CN110037290A - A kind of preparation method of coprinus comatus instant powder - Google Patents
A kind of preparation method of coprinus comatus instant powder Download PDFInfo
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- CN110037290A CN110037290A CN201910440742.9A CN201910440742A CN110037290A CN 110037290 A CN110037290 A CN 110037290A CN 201910440742 A CN201910440742 A CN 201910440742A CN 110037290 A CN110037290 A CN 110037290A
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- coprinus comatus
- instant powder
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- 244000234623 Coprinus comatus Species 0.000 title claims abstract description 49
- 235000004439 Coprinus comatus Nutrition 0.000 title claims abstract description 49
- 239000000843 powder Substances 0.000 title claims abstract description 28
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 238000000605 extraction Methods 0.000 claims abstract description 52
- 239000000287 crude extract Substances 0.000 claims abstract description 21
- 230000005686 electrostatic field Effects 0.000 claims abstract description 19
- 239000000706 filtrate Substances 0.000 claims abstract description 16
- 235000013339 cereals Nutrition 0.000 claims abstract description 13
- 239000011812 mixed powder Substances 0.000 claims abstract description 13
- 239000011664 nicotinic acid Substances 0.000 claims abstract description 9
- -1 sucrose fatty ester Chemical class 0.000 claims abstract description 9
- 229930006000 Sucrose Natural products 0.000 claims abstract description 8
- DPXJVFZANSGRMM-UHFFFAOYSA-N acetic acid;2,3,4,5,6-pentahydroxyhexanal;sodium Chemical compound [Na].CC(O)=O.OCC(O)C(O)C(O)C(O)C=O DPXJVFZANSGRMM-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000001768 carboxy methyl cellulose Substances 0.000 claims abstract description 8
- 235000019812 sodium carboxymethyl cellulose Nutrition 0.000 claims abstract description 8
- 229920001027 sodium carboxymethylcellulose Polymers 0.000 claims abstract description 8
- 239000005720 sucrose Substances 0.000 claims abstract description 8
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 6
- 239000004382 Amylase Substances 0.000 claims abstract description 5
- 102000013142 Amylases Human genes 0.000 claims abstract description 5
- 108010065511 Amylases Proteins 0.000 claims abstract description 5
- 235000019418 amylase Nutrition 0.000 claims abstract description 5
- 239000012528 membrane Substances 0.000 claims abstract description 3
- 238000002525 ultrasonication Methods 0.000 claims abstract description 3
- 239000007788 liquid Substances 0.000 claims description 14
- 241000209094 Oryza Species 0.000 claims description 9
- 235000007164 Oryza sativa Nutrition 0.000 claims description 9
- 235000009566 rice Nutrition 0.000 claims description 9
- 102000004139 alpha-Amylases Human genes 0.000 claims description 8
- 108090000637 alpha-Amylases Proteins 0.000 claims description 8
- 229940024171 alpha-amylase Drugs 0.000 claims description 8
- 239000000284 extract Substances 0.000 claims description 8
- 230000000694 effects Effects 0.000 claims description 4
- 239000000463 material Substances 0.000 claims description 4
- 239000000654 additive Substances 0.000 claims description 2
- 230000000996 additive effect Effects 0.000 claims description 2
- 239000003595 mist Substances 0.000 claims description 2
- CKQVRZJOMJRTOY-UHFFFAOYSA-N octadecanoic acid;propane-1,2,3-triol Chemical class OCC(O)CO.CCCCCCCCCCCCCCCCCC(O)=O CKQVRZJOMJRTOY-UHFFFAOYSA-N 0.000 claims description 2
- 239000007921 spray Substances 0.000 claims description 2
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 1
- 235000010948 carboxy methyl cellulose Nutrition 0.000 claims 1
- 229910052708 sodium Inorganic materials 0.000 claims 1
- 239000011734 sodium Substances 0.000 claims 1
- 150000004676 glycans Chemical class 0.000 abstract description 14
- 229920001282 polysaccharide Polymers 0.000 abstract description 14
- 239000005017 polysaccharide Substances 0.000 abstract description 14
- 238000001035 drying Methods 0.000 abstract description 12
- 102000004169 proteins and genes Human genes 0.000 abstract description 10
- 108090000623 proteins and genes Proteins 0.000 abstract description 10
- 239000000203 mixture Substances 0.000 abstract description 4
- 238000011084 recovery Methods 0.000 abstract description 4
- 210000002784 stomach Anatomy 0.000 abstract description 2
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 12
- 238000000034 method Methods 0.000 description 9
