CN109534679A - A kind of metal dry granular glaze and preparation method thereof and metal dry granular overglaze dazzle the preparation method for throwing brick - Google Patents

A kind of metal dry granular glaze and preparation method thereof and metal dry granular overglaze dazzle the preparation method for throwing brick Download PDF

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Publication number
CN109534679A
CN109534679A CN201811617953.7A CN201811617953A CN109534679A CN 109534679 A CN109534679 A CN 109534679A CN 201811617953 A CN201811617953 A CN 201811617953A CN 109534679 A CN109534679 A CN 109534679A
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CN
China
Prior art keywords
dry granular
metal dry
glaze
metal
brick
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201811617953.7A
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Chinese (zh)
Inventor
麦文英
汪加武
叶建明
王礼
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GUANGDONG OVERLAND CERAMICS CO Ltd
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GUANGDONG OVERLAND CERAMICS CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Priority to CN201811617953.7A priority Critical patent/CN109534679A/en
Publication of CN109534679A publication Critical patent/CN109534679A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C8/00Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
    • C03C8/02Frit compositions, i.e. in a powdered or comminuted form
    • C03C8/10Frit compositions, i.e. in a powdered or comminuted form containing lead
    • C03C8/12Frit compositions, i.e. in a powdered or comminuted form containing lead containing titanium or zirconium
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/45Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
    • C04B41/52Multiple coating or impregnating multiple coating or impregnating with the same composition or with compositions only differing in the concentration of the constituents, is classified as single coating or impregnation
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/80After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
    • C04B41/81Coating or impregnation
    • C04B41/89Coating or impregnation for obtaining at least two superposed coatings having different compositions

Abstract

The present invention discloses a kind of metal dry granular glaze and preparation method thereof and metal dry granular overglaze dazzles the preparation method for throwing brick, and metal dry granular glaze includes each component of following mass fraction: albite 30-40%, red lead 10-15%, manganese oxide 10-15%, quartz 5-10%, calcium carbonate 5-10%, clay 5-10%, zinc oxide 2-5%, copper oxide 2-5% nickel protoxide 2-5%, titanium oxide 1-5%, cobalt oxide 1-5%.It prepares metal dry granular overglaze and dazzles the method for throwing brick the following steps are included: step B001: preparing metal dry granular;Step B002: preparation Ceramic Tiles green body forms decoration glaze layer in ceramic brick surface spraying or the glaze layer of printer belt decorative effect;Step B003: the metal dry granular prepared in ceramic brick surface secondary material distributing step B001, printing production figure, then the clear frit in the spraying of brick body surface for polishing;Step B004: being put into kiln firing for brick body, dazzles throwing technology using diamond and carries out dazzling throwing to brick body surface, obtains metal dry granular overglaze and dazzle throwing brick.

