CN109650971A - A kind of foliar fertilizer and preparation method thereof promoting the secretion of tobacco oil - Google Patents

A kind of foliar fertilizer and preparation method thereof promoting the secretion of tobacco oil Download PDF

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Publication number
CN109650971A
CN109650971A CN201811579243.XA CN201811579243A CN109650971A CN 109650971 A CN109650971 A CN 109650971A CN 201811579243 A CN201811579243 A CN 201811579243A CN 109650971 A CN109650971 A CN 109650971A
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China
Prior art keywords
parts
foliar fertilizer
fertilizer
organic fertilizer
tobacco
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CN201811579243.XA
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CN109650971B (en
Inventor
芶剑渝
孟源
廖恒
刘京
韩小斌
彭玉龙
赵建
刘明宏
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GUIZHOU TOBACCO Co ZUNYI BRANCH
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GUIZHOU TOBACCO Co ZUNYI BRANCH
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F3/00Fertilisers from human or animal excrements, e.g. manure
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05CNITROGENOUS FERTILISERS
    • C05C3/00Fertilisers containing other salts of ammonia or ammonia itself, e.g. gas liquor
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/40Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Fertilizers (AREA)

Abstract

The invention belongs to foliar fertilizer technical fields, and in particular to a kind of foliar fertilizer and preparation method thereof for promoting the secretion of tobacco oil.A kind of foliar fertilizer promoting the secretion of tobacco oil, including following raw material: 10~40 parts of organic fertilizer of fermentation;1~10 part of inorganic acid;3~10 parts of alkali containing potassium element;2~8 parts of ammonium hydroxide;150~270 parts of water.The effective components factor such as amino acid needed for foliar fertilizer of the invention can supplement tobacco, phytic acid and phosphatide, can effectively improve cured tobacco leaf oil content, further increase Aroma Quality of Flue-cured, and miscellaneous gas is lighter, be conducive to the subsequent processing of flue-cured tobacco, production.

