CN1094753C - 皮肤调色制剂 - Google Patents
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Abstract
本发明提供包含吸油粉、增稠剂、溶角蛋白剂和醇的皮肤清洁剂和收敛剂组合物。所述组合物也包括水、香料、着色剂、润肤剂和润湿剂。
Description
先有技术
产品使用者越来越认识到不良皮肤疾病可由本身的皮肤油脂或存在于包括化妆品在内的各种产品中的油脂所引起或所加重。最不良的皮肤疾病之一是痤疮。
先有技术的皮肤清洁组合物已试图用来吸收皮肤表面的油脂和碎屑。这些皮肤清洁组合物可归纳为油基的、乳化液型的或水基的表面活性剂系统。
油基的皮肤清洁组合物包含油和酯的混合物。由于这些组合物可能含有表面活性剂以及由于它们易在皮肤上留下一层脂膜,所以这些组合物可能是刺激性的,在敏感皮肤上使用时更是如此。乳液型的皮肤清洁组合物通常是基于一类称为乳化剂的表面活性剂。任何表面活性剂均可能是刺激性的,特别是在眼附近使用时。
水包油乳液是最常见的,但油包水乳液也是可用的。乳液型制剂包含有油和/或蜡并易造成皮肤油腻感。
为减轻这个问题,美国专利5480633尝试提供针对肥皂和表面活性剂残留物的含水洗肤制剂。其权利要求书称按该发明进行的洗面在减少皮肤的肥皂和表面活性剂的沉积方面是有效的。
美国专利4640932公开了一种组合物,该组合物含有一种含过氧化苯甲酰作为主要活性成分的独特的面膜,其提供了出人意外的有效的、高效率的和可接受的用以控制和减轻易于感染普通痤疮的个体的方法。
现在已存在试图通过吸油粉末显著控制油性面上发光的产品。这些产品并不具有消毒性,此外由于其粘的、白垩状外观和/或缺乏均匀性,这些产品美观上并不具吸引力。
本发明提供具有收敛性、消毒性、脱油性的、持久控油的无油(nonoilly)留存(leave-on)皮肤清洁组合物。
本发明概述
本发明提供具收敛性、消毒性和脱油性的留存皮肤清洁组合物。所述组合物包含作为基本组份的吸油粉、增稠剂和溶角蛋白剂以及醇。本发明的组合物也包括水、香料、着色剂、润肤剂和润湿剂。吸油粉的量为约1-约3%(重量)、增稠剂的量为约0.1-约1%(重量)、溶角蛋白剂的量为约0.01-约2%(重量)、醇的量为约10-约40%(重量)。
本发明也提供制备本发明组合物的方法。先将吸油粉和增稠剂在水中混合成悬浮液。并将这种悬浮液的pH调到约3-约4。将溶角蛋白剂溶于醇中形成酸-醇混合物并将其pH调到约3-约4。将所述悬浮液和酸-醇混合物合并,并将pH调到约3-约4。将润湿剂和所述悬浮液混合,将润肤剂和所述酸-醇混合物混合。
本发明还提供清洁皮肤的方法。该方法包括下列步骤:将有效量的本发明的组合物涂抹到皮肤上,让涂抹的组合物完全干燥,然后让干燥的组合物在涂抹的皮肤上继续吸油和控制油光。
优选实施方案的叙述
本发明的新组合物提供了具有收敛性、消毒性和脱油性的水性局部用制剂。
所述新组合物包括在适合载体中的四类基本成份。这四类成份一般被称为吸油粉、增稠剂、溶角蛋白剂和低级烷基醇。
吸油粉是可除去皮肤的油分泌物的任何物质。吸油粉的例子包括玉米淀粉、燕麦片、滑石、涂盖硅石的云母、涂盖二氧化钛的云母和和水辉石型粘土。吸油粉存在的量为约1-约3%(重量),优选约1.8-2.2%(重量)。
此中所用的术语“水辉石型粘土”包括天然存在的和合成的水辉石粘土,例如可从Southern Clay Products,Inc.购买的品名为LaponiteXLS和XLG的水辉石粘土。它们在本领域为人熟知并用于个人护理和化妆品领域,即用于诸如香波、面膜、润肤乳和化妆品等产品中。一些Laponite的优点包括改善洗剂和乳膏的用法和触感,稳定乳液、悬浮液和溶液,减少乳液的油腻感和用作脂和油的吸收剂。因为Laponite不仅赋予所述组合物更好的触感而且提供了即刻可见的吸收皮肤油脂的感性效果,所以Laponite是一种优选的吸油粉。
本发明的组合物也包括增稠剂。增稠剂的例子包括由膨润土、聚羧乙烯制剂、角叉菜胶、地蜡、糊精、明胶和纤维素树脂如黄原胶构成的增稠剂。存在的增稠剂的量为约0.1-约1%(重量)、优选约0.23-约0.27%(重量)。
