CN110037290A - A kind of preparation method of coprinus comatus instant powder - Google Patents

A kind of preparation method of coprinus comatus instant powder Download PDF

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Publication number
CN110037290A
CN110037290A CN201910440742.9A CN201910440742A CN110037290A CN 110037290 A CN110037290 A CN 110037290A CN 201910440742 A CN201910440742 A CN 201910440742A CN 110037290 A CN110037290 A CN 110037290A
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coprinus comatus
instant powder
extraction
preparation
powder
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肖志勇
方丽金
郑秋芳
叶艳鹏
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Fujian Tuotian Bio-Technology Co Ltd
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Fujian Tuotian Bio-Technology Co Ltd
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L31/00Edible extracts or preparations of fungi; Preparation or treatment thereof
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L5/00Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
    • A23L5/30Physical treatment, e.g. electrical or magnetic means, wave energy or irradiation
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L5/00Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
    • A23L5/30Physical treatment, e.g. electrical or magnetic means, wave energy or irradiation
    • A23L5/32Physical treatment, e.g. electrical or magnetic means, wave energy or irradiation using phonon wave energy, e.g. sound or ultrasonic waves
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L7/00Cereal-derived products; Malt products; Preparation or treatment thereof
    • A23L7/10Cereal-derived products
    • A23L7/104Fermentation of farinaceous cereal or cereal material; Addition of enzymes or microorganisms
    • A23L7/107Addition or treatment with enzymes not combined with fermentation with microorganisms
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L7/00Cereal-derived products; Malt products; Preparation or treatment thereof
    • A23L7/10Cereal-derived products
    • A23L7/198Dry unshaped finely divided cereal products, not provided for in groups A23L7/117 - A23L7/196 and A23L29/00, e.g. meal, flour, powder, dried cereal creams or extracts
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23PSHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
    • A23P10/00Shaping or working of foodstuffs characterised by the products
    • A23P10/40Shaping or working of foodstuffs characterised by the products free-flowing powder or instant powder, i.e. powder which is reconstituted rapidly when liquid is added
    • A23P10/47Shaping or working of foodstuffs characterised by the products free-flowing powder or instant powder, i.e. powder which is reconstituted rapidly when liquid is added using additives, e.g. emulsifiers, wetting agents or dust-binding agents
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Biotechnology (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)

Abstract

The preparation method of a kind of coprinus comatus instant powder disclosed by the invention, comprising the following steps: (1) using cereal and coprinus comatus mixture as raw material, be ground up, sieved to obtain mixed-powder;(2) mixed-powder is dissolved in solution, ultrasonication and rupture of membranes under the conditions of electrostatic field are centrifuged to obtain crude extract;(3) crude extract is freeze-dried, then carries out semi-bionic extraction method, take filtrate;(4) glycerin monostearate, sucrose fatty ester, sodium carboxymethylcellulose, amylase are successively added in the filtrate;(5) mixed liquor being spray-dried in the step (4), up to the coprinus comatus instant powder, prepared coprinus comatus instant powder protein utilization rate is big, and polysaccharide and activated protein recovery rate are high, stomach absorptivity is strong, and drying process with atomizing can be completed without adding drying aid.