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 8
- 238000004140 cleaning Methods 0.000 description 8
- 235000018102 proteins Nutrition 0.000 description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
- 230000005684 electric field Effects 0.000 description 6
- 229920001353 Dextrin Polymers 0.000 description 4
- 239000004375 Dextrin Substances 0.000 description 4
- 241000196324 Embryophyta Species 0.000 description 4
- 229920002472 Starch Polymers 0.000 description 4
- 239000002253 acid Substances 0.000 description 4
- 235000019425 dextrin Nutrition 0.000 description 4
- 239000012153 distilled water Substances 0.000 description 4
- 238000002156 mixing Methods 0.000 description 4
- 230000008569 process Effects 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 230000005855 radiation Effects 0.000 description 4
- 238000007873 sieving Methods 0.000 description 4
- 235000019698 starch Nutrition 0.000 description 4
- 239000008107 starch Substances 0.000 description 4
- 239000006228 supernatant Substances 0.000 description 4
- 230000002195 synergetic effect Effects 0.000 description 4
- 241000233866 Fungi Species 0.000 description 3
- 229920002774 Maltodextrin Polymers 0.000 description 3
- 239000005913 Maltodextrin Substances 0.000 description 3
- 238000007792 addition Methods 0.000 description 3
- 210000004027 cell Anatomy 0.000 description 3
- 210000000170 cell membrane Anatomy 0.000 description 3
- 235000013305 food Nutrition 0.000 description 3
- 229940035034 maltodextrin Drugs 0.000 description 3
- 238000002604 ultrasonography Methods 0.000 description 3
- 102000004190 Enzymes Human genes 0.000 description 2
- 108090000790 Enzymes Proteins 0.000 description 2
- 241000287828 Gallus gallus Species 0.000 description 2
- KDXKERNSBIXSRK-UHFFFAOYSA-N Lysine Natural products NCCCCC(N)C(O)=O KDXKERNSBIXSRK-UHFFFAOYSA-N 0.000 description 2
- 239000004472 Lysine Substances 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 235000001014 amino acid Nutrition 0.000 description 2
- 150000001413 amino acids Chemical class 0.000 description 2
- 210000002421 cell wall Anatomy 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 229940079593 drug Drugs 0.000 description 2
- 229940088598 enzyme Drugs 0.000 description 2
- 210000001035 gastrointestinal tract Anatomy 0.000 description 2
- 125000002791 glucosyl group Chemical group C1([C@H](O)[C@@H](O)[C@H](O)[C@H](O1)CO)* 0.000 description 2
- 230000007062 hydrolysis Effects 0.000 description 2
- 238000006460 hydrolysis reaction Methods 0.000 description 2
- 230000003301 hydrolyzing effect Effects 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 235000013372 meat Nutrition 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 239000013076 target substance Substances 0.000 description 2
- 235000001674 Agaricus brunnescens Nutrition 0.000 description 1
- 102000009091 Amyloidogenic Proteins Human genes 0.000 description 1
- 108010048112 Amyloidogenic Proteins Proteins 0.000 description 1
- 229920000945 Amylopectin Polymers 0.000 description 1
- 229920000856 Amylose Polymers 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 229920002261 Corn starch Polymers 0.000 description 1
- 229920000858 Cyclodextrin Polymers 0.000 description 1
- 239000001116 FEMA 4028 Substances 0.000 description 1
- WHUUTDBJXJRKMK-UHFFFAOYSA-N Glutamic acid Natural products OC(=O)C(N)CCC(O)=O WHUUTDBJXJRKMK-UHFFFAOYSA-N 0.000 description 1
- CKLJMWTZIZZHCS-REOHCLBHSA-N L-aspartic acid Chemical compound OC(=O)[C@@H](N)CC(O)=O CKLJMWTZIZZHCS-REOHCLBHSA-N 0.000 description 1
- WHUUTDBJXJRKMK-VKHMYHEASA-N L-glutamic acid Chemical compound OC(=O)[C@@H](N)CCC(O)=O WHUUTDBJXJRKMK-VKHMYHEASA-N 0.000 description 1
- 240000000111 Saccharum officinarum Species 0.000 description 1
- 235000007201 Saccharum officinarum Nutrition 0.000 description 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 230000000259 anti-tumor effect Effects 0.000 description 1
- 235000003704 aspartic acid Nutrition 0.000 description 1
- 238000000889 atomisation Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- OQFSQFPPLPISGP-UHFFFAOYSA-N beta-carboxyaspartic acid Natural products OC(=O)C(N)C(C(O)=O)C(O)=O OQFSQFPPLPISGP-UHFFFAOYSA-N 0.000 description 1
- WHGYBXFWUBPSRW-FOUAGVGXSA-N beta-cyclodextrin Chemical compound OC[C@H]([C@H]([C@@H]([C@H]1O)O)O[C@H]2O[C@@H]([C@@H](O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O3)[C@H](O)[C@H]2O)CO)O[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@@H]3O[C@@H]1CO WHGYBXFWUBPSRW-FOUAGVGXSA-N 0.000 description 1
