CN109702945A - Phenolic resin glass fiber compound material colliery monitoring substation method for producing shell - Google Patents

Phenolic resin glass fiber compound material colliery monitoring substation method for producing shell Download PDF

Info

Publication number
CN109702945A
CN109702945A CN201811590176.1A CN201811590176A CN109702945A CN 109702945 A CN109702945 A CN 109702945A CN 201811590176 A CN201811590176 A CN 201811590176A CN 109702945 A CN109702945 A CN 109702945A
Authority
CN
China
Prior art keywords
shell
pressure
monitoring substation
mould
housing mould
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201811590176.1A
Other languages
Chinese (zh)
Inventor
贾柏青
陈淮荣
陈忠明
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
ZHEJIANG ZHONGMEI ELECTRON CO Ltd
Original Assignee
ZHEJIANG ZHONGMEI ELECTRON CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by ZHEJIANG ZHONGMEI ELECTRON CO Ltd filed Critical ZHEJIANG ZHONGMEI ELECTRON CO Ltd
Priority to CN201811590176.1A priority Critical patent/CN109702945A/en
Publication of CN109702945A publication Critical patent/CN109702945A/en
Pending legal-status Critical Current

Links

Landscapes

  • Reinforced Plastic Materials (AREA)

Abstract

The invention discloses a kind of phenolic resin glass fiber compound material colliery monitoring substation method for producing shell, comprising the following steps: 1) prepares material: 45% polyvinyl butyral phenol-formaldehyde resin modified, 54% alkali-free glass fibre, 0.5% release agent, 0.5% stable resin emulsifier;Release agent is zinc stearate, and stable resin emulsifier is hexadecyltrimethylammonium chloride;2) chopping, loose wire, drying;3) mixture is weighed according to the weight of colliery monitoring substation shell specification requirement, block is cold-pressed into pre-pressing die;4) housing mould is preheating to 150 DEG C ± 5 DEG C and kept, block filling housing mould is intracavitary;5) upper and lower mould of housing mould is molded, is pressurizeed;6) it is vented;7) continue to continue retention time T at 145 DEG C of temperature and the pressure of setting after exhaust;8) it demoulds.Colliery monitoring substation shell of the present invention substitutes existing metal shell, light, firm, meets the requirement of national standard GB3836.