Description

A kind of foliar fertilizer and preparation method thereof promoting the secretion of tobacco oil
Technical field
The invention belongs to foliar fertilizer technical fields, and in particular to it is a kind of promote tobacco oil secretion foliar fertilizer and its preparation Method.
Background technique
Nicotiana eggplant mesh, Solanaceae herbaceous plant originate in South America.It is widely distributed as a kind of important industrial crops In the South and the North each province, China, tobacco leaf oil is also referred to as leaf point or fat, is often referred to the soft semiliquid contained in tobacco leaf cells or liquid Body substance, oil content height directly reflect the quality of quality of tobacco, are the important indicators for measuring quality of tobacco, and tobacco leaf oil is come Derived from Tobacco Glandular Trichome secretion.Tobacco Glandular Trichome is the important tissue of tobacco leaf surface, is the main place for synthesizing tobacco aroma object, right The aroma quality of tobacco leaf has significant contribution.
Foliar fertilizer is very universal, as the supplement of exoroot nutrition, is quickly absorbed by plant leaf blade, is supplement plant battalion It supports, promotes plant growth, improve the effective way of yield.During tobacco growing, plant phytic acid, phosphatide and related inorganic are supported The synthesis and accumulation for dividing the absorption of substance to be all conducive to tobacco leaf oil promote tobacco leaf surface glandular hairs to secrete related oil substance, cigarette Leaf oil point directly affects the quality and industrial plasticity of flue-cured tobacco, therefore, develops a kind of promotion tobacco oil secretion, improves roasting The foliar fertilizer of tobacco quality quite it is necessary to.
Summary of the invention
In order to solve the above-mentioned technical problem, the first aspect of the invention provides a kind of leaf of promotion tobacco oil secretion Leaven, including following raw material: 10~40 parts of organic fertilizer of fermentation;1~10 part of inorganic acid;3~10 parts of alkali containing potassium element; 2~8 parts of ammonium hydroxide;150~270 parts of water.
As a kind of perferred technical scheme, the foliar fertilizer includes following raw material: fermentation organic fertilizer 17~30 Part;5~7.5 parts of inorganic acid;5~6.5 parts of alkali containing potassium element;3~4..5 parts of ammonium hydroxide;180~250 parts of water.
As a kind of perferred technical scheme, the fermentation organic fertilizer be selected from rape cake, chicken manure, sheep dung, cow dung, pig manure, At least one of soya-bean cake, cottonseed cake.
As a kind of perferred technical scheme, the fermentation organic fertilizer is rape cake and/or chicken manure.
As a kind of perferred technical scheme, the fermentation organic fertilizer is made of rape cake and chicken manure.
As a kind of perferred technical scheme, the inorganic acid is sulfuric acid and/or nitric acid.
As a kind of perferred technical scheme, the inorganic acid is sulfuric acid.
As a kind of perferred technical scheme, the alkali containing potassium element is potassium hydroxide and/or potassium carbonate.
The second aspect of the present invention provides the preparation method of the foliar fertilizer, comprising the following steps:
1) ammonium hydroxide is uniformly sprayed on fermentation organic fertilizer, seals 3~4 hours, places into autoclave sterilization pot, Under certain temperature, 45~60min is handled;
2) by autoclave sterilization, treated that product is placed in bucket, and inorganic acid is added, and water sufficiently stirs evenly, and covers bung, Stirring in every 3~5 days is primary, places 15~25 days;
3) step 2) product is shifted with filtered through gauze, be added the alkali containing potassium element, adjust pH to 7 to get.
As a kind of perferred technical scheme, temperature is 120~130 DEG C in the step 1).
The utility model has the advantages that foliar fertilizer of the invention can supplement tobacco needed for amino acid, phytic acid and phosphatide etc. effectively at Molecular group can effectively improve cured tobacco leaf oil content, further increase Aroma Quality of Flue-cured, and miscellaneous gas is lighter, is conducive to bake The subsequent processing of cigarette, production.
Specific embodiment
For the purpose of following detailed description, it should be understood that the present invention can be used various substitutions variation and step it is suitable Sequence, unless specifically stated on the contrary.In addition, being indicated in the case where in addition in any operational instances or otherwise pointing out Such as all numbers of the amount of ingredient used in description and claims should be understood in all cases by term " about " it modifies.Therefore, unless indicated to the contrary, the numerical parameter otherwise illustrated in the following description and appended dependent claims is root The approximation changed according to the expected performance of the invention to be obtained.It is at least not intended to for the applicable of doctrine of equivalents being limited in In the scope of the claims, each numerical parameter should at least be given up according to the number of the effective digital of report and by the way that application is common Enter technology to explain.
Although illustrating that broad range of numberical range and parameter of the invention are approximations, listed in specific example Numerical value is reported as accurately as possible.However, any numerical value inherently includes the standard deviation by finding in its each self-test measurement The certain errors necessarily led to.
When a numberical range disclosed herein, above range is considered as continuously, and the minimum value including the range and most Big value and each value between this minimum value and maximum value.Further, when range refers to integer, including the model Each integer between minimum value and maximum value enclosed.In addition, when providing multiple range Expressive Features or characteristic, Ke Yihe And the range.In other words, unless otherwise specified, otherwise all ranges disclosed herein are understood to include and are wherein included into Any and all subrange.For example, should be regarded as including between minimum value 1 and maximum value 10 from the specified range of " 1 to 10 " Any and all subrange.The Exemplary range of range 1 to 10 include but is not limited to 1 to 6.1,3.5 to 7.8,5.5 to 10 etc..
To solve the above-mentioned problems, including following heavy the present invention provides a kind of foliar fertilizer of promotion tobacco oil secretion Measure part raw material: 10~40 parts of organic fertilizer of fermentation;1~10 part of inorganic acid;3~10 parts of alkali containing potassium element;2~8 parts of ammonium hydroxide;Water 150~270 parts.