- 235000011175 beta-cyclodextrine Nutrition 0.000 description 1
- 229960004853 betadex Drugs 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
- 235000014633 carbohydrates Nutrition 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000000295 complement effect Effects 0.000 description 1
- 238000013329 compounding Methods 0.000 description 1
- 239000008120 corn starch Substances 0.000 description 1
- 229940099112 cornstarch Drugs 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 238000004520 electroporation Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000002255 enzymatic effect Effects 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 210000004051 gastric juice Anatomy 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 235000013922 glutamic acid Nutrition 0.000 description 1
- 239000004220 glutamic acid Substances 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 230000000968 intestinal effect Effects 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 235000004213 low-fat Nutrition 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 230000010534 mechanism of action Effects 0.000 description 1
- 230000000813 microbial effect Effects 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 239000000419 plant extract Substances 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 238000004088 simulation Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000001694 spray drying Methods 0.000 description 1
- 230000001360 synchronised effect Effects 0.000 description 1
- 238000002137 ultrasound extraction Methods 0.000 description 1
- 235000020795 whole food diet Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L31/00—Edible extracts or preparations of fungi; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/30—Physical treatment, e.g. electrical or magnetic means, wave energy or irradiation
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/30—Physical treatment, e.g. electrical or magnetic means, wave energy or irradiation
- A23L5/32—Physical treatment, e.g. electrical or magnetic means, wave energy or irradiation using phonon wave energy, e.g. sound or ultrasonic waves
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L7/00—Cereal-derived products; Malt products; Preparation or treatment thereof
- A23L7/10—Cereal-derived products
- A23L7/104—Fermentation of farinaceous cereal or cereal material; Addition of enzymes or microorganisms
- A23L7/107—Addition or treatment with enzymes not combined with fermentation with microorganisms
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L7/00—Cereal-derived products; Malt products; Preparation or treatment thereof
- A23L7/10—Cereal-derived products
- A23L7/198—Dry unshaped finely divided cereal products, not provided for in groups A23L7/117 - A23L7/196 and A23L29/00, e.g. meal, flour, powder, dried cereal creams or extracts
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
- A23P10/00—Shaping or working of foodstuffs characterised by the products
- A23P10/40—Shaping or working of foodstuffs characterised by the products free-flowing powder or instant powder, i.e. powder which is reconstituted rapidly when liquid is added
- A23P10/47—Shaping or working of foodstuffs characterised by the products free-flowing powder or instant powder, i.e. powder which is reconstituted rapidly when liquid is added using additives, e.g. emulsifiers, wetting agents or dust-binding agents
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Biotechnology (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The preparation method of a kind of coprinus comatus instant powder disclosed by the invention, comprising the following steps: (1) using cereal and coprinus comatus mixture as raw material, be ground up, sieved to obtain mixed-powder;(2) mixed-powder is dissolved in solution, ultrasonication and rupture of membranes under the conditions of electrostatic field are centrifuged to obtain crude extract;(3) crude extract is freeze-dried, then carries out semi-bionic extraction method, take filtrate;(4) glycerin monostearate, sucrose fatty ester, sodium carboxymethylcellulose, amylase are successively added in the filtrate;(5) mixed liquor being spray-dried in the step (4), up to the coprinus comatus instant powder, prepared coprinus comatus instant powder protein utilization rate is big, and polysaccharide and activated protein recovery rate are high, stomach absorptivity is strong, and drying process with atomizing can be completed without adding drying aid.