Description

Phenolic resin glass fiber compound material colliery monitoring substation method for producing shell
Technical field
The present invention relates to a kind of colliery monitoring substations more particularly to a kind of phenolic resin glass fiber compound material coal mine to supervise Substation method for producing shell is controlled, mining equipment technical field is belonged to.
Background technique
Traditional colliery monitoring substation shell is made of metal material.Volume is big and heavy, and a people can not carry, it is necessary to It could transport and move by the vehicles, movement is extremely inconvenient in mine small space.If light, firm non-gold can be used Belong to the traditional metal shell of material substitution, then has a vast market application prospect.
Outstation enclosure interior is divided into two cavitys, and explosion-proof chamber and intrinsic safety chamber divide chamber to design, there is power supply change in explosion-proof chamber Depressor, plug-in power panel, battery pack.Intrinsic safety is intracavitary plug-in outstation mainboard.According to the requirement of national standard GB3836, coal Mine outstation shell must have the explosion-proof chamber that can bear 1.5MPa pressure, can bear the disengaging of 5000V AC power frequency cable, Flame proof grade is greater than 5000V, is resistant to 20000 hours aging thermal stability and examines.Therefore, if substituted using nonmetallic materials Traditional metal shell, then nonmetallic materials shell must satisfy the strict demand of national standard GB3836.
Summary of the invention
The purpose of the present invention is to provide a kind of production of phenolic resin glass fiber compound material colliery monitoring substation shell Method, using phenolic resin glass fiber compound material, process according to the invention, which is produced, to be met national standard GB3836 and wants The colliery monitoring substation shell asked, substitutes existing metal shell.
The purpose of the present invention is achieved by the following technical programs:
A kind of phenolic resin glass fiber compound material colliery monitoring substation method for producing shell, comprising the following steps:
1) prepare material: 45% polyvinyl butyral phenol-formaldehyde resin modified, 54% alkali-free glass fibre, 0.5% Release agent, 0.5% stable resin emulsifier;Release agent is zinc stearate, and stable resin emulsifier is cetyl front three Ammonium chloride;
2) alkali-free glass fibre cuts into the length of 5-8cm, and with polyvinyl butyral phenol-formaldehyde resin modified, demoulding Agent, stable resin emulsifier for mixing;Then the mixture mediated is fluffy, drying;
3) mixture is weighed according to the weight of colliery monitoring substation shell specification requirement, bulk is cold-pressed into pre-pressing die Object, small in size the 30% of the volume ratio colliery monitoring substation shell of block;
4) housing mould is preheating to 150 DEG C ± 5 DEG C and kept, block filling housing mould is intracavitary;
5) upper and lower mould of housing mould is molded, pressure can be increased to housing mould closure and pressurizeed to raw material, really It protects compressive load per unit area on forming direction and reaches 45 ± 5MPa/cm2
6) it is exhausted after continuing 60-100 seconds to raw material pressurization, deairing step are as follows: it unloads and is depressed into housing mould no pressure, then Pressurization, repetitive operation 3-5 times, gas releases in mold;
7) continue to continue retention time T, shell at 145 DEG C of temperature and the pressure of setting after the completion of deairing step Wall thickness is n millimeters, then retention time T=n minutes;
8) it demoulds.
The purpose of the present invention can also be further realized by following technical measures:
Aforementioned phenolic resin glass fiber compound material colliery monitoring substation method for producing shell, the setting of step 5) pressure By the following method: shell materials weight is less than or equal to 1 kilogram and is suppressed using 100 t hydraulic press, design of pressure 80T;Shell Materials weight is greater than 1 kilogram and is less than or equal to 3 kilograms is suppressed with 200 t hydraulic press, design of pressure 160T;Shell materials weight Amount is greater than 3 kilograms and is suppressed less than 10 kilograms with 315 t hydraulic press, design of pressure 260T.
Compared with prior art, the beneficial effects of the present invention are: the phenolic resin glass fibre of the method for the present invention production is multiple Condensation material colliery monitoring substation shell, explosion-proof chamber can bear 1.5MPa pressure, can bear the disengaging of 5000V AC power frequency cable, Flame proof grade is greater than 5000V, is resistant to 20000 hours aging thermal stability and examines.Phenolic resin glass fiber compound material coal Mine outstation shell substitutes existing metal shell, light, firm, meets the requirement of national standard GB3836.
Detailed description of the invention
Fig. 1 is outstation shell structure front schematic view of the invention;
Fig. 2 is outstation shell structure schematic rear view of the invention.
Specific embodiment
The present invention is further explained in the light of specific embodiments.
According to national standard GB3836 and the standard and requirement of colliery industry, phenolic resin glass fiber compound material coal mine prison Each technical parameter of control substation shell should meet following index:
Relative density: 1.75-1.85;
Shrinking percentage≤0.15%;
Martin heat resistance >=280 DEG C;
Mobility (La Xige): 80-200mm;
Impact strength >=35KJ/m2
Bending strength >=120MPa;
Compressive strength >=100MPa;
Tensile strength >=80MPa;
Surface resistivity >=1 × 1012
Volume resistivity >=1 × 1010Ω.cm;
Dielectric strength >=13KV/mm;
Moisture content volatile matter: 3-7.5%.
The structure of phenolic resin glass fiber compound material colliery monitoring substation shell is as shown in Figure 1, 2, production method It is as follows:
1) prepare material: 45% polyvinyl butyral phenol-formaldehyde resin modified, 54% alkali-free glass fibre, 0.5% Release agent, 0.5% stable resin emulsifier;Release agent is zinc stearate, and stable resin emulsifier is cetyl front three Ammonium chloride;
2) alkali-free glass fibre cuts into the length of 5-8cm, and with polyvinyl butyral phenol-formaldehyde resin modified, demoulding Agent, stable resin emulsifier for mixing;Then the mixture mediated is fluffy, drying;
3) mixture is weighed according to the weight of colliery monitoring substation shell specification requirement, bulk is cold-pressed into pre-pressing die Object can expand after being heated in subsequent handling due to mixture, the volume of block should than colliery monitoring substation shell at Product it is small in size, the present embodiment takes small in size the 30% of the volume ratio shell of block, in this way to avoid block-like mixture by Excessive overlap is thermally expanded and generated after being pressed, materials can be saved;
4) housing mould is preheating to 150 DEG C ± 5 DEG C and kept, block filling housing mould is intracavitary;
5) upper and lower mould of housing mould is molded, when molding is first used quickly, is changed at a slow speed when upper and lower mould contact, first Prevent mold from abrading slowly after fast;Pressure can be increased to housing mould closure to pressurize to raw material, in molding and pressure process, block Shape object is heated to be pressurized, and expansion is melted, and is extruded flowing filling to each position of mold;
Mold pressing force is it is ensured that compressive load per unit area reaches 45 ± 5MPa/cm on forming direction2;Specific embodiment party The engineering method of following simplicity can be used in method: shell materials weight is less than or equal to 1 kilogram, is suppressed using 100 t hydraulic press, hydraulic Machine design of pressure is 80T;Shell materials weight is greater than 1 kilogram and is less than or equal to 3 kilograms is suppressed with 200 t hydraulic press, hydraulic Machine design of pressure is 160T;Shell materials weight is greater than 3 kilograms and is suppressed less than 10 kilograms with 315 t hydraulic press, hydraulic press Design of pressure is 260T;
6) it is exhausted after continuing 60-100 seconds to raw material pressurization, deairing step are as follows: it unloads and is depressed into housing mould no pressure, then Pressurization, repetitive operation 3-5 times, gas releases in mold;Bleeding can shorten curing time, improve the physics of shell Mechanical performance avoids enclosure interior from occurring being layered and bubble;
7) solidify: continuing the retention time T at 145 DEG C of temperature and the pressure of setting after the completion of deairing step, make The curing reaction of resin reaches requirement, and shell wall thickness is n millimeter, then and retention time T=n minutes, such as: wall thickness is 25 millimeters, Pressure maintaining 25 minutes;
8) demoulded using knock-pin, after demoulding, by shell burr repair to the greatest extent, and with sand paper polish shell.
Phenolic resin glass fiber compound material colliery monitoring substation shell meets above-mentioned each technical parameter index, explosion-proof chamber 1.5MPa pressure can be born, the disengaging of 5000V AC power frequency cable can be born, flame proof grade is greater than 5000V, by actual measurement, energy It is resistant to 20000 hours aging thermal stability to examine, meets the requirement of national standard GB3836.
In addition to the implementation, the present invention can also have other embodiments, all to use equivalent substitution or equivalent transformation shape At technical solution, be all fallen within the protection domain of application claims.

