CN109694676A - A kind of reflector plate protection glue, adhesive tape and preparation method thereof - Google Patents

A kind of reflector plate protection glue, adhesive tape and preparation method thereof Download PDF

Info

Publication number
CN109694676A
CN109694676A CN201811625568.7A CN201811625568A CN109694676A CN 109694676 A CN109694676 A CN 109694676A CN 201811625568 A CN201811625568 A CN 201811625568A CN 109694676 A CN109694676 A CN 109694676A
Authority
CN
China
Prior art keywords
weight
parts
reflector plate
glue
minutes
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201811625568.7A
Other languages
Chinese (zh)
Inventor
林子清
林克波
林克兴
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Fujian Youyi Adhesive Tape Group Co Ltd
Original Assignee
Fujian Youyi Adhesive Tape Group Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Fujian Youyi Adhesive Tape Group Co Ltd filed Critical Fujian Youyi Adhesive Tape Group Co Ltd
Priority to CN201811625568.7A priority Critical patent/CN109694676A/en
Publication of CN109694676A publication Critical patent/CN109694676A/en
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J133/00Adhesives based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Adhesives based on derivatives of such polymers
    • C09J133/04Homopolymers or copolymers of esters
    • C09J133/06Homopolymers or copolymers of esters of esters containing only carbon, hydrogen and oxygen, the oxygen atom being present only as part of the carboxyl radical
    • C09J133/08Homopolymers or copolymers of acrylic acid esters
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F220/00Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride ester, amide, imide or nitrile thereof
    • C08F220/02Monocarboxylic acids having less than ten carbon atoms; Derivatives thereof
    • C08F220/10Esters
    • C08F220/12Esters of monohydric alcohols or phenols
    • C08F220/16Esters of monohydric alcohols or phenols of phenols or of alcohols containing two or more carbon atoms
    • C08F220/18Esters of monohydric alcohols or phenols of phenols or of alcohols containing two or more carbon atoms with acrylic or methacrylic acids
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J7/00Adhesives in the form of films or foils
    • C09J7/20Adhesives in the form of films or foils characterised by their carriers
    • C09J7/22Plastics; Metallised plastics
    • C09J7/25Plastics; Metallised plastics based on macromolecular compounds obtained otherwise than by reactions involving only carbon-to-carbon unsaturated bonds
    • C09J7/255Polyesters
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F220/00Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride ester, amide, imide or nitrile thereof
    • C08F220/02Monocarboxylic acids having less than ten carbon atoms; Derivatives thereof
    • C08F220/10Esters
    • C08F220/12Esters of monohydric alcohols or phenols
    • C08F220/16Esters of monohydric alcohols or phenols of phenols or of alcohols containing two or more carbon atoms
    • C08F220/18Esters of monohydric alcohols or phenols of phenols or of alcohols containing two or more carbon atoms with acrylic or methacrylic acids
    • C08F220/1808C8-(meth)acrylate, e.g. isooctyl (meth)acrylate or 2-ethylhexyl (meth)acrylate
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J2203/00Applications of adhesives in processes or use of adhesives in the form of films or foils
    • C09J2203/318Applications of adhesives in processes or use of adhesives in the form of films or foils for the production of liquid crystal displays
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J2301/00Additional features of adhesives in the form of films or foils
    • C09J2301/10Additional features of adhesives in the form of films or foils characterized by the structural features of the adhesive tape or sheet
    • C09J2301/12Additional features of adhesives in the form of films or foils characterized by the structural features of the adhesive tape or sheet by the arrangement of layers
    • C09J2301/122Additional features of adhesives in the form of films or foils characterized by the structural features of the adhesive tape or sheet by the arrangement of layers the adhesive layer being present only on one side of the carrier, e.g. single-sided adhesive tape
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J2467/00Presence of polyester
    • C09J2467/006Presence of polyester in the substrate

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Adhesives Or Adhesive Processes (AREA)

Abstract

The present invention relates to a kind of reflector plate protection glue, adhesive tape and preparation method thereof; belong to adhesive tape processing technique field; a kind of reflector plate protection glue is formulated by following components according to following weight proportion: acrylic acid 2-5 parts by weight; Isooctyl acrylate monomer 17-20 parts by weight; butyl acrylate 7-10 parts by weight; vinyl acetate 5-8 parts by weight, ethyl acetate 57-60 parts by weight, BPO0.2-0.3 parts by weight.The reflector plate protects glue initial cohesiveness with higher and retention property, while having preferable stripping performance.