Description
Technical field
The present invention relates to food technology fields, and in particular to a kind of preparation method of coprinus comatus instant powder.
Background technique
Coprinus comatus is commonly called as coprinus comatus, because its shaped like chicken leg, meat meat flavour like shredded chicken due to gain the name, be manually to develop life in recent years
A kind of Rare edible fungus class with business potential of production.Due to coprinus comatus tool high protein, low fat, amino acid classes are complete etc.
Feature is known as " rising star in bacterium ".Except containing in addition to abundant protein in coprinus comatus, there are also carbohydrate abundant, coprinus comatus polysaccharide and
Albumen can improve immunity of organisms, and anti-tumor activity with higher.
The superiority and inferiority of extractive technique directly influences the quality of extract and the utilization rate of food resource, productivity and economic effect
Benefit, therefore, plant extracts are the core products of wholefood and Medicines and Health Product market, and the effective component of coprinus comatus is mainly
Polysaccharide and albumen extract the polysaccharide and activated protein of coprinus comatus with only having the matter amount of having, can just produce high-quality
Solid powder.
In the prior art, to the extraction method of plant be usually single Enzymatic Extraction, ultrasonic extraction, soda acid extract etc.,
These necessary conditions that all effective component in coprinus comatus developed cannot to greatest extent, and prepare instant powder are additions
Dextrin, dextrin quality is irregular on the market, and second purchase cost of material increases.
Summary of the invention
To solve the above problems, the present invention provides a kind of preparation method of coprinus comatus instant powder, prepared coprinus comatus speed
Molten amyloid proteins utilization rate is big, and polysaccharide and activated protein recovery rate are high, and stomach absorptivity is strong, and spray can be completed without adding drying aid
Mist drying process.
The technical solution that the present invention solves is to provide a kind of preparation method of coprinus comatus instant powder, comprising the following steps: (1)
Using cereal and coprinus comatus mixture as raw material, it is ground up, sieved to obtain mixed-powder;(2) mixed-powder is dissolved in solution,
Ultrasonication and rupture of membranes under the conditions of electrostatic field, are centrifuged to obtain crude extract;(3) crude extract is freeze-dried, then carries out half and imitates
It is raw to extract, take filtrate;(4) successively add glycerin monostearate, sucrose fatty ester, sodium carboxymethylcellulose, amylase in
In the filtrate;(5) mixed liquor in the step (4) is spray-dried to get the coprinus comatus instant powder.
Preferably, ultrasonic power is 800-1000W in the step (2), and ultrasonic temperature is 30-40 DEG C, and ultrasonic time is
2-3min。
Preferably, electrostatic field voltage is 5-8V in the step (2), and electrostatic field extraction time is 20-30min.
Preferably, the step of semi-bionic extraction method is as follows: (3.1) are slightly mentioned for the extracting solution of 3.5-4.0 to described with pH
Liquid is extracted, the extraction temperature be 40-50 DEG C, extraction time 40-60min, solid-liquid ratio 1:20,3000r/min from
The heart 5 minutes simultaneously filters, and obtains an extracting solution;(3.2) crude extract is extracted for the extracting solution of 8.5-9.0 with pH, institute
It states extraction temperature and is 40-50 DEG C, extraction time 40-60min, solid-liquid ratio 1:20,3000r/min and be centrifuged 5 minutes and filter,
Obtain secondary raffinate;(3.3) merge an extracting solution and secondary raffinate, that is, step (3) described filtrate.
Preferably, the cereal is one of polished rice, long-grained nonglutinous rice, and the material ratio of the cereal and coprinus comatus is 8:3.
Preferably, in the step (4), the mass fraction of additive are as follows: 5-10 parts of glycerin monostearates, 5-10 parts of sugarcanes
Sugar fatty acid ester, 1-5 part sodium carboxymethylcellulose, 2-10 parts of amylase, and the mixed-powder mass fraction is 60-80 parts,
The amylase activity is 100U/g.