Description

A kind of preparation method of coprinus comatus instant powder
Technical field
The present invention relates to food technology fields, and in particular to a kind of preparation method of coprinus comatus instant powder.
Background technique
Coprinus comatus is commonly called as coprinus comatus, because its shaped like chicken leg, meat meat flavour like shredded chicken due to gain the name, be manually to develop life in recent years A kind of Rare edible fungus class with business potential of production.Due to coprinus comatus tool high protein, low fat, amino acid classes are complete etc. Feature is known as " rising star in bacterium ".Except containing in addition to abundant protein in coprinus comatus, there are also carbohydrate abundant, coprinus comatus polysaccharide and Albumen can improve immunity of organisms, and anti-tumor activity with higher.
The superiority and inferiority of extractive technique directly influences the quality of extract and the utilization rate of food resource, productivity and economic effect Benefit, therefore, plant extracts are the core products of wholefood and Medicines and Health Product market, and the effective component of coprinus comatus is mainly Polysaccharide and albumen extract the polysaccharide and activated protein of coprinus comatus with only having the matter amount of having, can just produce high-quality Solid powder.
In the prior art, to the extraction method of plant be usually single Enzymatic Extraction, ultrasonic extraction, soda acid extract etc., These necessary conditions that all effective component in coprinus comatus developed cannot to greatest extent, and prepare instant powder are additions Dextrin, dextrin quality is irregular on the market, and second purchase cost of material increases.
Summary of the invention
To solve the above problems, the present invention provides a kind of preparation method of coprinus comatus instant powder, prepared coprinus comatus speed Molten amyloid proteins utilization rate is big, and polysaccharide and activated protein recovery rate are high, and stomach absorptivity is strong, and spray can be completed without adding drying aid Mist drying process.
The technical solution that the present invention solves is to provide a kind of preparation method of coprinus comatus instant powder, comprising the following steps: (1) Using cereal and coprinus comatus mixture as raw material, it is ground up, sieved to obtain mixed-powder;(2) mixed-powder is dissolved in solution, Ultrasonication and rupture of membranes under the conditions of electrostatic field, are centrifuged to obtain crude extract;(3) crude extract is freeze-dried, then carries out half and imitates It is raw to extract, take filtrate;(4) successively add glycerin monostearate, sucrose fatty ester, sodium carboxymethylcellulose, amylase in In the filtrate;(5) mixed liquor in the step (4) is spray-dried to get the coprinus comatus instant powder.
Preferably, ultrasonic power is 800-1000W in the step (2), and ultrasonic temperature is 30-40 DEG C, and ultrasonic time is 2-3min。
Preferably, electrostatic field voltage is 5-8V in the step (2), and electrostatic field extraction time is 20-30min.
Preferably, the step of semi-bionic extraction method is as follows: (3.1) are slightly mentioned for the extracting solution of 3.5-4.0 to described with pH Liquid is extracted, the extraction temperature be 40-50 DEG C, extraction time 40-60min, solid-liquid ratio 1:20,3000r/min from The heart 5 minutes simultaneously filters, and obtains an extracting solution;(3.2) crude extract is extracted for the extracting solution of 8.5-9.0 with pH, institute It states extraction temperature and is 40-50 DEG C, extraction time 40-60min, solid-liquid ratio 1:20,3000r/min and be centrifuged 5 minutes and filter, Obtain secondary raffinate;(3.3) merge an extracting solution and secondary raffinate, that is, step (3) described filtrate.
Preferably, the cereal is one of polished rice, long-grained nonglutinous rice, and the material ratio of the cereal and coprinus comatus is 8:3.
Preferably, in the step (4), the mass fraction of additive are as follows: 5-10 parts of glycerin monostearates, 5-10 parts of sugarcanes Sugar fatty acid ester, 1-5 part sodium carboxymethylcellulose, 2-10 parts of amylase, and the mixed-powder mass fraction is 60-80 parts, The amylase activity is 100U/g.
This programme can destroy plant cell wall using mixed-powder described in the coarse extraction of ultrasonic synergistic electrostatic field, ultrasound, electricity The mechanism of action of field is directly to be acted on by external electrical field plant or microbial cell film, and cell membrane is caused to generate electroporation Phenomenon improves cell membrane mass-transfer efficiency, can destroy plant cell membrane, therefore ultrasound and electric field cooperate with to extract and can accelerate target Substance enters the process of solvent from cell, and in the extraction process of supersonic synergic electric field, ultrasonic cavitation is to improve extraction efficiency Main cause, and the presence of electric field enhances cavitation effect, ultrasound and electric field synergistic extraction can accelerate target substance from cell into Enter the process of solvent, shorten extraction time, improve product quality, reduce energy consumption, obtains more high extracting efficiency.