黄原胶是商品名为Keltrol的可购商品。黄原胶是已在食品和制药领域应用的一种高分子量多糖。作为商品提供的黄原胶颗粒物的一般粒径范围为75-250μm。由于其极大的悬浮活性和极小的粘度,黄原胶是一种优选的增稠剂。
本发明的组合物也包括溶角蛋白剂。这种剂的实例包括水杨酸、硼酸和水杨酸甲酯。溶角蛋白剂存在的量为约0.01-约2%(重量)、优选约0.5-约1.5%(重量)。
水杨酸通常被称为局部溶角蛋白剂并外用作消毒剂和杀真菌剂。水杨酸起收敛剂的作用并且通过降低其粘着性或粘结力来加速角质细胞的去除。由于水杨酸集最佳功效与防腐为一体并同时提供了增溶作用的便易,所以水杨酸是一种优选的溶角蛋白剂。
醇,特别是低级烷基醇,是本发明新组合物的基本成份。所述醇的例子包括乙醇、异丙醇和其混合物。所述醇适合作为所述溶角蛋白剂的溶媒并且起防腐剂和收敛剂的作用。在所述组合物中该醇的存在量为约10-约40%(重量),优选约20-约30%(重量)。
除基本成份外,本发明的组合物也可包含非基本成份。这些成份一般是润湿剂、润肤剂、着色剂、香料等。
可包括于本发明组合物中的润肤剂依其保持在皮肤表面或在角质层中的能力而起润滑剂的作用、减少剥落的作用和改善皮肤外观的作用。典型的润肤剂包括脂肪酯、脂肪醇、矿物油、聚醚硅氧烷共聚物等等。润肤剂的例子包括(但不限于)PPG-15十八烷醚,PPG-10十六烷醚、steareth-10、oleth-8和PPG-4月桂醚。优选的润肤剂是PPG-15十八烷醚,存在的量多至约5%(重量),优选约2.5%(重量),其中润肤剂如PPG-15十八烷醚的量还可为多至约0.5%(重量)。
多元醇型的润湿剂可包括于本发明的组合物。所述润湿剂有助于提高润肤剂的效能、减少脱皮、促进积屑的去除和改善皮肤触感。典型的多元醇包括丙三醇(也称为甘油)、聚烷二醇,更优选的是alkelene多元醇和其衍生物,包括丙二醇、二丙二醇、聚丙二醇、聚乙二醇和其衍生物、山梨醇、羟丙基山梨醇、己二醇、二聚1,3-丁二醇(1,3-dibutylene glycol)、1,2,6-己三醇、乙氧基化甘油、丙氧基化甘油和其混合物。为得到最佳效果,优选使用二聚1,3-丁二醇,其存在的量多至约5%(重量),优选多至约2.5%(重量)。其中润湿剂如二聚1,3-丁二醇的量还可为多至约0.5%(重量)。
另外的非基本组份包括为人熟知的着色剂如FD&C Blue#1和D&C Yellow#10以及香料如桉树油、合成樟脑、薄荷油和丁子香油。为达到最佳效果,着色剂可按需添加,其量多至约1%(重量)、优选多至约0.5%(重量)。香料可按需加入,其量多至约0.5%(重量),优选多至约0.36%(重量)。
按照本发明,所述吸油粉、增稠剂和溶角蛋白剂与适合的溶媒或载体系统混合。对吸油粉和增稠剂来说优选的载体包括水。将水按需要量混合,溶角蛋白剂则和醇混合。如需用非基本组份,则将它们混入适合的溶媒或载体系统中。对于润湿剂来说优选的载体包括水,对于润肤剂和香料来说则是醇。
首先将吸油粉和增稠剂在水中混合成悬浮液。润湿剂也可任选地加入混合。混合后,使用本领域熟知的酸将pH调节到约3-约4。优选的酸是柠檬酸。
将溶角蛋白剂混于醇中形成酸-醇混合物。润肤剂和香料也可任选地混入到酸-醇混合物中。混合后,用本领域熟知的碱将pH调节到约3-约4。优选的碱是氢氧化钾。
将所述水悬浮液和酸-醇混合物合并。着色剂可任选地混入,并将pH调节到约3-约4,优选约3.3-约3.5。
本发明的新组合物产生皮肤清洁收敛、消毒和脱油的制剂。这种制剂是水性悬浮液,它可以作为留存皮肤清洁剂使用。将本发明的组合物涂抹到脸(或其它皮肤表面)上并让其完全干燥。让干燥的组合物留存在皮肤表面上继续吸油和控制油光。
根据下列实施例来进一步阐述本发明:
相 组分 %(重量)
A 水 q.s.至100
Laponite 2
黄原胶 0.25
二聚1,3-丁二醇 2
B 乙醇 20
水杨酸 2
PPG-15十八烷醚 2
A+B 香料 q.s.