This programme can destroy plant cell wall using mixed-powder described in the coarse extraction of ultrasonic synergistic electrostatic field, ultrasound, electricity
The mechanism of action of field is directly to be acted on by external electrical field plant or microbial cell film, and cell membrane is caused to generate electroporation
Phenomenon improves cell membrane mass-transfer efficiency, can destroy plant cell membrane, therefore ultrasound and electric field cooperate with to extract and can accelerate target
Substance enters the process of solvent from cell, and in the extraction process of supersonic synergic electric field, ultrasonic cavitation is to improve extraction efficiency
Main cause, and the presence of electric field enhances cavitation effect, ultrasound and electric field synergistic extraction can accelerate target substance from cell into
Enter the process of solvent, shorten extraction time, improve product quality, reduce energy consumption, obtains more high extracting efficiency.
Since total sugar content is high in extracting solution, cause atomization uneven, it is serious to glue wall, obtain that powder rate is low, and product hygroscopicity is strong,
To be addressed the reason of making to be spray-dried viscous wall, rapid-curing cutback powder moisture absorption, a certain proportion of drying aid, the drying aid are generally added
It can be maltodextrin, beta-cyclodextrin, cornstarch, and maltodextrin is raw material by starch, controls hydrolysis through enzyme method technique
It forms, alpha-amylase is from -1.4 glycosidic bond of hydrolyzing alpha inside starch molecule, to change amylose and amylopectin linearity side
The degree of polymerization of chain makes Starch Hydrolysis generate soluble dextrins, and fungi polysaccharide, especially mushroom class, as the polysaccharide in coprinus comatus is
A kind of living polymer compound, main chain is by β-D(1-73) connection glucosyl group form, along the same β-D of main chain random distribution
The glucosyl group that the side (1-73) connects is in pectinate texture, and shape is in 3 D stereo helical form, belongs to β-type polysaccharide, according to the special of enzyme
One property, using cereal as one of raw material in this programme, on the one hand reduces subsequent addition dextrin as helping not by amylorrhexis
The step of dry agent, another aspect protein complementary action is the effective way for promoting nutrient protein value, by cereal and coprinus comatus
It is also a kind of effective means that albumen, which carries out compounding, but two kinds of material proteins are simply mixed that may result in component unevenly distributed,
Nutrition is uneven, and lysine lacks in cereal, and lysine is abundant in coprinus comatus, and the delicious amino acids such as glutamic acid and aspartic acid contain
Amount is high, and miscible albumen uniformity can be improved in synchronous extract, and shortens extraction time, simplifies albumen and compounds process.
Semi-bionic extraction, is the bionic component part of food, and the principle of this extractive technique is to imitate to take orally
Drug carries out continuous extraction successively using the acid water and alkaline water that determine pH value in the mechanism of the transhipment of gastrointestinal tract.Half
The main purpose of bionic extraction method be extract it is high " active mixture " containing index components, in the semi-bionic extraction method of this programme,
PH value when primary extraction is that simulate the gastric juice absorbs environment set, if pH value is too small, acid excessive, the glycosidic bond meeting of polysaccharide
It is destroyed by H+, so that polyoses content reduces and reduced sugar raising, but under the extraction environment of weak acid, the acidity in coprinus comatus is more
The electrostatic repulsion ability of sugar will increase, and such coprinus comatus polysaccharide is just easier to be dissolved in water, and recovery rate increases, and mention for the second time
PH value simulation human body intestinal canal when taking absorbs environment set, and certain alkali plays destruction to the cell wall of coprinus comatus, favorably
In the dissolution of acidic polysaccharose, so that the recovery rate of coprinus comatus polysaccharide increases, but when extraction environment is strong alkali environment, coprinus comatus is more
The glycosidic bond of sugar can be by the variation for being allowed to fracture and occurred conformation be destroyed, so as to cause the reduction of coprinus comatus polysaccharide extract rate.
Beneficial effects of the present invention are as follows: 1., which carry out broken wall to coprinus comatus and cereal using supersonic synergic electric field action, breaks
Film process shortens extraction time, target component is allowed to be fully dissolved out;2. utilizing the polysaccharide in semi-bionic extraction method coprinus comatus and cereal
And protein, the loss of effective ingredient can be reduced in extraction process, not only with respect to the work of mixture during extraction
Property ingredient also adequately controls the monomer component to be extracted, the operating feelings of half bionical extraction process simulated gastrointestinal tract etc.
Condition, extract is to the more adaptable of human body;3. by the drying aid in alpha-amylase alternate subsequent step, effective hydrolyzed cereal
In starch be maltodextrin without hydrolyzing other fungi polysaccharides, be conducive to spray drying, and no longer need to addition drying aid, to paddy
Object has carried out sufficient utilization.