Since total sugar content is high in extracting solution, cause atomization uneven, it is serious to glue wall, obtain that powder rate is low, and product hygroscopicity is strong, To be addressed the reason of making to be spray-dried viscous wall, rapid-curing cutback powder moisture absorption, a certain proportion of drying aid, the drying aid are generally added It can be maltodextrin, beta-cyclodextrin, cornstarch, and maltodextrin is raw material by starch, controls hydrolysis through enzyme method technique It forms, alpha-amylase is from -1.4 glycosidic bond of hydrolyzing alpha inside starch molecule, to change amylose and amylopectin linearity side The degree of polymerization of chain makes Starch Hydrolysis generate soluble dextrins, and fungi polysaccharide, especially mushroom class, as the polysaccharide in coprinus comatus is A kind of living polymer compound, main chain is by β-D(1-73) connection glucosyl group form, along the same β-D of main chain random distribution The glucosyl group that the side (1-73) connects is in pectinate texture, and shape is in 3 D stereo helical form, belongs to β-type polysaccharide, according to the special of enzyme One property, using cereal as one of raw material in this programme, on the one hand reduces subsequent addition dextrin as helping not by amylorrhexis The step of dry agent, another aspect protein complementary action is the effective way for promoting nutrient protein value, by cereal and coprinus comatus It is also a kind of effective means that albumen, which carries out compounding, but two kinds of material proteins are simply mixed that may result in component unevenly distributed, Nutrition is uneven, and lysine lacks in cereal, and lysine is abundant in coprinus comatus, and the delicious amino acids such as glutamic acid and aspartic acid contain Amount is high, and miscible albumen uniformity can be improved in synchronous extract, and shortens extraction time, simplifies albumen and compounds process.
Semi-bionic extraction, is the bionic component part of food, and the principle of this extractive technique is to imitate to take orally Drug carries out continuous extraction successively using the acid water and alkaline water that determine pH value in the mechanism of the transhipment of gastrointestinal tract.Half The main purpose of bionic extraction method be extract it is high " active mixture " containing index components, in the semi-bionic extraction method of this programme, PH value when primary extraction is that simulate the gastric juice absorbs environment set, if pH value is too small, acid excessive, the glycosidic bond meeting of polysaccharide It is destroyed by H+, so that polyoses content reduces and reduced sugar raising, but under the extraction environment of weak acid, the acidity in coprinus comatus is more The electrostatic repulsion ability of sugar will increase, and such coprinus comatus polysaccharide is just easier to be dissolved in water, and recovery rate increases, and mention for the second time PH value simulation human body intestinal canal when taking absorbs environment set, and certain alkali plays destruction to the cell wall of coprinus comatus, favorably In the dissolution of acidic polysaccharose, so that the recovery rate of coprinus comatus polysaccharide increases, but when extraction environment is strong alkali environment, coprinus comatus is more The glycosidic bond of sugar can be by the variation for being allowed to fracture and occurred conformation be destroyed, so as to cause the reduction of coprinus comatus polysaccharide extract rate.
Beneficial effects of the present invention are as follows: 1., which carry out broken wall to coprinus comatus and cereal using supersonic synergic electric field action, breaks Film process shortens extraction time, target component is allowed to be fully dissolved out;2. utilizing the polysaccharide in semi-bionic extraction method coprinus comatus and cereal And protein, the loss of effective ingredient can be reduced in extraction process, not only with respect to the work of mixture during extraction Property ingredient also adequately controls the monomer component to be extracted, the operating feelings of half bionical extraction process simulated gastrointestinal tract etc. Condition, extract is to the more adaptable of human body;3. by the drying aid in alpha-amylase alternate subsequent step, effective hydrolyzed cereal In starch be maltodextrin without hydrolyzing other fungi polysaccharides, be conducive to spray drying, and no longer need to addition drying aid, to paddy Object has carried out sufficient utilization.
Specific embodiment
In order to make content of the present invention easily facilitate understanding, With reference to embodiment to of the present invention Technical solution is described further, but the present invention is not limited only to this.
Raw material used in the present invention be unless otherwise specified it is common commercially available, AR is pure.
Embodiment 1
80g long-grained nonglutinous rice, 30g coprinus comatus mycorhiza are taken, 40 DEG C of drying are ground, and are crossed 80 meshes and are added the mixed-powder after sieving Enter 1000ml distilled water, supersonic cleaning machine is put into electrostatic field generator radiation scope, adjustment electrostatic field generator is 8V, institute It states electrostatic field generator model Wuxi Wan Jiali and closes agricultural development Co., Ltd WJ- II, adjust supersonic cleaning machine ultrasonic power For 800W, ultrasonic temperature is 30 DEG C, and ultrasonic 2min, 4000r/min are centrifuged 10min, take supernatant, as crude extract.