Description

A kind of metal dry granular glaze and preparation method thereof and metal dry granular overglaze dazzle the system for throwing brick Preparation Method
Technical field
The present invention relates to ceramic technology field more particularly to a kind of metal dry granular glaze and preparation method thereof and metal dry granulars Overglaze dazzles the preparation method for throwing brick.
Background technique
Dry granular glaze is by secondary material distributing technology, and the ceramic tile decoration new varieties researched and developed, produced, it is widely used in ceramic On the decoration of glaze brick product, have the effects that anti-skidding, wear-resisting, dry granular glaze belongs to Sub-shine glaze product, its shape on earthenware brick glaze At rough surface, generate matt and the using effects such as anti-skidding, 1200 degrees Celsius at a temperature of be burnt into, the water suction of ceramic tile For rate less than 0.3%, consistency is high, and wearability is good.Metallic Ceramic Tiles usually in one layer of metal glaze layer of adobe surface charity or Metal dry granular, through high temperature sintering, ceramic brick surface has metallic luster.But the metallic Ceramic Tiles gold of existing technology production It is single to belong to sense, decoration stereovision is not strong, and not true to nature enough, common metal dry granular glaze is easy to get confused, and color is not bright-coloured enough, not can be carried out Dazzle throwing.
Summary of the invention
Aiming at the problems existing in the prior art, the purpose of the present invention is to provide a kind of metal dry granular glaze and its preparations Method and metal dry granular overglaze dazzle the method for throwing brick preparation.The metal dry granular glaze has high glaze copper gold effect, uses this The Ceramic Tiles metallic visual sense of metal dry granular glaze preparation is different, and each angle, which is seen, shows different metal senses;Metal Dry granular glaze corner angle of dry granular after high temperature firing are melted, so that ceramic tile texture is gentle, feel exquisiteness while reaches resistance to Grind antiskid effect.
To achieve the above objectives, the present invention adopts the following technical scheme:
A kind of metal dry granular glaze, each component including following mass fraction: albite 30-40%, red lead 10-15%, Manganese oxide 10-15%, quartz 5-10%, calcium carbonate 5-10%, clay 5-10%, zinc oxide 2-5%, copper oxide 2-5%, oxidation Sub- nickel 2-5%, titanium oxide 1-5%, cobalt oxide 1-5%.Metal of the 1-5% titanium oxide that the metal dry granular glaze is added to glaze Glossiness has a direct impact, because the glossiness of the bigger glaze of the refractive index of object phase is relatively higher.At partial oxidation during glaze Titanium forms the big rutile of refractive index, and the recrystallization of titanate is generated around simultaneous oxidation titanium, these crystallizations are in glaze layer surface shape It is regularly aligned at enrichment, and neatly, mirror-reflection is occurred to light and generates metallic luster.
As a further illustration of the above scheme, the metal glaze includes each component of following mass fraction: albite 35%, red lead 16%, manganese oxide 12%, quartz 8%, calcium carbonate 7%, clay 6%, zinc oxide 4%, copper oxide 4%, oxidation are sub- Nickel 3%, titanium oxide 3%, cobalt oxide 2%.
As a further illustration of the above scheme, the metal glaze includes each component of following mass fraction: albite 38%, red lead 12%, manganese oxide 14%, quartz 5%, calcium carbonate 9%, clay 8%, zinc oxide 3%, copper oxide 2%, oxidation are sub- Nickel 1%, titanium oxide 5%, cobalt oxide 3%.
A method of preparing above-mentioned metal dry granular glaze, which comprises the following steps:
Step A001: raw material is pressed into formula rate ingredient, puts into batch mixer and is uniformly mixed;
Step A002: heating melting in kiln is added in mixed raw material, glass metal is made;
Step A003: glass metal through water quenching, dry, crush and screen after be made metal dry granular.
As a further illustration of the above scheme, the heating temperature in the step A002 is 1500 DEG C
- 1650 DEG C, heated hold time is 0.5-1.5 hours.
As a further illustration of the above scheme, the metal dry granular fineness by screening in the step A003 is 30- 60 mesh.
A method of it preparing metal dry granular overglaze and dazzles throwing brick, which comprises the following steps: step B001: root Metal dry granular is prepared according to the above method;
Step B002: preparation Ceramic Tiles green body forms decoration glaze in ceramic brick surface spraying or the glaze layer of printer belt decorative effect Layer;
Step B003: the metal dry granular prepared in ceramic brick surface secondary material distributing step B001, printing production figure, then upper one Transparent glaze layer for polishing;
Step B004: brick body is put into heat in kiln and is burnt into, throwing technology is dazzled using diamond, brick body surface is carried out to dazzle throwing, obtained Metal dry granular overglaze dazzles throwing brick.
As a further illustration of the above scheme, the metal dry granular trailing in the step B003 is screen printing brushing Grain method or leaching dry granular method.
As a further illustration of the above scheme, heating firing temperature in the step B004 is 1000 DEG C
- 1250 DEG C, firing time is 1-2 hours.
