CN109527175A - Sugar free health care sweet Momordica grosvenori ice and preparation method thereof - Google Patents
Sugar free health care sweet Momordica grosvenori ice and preparation method thereof Download PDFInfo
- Publication number
- CN109527175A CN109527175A CN201811535855.9A CN201811535855A CN109527175A CN 109527175 A CN109527175 A CN 109527175A CN 201811535855 A CN201811535855 A CN 201811535855A CN 109527175 A CN109527175 A CN 109527175A
- Authority
- CN
- China
- Prior art keywords
- preparation
- ice
- momordica grosvenori
- triterpene
- medicinal extract
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 235000011171 Thladiantha grosvenorii Nutrition 0.000 title claims abstract description 18
- 235000009508 confectionery Nutrition 0.000 title claims abstract description 18
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- 235000000346 sugar Nutrition 0.000 title claims abstract description 13
- 241001409321 Siraitia grosvenorii Species 0.000 title claims 5
- 150000003648 triterpenes Chemical class 0.000 claims abstract description 19
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 12
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 12
- 235000001727 glucose Nutrition 0.000 claims abstract description 8
- UNXHWFMMPAWVPI-UHFFFAOYSA-N Erythritol Natural products OCC(O)C(O)CO UNXHWFMMPAWVPI-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000003814 drug Substances 0.000 claims abstract description 7
- UNXHWFMMPAWVPI-ZXZARUISSA-N erythritol Chemical compound OC[C@H](O)[C@H](O)CO UNXHWFMMPAWVPI-ZXZARUISSA-N 0.000 claims abstract description 7
- 238000001816 cooling Methods 0.000 claims abstract description 4
- 238000004090 dissolution Methods 0.000 claims abstract description 4
- 150000002304 glucoses Chemical class 0.000 claims abstract description 4
- 238000010438 heat treatment Methods 0.000 claims abstract description 4
- 238000005520 cutting process Methods 0.000 claims description 4
- 230000004048 modification Effects 0.000 claims description 2
- 238000012986 modification Methods 0.000 claims description 2
- 150000003505 terpenes Chemical class 0.000 claims description 2
- 235000007586 terpenes Nutrition 0.000 claims description 2
- 244000185386 Thladiantha grosvenorii Species 0.000 abstract description 13
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 abstract description 5
- 235000013305 food Nutrition 0.000 abstract description 5
- 239000008103 glucose Substances 0.000 abstract description 4
- 239000000126 substance Substances 0.000 abstract description 4
- 125000001033 ether group Chemical group 0.000 abstract description 3
- 235000019605 sweet taste sensations Nutrition 0.000 abstract description 3
- 244000246386 Mentha pulegium Species 0.000 abstract description 2
- 235000016257 Mentha pulegium Nutrition 0.000 abstract description 2
- 235000004357 Mentha x piperita Nutrition 0.000 abstract description 2
- 150000002016 disaccharides Chemical class 0.000 abstract description 2
- 235000012907 honey Nutrition 0.000 abstract description 2
- 235000001050 hortel pimenta Nutrition 0.000 abstract description 2
- 150000002772 monosaccharides Chemical class 0.000 abstract description 2
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 2
- RRHGJUQNOFWUDK-UHFFFAOYSA-N Isoprene Chemical compound CC(=C)C=C RRHGJUQNOFWUDK-UHFFFAOYSA-N 0.000 description 2
- 229930006000 Sucrose Natural products 0.000 description 2
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 2
- 229940079593 drug Drugs 0.000 description 2
- 235000013399 edible fruits Nutrition 0.000 description 2
- 235000021022 fresh fruits Nutrition 0.000 description 2
- 239000005720 sucrose Substances 0.000 description 2
- QCVGEOXPDFCNHA-UHFFFAOYSA-N 5,5-dimethyl-2,4-dioxo-1,3-oxazolidine-3-carboxamide Chemical compound CC1(C)OC(=O)N(C(N)=O)C1=O QCVGEOXPDFCNHA-UHFFFAOYSA-N 0.000 description 1
- 240000002791 Brassica napus Species 0.000 description 1
- 235000004977 Brassica sinapistrum Nutrition 0.000 description 1
- 206010011224 Cough Diseases 0.000 description 1
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 description 1
- 102000002322 Egg Proteins Human genes 0.000 description 1
- 108010000912 Egg Proteins Proteins 0.000 description 1