Description

A kind of reflector plate protection glue, adhesive tape and preparation method thereof
Technical field
The invention belongs to adhesive tape processing technique fields, and in particular to a kind of reflector plate protection glue, adhesive tape and its preparation side Method.
Background technique
Reflector plate can be made up of a kind of the slide that its back side generates reflection, slide have one partly Or the front being all made of multiple composite surfaces, each composite surface are from only to the inclined cylindrical surface in a direction and Xiang Fanfang It is formed to inclined curved surface or plane, above-mentioned composite surface continuously or is therebetween inserted with plane, and its structure is Cylindrical surface accounts for most of area of composite surface, and above-mentioned slide also has the back being made of multiple adjacent right-angle prisms Face.
In order to improve the utilization efficiency of light commonly using light reflecting material.For example, being arranged light reflecting material in liquid crystal display The most back side of curtain, so that the light that the light sources such as LED or cold-cathode fluorescence lamp (CCFL) issue is reflected into front with preferable efficiency. In addition, also light reflecting material is mounted on fluorescent lamp or LED type lighting device to good efficiency reflected light.
In the production process of LCD screen, in the transportational process especially before reflector plate assembling, reflector plate in order to prevent It is destroyed, usually uses reflector plate protective glue band, cut into small strip, glued on the protection sheet on one side, another side is sticked to On reflector plate;Reflector plate protective glue band is torn when assembling;Realize that the transportational process of the reflector plate of mould group below LCD screen is protected Shield.
Existing reflector plate protective glue band or not easy to attach, easily falls;When tearing, the more difficult removing from reflector plate It falls off, and destruction can be generated to reflector plate, there are residue glues for meeting.
Summary of the invention
In order to solve the above technical problems, the present invention provides a kind of reflector plate protection glue, initial cohesiveness with higher And retention property, while there is preferable stripping performance.
Another object of the present invention is to provide a kind of preparation method of reflector plate protective glue band.
The technical scheme is that:
Scheme one:
A kind of reflector plate protection glue, is formulated by following components according to following weight proportion:
Scheme two:
A kind of preparation method of reflector plate protection glue, comprising the following steps:
Step 1: by the acrylic acid of 2-5 parts by weight, the Isooctyl acrylate monomer of 17-20 parts by weight, 7-10 parts by weight propylene Acid butyl ester, 5-8 parts by weight vinyl acetate mixed with the ethyl acetate of 49-52 parts by weight;
Step 2: opening blender, and revolving speed is controlled in 25 turns/min, is warming up to 80 DEG C, starts to titrate 0.2-0.3 parts by weight The titrating solution that BPO and the ethyl acetate of 8 parts by weight are formulated titrates 20 minutes, and temperature rises to 85-86 DEG C, stops titration;
Step 3: starting to cool down, and temperature continues to titrate when being down to 80 DEG C, and the used time 100 minutes, heat preservation 4 hours after having titrated It crosses cooling and unloads glue;Obtain finished product reflector plate protection glue.
Scheme three:
A kind of preparation method of reflector plate protective glue band, the reflector plate protective glue prepared using preparation method described in scheme two Water, the preparation method comprises the following steps:
Step 1: it comes unglued: the modified terpene phenol resin of 5 parts by weight and 9 resin of carbon of 5 parts by weight is put into 100 parts by weight Reflector plate protection glue in stirring to dissolve, add 0.5-0.9 parts by weight polyurethane curing agent stir 30 minutes;
Step 2: coating: head release paper gluing, tail are made into single side with 12uPET is compound, and head uses release paper again Gluing, tail is compound with ready-made single side, pulls out one layer of release paper, is made into the two-sided of 50u, temperature setting: 60,80,90,95, 100,105,100,90;Interval time 3 minutes;Speed: 13-15 ms/min;Obtain reflector plate protective glue band finished product.
Compared with prior art, the beneficial effects of the present invention are:
1, the present invention can be improved the initial cohesiveness and retention property of glue, control stripping performance.
2, the present invention can be such that adhesive tape is attached on reflector plate, can not only be easier to be bonded, be not easy to fall, be easy when removing from It falls off on reflector plate, and destruction will not be generated to reflector plate, it will not residue glue.
3, reflector plate protective glue band of the invention will not occur tacky film and be partially stripped when adhesive layer is removed from adherend The case where, while can get stable physical property.
Specific embodiment