Specific embodiment
In order to make content of the present invention easily facilitate understanding, With reference to embodiment to of the present invention
Technical solution is described further, but the present invention is not limited only to this.
Raw material used in the present invention be unless otherwise specified it is common commercially available, AR is pure.
Embodiment 1
80g long-grained nonglutinous rice, 30g coprinus comatus mycorhiza are taken, 40 DEG C of drying are ground, and are crossed 80 meshes and are added the mixed-powder after sieving
Enter 1000ml distilled water, supersonic cleaning machine is put into electrostatic field generator radiation scope, adjustment electrostatic field generator is 8V, institute
It states electrostatic field generator model Wuxi Wan Jiali and closes agricultural development Co., Ltd WJ- II, adjust supersonic cleaning machine ultrasonic power
For 800W, ultrasonic temperature is 30 DEG C, and ultrasonic 2min, 4000r/min are centrifuged 10min, take supernatant, as crude extract.
By crude extract in batches -70 DEG C be freeze-dried for 24 hours after, merge powder, for the first time with pH be 3.5 hydrochloric acid solution
The crude extract is extracted, the extraction temperature is 40 DEG C, extraction time 40min, solid-liquid ratio 1:20,3000r/
Min is centrifuged 5 minutes and filters, and obtains an extracting solution;Second with pH be 8.5 NaOH solution to the filter residue in above-mentioned steps into
Row extraction, the extraction temperature are 40 DEG C, extraction time 40min, and solid-liquid ratio 1:20,3000r/min are centrifuged 5 minutes and mistake
Filter, obtains secondary raffinate;Merge an extracting solution and secondary raffinate i.e. filtrate.
2g glycerin monostearate, 2g sucrose fatty ester, 1g sodium carboxymethylcellulose, 2g alpha-amylase are weighed in described
In filtrate, 1h is stirred at 45 DEG C, after mixing, is spray-dried to get coprinus comatus instant powder.
Embodiment 2
40g long-grained nonglutinous rice, 15g coprinus comatus mycorhiza are taken, 40 DEG C of drying are ground, and are crossed 80 meshes and are added the mixed-powder after sieving
Enter 500ml distilled water, supersonic cleaning machine is put into electrostatic field generator radiation scope, adjustment electrostatic field generator is 5V, institute
It states electrostatic field generator model Wuxi Wan Jiali and closes agricultural development Co., Ltd WJ- II, adjust supersonic cleaning machine ultrasonic power
For 1000W, ultrasonic temperature is 40 DEG C, and ultrasonic 3min, 4000r/min are centrifuged 10min, take supernatant, as crude extract.
By crude extract in batches -70 DEG C be freeze-dried for 24 hours after, merge powder, for the first time with pH be 4 hydrochloric acid solution pair
The crude extract is extracted, and the extraction temperature is 60 DEG C, extraction time 50min, solid-liquid ratio 1:20,3000r/min
It is centrifuged 5 minutes and filters, obtain an extracting solution;The filter residue in above-mentioned steps is soaked with the NaOH solution that pH is 9 for the second time
It mentioning, the extraction temperature is 40 DEG C, extraction time 60min, solid-liquid ratio 1:20,3000r/min and is centrifuged 5 minutes and filters,
Obtain secondary raffinate;Merge an extracting solution and secondary raffinate i.e. filtrate.
1g glycerin monostearate, 1g sucrose fatty ester, 0.5g sodium carboxymethylcellulose, 1g alpha-amylase are weighed in institute
It states in filtrate, 1h is stirred at 45 DEG C, after mixing, be spray-dried to get coprinus comatus instant powder.
Embodiment 3
40g polished rice, 15g coprinus comatus mycorhiza are taken, 40 DEG C of drying are ground, and are crossed 80 meshes and are added the mixed-powder after sieving
Enter 500ml distilled water, supersonic cleaning machine is put into electrostatic field generator radiation scope, adjustment electrostatic field generator is 7V, institute
It states electrostatic field generator model Wuxi Wan Jiali and closes agricultural development Co., Ltd WJ- II, adjust supersonic cleaning machine ultrasonic power
For 900W, ultrasonic temperature is 35 DEG C, and ultrasonic 3min, 4000r/min are centrifuged 10min, take supernatant, as crude extract.