- 229930091371 Fructose Natural products 0.000 description 1
- 239000005715 Fructose Substances 0.000 description 1
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 description 1
- 206010036790 Productive cough Diseases 0.000 description 1
- 244000269722 Thea sinensis Species 0.000 description 1
- 229930003268 Vitamin C Natural products 0.000 description 1
- 238000003556 assay Methods 0.000 description 1
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 1
- 235000014103 egg white Nutrition 0.000 description 1
- 210000000969 egg white Anatomy 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 235000003599 food sweetener Nutrition 0.000 description 1
- 229930182478 glucoside Natural products 0.000 description 1
- 150000008131 glucosides Chemical class 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 208000024794 sputum Diseases 0.000 description 1
- 210000003802 sputum Anatomy 0.000 description 1
- 150000005846 sugar alcohols Chemical class 0.000 description 1
- 239000003765 sweetening agent Substances 0.000 description 1
- 235000019154 vitamin C Nutrition 0.000 description 1
- 239000011718 vitamin C Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/36—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
- A23G3/48—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds containing plants or parts thereof, e.g. fruits, seeds, extracts
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/30—Artificial sweetening agents
- A23L27/33—Artificial sweetening agents containing sugars or derivatives
- A23L27/34—Sugar alcohols
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Proteomics, Peptides & Aminoacids (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Botany (AREA)
- Inorganic Chemistry (AREA)
- Confectionery (AREA)
- Steroid Compounds (AREA)
Abstract
The invention discloses a kind of sugar free health care sweet Momordica grosvenori ice and preparation method thereof, it is first to be modified the tetracyclic triterpene of fresh fructus momordicae, separate, and is concentrated under reduced pressure into vacuum kettle in medicinal extract shape；Then antierythrite is heated to 170-180 DEG C, reacts after its dissolution in fructus momordicae tetranuclear triterpene medicinal extract, the two mixing after watery, is added, stop heating, it is to end of reaction until cooling, with mold be made bulk or be crushed to it is granular, sweet Momordica grosvenori ice.The invention has the advantages that since the chemical structure of tetracyclic triterpene is in ether chain structure, there are 3 carbon potentials on the left side, there are 24 carbon potentials on the right, it respectively ins succession five molecule glucoses, preparation method of the present invention cuts off connected five molecule glucose of two carbon potentials, to remove medicine gas, and distribute mellowness, sweet taste approximation honey, it eats refreshing in the ice as peppermint candy in the mouth, through examining, product total reducing sugar (monosaccharide and disaccharide) content is in 0.15% and 0.203% respectively, meets the sugarfree foods standard of national standard GB13432 total reducing sugar≤0.5%.
Description
Technical field
The present invention relates to field of food, specifically a kind of sugar free health care sweet Momordica grosvenori ice and preparation method thereof.
Background technique
Siraitia grosvenorii is one of the dual-purpose of drug and food material that country ratifies in the first batch, and primary efficacy is can be relieving cough and reducing sputum.Fruit battalion
Feeding value is very high, containing vitamin C abundant (containing 400-500 milligrams in every 100 grams of fresh fruits) and glucoside, fructose, glucose, egg
White matter and lipid etc..Sweet ingredient-tetracyclic triterpene of Siraitia grosvenorii, molecular formula C30H52O4 H2O is made of six isoprene.
But new fresh fructus momordicae can sprout one flavour of a drug for allowing people to suffocate, and fresh fruit pulp has included oxidizing ferment, directly edible tongue to be made to send out
Fiber crops, or even puncture tongue.
Summary of the invention
The invention aims to provide a kind of sugar free health care sweet Momordica grosvenori ice and preparation method thereof.