The following examples are used to illustrate the present invention, but are not intended to limit the scope of the present invention..
Embodiment 1:
A kind of preparation method of reflector plate protective glue band, comprising the following steps:
Step 1: by the acrylic acid of 2 parts by weight, the Isooctyl acrylate monomer of 17 parts by weight, the butyl acrylate of 7 parts by weight, 5 The vinyl acetate of parts by weight is mixed with the ethyl acetate of 49 parts by weight;
Step 2: opening blender, and revolving speed is controlled in 25 turns/min, is warming up to 80 DEG C, starts to titrate 0.2 parts by weight BPO The titrating solution being formulated with the ethyl acetate of 8 parts by weight titrates 20 minutes, and temperature rises to 85 DEG C, stops titration;
Step 3: starting to cool down, and temperature continues to titrate when being down to 80 DEG C, and the used time 100 minutes, heat preservation 4 hours after having titrated It crosses cooling and unloads glue;Obtain finished product reflector plate protection glue;
Step 4: it comes unglued: the modified terpene phenol resin of 5 parts by weight and 9 resin of carbon of 5 parts by weight is put into 100 parts by weight Reflector plate protection glue in stirring to dissolve, add 0.5 parts by weight polyurethane curing agent stir 30 minutes;
Step 5: coating: head release paper gluing, tail are made into single side with 12uPET is compound, and head uses release paper again Gluing, tail is compound with ready-made single side, pulls out one layer of release paper, is made into the two-sided of 50u, temperature setting: 60,80,90,95, 100,105,100,90;Interval time 3 minutes;Speed: 13 ms/min;Obtain reflector plate protective glue band finished product.
Embodiment 2:
A kind of preparation method of reflector plate protective glue band, comprising the following steps:
Step 1: by the acrylic acid of 5 parts by weight, the Isooctyl acrylate monomer of 20 parts by weight, 10 parts by weight butyl acrylate, The vinyl acetate of 8 parts by weight is mixed with the ethyl acetate of 52 parts by weight;
Step 2: opening blender, and revolving speed is controlled in 25 turns/min, is warming up to 80 DEG C, starts to titrate 0.3 parts by weight BPO The titrating solution being formulated with the ethyl acetate of 8 parts by weight titrates 20 minutes, and temperature rises to 86 DEG C, stops titration;
Step 3: starting to cool down, and temperature continues to titrate when being down to 80 DEG C, and the used time 100 minutes, heat preservation 4 hours after having titrated It crosses cooling and unloads glue;Obtain finished product reflector plate protection glue;
Step 4: it comes unglued: the modified terpene phenol resin of 5 parts by weight and 9 resin of carbon of 5 parts by weight is put into 100 parts by weight Reflector plate protection glue in stirring to dissolve, add 0.6 parts by weight polyurethane curing agent stir 30 minutes;
Step 5: coating: head release paper gluing, tail are made into single side with 12uPET is compound, and head uses release paper again Gluing, tail is compound with ready-made single side, pulls out one layer of release paper, is made into the two-sided of 50u, temperature setting: 60,80,90,95, 100,105,100,90;Interval time 3 minutes;Speed: 15 ms/min;Obtain reflector plate protective glue band finished product.
Embodiment 3:
A kind of preparation method of reflector plate protective glue band, comprising the following steps:
Step 1: by the acrylic acid of 3.5 parts by weight, the Isooctyl acrylate monomer of 18.5 parts by weight, 8.5 parts by weight acrylic acid Butyl ester, 6.5 parts by weight vinyl acetate mixed with the ethyl acetate of 50.5 parts by weight;
Step 2: opening blender, and revolving speed is controlled in 25 turns/min, is warming up to 80 DEG C, starts to titrate 0.25 parts by weight BPO The titrating solution being formulated with the ethyl acetate of 8 parts by weight titrates 20 minutes, and temperature rises to 85.5 DEG C, stops titration;
Step 3: starting to cool down, and temperature continues to titrate when being down to 80 DEG C, and the used time 100 minutes, heat preservation 4 hours after having titrated It crosses cooling and unloads glue;Obtain finished product reflector plate protection glue;
Step 4: it comes unglued: the modified terpene phenol resin of 5 parts by weight and 9 resin of carbon of 5 parts by weight is put into 100 parts by weight Reflector plate protection glue in stirring to dissolve, add 0.7 parts by weight polyurethane curing agent stir 30 minutes;
Step 5: coating: head release paper gluing, tail are made into single side with 12uPET is compound, and head uses release paper again Gluing, tail is compound with ready-made single side, pulls out one layer of release paper, is made into the two-sided of 50u, temperature setting: 60,80,90,95, 100,105,100,90;Interval time 3 minutes;Speed: 14 ms/min;Obtain reflector plate protective glue band finished product.
Embodiment 4:
A kind of preparation method of reflector plate protective glue band, comprising the following steps:
Step 1: by the acrylic acid of 2 parts by weight, the Isooctyl acrylate monomer of 20 parts by weight, the butyl acrylate of 7 parts by weight, 8 The vinyl acetate of parts by weight is mixed with the ethyl acetate of 49 parts by weight;