By crude extract in batches -70 DEG C be freeze-dried for 24 hours after, merge powder, for the first time with pH be 3.5 hydrochloric acid solution The crude extract is extracted, the extraction temperature is 40 DEG C, extraction time 40min, solid-liquid ratio 1:20,3000r/ Min is centrifuged 5 minutes and filters, and obtains an extracting solution;Second with pH be 8.5 NaOH solution to the filter residue in above-mentioned steps into Row extraction, the extraction temperature are 40 DEG C, extraction time 40min, and solid-liquid ratio 1:20,3000r/min are centrifuged 5 minutes and mistake Filter, obtains secondary raffinate;Merge an extracting solution and secondary raffinate i.e. filtrate.
2g glycerin monostearate, 2g sucrose fatty ester, 1g sodium carboxymethylcellulose, 2g alpha-amylase are weighed in described In filtrate, 1h is stirred at 45 DEG C, after mixing, is spray-dried to get coprinus comatus instant powder.
Embodiment 2
40g long-grained nonglutinous rice, 15g coprinus comatus mycorhiza are taken, 40 DEG C of drying are ground, and are crossed 80 meshes and are added the mixed-powder after sieving Enter 500ml distilled water, supersonic cleaning machine is put into electrostatic field generator radiation scope, adjustment electrostatic field generator is 5V, institute It states electrostatic field generator model Wuxi Wan Jiali and closes agricultural development Co., Ltd WJ- II, adjust supersonic cleaning machine ultrasonic power For 1000W, ultrasonic temperature is 40 DEG C, and ultrasonic 3min, 4000r/min are centrifuged 10min, take supernatant, as crude extract.
By crude extract in batches -70 DEG C be freeze-dried for 24 hours after, merge powder, for the first time with pH be 4 hydrochloric acid solution pair The crude extract is extracted, and the extraction temperature is 60 DEG C, extraction time 50min, solid-liquid ratio 1:20,3000r/min It is centrifuged 5 minutes and filters, obtain an extracting solution;The filter residue in above-mentioned steps is soaked with the NaOH solution that pH is 9 for the second time It mentioning, the extraction temperature is 40 DEG C, extraction time 60min, solid-liquid ratio 1:20,3000r/min and is centrifuged 5 minutes and filters, Obtain secondary raffinate;Merge an extracting solution and secondary raffinate i.e. filtrate.
1g glycerin monostearate, 1g sucrose fatty ester, 0.5g sodium carboxymethylcellulose, 1g alpha-amylase are weighed in institute It states in filtrate, 1h is stirred at 45 DEG C, after mixing, be spray-dried to get coprinus comatus instant powder.
Embodiment 3
40g polished rice, 15g coprinus comatus mycorhiza are taken, 40 DEG C of drying are ground, and are crossed 80 meshes and are added the mixed-powder after sieving Enter 500ml distilled water, supersonic cleaning machine is put into electrostatic field generator radiation scope, adjustment electrostatic field generator is 7V, institute It states electrostatic field generator model Wuxi Wan Jiali and closes agricultural development Co., Ltd WJ- II, adjust supersonic cleaning machine ultrasonic power For 900W, ultrasonic temperature is 35 DEG C, and ultrasonic 3min, 4000r/min are centrifuged 10min, take supernatant, as crude extract.
By crude extract in batches -70 DEG C be freeze-dried for 24 hours after, merge powder, for the first time with pH be 4 hydrochloric acid solution pair The crude extract is extracted, and the extraction temperature is 50 DEG C, extraction time 50min, solid-liquid ratio 1:20,3000r/min It is centrifuged 5 minutes and filters, obtain an extracting solution;The filter residue in above-mentioned steps is soaked with the NaOH solution that pH is 9 for the second time It mentioning, the extraction temperature is 50 DEG C, extraction time 60min, solid-liquid ratio 1:20,3000r/min and is centrifuged 5 minutes and filters, Obtain secondary raffinate;Merge an extracting solution and secondary raffinate i.e. filtrate.
1g glycerin monostearate, 1g sucrose fatty ester, 0.5g sodium carboxymethylcellulose, 1g alpha-amylase are weighed in institute It states in filtrate, 1h is stirred at 45 DEG C, after mixing, be spray-dried to get coprinus comatus instant powder.
Embodiment 4
40g polished rice, 15g coprinus comatus mycorhiza are taken, 40 DEG C of drying are ground, and are crossed 80 meshes and are added the mixed-powder after sieving Enter 500ml distilled water, supersonic cleaning machine is put into electrostatic field generator radiation scope, adjustment electrostatic field generator is 8V, institute It states electrostatic field generator model Wuxi Wan Jiali and closes agricultural development Co., Ltd WJ- II, adjust supersonic cleaning machine ultrasonic power For 900W, ultrasonic temperature is 35 DEG C, and ultrasonic 3min, 4000r/min are centrifuged 10min, take supernatant, as crude extract.
By crude extract in batches -70 DEG C be freeze-dried for 24 hours after, merge powder, for the first time with pH be 3.8 hydrochloric acid solution The crude extract is extracted, the extraction temperature is 50 DEG C, extraction time 50min, solid-liquid ratio 1:20,3000r/ Min is centrifuged 5 minutes and filters, and obtains an extracting solution;Second with pH be 8.7 NaOH solution to the filter residue in above-mentioned steps into Row extraction, the extraction temperature are 50 DEG C, extraction time 50min, and solid-liquid ratio 1:20,3000r/min are centrifuged 5 minutes and mistake Filter, obtains secondary raffinate;Merge an extracting solution and secondary raffinate i.e. filtrate.
2g glycerin monostearate, 2g sucrose fatty ester, 1g sodium carboxymethylcellulose, 2g alpha-amylase are weighed in described In filtrate, 1h is stirred at 45 DEG C, after mixing, is spray-dried to get coprinus comatus instant powder.
The foregoing is merely presently preferred embodiments of the present invention, all equivalent changes done according to scope of the present invention patent with Modification, is all covered by the present invention.