Realizing the technical solution of the object of the invention is:
The preparation method of sugar free health care sweet Momordica grosvenori ice of the present invention, includes the following steps:
(1) tetracyclic triterpene of fresh fructus momordicae is modified；
(2) modified tetracyclic triterpene is separated, is concentrated under reduced pressure into vacuum kettle in medicinal extract shape；
(3) antierythrite is heated to 170-180 DEG C, after its dissolution is in watery, the fructus momordicae tetranuclear triterpene of step (2) is added
Medicinal extract, the two mixing react, and stop heating；
(4) to end of reaction until cooling, with mold be made bulk or be crushed to it is granular, sweet Momordica grosvenori ice.
Modification described in step (1) is connected five molecule glucose between carbon potential in the chemical structure by tetracyclic triterpene
Cutting, to remove medicine gas.
Step (2) is described to be concentrated under reduced pressure with vacuum kettle, negative pressure 0.08MPa, and being concentrated into Baume degrees is 22-26 degree.
Step (3) antierythrite and the additional amount of fructus momordicae tetranuclear triterpene medicinal extract are calculated as by weight ratio: red moss
Sugar alcohol: fructus momordicae tetranuclear triterpene medicinal extract=1: 0.15.
The invention has the advantages that the chemical structure due to tetracyclic triterpene is in ether chain structure, there are 3 carbon potentials on the left side, right
While there is 24 carbon potentials, five molecule glucoses of respectively ining succession, preparation method of the present invention is by two carbon potential connected five molecule Portugals
The cutting of grape sugar, to remove medicine gas, and distributes mellowness, sweet taste approximation honey, eats ice is refreshing as peppermint candy in the mouth, through wide
Unit assay detects in western Guilin City and Beijing, and product total reducing sugar (monosaccharide and disaccharide) content is in 0.15% and 0.203% respectively, is met
The sugarfree foods standard of national standard GB13432 total reducing sugar≤0.5%.
Specific embodiment
Embodiment:
The preparation method of sugar free health care sweet Momordica grosvenori ice of the present invention is:
(1) tetracyclic triterpene of fresh fructus momordicae is modified, since the chemical structure of tetracyclic triterpene is in ether chain structure, the left side has
There are 24 carbon potentials on one 3 carbon potential, the right, five molecule glucoses of ining succession between each carbon potential, by two carbon potentials connected five
Molecule glucose cutting, to remove medicine gas；
(2) modified tetracyclic triterpene is separated, is concentrated under reduced pressure into vacuum kettle in medicinal extract shape, negative pressure 0.08MPa, concentration
It is 24 degree to Baume degrees；
(3) 1000g antierythrite is heated to 174 DEG C, after its dissolution is in watery, the Siraitia grosvenorii Fourth Ring three of step (2) is added
Terpene medicinal extract 150g, the two mixing react, and stop heating；
(4) bulk is made with mold or is crushed to the fine grained of rapeseed shape with pulverizer up to cooling to end of reaction,
Sweet Momordica grosvenori ice.
Product is tested through sugariness: taking 0.5 gram of sweet Momordica grosvenori ice to be respectively placed in cup with 5 grams of white sucrose, 100ml is respectively added
80 DEG C or so of warm water dissolves the two respectively, and then comparison is tasted, and the two sweet taste, sugariness are quite similar, thus prove arhat
The sugariness of fruit sweet tea ice is 10 times of white sucrose, and need not addition sweetener progress flavoring in production sugarfree foods.
Claims (5)
1. the preparation method of sugar free health care sweet Momordica grosvenori ice, it is characterized in that: including the following steps:
(1) tetracyclic triterpene of fresh fructus momordicae is modified；
(2) modified tetracyclic triterpene is separated, is concentrated under reduced pressure into vacuum kettle in medicinal extract shape；
(3) antierythrite is heated to 170-180 DEG C, after its dissolution is in watery, the fructus momordicae tetranuclear triterpene of step (2) is added
Medicinal extract, the two mixing react, and stop heating；
(4) to end of reaction until cooling, with mold be made bulk or be crushed to it is granular, sweet Momordica grosvenori ice.
2. preparation method according to claim 1, it is characterized in that: modification described in step (1), is by the change of tetracyclic triterpene
Connected five molecule glucoses cutting between carbon potential in structure is learned, to remove medicine gas.