着色剂 q.s.
缩写词“q.s.”是指标准配药处方用语,指“适量”或“足量”。相A
在室温下将Laponite分散在水中并混合足够时间至分散。然后也在室温下将黄原胶加到分散液中并再混合足够时间直到分散液变稠。或者也可先分散黄原胶再加入Laponite。二聚1,3-丁二醇可任选地在分散液形成过程中加入。用酸将分散液的pH调节到约3-约4。相B
在室温下,将水杨酸和乙醇相混合直到酸溶解于醇中。可任选地加入PPG-15十八烷醚和香料。用碱将pH调节到约3-约4。相A+B
将相A和B相混合并任选地加入着色剂。通过加入适当的酸或碱将pH调节到约3.3-约4。在生产时目标pH是约3.5。
尽管本说明书叙述了本发明的原理,可以理解在本发明范围内的其它方面、优点和更改对本领域技术人员来说是显而易见的。
Claims (18)
1.皮肤清洁剂和收敛剂组合物,包括:
量为1-3重量%的吸油粉;
量为0.1-1重量%的增稠剂;
量为0.01-2重量%的溶角蛋白剂;
量为10-40重量%的醇,所述醇选自乙醇和异丙醇;和
适量水、香料和着色剂,其中所述组合物的pH被调节到3-4。
2.权利要求1的组合物,还包含多至0.5重量%的润肤剂。
3.权利要求1的组合物,还包含多至0.5重量%的润湿剂。
4.权利要求2的组合物,还包含多至0.5重量%的润湿剂。
5.皮肤清洁剂和收敛剂组合物,包含:
量为1-3重量%的水辉石型粘土;
量为0.1-1重量%的黄原胶;
量为0.1-2重量%的水杨酸;
量为10-40重量%的醇,所述醇选自乙醇和异丙醇;和
适量水、香料和着色剂,其中所述组合物的pH调节到3-4。
6.权利要求5的组合物,还包括多至0.5重量%的PPG-15十八烷醚。
7.权利要求5的组合物,还包括多至0.5重量%的二聚1,3-丁二醇。
8.权利要求6的组合物,还包括多至0.5重量%的二聚1,3-丁二醇。
9.皮肤清洁剂和收敛剂组合物,包括:
2重量%合成锂皂石;
0.25重量%黄原胶;
2重量%水杨酸;
20重量%低级烷基醇;和
适量水、香料和着色剂,其中所述组合物的pH调节到3-4。
10.权利要求9的组合物,还包括2重量%的PPG-15十八烷醚。
11.权利要求9的组合物,还包括2重量%的二聚1,3-丁二醇。
12.权利要求10的组合物,还包括2重量%的二聚1,3-丁二醇。
13.通过下列步骤制备的皮肤清洁剂和收敛剂组合物:
将1-3重量%量的吸油粉和0.1-1重量%量的增稠剂在水中混合形成悬浮液,并将所述悬浮液的pH调节到3-4;
将0.01-2重量%的溶角蛋白剂溶于10-40重量%的醇中形成酸-醇混合物,所述醇选自乙醇和异丙醇,将所述混合物的pH调节到3-4;和
将所述悬浮液和所述酸-醇混合物合并形成所述组合物,并将所述组合物的pH调节到3-4。
14.权利要求13的组合物,其制备步骤还包括将多至0.5重量%的润湿剂混入所述悬浮液中。
15.权利要求13的组合物,其制备步骤还包括将多至0.5重量%的润肤剂和多至至0.50重量%的香料与所述酸-醇混合物混合。
16.通过下列步骤制备的皮肤清洁剂和收敛剂组合物:
将1-3重量%量的合成锂皂石和0.1-1重量%的黄原胶在水中混合成悬浮液,并将所述悬浮液的pH调节到3-4;
将0.01-2重量%的水杨酸溶于10-40重量%低级烷基醇中形成酸-醇混合物,所述低级烷基醇选自乙醇和异丙醇,并将所述混合物的pH调节到3-4;和
将所述悬浮液和所述酸-醇混合物合并形成所述组合物,并将所述组合物的pH调节到3-4。
17.权利要求16的组合物,其制备步骤还包括将多至0.5重量%的二聚1,3-丁二醇与所述悬浮液混合。
18.权利要求16的组合物,其制备步骤还包括将多至0.5重量%的PPG-15十八烷醚和多至0.50重量%的香料与所述酸-醇混合物混合。
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Application Number | Priority Date | Filing Date | Title |
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US08/609,016 US5871764A (en) | 1996-02-29 | 1996-02-29 | Skin toning formulation |
US08/609,016 | 1996-02-29 |
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CN1216916A CN1216916A (zh) | 1999-05-19 |
CN1094753C true CN1094753C (zh) | 2002-11-27 |
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Application Number | Title | Priority Date | Filing Date |
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CN97194113A Expired - Fee Related CN1094753C (zh) | 1996-02-29 | 1997-02-28 | 皮肤调色制剂 |
Country Status (21)
Country | Link |
---|---|
US (1) | US5871764A (zh) |
EP (1) | EP0918505B1 (zh) |
JP (1) | JP2001508396A (zh) |
KR (1) | KR19990087390A (zh) |
CN (1) | CN1094753C (zh) |
AR (1) | AR006050A1 (zh) |
AT (1) | ATE217520T1 (zh) |
AU (1) | AU717000B2 (zh) |
BR (1) | BR9707894A (zh) |
CO (1) | CO4780016A1 (zh) |
CZ (1) | CZ271798A3 (zh) |
DE (1) | DE69712624T2 (zh) |
DK (1) | DK0918505T3 (zh) |
ES (1) | ES2176700T3 (zh) |
IL (1) | IL125920A0 (zh) |
MY (1) | MY129958A (zh) |
PL (1) | PL328867A1 (zh) |
PT (1) | PT918505E (zh) |
TW (1) | TW510801B (zh) |
WO (1) | WO1997031619A1 (zh) |
ZA (1) | ZA971788B (zh) |
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DE19816664A1 (de) * | 1998-04-15 | 1999-10-21 | Henkel Kgaa | Mild abrasive Hautreinigungsmittel |