As a preferred embodiment, the foliar fertilizer includes following raw material: fermentation organic fertilizer 17~30 Part;5~7.5 parts of inorganic acid;5~6.5 parts of alkali containing potassium element;3~4..5 parts of ammonium hydroxide;180~250 parts of water.
Preferably, the foliar fertilizer includes following raw material: 24 parts of organic fertilizer of fermentation;5 parts of inorganic acid;Containing potassium element 6 parts of alkali;4 parts of ammonium hydroxide;180 parts of water.
As a preferred embodiment, the fermentation organic fertilizer be selected from rape cake, chicken manure, sheep dung, cow dung, pig manure, At least one of soya-bean cake, cottonseed cake.
The rape cake is the by-product after rapeseed oil, for supplementing amino acid, phytic acid and phosphatide;The soya-bean cake For the by-product after soybean extract oil, for supplementing amino acid;The cottonseed cake is the by-product after cottonseed oil expression, for supplementing ammonia Base acid;The chicken manure, sheep dung, cow dung, pig manure supplement organic materials.
As a preferred embodiment, the fermentation organic fertilizer is rape cake and/or chicken manure.
As a preferred embodiment, the fermentation organic fertilizer is made of rape cake and chicken manure.
The fermentation organic fertilizer the preparation method comprises the following steps: rape cake is mixed well with chicken manure, is accumulated, spontaneous fermentation 15-20 It is to get fermentation organic fertilizer.
In the application, by the way that the fermentation organic fertilizer being made of rape cake and chicken manure is added in foliar fertilizer, can effectively it mention High tobacco oil content.The possible reason is when rape cake and chicken manure exist simultaneously, the effective component factor each other can be promoted It is precipitated, the effective component of precipitation is absorbed by tobacco, to improve the secretion of tobacco oil.
Preferably, it is described fermentation organic fertilizer in rape cake and chicken manure weight part ratio are as follows: (3~6): 1.
It is highly preferred that it is described fermentation organic fertilizer in rape cake and chicken manure weight part ratio are as follows: 5:1.
As a preferred embodiment, the inorganic acid is sulfuric acid and/or nitric acid.
As a preferred embodiment, the inorganic acid is sulfuric acid.
Preferably, the inorganic acid is the concentrated sulfuric acid.
The concentrated sulfuric acid have strong oxidizer, corrosivity, can decompose, extract ferment organic fertilizer in effective component because Son.
As a preferred embodiment, the alkali containing potassium element is potassium hydroxide and/or potassium carbonate.
As a preferred embodiment, the alkali containing potassium element is potassium hydroxide.
The alkali containing potassium element can not only neutralize extra acid, and potassium element, tobacco can also be provided for tobacco growing The crop of nitrogen is needed as happiness potassium, the supplement of potassium element can effectively facilitate the growth and development of flue-cured tobacco.
The second aspect of the present invention provides the preparation method of the foliar fertilizer, comprising the following steps:
1) ammonium hydroxide is uniformly sprayed on fermentation organic fertilizer, seals 3~4 hours, places into autoclave sterilization pot, Under certain temperature, 45~60min is handled;
2) by autoclave sterilization, treated that product is placed in bucket, and inorganic acid is added, and water sufficiently stirs evenly, and covers bung, Stirring in every 3~5 days is primary, places 15~25 days;
3) step 2) product is shifted with filtered through gauze, be added the alkali containing potassium element, adjust pH to 7 to get.
As a preferred embodiment, the preparation method of the foliar fertilizer, comprising the following steps:
1) ammonium hydroxide is uniformly sprayed on fermentation organic fertilizer, seals 3~4 hours, places into autoclave sterilization pot, At a temperature of 120~130 DEG C, 45~60min is handled;
2) by autoclave sterilization, treated that product is placed in bucket, and inorganic acid is added, and water sufficiently stirs evenly, and covers bung, Stirring in every 3~5 days is primary, places 15~25 days;
3) step 2) product is shifted with filtered through gauze, be added the alkali containing potassium element, adjust pH to 7 to get.
The present invention is specifically described below by embodiment.It is necessarily pointed out that following embodiment is only used In the invention will be further described, it should not be understood as limiting the scope of the invention, professional and technical personnel in the field The some nonessential modifications and adaptations made according to the content of aforementioned present invention, still fall within protection scope of the present invention.
In addition, if without other explanations, it is raw materials used to be all commercially available.
Embodiment
Embodiment 1
A kind of foliar fertilizer promoting the secretion of tobacco oil, including following raw material: 10 parts of organic fertilizer of fermentation;Inorganic acid 1 part;3 parts of alkali containing potassium element;2 parts of ammonium hydroxide;150 parts of water.
The weight part ratio of rape cake and chicken manure in the fermentation organic fertilizer are as follows: 3:1;
The fermentation organic fertilizer the preparation method comprises the following steps: rape cake is mixed well with chicken manure, is accumulated, spontaneous fermentation 20 days, Up to fermentation organic fertilizer.
The inorganic acid is the concentrated sulfuric acid;
The alkali containing potassium element is potassium hydroxide.
The preparation method of the foliar fertilizer, comprising the following steps:
1) ammonium hydroxide is uniformly sprayed on fermentation organic fertilizer, seals 4 hours, places into autoclave sterilization pot, 120 At a temperature of DEG C, 60min is handled;
2) by autoclave sterilization, treated that product is placed in bucket, and inorganic acid is added, and water sufficiently stirs evenly, and covers bung, Stirring in every 3 days is primary, places 20 days;
3) step 2) product is shifted with filtered through gauze, be added the alkali containing potassium element, adjust pH to 7 to get.
Embodiment 2
A kind of foliar fertilizer promoting the secretion of tobacco oil, including following raw material: 40 parts of organic fertilizer of fermentation;Inorganic acid 10 parts;10 parts of alkali containing potassium element;8 parts of ammonium hydroxide;270 parts of water.
The weight part ratio of rape cake and chicken manure in the fermentation organic fertilizer are as follows: 3:1, the specific side of preparation of the fermentation organic fertilizer Method is the same as embodiment 1;
The inorganic acid is the concentrated sulfuric acid;
The alkali containing potassium element is potassium hydroxide.
The preparation method of the foliar fertilizer, the specific steps are the same as those in embodiment 1.
Embodiment 3