3. preparation method according to claim 1 is concentrated under reduced pressure it is characterized in that: step (2) is described with vacuum kettle, negative pressure
For 0.08MPa, being concentrated into Baume degrees is 22-26 degree.
4. preparation method according to claim 1, it is characterized in that: step (3) antierythrite and Siraitia grosvenorii Fourth Ring three
The additional amount of terpene medicinal extract is calculated as by weight ratio: antierythrite: fructus momordicae tetranuclear triterpene medicinal extract=1: 0.15.
5. the sugar free health care sweet Momordica grosvenori ice of preparation method preparation described in one of claim 1-4.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811535855.9A CN109527175A (en) | 2018-12-15 | 2018-12-15 | Sugar free health care sweet Momordica grosvenori ice and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811535855.9A CN109527175A (en) | 2018-12-15 | 2018-12-15 | Sugar free health care sweet Momordica grosvenori ice and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109527175A true CN109527175A (en) | 2019-03-29 |
Family
ID=65856308
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811535855.9A Pending CN109527175A (en) | 2018-12-15 | 2018-12-15 | Sugar free health care sweet Momordica grosvenori ice and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109527175A (en) |
Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1437128A1 (en) * | 2003-01-07 | 2004-07-14 | Michael Kaufmann | Pellet made from a matrix comprising tee as starting material and its method of preparation |
| CN101204221A (en) * | 2006-12-19 | 2008-06-25 | 张雨生 | Sugar free health care grosvenori crystal and manufacture method thereof |
| CN103461812A (en) * | 2012-11-07 | 2013-12-25 | 张雨生 | Sugarless sweet glutinous rice soft cake with health-care function |
| CN103461446A (en) * | 2012-11-07 | 2013-12-25 | 张雨生 | Healthcare sugarless sweet biscuit |
| CN104059959A (en) * | 2013-03-20 | 2014-09-24 | 广西壮族自治区中国科学院广西植物研究所 | Method for synthesizing sweet saponin with bitter and fallen grosvenor momordica fruit as raw material |
| CN104621318A (en) * | 2015-01-27 | 2015-05-20 | 张雨生 | Zero-calorie health care type siraitia grosvenorii candy and preparation method thereof |
| CN105168387A (en) * | 2015-09-15 | 2015-12-23 | 崇州市地龙海龙生物制品开发研究所 | Method for preparing preparation for treating mastitis |
| CN106350564A (en) * | 2015-07-20 | 2017-01-25 | 中国科学院天津工业生物技术研究所 | Synthesis method of terpenoid and glycosylation products thereof in synthesis route of mogrol |
-
2018
- 2018-12-15 CN CN201811535855.9A patent/CN109527175A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1437128A1 (en) * | 2003-01-07 | 2004-07-14 | Michael Kaufmann | Pellet made from a matrix comprising tee as starting material and its method of preparation |
| CN101204221A (en) * | 2006-12-19 | 2008-06-25 | 张雨生 | Sugar free health care grosvenori crystal and manufacture method thereof |
| CN103461812A (en) * | 2012-11-07 | 2013-12-25 | 张雨生 | Sugarless sweet glutinous rice soft cake with health-care function |
| CN103461446A (en) * | 2012-11-07 | 2013-12-25 | 张雨生 | Healthcare sugarless sweet biscuit |
| CN104059959A (en) * | 2013-03-20 | 2014-09-24 | 广西壮族自治区中国科学院广西植物研究所 | Method for synthesizing sweet saponin with bitter and fallen grosvenor momordica fruit as raw material |
| CN104621318A (en) * | 2015-01-27 | 2015-05-20 | 张雨生 | Zero-calorie health care type siraitia grosvenorii candy and preparation method thereof |
| CN106350564A (en) * | 2015-07-20 | 2017-01-25 | 中国科学院天津工业生物技术研究所 | Synthesis method of terpenoid and glycosylation products thereof in synthesis route of mogrol |
| CN105168387A (en) * | 2015-09-15 | 2015-12-23 | 崇州市地龙海龙生物制品开发研究所 | Method for preparing preparation for treating mastitis |
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Application publication date: 20190329 |
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