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FR2804018B1 (fr) | 2000-01-24 | 2008-07-11 | Oreal | Composition sans transfert structuree sous forme rigide par un polymere |
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US6670313B1 (en) | 2000-06-05 | 2003-12-30 | Colormetric Laboratories, Inc. | Method and composition for minimizing percutaneous absorption of industrial chemicals |
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US6482446B2 (en) | 2000-12-01 | 2002-11-19 | Neutrogena Corporation | Astringent composition and method of use |
WO2002047624A1 (en) * | 2000-12-12 | 2002-06-20 | L'oreal Sa | Cosmetic compositions containing at least one heteropolymer and at least one gelling agent and methods of using the same |
US7276547B2 (en) * | 2000-12-12 | 2007-10-02 | L'oreal S.A. | Compositions comprising heteropolymers and at least one oil-soluble polymers chosen from alkyl celluloses and alkylated guar gums |
US20020107314A1 (en) * | 2000-12-12 | 2002-08-08 | Carlos Pinzon | Compositions containing heteropolymers and oil-soluble esters and methods of using same |
US6835399B2 (en) * | 2000-12-12 | 2004-12-28 | L'ORéAL S.A. | Cosmetic composition comprising a polymer blend |
WO2002047623A1 (en) | 2000-12-12 | 2002-06-20 | L'oreal Sa | Composition comprising at least one heteropolymer and at least one inert filler and methods for use |
AU2002217252A1 (en) * | 2000-12-12 | 2002-06-24 | L Oreal | Cosmetic composition comprising a mixture of polymers |
FR2817740B1 (fr) * | 2000-12-12 | 2006-08-04 | Oreal | Procede de fabrication d'une composition cosmetique coloree de maquillage a transmittance controlee |
US6881400B2 (en) * | 2000-12-12 | 2005-04-19 | L'oreal S.A. | Use of at least one polyamide polymer in a mascara composition for increasing the adhesion of and/or expressly loading make-up deposited on eyelashes |
WO2002047626A1 (en) * | 2000-12-12 | 2002-06-20 | L'oreal Sa | Cosmetic composition comprising heteropolymers and a solid substance and method of using same |
US20020111330A1 (en) * | 2000-12-12 | 2002-08-15 | Carlos Pinzon | Compositions containing heteropolymers and methods of using same |
US8080257B2 (en) | 2000-12-12 | 2011-12-20 | L'oreal S.A. | Cosmetic compositions containing at least one hetero polymer and at least one film-forming silicone resin and methods of using |
FR2817739B1 (fr) * | 2000-12-12 | 2005-01-07 | Oreal | Composition cosmetique coloree transparente ou translucide |
AU2001225392A1 (en) * | 2000-12-13 | 2002-06-24 | L Oreal | Composition structured with a polymer containing a heteroatom and an organogelator |
FR2819400B1 (fr) * | 2001-01-15 | 2004-12-03 | Oreal | Composition cosmetique de maquillage ou de soin des matieres keratiniques comprenant un melange de polymeres |
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US20030059446A1 (en) * | 2001-09-18 | 2003-03-27 | Kulkarni Arun B. | Physically stable sprayable gel composition |