A kind of foliar fertilizer promoting the secretion of tobacco oil, including following raw material: 24 parts of organic fertilizer of fermentation;Inorganic acid 5 parts;6 parts of alkali containing potassium element;4 parts of ammonium hydroxide;180 parts of water.
The weight part ratio of rape cake and chicken manure in the fermentation organic fertilizer are as follows: 3:1, the specific side of preparation of the fermentation organic fertilizer Method is the same as embodiment 1;
The inorganic acid is the concentrated sulfuric acid;
The alkali containing potassium element is potassium hydroxide.
The preparation method of the foliar fertilizer, the specific steps are the same as those in embodiment 1.
Embodiment 4
A kind of foliar fertilizer promoting the secretion of tobacco oil, including following raw material: 24 parts of organic fertilizer of fermentation;Inorganic acid 5 parts;6 parts of alkali containing potassium element;4 parts of ammonium hydroxide;180 parts of water.
The weight part ratio of rape cake and chicken manure in the fermentation organic fertilizer are as follows: 5.8:1, the fermentation organic fertilizer are specifically prepared Method is the same as embodiment 1;
The inorganic acid is the concentrated sulfuric acid;
The alkali containing potassium element is potassium hydroxide.
The preparation method of the foliar fertilizer, the specific steps are the same as those in embodiment 1.
Embodiment 5
A kind of foliar fertilizer promoting the secretion of tobacco oil, including following raw material: 24 parts of organic fertilizer of fermentation;Inorganic acid 5 parts;6 parts of alkali containing potassium element;4 parts of ammonium hydroxide;180 parts of water.
The weight part ratio of rape cake and chicken manure in the fermentation organic fertilizer are as follows: 5:1, the specific side of preparation of the fermentation organic fertilizer Method is the same as embodiment 1;
The inorganic acid is the concentrated sulfuric acid;
The alkali containing potassium element is potassium hydroxide.
The preparation method of the foliar fertilizer, the specific steps are the same as those in embodiment 1.
Comparative example 1
A kind of foliar fertilizer promoting the secretion of tobacco oil, including following raw material: 24 parts of organic fertilizer of fermentation;Inorganic acid 5 parts;6 parts of alkali containing potassium element;4 parts of ammonium hydroxide;180 parts of water.
The fermentation organic fertilizer is chicken manure;The chicken manure fermenting organic fertilizer the preparation method comprises the following steps: chicken manure is accumulated, send out naturally Ferment 20 days to get fermentation organic fertilizer.
The inorganic acid is the concentrated sulfuric acid;
The alkali containing potassium element is potassium hydroxide.
The preparation method of the foliar fertilizer, the specific steps are the same as those in embodiment 1.
Comparative example 2
A kind of foliar fertilizer promoting the secretion of tobacco oil, including following raw material: 24 parts of organic fertilizer of fermentation;Inorganic acid 5 parts;6 parts of alkali containing potassium element;4 parts of ammonium hydroxide;180 parts of water.
The fermentation organic fertilizer be rape cake, the organic fertilizer prepared by fermenting rapeseed cakes the preparation method comprises the following steps: rape cake is abundant Accumulation, spontaneous fermentation 20 days to get fermentation organic fertilizer.
The inorganic acid is the concentrated sulfuric acid;
The alkali containing potassium element is potassium hydroxide.
The preparation method of the foliar fertilizer, the specific steps are the same as those in embodiment 1.
Comparative example 3
A kind of foliar fertilizer promoting the secretion of tobacco oil, including following raw material: 24 parts of organic fertilizer of fermentation;Inorganic acid 5 parts;6 parts of alkali containing potassium element;4 parts of ammonium hydroxide;180 parts of water.
The fermentation organic fertilizer is the mixture of organic fertilizer prepared by fermenting rapeseed cakes and chicken manure fermenting organic fertilizer;
The fermentation organic fertilizer the preparation method comprises the following steps: (1) accumulates rape cake, spontaneous fermentation 20 days, obtain rape cake fermentation Organic fertilizer;(2) chicken manure is accumulated, spontaneous fermentation 20 days, obtains chicken manure fermenting organic fertilizer;(3) by organic fertilizer prepared by fermenting rapeseed cakes and chicken Manure fermentation organic fertilizer mixing to get.
The inorganic acid is the concentrated sulfuric acid;
The alkali containing potassium element is potassium hydroxide.
The preparation method of the foliar fertilizer, the specific steps are the same as those in embodiment 1.
Comparative example 4
A kind of foliar fertilizer promoting the secretion of tobacco oil, including following raw material: 24 parts of organic fertilizer of fermentation;Inorganic acid 5 parts;6 parts of alkali containing potassium element;180 parts of water.
The weight part ratio of rape cake and chicken manure in the fermentation organic fertilizer are as follows: 5:1, the specific side of preparation of the fermentation organic fertilizer Method is the same as embodiment 1;
The inorganic acid is the concentrated sulfuric acid;
The alkali containing potassium element is potassium hydroxide.
The preparation method of the foliar fertilizer, comprising the following steps:
1) fermentation organic fertilizer is put into autoclave sterilization pot, at a temperature of 120 DEG C, handles 60min;
2) by autoclave sterilization, treated that product is placed in bucket, and inorganic acid is added, and water sufficiently stirs evenly, and covers bung, Stirring in every 3 days is primary, places 20 days;
3) step 2) product is shifted with filtered through gauze, be added the alkali containing potassium element, adjust pH to 7 to get.
Performance test
The effect of foliar fertilizer described in testing example 1~5 and comparative example 1~4.
Tobacco bred: K326 and cloud and mist 87;
The foliar fertilizer described in Examples 1 to 5 and comparative example 1~4 is sprayed in the phase of group and prosperous growth phase, is taken after flue-cured tobacco is roasting Sample measures oil content, using petroleum ether as extract.
The effect of foliar fertilizer described in 1 Examples 1 to 5 of table and comparative example 1~4
The above described is only a preferred embodiment of the present invention, be not the limitation for making other forms to invention, it is any Those skilled in the art are changed or are changed to the equivalent of equivalent variations possibly also with the technology contents of the disclosure above Embodiment, but without departing from the technical solutions of the present invention, above embodiments are made according to the technical essence of the invention Any simple modification, equivalent variations and remodeling, still fall within the protection scope of technical solution of the present invention.