Claims (2)

1. a kind of phenolic resin glass fiber compound material colliery monitoring substation method for producing shell, which is characterized in that including with Lower step:
1) prepare material: 45% polyvinyl butyral phenol-formaldehyde resin modified, 54% alkali-free glass fibre, 0.5% it is de- Mould agent, 0.5% stable resin emulsifier;Release agent is zinc stearate, and stable resin emulsifier is cetyl trimethyl chlorine Change ammonium;
2) alkali-free glass fibre cuts into the length of 5-8cm, and with polyvinyl butyral phenol-formaldehyde resin modified, release agent, Stable resin emulsifier for mixing;Then the mixture mediated is fluffy, drying;
3) mixture is weighed according to the weight of colliery monitoring substation shell specification requirement, block is cold-pressed into pre-pressing die, Small in size the 30% of the volume ratio colliery monitoring substation shell of block;
4) housing mould is preheating to 150 DEG C ± 5 DEG C and kept, block filling housing mould is intracavitary;
5) upper and lower mould of housing mould is molded, pressure can be increased to housing mould closure and pressurizeed to raw material, it is ensured that at Compressive load per unit area reaches 45 ± 5MPa/cm on type direction2
6) it is exhausted after continuing 60-100 seconds to raw material pressurization, deairing step are as follows: it unloads and is depressed into housing mould no pressure, then plus Pressure, repetitive operation 3-5 times release gas in mold;
7) continue to continue retention time T, shell wall thickness at 145 DEG C of temperature and the pressure of setting after the completion of deairing step It is n millimeters, then retention time T=n minutes;
8) it demoulds.
2. phenolic resin glass fiber compound material colliery monitoring substation method for producing shell as described in claim 1, special Sign is, the setting of the step 5) pressure by the following method: shell materials weight be less than or equal to 1 kilogram it is hydraulic using 100 tons Machine compacting, design of pressure 80T;Shell materials weight is greater than 1 kilogram and is less than or equal to 3 kilograms is suppressed with 200 t hydraulic press, Design of pressure is 160T;Shell materials weight is greater than 3 kilograms and is suppressed less than 10 kilograms with 315 t hydraulic press, and pressure value is set It is set to 260T.
CN201811590176.1A 2018-12-25 2018-12-25 Phenolic resin glass fiber compound material colliery monitoring substation method for producing shell Pending CN109702945A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201811590176.1A CN109702945A (en) 2018-12-25 2018-12-25 Phenolic resin glass fiber compound material colliery monitoring substation method for producing shell

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201811590176.1A CN109702945A (en) 2018-12-25 2018-12-25 Phenolic resin glass fiber compound material colliery monitoring substation method for producing shell

Publications (1)

Publication Number Publication Date
CN109702945A true CN109702945A (en) 2019-05-03

Family

ID=66257515

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201811590176.1A Pending CN109702945A (en) 2018-12-25 2018-12-25 Phenolic resin glass fiber compound material colliery monitoring substation method for producing shell

Country Status (1)

Country Link
CN (1) CN109702945A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113815177A (en) * 2021-08-16 2021-12-21 维达力实业(赤壁)有限公司 Compression molding method of composite board, composite board cover plate and preparation method thereof