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US20080057011A1 (en) * | 2001-12-12 | 2008-03-06 | L'oreal S.A., | Composition structured with a polymer containing a heteroatom and an Organogelator |
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US20040042980A1 (en) * | 2002-06-12 | 2004-03-04 | L'oreal | Cosmetic emulsions containing at least one hetero polymer and at least one sunscreen, and methods of using same |
US7008629B2 (en) * | 2002-07-22 | 2006-03-07 | L'ORéAL S.A. | Compositions comprising at least one heteropolymer and fibers, and methods of using the same |
US20040166133A1 (en) * | 2003-01-21 | 2004-08-26 | L'oreal | Method of making a mascara composition comprising polyamide polymer and at least one solid substance having a melting point of 45oC or greater |
US20040191330A1 (en) * | 2003-03-31 | 2004-09-30 | Keefe Candace R. | Daily skin care regimen |
US20060074029A1 (en) * | 2004-10-04 | 2006-04-06 | Scott Leece | Topical antimicrobial composition having improved moisturization properties |
US20100040654A1 (en) * | 2005-03-21 | 2010-02-18 | Masoomeh Wake | Exfoliating and moisturizing composition and method |
US20060210519A1 (en) * | 2005-03-21 | 2006-09-21 | Masoomeh Wake | Exfoliating and moisturizing composition and method |
AR065378A1 (es) * | 2007-02-16 | 2009-06-03 | Procter & Gamble | Articulo absorbente con locion que comprende un material de polipropilenglicol |
US8609601B2 (en) * | 2008-11-20 | 2013-12-17 | Conopco Inc. | Personal cleansing composition |
US8673837B2 (en) | 2009-08-17 | 2014-03-18 | Conopco Inc. | Shaped solid cleaning composition |
FR2960427B1 (fr) * | 2010-05-26 | 2015-03-27 | Oreal | Composition cosmetique comprenant une huile et un polymere portant tous deux un groupe de jonction generateur de liaisons hydrogene, et procede de traitement cosmetique |
FR2960434B1 (fr) * | 2010-05-26 | 2012-08-17 | Oreal | Composition cosmetique a base d'un polymere supramoleculaire et d'un charge absorbante |
EP2822532B1 (en) | 2012-03-09 | 2018-09-19 | Covestro Deutschland AG | Aqueous polyurethane dispersion in the treatment of acne |
EP3641725A1 (en) | 2017-06-23 | 2020-04-29 | The Procter and Gamble Company | Composition and method for improving the appearance of skin |
CN112437657A (zh) | 2018-07-03 | 2021-03-02 | 宝洁公司 | 处理皮肤状况的方法 |
US10959933B1 (en) | 2020-06-01 | 2021-03-30 | The Procter & Gamble Company | Low pH skin care composition and methods of using the same |
US11583488B2 (en) | 2020-06-01 | 2023-02-21 | The Procter & Gamble Company | Method of improving penetration of a vitamin B3 compound into skin |
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US4640932A (en) * | 1985-03-18 | 1987-02-03 | Neutrogena Corporation | Compositions for treating acne vulgaris and methods of making and using same |
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JP2865320B2 (ja) * | 1989-08-07 | 1999-03-08 | 株式会社資生堂 | 固型化粧料組成物 |
KR940001127B1 (ko) * | 1989-10-19 | 1994-02-14 | 가부시키가이샤 시세이도 | 친수성 중합체-실리케이트 광물 복합체 및 이의 용도 |
US5139782A (en) * | 1991-12-23 | 1992-08-18 | Uop | Facial cleansing mineral compositions |