As a further illustration of the above scheme, diamond, which dazzles throwing technology, in the step B004 is added on brick body surface Diamond polishing liquid carries out brick face using bistrique to dazzle throwing.
The beneficial effects of the present invention are:
One, metal dry granular glaze provided by the invention has high glaze copper gold effect, uses the metal dry granular glaze system Standby Ceramic Tiles metallic visual sense is different, and each angle, which is seen, shows different metal senses;The fineness of metal dry granular is 30- 60 mesh, the corner angle of dry granular are melted after high temperature firing, so that brick body texture is gentle, feel exquisiteness while reaches wear-resisting anti- Sliding effect.
Two, metal dry granular glaze of the invention makes dark metal decorative cover issue clear color, dazzles throwing using diamond Technology keeps surface luminous intensity consistent with metallic luster, and brick face is smooth, and decorative effect is more preferable.
Specific embodiment
Below with reference to embodiment, invention is further described in detail.
Embodiment 1:
The metal glaze includes each component of following mass fraction: albite 35, red lead 16%, manganese oxide 12%, stone English 8%, calcium carbonate 7%, clay 6%, zinc oxide 3%, copper oxide 4%, nickel protoxide 3%, titanium oxide 2%, cobalt oxide 2%.
Raw material is pressed into formula rate ingredient, puts into batch mixer and is uniformly mixed, 1500-1650 is added in mixed raw material DEG C tank furnace in melt after glass metal is made;Glass metal is flowed at fluidization tower shape in the pond of 20-70 DEG C of water temperature, is broken into water flow punching Particle, melt through water quenching, dry, crush and screen after metal dry granular is made, metal dry granular fineness after screening is 30-60 mesh.
Press ceramic basis moulded pottery not yet put in a kiln to bake body is formed in ceramic brick surface spraying or the glaze layer of printer belt decorative effect after drying Glaze layer is decorated, decoration glaze layer is also possible to metal glaze layer;In ceramic brick surface screen-printed metal dry granular, printing production is schemed, then Transparent glaze layer of the spraying for polishing;Brick body is put into kiln and is heated to 1250 DEG C.Firing time is 80 minutes, uses gold after cooling Hard rock dazzles throwing technology and carries out dazzling throwing to brick body surface, obtains metal dry granular overglaze and dazzles throwing brick.
Embodiment 2:
The metal glaze includes each component of following mass fraction: albite 38%, red lead 12%, manganese oxide 14%, Quartzy 5%, calcium carbonate 9%, clay 8%, zinc oxide 3%, copper oxide 2%, nickel protoxide 1%, titanium oxide 5%, cobalt oxide 3%.
Raw material is pressed into formula rate ingredient, puts into batch mixer and is uniformly mixed, 1500-1650 is added in mixed raw material DEG C tank furnace in melt after glass metal is made;Glass metal is flowed at fluidization tower shape in the pond of 20-70 DEG C of water temperature, is broken into water flow punching Particle, melt through water quenching, dry, crush and screen after metal dry granular is made, metal dry granular fineness after screening is 30-60 mesh.
Press ceramic basis moulded pottery not yet put in a kiln to bake body is formed in ceramic brick surface spraying or the glaze layer of printer belt decorative effect after drying Glaze layer is decorated, decoration glaze layer is also possible to metal glaze layer;Metal dry granular and dry granular fixative are mixed, get rid of glaze equipment with bimodal It, will by the mixture of metal dry granular and dry granular fixative decoration in decoration glaze layer surface, then in the transparent glaze layer of brick body surface spraying Brick body is put into kiln and is heated to 1150 DEG C.Firing time is 90 minutes, it is cooling after using diamond dazzle throwing technology to brick body surface into Row dazzles throwing, obtains metal dry granular overglaze and dazzles throwing brick.
Compared with prior art, a kind of metal dry granular overglaze provided by the invention dazzles the preparation method for throwing brick, has following Feature: 1) metal dry granular glaze provided by the invention has high glaze copper gold effect, is prepared using the metal dry granular glaze Ceramic Tiles metallic visual sense is different, and each angle, which is seen, shows different metal senses;The fineness of metal dry granular is 30-60 Mesh, the corner angle of dry granular are melted after high temperature firing, so that brick body texture is gentle, feel exquisiteness while reaches wear-resisting antiskid Effect.2) metal dry granular glaze of the invention makes dark metal decorative cover issue clear color, dazzles throwing technology using diamond, Keep surface luminous intensity consistent with metallic luster, brick face is smooth, and decorative effect is more preferable.
By the description of the above embodiments and principle, it should be understood by those skilled in the art that, the present invention is not It is confined to above-mentioned specific embodiment, this is all fallen within using the improvement of techniques well known and substitution on the basis of the present invention The protection scope of invention, protection scope of the present invention should limit it by each claim and its equivalent.Specific embodiment In the part that does not illustrate be the prior art or common knowledge.