By crude extract in batches -70 DEG C be freeze-dried for 24 hours after, merge powder, for the first time with pH be 4 hydrochloric acid solution pair
The crude extract is extracted, and the extraction temperature is 50 DEG C, extraction time 50min, solid-liquid ratio 1:20,3000r/min
It is centrifuged 5 minutes and filters, obtain an extracting solution;The filter residue in above-mentioned steps is soaked with the NaOH solution that pH is 9 for the second time
It mentioning, the extraction temperature is 50 DEG C, extraction time 60min, solid-liquid ratio 1:20,3000r/min and is centrifuged 5 minutes and filters,
Obtain secondary raffinate;Merge an extracting solution and secondary raffinate i.e. filtrate.
1g glycerin monostearate, 1g sucrose fatty ester, 0.5g sodium carboxymethylcellulose, 1g alpha-amylase are weighed in institute
It states in filtrate, 1h is stirred at 45 DEG C, after mixing, be spray-dried to get coprinus comatus instant powder.
Embodiment 4
40g polished rice, 15g coprinus comatus mycorhiza are taken, 40 DEG C of drying are ground, and are crossed 80 meshes and are added the mixed-powder after sieving
Enter 500ml distilled water, supersonic cleaning machine is put into electrostatic field generator radiation scope, adjustment electrostatic field generator is 8V, institute
It states electrostatic field generator model Wuxi Wan Jiali and closes agricultural development Co., Ltd WJ- II, adjust supersonic cleaning machine ultrasonic power
For 900W, ultrasonic temperature is 35 DEG C, and ultrasonic 3min, 4000r/min are centrifuged 10min, take supernatant, as crude extract.
By crude extract in batches -70 DEG C be freeze-dried for 24 hours after, merge powder, for the first time with pH be 3.8 hydrochloric acid solution
The crude extract is extracted, the extraction temperature is 50 DEG C, extraction time 50min, solid-liquid ratio 1:20,3000r/
Min is centrifuged 5 minutes and filters, and obtains an extracting solution;Second with pH be 8.7 NaOH solution to the filter residue in above-mentioned steps into
Row extraction, the extraction temperature are 50 DEG C, extraction time 50min, and solid-liquid ratio 1:20,3000r/min are centrifuged 5 minutes and mistake
Filter, obtains secondary raffinate;Merge an extracting solution and secondary raffinate i.e. filtrate.
2g glycerin monostearate, 2g sucrose fatty ester, 1g sodium carboxymethylcellulose, 2g alpha-amylase are weighed in described
In filtrate, 1h is stirred at 45 DEG C, after mixing, is spray-dried to get coprinus comatus instant powder.
The foregoing is merely presently preferred embodiments of the present invention, all equivalent changes done according to scope of the present invention patent with
Modification, is all covered by the present invention.
Claims (6)
1. a kind of preparation method of coprinus comatus instant powder, which comprises the following steps: (1) mixed with cereal and coprinus comatus
Object is closed as raw material, is ground up, sieved to obtain mixed-powder;(2) mixed-powder is dissolved in solution, ultrasonication and in electrostatic
Rupture of membranes under field condition is centrifuged to obtain crude extract;(3) crude extract is freeze-dried, then carries out semi-bionic extraction method, take filtrate;(4)
Glycerin monostearate, sucrose fatty ester, sodium carboxymethylcellulose, alpha-amylase are successively added in the filtrate;(5) it sprays
Mixed liquor in the dry step (4) of mist is to get the coprinus comatus instant powder.
2. a kind of preparation method of coprinus comatus instant powder according to claim 1, which is characterized in that in the step (2)
Ultrasonic power is 800-1000W, and ultrasonic temperature is 30-40 DEG C, ultrasonic time 2-3min.
3. a kind of preparation method of coprinus comatus instant powder according to claim 1, which is characterized in that in the step (2)
Electrostatic field voltage is 5-8V, and electrostatic field extraction time is 20-30min.
4. a kind of preparation method of coprinus comatus instant powder according to claim 1, which is characterized in that the semi-bionic extraction method
The step of it is as follows: (3.1) extract the crude extract for the extracting solution of 3.5-4.0 with pH, the extraction temperature be 40-50
DEG C, extraction time 40-60min, solid-liquid ratio 1:20,3000r/min are centrifuged 5 minutes and filter, and obtain an extracting solution;
(3.2) crude extract is extracted for the extracting solution of 8.5-9.0 with pH, the extraction temperature is 40-50 DEG C, extraction time
For 40-60min, solid-liquid ratio 1:20,3000r/min are centrifuged 5 minutes and filter, and obtain secondary raffinate;(3.3) merge and once mention
Take liquid and secondary raffinate i.e. step (3) described filtrate.