US5422112A (en) * | 1994-06-09 | 1995-06-06 | Chesebrough-Pond's Usa Co., Division Of Conopco, Inc. | Thickened cosmetic compositions |
US5534265A (en) * | 1994-08-26 | 1996-07-09 | The Procter & Gamble Company | Thickened nonabrasive personal cleansing compositions |
US5702709A (en) * | 1995-04-18 | 1997-12-30 | Enviroderm Pharmaceuticals, Inc. | Skin allergen and irritant barrier lotion |
-
1996
- 1996-02-29 US US08/609,016 patent/US5871764A/en not_active Expired - Lifetime
-
1997
- 1997-02-26 CO CO97010282A patent/CO4780016A1/es unknown
- 1997-02-28 DK DK97907923T patent/DK0918505T3/da active
- 1997-02-28 AR ARP970100819A patent/AR006050A1/es active IP Right Grant
- 1997-02-28 KR KR1019980706805A patent/KR19990087390A/ko not_active Application Discontinuation
- 1997-02-28 EP EP97907923A patent/EP0918505B1/en not_active Expired - Lifetime
- 1997-02-28 JP JP53112297A patent/JP2001508396A/ja active Pending
- 1997-02-28 DE DE69712624T patent/DE69712624T2/de not_active Expired - Fee Related
- 1997-02-28 PL PL97328867A patent/PL328867A1/xx unknown
- 1997-02-28 ES ES97907923T patent/ES2176700T3/es not_active Expired - Lifetime
- 1997-02-28 PT PT97907923T patent/PT918505E/pt unknown
- 1997-02-28 CZ CZ982717A patent/CZ271798A3/cs unknown
- 1997-02-28 WO PCT/US1997/003096 patent/WO1997031619A1/en not_active Application Discontinuation
- 1997-02-28 IL IL12592097A patent/IL125920A0/xx unknown
- 1997-02-28 MY MYPI97000821A patent/MY129958A/en unknown
- 1997-02-28 ZA ZA971788A patent/ZA971788B/xx unknown
- 1997-02-28 AT AT97907923T patent/ATE217520T1/de not_active IP Right Cessation
- 1997-02-28 BR BR9707894A patent/BR9707894A/pt not_active IP Right Cessation
- 1997-02-28 AU AU19799/97A patent/AU717000B2/en not_active Ceased
- 1997-02-28 CN CN97194113A patent/CN1094753C/zh not_active Expired - Fee Related
- 1997-03-24 TW TW086103658A patent/TW510801B/zh not_active IP Right Cessation
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4640932A (en) * | 1985-03-18 | 1987-02-03 | Neutrogena Corporation | Compositions for treating acne vulgaris and methods of making and using same |
Also Published As
Publication number | Publication date |
---|---|
MY129958A (en) | 2007-05-31 |
IL125920A0 (en) | 1999-04-11 |
ES2176700T3 (es) | 2002-12-01 |
AU717000B2 (en) | 2000-03-16 |
WO1997031619A1 (en) | 1997-09-04 |
ZA971788B (en) | 1998-08-28 |
DE69712624T2 (de) | 2002-10-10 |
BR9707894A (pt) | 1999-07-27 |
US5871764A (en) | 1999-02-16 |
EP0918505B1 (en) | 2002-05-15 |
CN1216916A (zh) | 1999-05-19 |
AR006050A1 (es) | 1999-07-21 |
AU1979997A (en) | 1997-09-16 |
CZ271798A3 (cs) | 1999-03-17 |
JP2001508396A (ja) | 2001-06-26 |
CO4780016A1 (es) | 1999-05-26 |
PL328867A1 (en) | 1999-03-01 |
EP0918505A1 (en) | 1999-06-02 |
DE69712624D1 (de) | 2002-06-20 |
ATE217520T1 (de) | 2002-06-15 |
TW510801B (en) | 2002-11-21 |
DK0918505T3 (da) | 2002-09-09 |
PT918505E (pt) | 2002-09-30 |
KR19990087390A (ko) | 1999-12-27 |
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