Claims (6)

1. a kind of preparation method of coprinus comatus instant powder, which comprises the following steps: (1) mixed with cereal and coprinus comatus Object is closed as raw material, is ground up, sieved to obtain mixed-powder;(2) mixed-powder is dissolved in solution, ultrasonication and in electrostatic Rupture of membranes under field condition is centrifuged to obtain crude extract;(3) crude extract is freeze-dried, then carries out semi-bionic extraction method, take filtrate;(4) Glycerin monostearate, sucrose fatty ester, sodium carboxymethylcellulose, alpha-amylase are successively added in the filtrate;(5) it sprays Mixed liquor in the dry step (4) of mist is to get the coprinus comatus instant powder.
2. a kind of preparation method of coprinus comatus instant powder according to claim 1, which is characterized in that in the step (2) Ultrasonic power is 800-1000W, and ultrasonic temperature is 30-40 DEG C, ultrasonic time 2-3min.
3. a kind of preparation method of coprinus comatus instant powder according to claim 1, which is characterized in that in the step (2) Electrostatic field voltage is 5-8V, and electrostatic field extraction time is 20-30min.
4. a kind of preparation method of coprinus comatus instant powder according to claim 1, which is characterized in that the semi-bionic extraction method The step of it is as follows: (3.1) extract the crude extract for the extracting solution of 3.5-4.0 with pH, the extraction temperature be 40-50 DEG C, extraction time 40-60min, solid-liquid ratio 1:20,3000r/min are centrifuged 5 minutes and filter, and obtain an extracting solution; (3.2) crude extract is extracted for the extracting solution of 8.5-9.0 with pH, the extraction temperature is 40-50 DEG C, extraction time For 40-60min, solid-liquid ratio 1:20,3000r/min are centrifuged 5 minutes and filter, and obtain secondary raffinate;(3.3) merge and once mention Take liquid and secondary raffinate i.e. step (3) described filtrate.
5. a kind of preparation method of coprinus comatus instant powder according to claim 1, which is characterized in that the cereal is round-grained rice One of rice, long-grained nonglutinous rice, the material ratio of the cereal and coprinus comatus are 8:3.
6. a kind of preparation method of coprinus comatus instant powder according to claim 1, which is characterized in that in the step (4), The mass fraction of additive are as follows: 5-10 parts of glycerin monostearates, 5-10 parts of sucrose fatty esters, 1-5 parts of carboxymethyl celluloses Sodium, 2-10 part alpha-amylase, and the mixed-powder mass fraction is 60-80 parts, the amylase activity is 100U/g.
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李毅花: "超声协同高压静电场提取黄花菜多糖的机理研究及其结构表征", 《中国优秀硕士学位论文全文数据库工程科技I辑》 *
杨日福等: "超声协同静电场提取黄花菜中总黄酮的研究", 《声学技术》 *
董思敏等: "高压脉冲电场法联合提取鹿茸中蛋白质、多糖的工艺优化", 《中国药学杂志》 *

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Publication number Priority date Publication date Assignee Title
CN112029576A (en) * 2020-08-26 2020-12-04 芜湖美町宝植物科技有限公司 Supercritical carbon dioxide extraction method for sea buckthorn seed oil

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