5. a kind of preparation method of coprinus comatus instant powder according to claim 1, which is characterized in that the cereal is round-grained rice
One of rice, long-grained nonglutinous rice, the material ratio of the cereal and coprinus comatus are 8:3.
6. a kind of preparation method of coprinus comatus instant powder according to claim 1, which is characterized in that in the step (4),
The mass fraction of additive are as follows: 5-10 parts of glycerin monostearates, 5-10 parts of sucrose fatty esters, 1-5 parts of carboxymethyl celluloses
Sodium, 2-10 part alpha-amylase, and the mixed-powder mass fraction is 60-80 parts, the amylase activity is 100U/g.
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112029576A (en) * | 2020-08-26 | 2020-12-04 | 芜湖美町宝植物科技有限公司 | Supercritical carbon dioxide extraction method for sea buckthorn seed oil |
Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102786606A (en) * | 2012-09-05 | 2012-11-21 | 龙海市颖欣农业科技有限公司 | Processing method of lentinan |
CN103564145A (en) * | 2013-11-06 | 2014-02-12 | 东北农业大学 | Method for extracting high-solubility black soya bean protein |
CN105495554A (en) * | 2015-12-22 | 2016-04-20 | 山西农业大学 | Ganoderma lucidum mycelium instant powder and preparation method thereof |
CN106578891A (en) * | 2016-12-21 | 2017-04-26 | 安徽豆宝食品有限公司 | Sweet scented osmanthus stomach-invigorating corn brewing powder and preparation method thereof |
CN106937959A (en) * | 2017-05-03 | 2017-07-11 | 杭州医学院 | A kind of antitumor extra large Blatta seu periplaneta extract and its preparation technology and detection method and purposes |
CN107712263A (en) * | 2017-11-22 | 2018-02-23 | 南京财经大学 | A kind of method of synchronous extraction rice and golden mushroom residue protein |
CN108391692A (en) * | 2018-03-15 | 2018-08-14 | 浙江工业大学 | A kind of production method of high microsteping beans short paste work goods |
-
2019
- 2019-05-24 CN CN201910440742.9A patent/CN110037290A/en active Pending
Patent Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102786606A (en) * | 2012-09-05 | 2012-11-21 | 龙海市颖欣农业科技有限公司 | Processing method of lentinan |
CN103564145A (en) * | 2013-11-06 | 2014-02-12 | 东北农业大学 | Method for extracting high-solubility black soya bean protein |
CN105495554A (en) * | 2015-12-22 | 2016-04-20 | 山西农业大学 | Ganoderma lucidum mycelium instant powder and preparation method thereof |
CN106578891A (en) * | 2016-12-21 | 2017-04-26 | 安徽豆宝食品有限公司 | Sweet scented osmanthus stomach-invigorating corn brewing powder and preparation method thereof |
CN106937959A (en) * | 2017-05-03 | 2017-07-11 | 杭州医学院 | A kind of antitumor extra large Blatta seu periplaneta extract and its preparation technology and detection method and purposes |
CN107712263A (en) * | 2017-11-22 | 2018-02-23 | 南京财经大学 | A kind of method of synchronous extraction rice and golden mushroom residue protein |
CN108391692A (en) * | 2018-03-15 | 2018-08-14 | 浙江工业大学 | A kind of production method of high microsteping beans short paste work goods |
Non-Patent Citations (3)
Title |
---|
李毅花: "超声协同高压静电场提取黄花菜多糖的机理研究及其结构表征", 《中国优秀硕士学位论文全文数据库工程科技I辑》 * |
杨日福等: "超声协同静电场提取黄花菜中总黄酮的研究", 《声学技术》 * |
董思敏等: "高压脉冲电场法联合提取鹿茸中蛋白质、多糖的工艺优化", 《中国药学杂志》 * |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112029576A (en) * | 2020-08-26 | 2020-12-04 | 芜湖美町宝植物科技有限公司 | Supercritical carbon dioxide extraction method for sea buckthorn seed oil |
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