Step 2: opening blender, and revolving speed is controlled in 25 turns/min, is warming up to 80 DEG C, starts to titrate 0.3 parts by weight BPO The titrating solution being formulated with the ethyl acetate of 8 parts by weight titrates 20 minutes, and temperature rises to 85 DEG C, stops titration;
Step 3: starting to cool down, and temperature continues to titrate when being down to 80 DEG C, and the used time 100 minutes, heat preservation 4 hours after having titrated It crosses cooling and unloads glue;Obtain finished product reflector plate protection glue;
Step 4: it comes unglued: the modified terpene phenol resin of 5 parts by weight and 9 resin of carbon of 5 parts by weight is put into 100 parts by weight Reflector plate protection glue in stirring to dissolve, add 0.8 parts by weight polyurethane curing agent stir 30 minutes;
Step 5: coating: head release paper gluing, tail are made into single side with 12uPET is compound, and head uses release paper again Gluing, tail is compound with ready-made single side, pulls out one layer of release paper, is made into the two-sided of 50u, temperature setting: 60,80,90,95, 100,105,100,90;Interval time 3 minutes;Speed: 15 ms/min;Obtain reflector plate protective glue band finished product.
Embodiment 5:
A kind of preparation method of reflector plate protective glue band, comprising the following steps:
Step 1: by the acrylic acid of 5 parts by weight, the Isooctyl acrylate monomer of 17 parts by weight, 10 parts by weight butyl acrylate, The vinyl acetate of 5 parts by weight is mixed with the ethyl acetate of 52 parts by weight;
Step 2: opening blender, and revolving speed is controlled in 25 turns/min, is warming up to 80 DEG C, starts to titrate 0.2 parts by weight BPO The titrating solution being formulated with the ethyl acetate of 8 parts by weight titrates 20 minutes, and temperature rises to 86 DEG C, stops titration;
Step 3: starting to cool down, and temperature continues to titrate when being down to 80 DEG C, and the used time 100 minutes, heat preservation 4 hours after having titrated It crosses cooling and unloads glue;Obtain finished product reflector plate protection glue;
Step 4: it comes unglued: the modified terpene phenol resin of 5 parts by weight and 9 resin of carbon of 5 parts by weight is put into 100 parts by weight Reflector plate protection glue in stirring to dissolve, add 0.9 parts by weight polyurethane curing agent stir 30 minutes;
Step 5: coating: head release paper gluing, tail are made into single side with 12uPET is compound, and head uses release paper again Gluing, tail is compound with ready-made single side, pulls out one layer of release paper, is made into the two-sided of 50u, temperature setting: 60,80,90,95, 100,105,100,90;Interval time 3 minutes;Speed: 13 ms/min;Obtain reflector plate protective glue band finished product.
Experimental data
The present invention surveys reflector plate protective glue band finished product prepared in specific embodiment according to following experimental method Examination:
1, peeling force is measured
The release film of tacky film on reflector plate is removed, 1 inch × 1 inch of tablet is then cut into.Use matter Amount is that the roller reciprocating rolling of 2Kg is primary, and tacky film is attached to one block of non-alkali glass plate, with autoclave at 50 DEG C and It handles under conditions of 0.5MPa 30 minutes, places two hours at room temperature.Then, using Instron (Instron) measuring device With 180 ° of peeling forces of tachometric survey of 300mm/min.
2, initial bonding strength and retention time are measured
Initial bonding strength performance test methods: the one side that test agent double faced adhesive tape is not tested with 25 μm of PET films it is laminating after, cut At 20mm × 150mm, one face stripping film is torn when testing one side, in PC, GLASS, containing being bonded on APCF layers of polaroid, then is used The pressing device of 2Kg pressurizes three and is placed in 23 DEG C × 65%RH environment back and forth, after keeping r, 48hr, 72hr for 24 hours, is placed in The test of 180 ° of pulling plates is carried out with 300mm/min in fixture, records data, a kind of sample will be measured in parallel two samples, be averaged Value, and record the retention time.
Reflector plate protective glue band of the invention is viscous relative to 10 average surface roughness Rz coated steel plate for being 8.0 μm Relay is 0.05N/20mm or more.Here, " coated steel plate that 10 average surface roughness Rz are 8.0 μm " refers to defined Adherend in the evaluation of the bonding force of reflector plate protective glue band of the invention as benchmark." 10 average surface roughness Rz " be as indicate surface roughness index and well known index.
The experimental data of reflector plate protection glue, tape performance in specific embodiments of the present invention
Initial bonding strength (#) Peel strength (N/25mm) Retention time (h)
Embodiment 1 13/14 8.5/8.9 24/ ﹥ 24 of ﹥
Embodiment 2 12/13 8.6/8.7 24/ ﹥ 24 of ﹥
Embodiment 3 13/12 8.0/8.3 24/ ﹥ 24 of ﹥
Embodiment 4 12/12 8.1/7.8 24/ ﹥ 24 of ﹥
Embodiment 5 12/12 7.5/7.6 24/ ﹥ 24 of ﹥
Protect glue, adhesive tape with higher from can be seen that reflector plate in specific embodiments of the present invention in above data Initial cohesiveness and retention property, while there is preferable stripping performance.