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0061132A2 (en) * 1981-03-16 1982-09-29 Nissan Motor Co., Ltd. Reinforcing member and its use for reinforcing a panel of an automobile
EP0370991A2 (en) * 1988-11-23 1990-05-30 Recticel Compressing and shaping thermoformable mats using superheated steam
US20110239851A1 (en) * 2010-03-29 2011-10-06 Jeff Mason Ballistic structural insulated panel
CN104669645A (en) * 2007-10-03 2015-06-03 阿克塞尔集团有限公司 Method Of Forming Composite Products By Pressure, Related Products And Apparatus
CN105219017A (en) * 2015-10-14 2016-01-06 常州市宏发纵横新材料科技股份有限公司 The preparation method of heat-reactive phenolic resin matrix material
CN107325481A (en) * 2017-08-16 2017-11-07 常州信息职业技术学院 A kind of phenoplasts inspection shaft well lid and preparation method thereof

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0061132A2 (en) * 1981-03-16 1982-09-29 Nissan Motor Co., Ltd. Reinforcing member and its use for reinforcing a panel of an automobile
EP0370991A2 (en) * 1988-11-23 1990-05-30 Recticel Compressing and shaping thermoformable mats using superheated steam
CN104669645A (en) * 2007-10-03 2015-06-03 阿克塞尔集团有限公司 Method Of Forming Composite Products By Pressure, Related Products And Apparatus
US20110239851A1 (en) * 2010-03-29 2011-10-06 Jeff Mason Ballistic structural insulated panel
CN105219017A (en) * 2015-10-14 2016-01-06 常州市宏发纵横新材料科技股份有限公司 The preparation method of heat-reactive phenolic resin matrix material
CN107325481A (en) * 2017-08-16 2017-11-07 常州信息职业技术学院 A kind of phenoplasts inspection shaft well lid and preparation method thereof

Non-Patent Citations (4)

* Cited by examiner, † Cited by third party
Title
七六一一课题组: "FX-530塑料的研制", 《工程塑料应用》 *
冯胜: "《精细化工手册 (下册)》", 30 March 1995, 广东科技出版社 *
贾立军 朱虹: "《复合材料加工工艺》", 30 September 2007, 天津大学出版社 *
韩长日 宋小平: "《橡塑助剂生产工艺与技术》", 30 November 2015, 科学技术文献出版社 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113815177A (en) * 2021-08-16 2021-12-21 维达力实业(赤壁)有限公司 Compression molding method of composite board, composite board cover plate and preparation method thereof
CN113815177B (en) * 2021-08-16 2023-11-07 维达力科技股份有限公司 Compression molding method of composite board, composite board cover plate and preparation method of composite board cover plate

Similar Documents

Publication Publication Date Title
CN102294831B (en) Compression moulding method for prepreg
CN103160098B (en) Thermosetting plastic
CN102139546A (en) Glass fiber reinforced heat-conducting insulation silicon rubber composite material and preparation method thereof
CN109702945A (en) Phenolic resin glass fiber compound material colliery monitoring substation method for producing shell
CN103087379A (en) Room-temperature silane cross-linked polyolefin and its preparation method
CN110590390A (en) Carbon fiber graphite crucible for metallurgical casting furnace and preparation method thereof
JP6624685B2 (en) Method and equipment for producing extruded billets
US3092437A (en) Process for making carbon articles
EP3907204A1 (en) Heat insulation plate raw material composition, heat insulation plate, and production process for heat insulation plate
CN100526386C (en) preparation process of thermally conductive and electrically insulating silicone rubber composite material
JP2017501038A5 (en)
CN102034626A (en) Method for manufacturing flake-like arc contact finger
CN202388689U (en) Forming device for thermal expansion auxiliary prepregs of silicon sheets
CN104327461A (en) Method for producing high-density environment-friendly plates by utilizing waste circuit board powdery and granular material
CN104250067A (en) Method for preparation of machinable mica glass ceramic insulating material from waste glass and phlogopite
CN102371616A (en) Ceramic body dry-pressing and forming process
CN105269836B (en) A kind of preparation method of SMC auto-parts product
CN103438128A (en) Method for reproducing brake blocks by utilizing waste drum-type brake blocks
CN106920639A (en) Cast-type mutual inductor is pressed in a kind of environment-friendly type
CN211000307U (en) Sandwich insulation operating rod
CN204303522U (en) A kind of U-shaped insulation pressing
CN218256995U (en) Add hot type forming device
CN112250336B (en) Waste rock wool regeneration slag powder and preparation method thereof
CN102962938A (en) Method for manufacturing composite thermal insulation board by utilizing rigid waste polyurethane foam and straws
CN102555034A (en) Rapid molding method of light aggregate and equipment thereof

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication

Application publication date: 20190503

RJ01 Rejection of invention patent application after publication