以下结合具体实施例详细说明本发明。实施例只为具体公开本发明测试含水率可控的单根待测木纤维弹性模量和强度的过程,不作为对本发明其他实施方式的限制。The present invention will be described in detail below with reference to specific embodiments. The examples are only to specifically disclose the process of the present invention for testing the elastic modulus and strength of a single wood fiber to be tested with a controllable moisture content, and are not intended to limit other embodiments of the present invention.
实施例:测量含水率为12%的杨木单纤维的微力学性能Example: Measurement of micromechanical properties of poplar single fibers with a moisture content of 12%
具体操作过程为:The specific operation process is as follows:
(1)选择杨木单纤维为实验试样,采用日本奥林巴斯BX51精密显微镜测得木材纤维的横截面面积S=176μm2。(1) Single poplar fiber was selected as the experimental sample, and the cross-sectional area S=176 μm 2 of the wood fiber was measured with a Japanese Olympus BX51 precision microscope.
(2)开启加湿器与加热片,运用温湿度控制器保持亚克力玻璃箱内维持在65%的湿度与20℃的温度。根据木材含水率与温湿度对应图可知,此时木材的含水率为12%。(2) Turn on the humidifier and heating plate, and use the temperature and humidity controller to keep the acrylic glass box at a humidity of 65% and a temperature of 20°C. According to the corresponding map of wood moisture content and temperature and humidity, the moisture content of wood is 12% at this time.
(3)采用紫外光固化胶粘剂将杨木纤维的一端先与第一底座粘连好,杨木纤维固定在第一底座的中心点;调节滑走式切片机的调节旋钮使L型支架下降至与杨木纤维另一端正好接触为止,此时用紫外光固化胶粘剂将二者粘连,杨木纤维此时仅受自身重力的作用,在第一底座与L型支架之间自然绷直;将电子天平的读数归零;(3) Adhere one end of the poplar fiber to the first base by using ultraviolet curing adhesive, and fix the poplar fiber at the center point of the first base; adjust the adjustment knob of the slide-away slicer to make the L-shaped bracket drop to the same level as the poplar fiber. The other end of the wood fiber just touches, at this time, the two are adhered with ultraviolet curing adhesive, and the poplar fiber is only under the action of its own gravity at this time, and naturally stretches between the first base and the L-shaped bracket; zero reading;
(4)在杨木纤维线弹性范围内,操作滑走式切片机使L型支架向上移动,从而使杨木纤维在竖直方向受到拉伸作用,通过控制面板显示将木材纤维拉伸至绝对伸长量dL=3.50μm,读取在该伸长量下的天平读数为-0.414g,即产生的拉力载荷F=-mg=-(-0.414)/1000×9.8N,此后,继续移动L型支架,拉伸木材纤维至绝对伸长量dL为5.50μm,7.50μm,9.50μm,11.5μm,读取电子天平对应的读数m为-0.786g,-1.095g,-1.351g,-1.759g;(4) Within the linear elasticity range of poplar fiber, operate the slide-away slicer to move the L-shaped bracket upward, so that the poplar fiber is stretched in the vertical direction, and the wood fiber is stretched to the absolute stretch through the control panel display. Length dL=3.50μm, the balance reading at this elongation is -0.414g, that is, the resulting tensile load F=-mg=-(-0.414)/1000×9.8N, after that, continue to move the L-shaped Bracket, stretch the wood fiber to the absolute elongation dL of 5.50μm, 7.50μm, 9.50μm, 11.5μm, the readings corresponding to the electronic balance m are -0.786g, -1.095g, -1.351g, -1.759g;
(5)利用调节旋钮进一步施加载荷直至杨木纤维断裂,记录断裂时的纤维伸长量117μm,电子天平的读数mc=-8.314g,计算临界载荷Fc=-mcg=-8.314/1000×9.8=0.0815N;(5) Use the adjusting knob to further apply the load until the poplar fiber breaks, record the fiber elongation at break of 117 μm, the reading of the electronic balance m c = -8.314g, and calculate the critical load F c = -m c g = -8.314/ 1000×9.8=0.0815N;
(6)木材纤维断裂后,操作滑走式切片机下移L型支架直至L型支架上的紫外固化胶与第一底座上的紫外固化胶正好触碰为止,记录此时显示的步进长度为-1054.3μm,即单根木材纤维的初始长度L=1054.3μm。(6) After the wood fiber is broken, operate the slide-away slicer to move the L-shaped bracket down until the UV-curing glue on the L-shaped bracket just touches the UV-curing glue on the first base, and record the displayed step length at this time as -1054.3 μm, that is, the initial length of a single wood fiber L=1054.3 μm.
(7)根据式(1),计算含水率为12%的杨木纤维绝对伸长量dL分别为3.50μm,5.50μm,7.50μm,9.50μm,11.5μm时,杨木纤维的弹性模量分别为6.96GPa,8.46GPa,8.59GPa,8.11GPa,8.99GPa,标准差为0.77GPa。为进一步了解其数据的可靠性,整理了5个不同载荷增量下的应力增量—应变增量数据拟合图(见图6),从图中6可以看出数据点都非常靠近拟合直线,相关系数R=0.999,非常接近1,说明线性相关性良好,数据可靠。(7) According to formula (1), when the absolute elongation dL of poplar fibers with a moisture content of 12% is calculated to be 3.50 μm, 5.50 μm, 7.50 μm, 9.50 μm, and 11.5 μm, respectively, the elastic moduli of poplar fibers are respectively It is 6.96GPa, 8.46GPa, 8.59GPa, 8.11GPa, 8.99GPa, and the standard deviation is 0.77GPa. In order to further understand the reliability of its data, the stress increment-strain increment data fitting graphs under 5 different load increments were sorted out (see Figure 6). From Figure 6, it can be seen that the data points are very close to the fitting. Straight line, the correlation coefficient R=0.999, very close to 1, indicating that the linear correlation is good and the data is reliable.
(8)根据式(2)可计算出含水率为12%的杨木单纤维的拉伸强度为463MPa。(8) According to the formula (2), the tensile strength of the poplar single fiber with a moisture content of 12% can be calculated to be 463 MPa.
综上所述,本发明所述的木材单纤微力学测量方法和装置可广泛应用于木材领域,可对几个微米到几十个微米的木材纤维进行测试,且无需添置新设备,仅对木材实验室中滑走式切片机加以改造即可,成本低廉,操作简单,对木材纤维力学性能评价及实验设备的改造利用具有重要意义。To sum up, the method and device for measuring the micromechanics of wood single fiber according to the present invention can be widely used in the field of wood, and can test wood fibers of several microns to dozens of microns without adding new equipment. The slide-away slicer in the wood laboratory can be modified. The cost is low and the operation is simple. It is of great significance for the evaluation of the mechanical properties of wood fibers and the modification and utilization of experimental equipment.
以上所述仅是本发明的优选实施方式,应当指出,对于本技术领域的普通技术人员来说,在不脱离本发明技术原理的前提下,还可以做出若干改进和变形,这些改进和变形也应视为本发明的保护范围。The above are only the preferred embodiments of the present invention. It should be pointed out that for those skilled in the art, without departing from the technical principle of the present invention, several improvements and modifications can also be made. These improvements and modifications It should also be regarded as the protection scope of the present invention.
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