Claims (3)

1. a kind of reflector plate protects glue, it is characterised in that:
It is formulated by following components according to following weight proportion:
2. the preparation method of reflector plate protection glue according to claim 1, it is characterised in that: the following steps are included:
Step 1: by the acrylic acid of 2-5 parts by weight, the Isooctyl acrylate monomer of 17-20 parts by weight, 7-10 parts by weight acrylic acid fourth Ester, 5-8 parts by weight vinyl acetate mixed with the ethyl acetate of 49-52 parts by weight;
Step 2: opening blender, and revolving speed is controlled in 25 turns/min, is warming up to 80 DEG C, starts to titrate 0.2-0.3 parts by weight BPO The titrating solution being formulated with the ethyl acetate of 8 parts by weight titrates 20 minutes, and temperature rises to 85-86 DEG C, stops titration;
Step 3: starting to cool down, and temperature continues to titrate when being down to 80 DEG C, the used time 100 minutes, kept the temperature 4 hours i.e. after having titrated Glue is unloaded in cooling;Obtain finished product reflector plate protection glue.
3. a kind of preparation method of reflector plate protective glue band, it is characterised in that: protected using the reflector plate of claim 1 vegetation Glue, the preparation method comprises the following steps:
Step 1: it comes unglued: the modified terpene phenol resin of 5 parts by weight and 9 resin of carbon of 5 parts by weight is put into the anti-of 100 parts by weight Penetrating stirring in piece protection glue, to dissolving, the polyurethane curing agent for adding 0.5-0.9 parts by weight stirs 30 minutes;
Step 2: coating: head release paper gluing, tail are made into single side with 12uPET is compound, and head uses release paper gluing again, Tail is compound with ready-made single side, pulls out one layer of release paper, is made into the two-sided of 50u, temperature setting: 60,80,90,95,100, 105,100,90;Interval time 3 minutes;Speed: 13-15 ms/min;Obtain reflector plate protective glue band finished product.
CN201811625568.7A 2018-12-28 2018-12-28 A kind of reflector plate protection glue, adhesive tape and preparation method thereof Pending CN109694676A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201811625568.7A CN109694676A (en) 2018-12-28 2018-12-28 A kind of reflector plate protection glue, adhesive tape and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201811625568.7A CN109694676A (en) 2018-12-28 2018-12-28 A kind of reflector plate protection glue, adhesive tape and preparation method thereof