Claims (10)

1. a kind of metal dry granular glaze, which is characterized in that the metal dry granular glaze includes each component of following mass fraction: sodium is long Stone 30-40%, red lead 10-15%, manganese oxide 10-15%, quartz 5-10%, calcium carbonate 5-10%, clay 5-10%, zinc oxide 2-5%, copper oxide 2-5%, nickel protoxide 2-5%, titanium oxide 1-5%, cobalt oxide 1-5%.
2. metal dry granular glaze according to claim 1, which is characterized in that the metal glaze includes following mass fraction Each component: albite 35%, red lead 16%, manganese oxide 12%, quartz 8%, calcium carbonate 7%, clay 6%, zinc oxide 4%, Copper oxide 4%, nickel protoxide 3%, titanium oxide 3%, cobalt oxide 2%.
3. metal dry granular glaze according to claim 1, which is characterized in that the metal glaze includes following mass fraction Each component: albite 38%, red lead 12%, manganese oxide 14%, quartz 5%, calcium carbonate 9%, clay 8%, zinc oxide 3%, Copper oxide 2%, nickel protoxide 1%, titanium oxide 5%, cobalt oxide 3%.
4. a kind of method for preparing metal dry granular glaze as described in claim 1, which comprises the following steps:
Step A001: raw material is pressed into formula rate ingredient, puts into batch mixer and is uniformly mixed;
Step A002: heating melting in kiln is added in mixed raw material, glass metal is made;
Step A003: glass metal through water quenching, dry, crush and screen after obtain metal dry granular.
5. metal dry granular glaze preparation method for material according to claim 4, which is characterized in that the heating in the step A002 Temperature is 1500 DEG C -1650 DEG C, and heated hold time is 0.5-1.5 hours.
6. metal dry granular glaze preparation method for material according to claim 4, which is characterized in that the process in the step A003 The metal dry granular fineness of screening is 30-60 mesh.
7. a kind of metal dry granular glaze using claim 1, which prepares metal dry granular overglaze, dazzles the method for throwing brick, which is characterized in that The following steps are included:
Step B001: the preparation method of metal dry granular glaze according to claim 4 prepares metal dry granular;
Step B002: preparation Ceramic Tiles green body forms decoration glaze in ceramic brick surface spraying or the glaze layer of printer belt decorative effect Layer;
Step B003: the metal dry granular prepared in ceramic brick surface secondary material distributing step B001, printing production figure, then upper one Transparent glaze layer for polishing;
Step B004: brick body is put into heat in kiln and is burnt into, throwing technology is dazzled using diamond, brick body surface is carried out to dazzle throwing, obtained Metal dry granular overglaze dazzles throwing brick.
8. the metal dry granular overglaze according to claim 7 for preparing dazzles the method for throwing brick, which is characterized in that the step B003 In metal dry granular trailing be silk-screen printing dry granular method or leaching dry granular method.
9. the metal dry granular overglaze according to claim 7 for preparing dazzles the method for throwing brick, which is characterized in that the step B004 Middle heating firing temperature is 1000 DEG C -1250 DEG C, and firing time is 1-2 hours.
10. the metal dry granular overglaze according to claim 7 for preparing dazzles the method for throwing brick, which is characterized in that the step It is to add diamond polishing liquid on brick body surface that diamond, which dazzles throwing technology, in B004, carries out dazzling throwing to brick face using bistrique.
CN201811617953.7A 2018-12-28 2018-12-28 A kind of metal dry granular glaze and preparation method thereof and metal dry granular overglaze dazzle the preparation method for throwing brick Pending CN109534679A (en)

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CN110357668A (en) * 2019-08-09 2019-10-22 东莞市唯美陶瓷工业园有限公司 A kind of full throwing glaze Ceramic Tiles and preparation method thereof with graininess flashing ornaments
CN111606718A (en) * 2020-04-28 2020-09-01 肇庆市将军陶瓷有限公司 Glazed brick containing metal dry particles
CN111848225A (en) * 2020-08-05 2020-10-30 佛山市华力达材料科技有限公司 Production process of ceramic tile with metal luster, ceramic tile and metal dry particle glaze
CN111847877A (en) * 2020-08-05 2020-10-30 佛山市华力达材料科技有限公司 Metal dry particle glaze, metal luster ceramic tile and preparation method thereof
CN112608029A (en) * 2020-12-28 2021-04-06 肇庆乐华陶瓷洁具有限公司 Dazzling archaized brick and preparation method thereof
CN113860887A (en) * 2021-10-22 2021-12-31 新明珠集团股份有限公司 Ceramic plate and preparation method thereof
CN115340414A (en) * 2022-10-18 2022-11-15 陶丽西(苏州)陶瓷釉色料有限公司 Metal particle for ceramic tile and preparation method and application thereof

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Publication number Priority date Publication date Assignee Title
CN110357668A (en) * 2019-08-09 2019-10-22 东莞市唯美陶瓷工业园有限公司 A kind of full throwing glaze Ceramic Tiles and preparation method thereof with graininess flashing ornaments
CN111606718A (en) * 2020-04-28 2020-09-01 肇庆市将军陶瓷有限公司 Glazed brick containing metal dry particles
CN111606718B (en) * 2020-04-28 2022-10-18 肇庆市将军陶瓷有限公司 Glazed brick containing metal dry particles
CN111848225A (en) * 2020-08-05 2020-10-30 佛山市华力达材料科技有限公司 Production process of ceramic tile with metal luster, ceramic tile and metal dry particle glaze
CN111847877A (en) * 2020-08-05 2020-10-30 佛山市华力达材料科技有限公司 Metal dry particle glaze, metal luster ceramic tile and preparation method thereof
CN111847877B (en) * 2020-08-05 2022-07-01 佛山市华力达材料科技有限公司 Metal dry particle glaze, metal luster ceramic tile and preparation method thereof
CN112608029A (en) * 2020-12-28 2021-04-06 肇庆乐华陶瓷洁具有限公司 Dazzling archaized brick and preparation method thereof
CN113860887A (en) * 2021-10-22 2021-12-31 新明珠集团股份有限公司 Ceramic plate and preparation method thereof
CN113860887B (en) * 2021-10-22 2022-08-30 新明珠集团股份有限公司 Ceramic plate and preparation method thereof
CN115340414A (en) * 2022-10-18 2022-11-15 陶丽西(苏州)陶瓷釉色料有限公司 Metal particle for ceramic tile and preparation method and application thereof

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Application publication date: 20190329