Claims (10)

1. a kind of foliar fertilizer for promoting the secretion of tobacco oil, which is characterized in that including following raw material: fermentation organic fertilizer 10 ~40 parts;1~10 part of inorganic acid;3~10 parts of alkali containing potassium element;2~8 parts of ammonium hydroxide;150~270 parts of water.
2. foliar fertilizer as described in claim 1, which is characterized in that including following raw material: fermentation organic fertilizer 17~30 Part;5~7.5 parts of inorganic acid;5~6.5 parts of alkali containing potassium element;3~4..5 parts of ammonium hydroxide;180~250 parts of water.
3. foliar fertilizer as described in claim 1, which is characterized in that the fermentation organic fertilizer be selected from rape cake, chicken manure, sheep dung, At least one of cow dung, pig manure, soya-bean cake, cottonseed cake.
4. foliar fertilizer as claimed in claim 3, which is characterized in that the fermentation organic fertilizer is rape cake and/or chicken manure.
5. foliar fertilizer as claimed in claim 4, which is characterized in that the fermentation organic fertilizer is made of rape cake and chicken manure.
6. foliar fertilizer as claimed in claim 5, which is characterized in that the inorganic acid is sulfuric acid and/or nitric acid.
7. foliar fertilizer as claimed in claim 6, which is characterized in that the inorganic acid is sulfuric acid.
8. foliar fertilizer as described in claim 1, which is characterized in that the alkali containing potassium element is potassium hydroxide and/or carbonic acid Potassium.
9. a kind of preparation method of foliar fertilizer as described in any one of claims 1 to 8, which comprises the following steps:
1) ammonium hydroxide is uniformly sprayed on fermentation organic fertilizer, seals 3~4 hours, places into autoclave sterilization pot, centainly At a temperature of, handle 45~60min;
2) by autoclave sterilization, treated that product is placed in bucket, and inorganic acid is added, and water sufficiently stirs evenly, and covers bung, and every 3 Stirring in~5 days is primary, places 15~25 days;
3) step 2) product is shifted with filtered through gauze, be added the alkali containing potassium element, adjust pH to 7 to get.
10. the preparation method of foliar fertilizer as claimed in claim 9, which is characterized in that in the step 1) temperature be 120~ 130℃。
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K.G.MACIOROWSKI等: "Effects on poultry and livestock of feed contamination with bacteria and fungi", 《ANIMAL FEED SCIENCE AND TECHNOLOGY》 *

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