Publications (1)

Publication Number Publication Date
CN109694676A true CN109694676A (en) 2019-04-30

Family

ID=66232338

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201811625568.7A Pending CN109694676A (en) 2018-12-28 2018-12-28 A kind of reflector plate protection glue, adhesive tape and preparation method thereof

Country Status (1)

Country Link
CN (1) CN109694676A (en)

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102250562A (en) * 2011-05-31 2011-11-23 东莞市苏粤电子包装材料有限公司 Termination adhesive tape and manufacture method thereof
WO2013101693A1 (en) * 2011-12-27 2013-07-04 3M Innovative Properties Company Adhesive tape composition and adhesive tape prepared from same
CN104152077A (en) * 2014-08-13 2014-11-19 隆昌羽玺新材料科技有限公司 Ultra-thin polyester double-sided adhesive tape, glue thereof, and preparation method thereof
CN108165196A (en) * 2017-12-29 2018-06-15 浙江仁丰科技有限公司 A kind of formula and processing technology of PI membrane adhesive tapes

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102250562A (en) * 2011-05-31 2011-11-23 东莞市苏粤电子包装材料有限公司 Termination adhesive tape and manufacture method thereof
WO2013101693A1 (en) * 2011-12-27 2013-07-04 3M Innovative Properties Company Adhesive tape composition and adhesive tape prepared from same
CN104152077A (en) * 2014-08-13 2014-11-19 隆昌羽玺新材料科技有限公司 Ultra-thin polyester double-sided adhesive tape, glue thereof, and preparation method thereof
CN108165196A (en) * 2017-12-29 2018-06-15 浙江仁丰科技有限公司 A kind of formula and processing technology of PI membrane adhesive tapes

Similar Documents

Publication Publication Date Title
TWI494394B (en) Adhesive layer and adhesive film
US7862898B2 (en) Adhesive composition and articles made therefrom
TWI568814B (en) Adhesive layer and adhesive film
TWI512067B (en) Adhesive layer and adhesive film
KR20120137288A (en) Carrier material for thin layer substrate
KR20060093663A (en) Pressure-sensitive adhesive composition, pressure-sensitive adhesive sheets and double-sided pressure-sensitive adhesive tape
JP4517696B2 (en) Removable double-sided adhesive tape
JP2012193264A (en) Adhesive sheet, and peeling method of the same
EP1593725A1 (en) Ultraviolet-crosslinkable transparent hot melt pressure -sensitive adhesive, transparent pressure-sensitive adhesive sheet and laminates
JP6645045B2 (en) Adhesive tape, protective member and electronic equipment
TW201425509A (en) Pressure-sensitive adhesive composition, pressure-sensitive adhesive sheet, and optical layered sheet
JP2002047463A (en) Pressure-sensitive adhesive sheets and method for fixing functional film
CN109694676A (en) A kind of reflector plate protection glue, adhesive tape and preparation method thereof
JP2001290138A (en) Film substrate assembly for liquid crystal display device
CN101831260A (en) Polaroid adhesive and polaroid using same
KR910006723B1 (en) Pressure sensitive adhesive tape
CN109666428A (en) A kind of mobile phone screen shading glue, adhesive tape and preparation method thereof
EP1928971A1 (en) Adhesive composition and articles made therefrom
CN116333653A (en) OCA optical cement for bonding vehicle-mounted display screen and preparation method thereof
JPWO2016009845A1 (en) Double-sided adhesive tape, protective member and electronic device
CN116285760A (en) Touch screen double-sided optical tape and preparation method thereof
CN113698882A (en) Double-sided shading adhesive tape and preparation method and application thereof
JPH0798926B2 (en) Acrylic adhesive composition
JP2005200498A (en) Removable double-coated adhesive tape
JPH04254803A (en) Adhesion type polarizing plate or adhesion type phase difference plate

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20190430