CN109279779A - A kind of preparation method of full space of a whole page dark color ceramic tile - Google Patents
A kind of preparation method of full space of a whole page dark color ceramic tile Download PDFInfo
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- CN109279779A CN109279779A CN201811218633.4A CN201811218633A CN109279779A CN 109279779 A CN109279779 A CN 109279779A CN 201811218633 A CN201811218633 A CN 201811218633A CN 109279779 A CN109279779 A CN 109279779A
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Classifications
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
- C03C8/20—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions containing titanium compounds; containing zirconium compounds
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/52—Multiple coating or impregnating multiple coating or impregnating with the same composition or with compositions only differing in the concentration of the constituents, is classified as single coating or impregnation
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/89—Coating or impregnation for obtaining at least two superposed coatings having different compositions
Abstract
The invention discloses a kind of preparation methods of full space of a whole page dark color ceramic tile, are sequentially prepared ground glaze layer, color glaze layer, decorative pattern, cover coat in billet surface, then dry, are fired into full space of a whole page dark color ceramic tile finished product.The present invention prepares full space of a whole page dark color ceramic tile using the technique that roller+ink-jet combines, and the defect problem of dark marble pattern ink-jet bracing wire, two tone colour can be effectively solved, so that clear patterns, stereovision are strong.
Description
Technical field
The present invention relates to ceramic tile preparation field more particularly to a kind of preparation methods of full space of a whole page dark color ceramic tile.
Background technique
With the development of manufacturing technology, the decoration of ceramic tile is also more and more abundant.People are also increasingly dedicated to imitating natural
Stone material, however, common imitation stone brick, is all not have three-dimensional sense in one layer pattern of surface printing, need to improve.
Since ceramic tile production used ink-jet technology after, although pattern definition, in terms of compare silk screen
(roller) has a great-jump-forward progress, but ink-jet technology is there is also one very big defect, for the ceramic tile of the pattern of the dark full space of a whole page,
In process of production because of the dosage of increasing ink-jet ink, causes ceramic tile to be easy to appear bracing wire between spray head, influence the whole of ceramic tile
Body quality.
Summary of the invention
Technical problem to be solved by the present invention lies in provide a kind of preparation method of full space of a whole page dark color ceramic tile, method
Simply, high-efficient, ceramic tile surface pattern texture obtained understands, bracing wire defect does not occur.
In order to solve the above-mentioned technical problems, the present invention provides a kind of preparation methods of full space of a whole page dark color ceramic tile, comprising:
(1) color glaze is prepared, it is 4-6 parts of calcined alumina, 2-4 parts quartzy by 45-50 parts of albite, 14-18 parts of dolomite,
Talcum 3-6 parts is burnt, 1-2 parts of calcining zinc oxide, 5-8 parts of kaolin, 10-13 parts of addition ball mills of clear frit are milled to default
Color glaze glaze slip is obtained after fineness；
(2) green body, ground coat enamel glaze slip, overglaze glaze slip and ink-jet ink are prepared respectively；
(3) ground coat enamel glaze slip is applied to form ground glaze layer in the billet surface of drying；
(4) roller printing technique is used to print color glaze glaze slip on the ground glaze layer to form color glaze layer, the face of color glaze layer
The 50-70% of light color of color ratio ceramic tile；
(5) ink-jet ink is printed on the color glaze layer using ink-jetting process, to form pattern；
(6) apply overglaze glaze slip in billet surface, to form cover coat；
(7) green body for obtaining step (6) is dried；
(8) green body for obtaining step (7) is burnt into, and obtains full space of a whole page dark color ceramic tile.
As an improvement of the above scheme, in step (4), the specific gravity of the color glaze glaze slip is 1.4-1.55g/ml, and flow velocity is
18-25 seconds.
As an improvement of the above scheme, in step (4), the glaze volume of the color glaze glaze slip is 110-130g/m2。
As an improvement of the above scheme, the chemical component of the color glaze glaze slip are as follows: SiO240-45%, Al2O316-19%,
Fe2O30.1-0.3%, TiO20.01-0.05%, CaO 6-8%, MgO 2-4%, K2O 1.5-3%, Na2O 2.0-3.5%,
ZnO 1-2%, surplus are impurity.
As an improvement of the above scheme, the ground coat enamel glaze slip is mixed by 70%XKB-938A and 30%XKB-954；
The XKB-938A is prepared by the raw material of following parts by weight: 35-40 parts of potassium feldspar, calcined alumina 15-18
Part, it is 6-9 parts of kaolin, wollastonite in powder 5-8,6-8 parts quartzy, 8-10 parts of calcined kaolin；
The XKB-954 is prepared by the raw material of following parts by weight: 18-22 parts of albite, 25-30 parts of potassium feldspar, being forged
Aluminium oxide 4-7 parts of burning, it is 6-9 parts of kaolin, 5-8 parts of wollastonite in powder, 10-15 parts quartzy, 5-8 parts of calcined kaolin.
As an improvement of the above scheme, in step (3), the specific gravity of the ground coat enamel glaze slip is 1.85-1.88g/ml, and flow velocity is
30-35 seconds.
As an improvement of the above scheme, in step (3), the glaze volume of the ground coat enamel is 500-530g/m2。
As an improvement of the above scheme, the overglaze glaze slip by 35%KG-14,40%KG-32 and 25%KG-25 mix and
At；
The KG-14 is prepared by the raw material of following parts by weight: 20-25 parts of potassium feldspar 20-25 albite, calcined oxide
2-4 parts of zinc, 5-8 parts of wollastonite, 8-13 parts of dolomite, 4-8 parts of calcination of talc, 6-9 parts of barium carbonate, 5-8 parts of kaolin, calcining is high
Soil 4-7 parts of ridge, 8-12 parts of clear frit；
The KG-32 is prepared by the raw material of following parts by weight: potassium feldspar 20-25,18-22 parts of albite, calcines oxygen
Change zinc 4-6 parts, 8-12 parts of wollastonite, 8-10 parts of dolomite, 6-8 parts of calcination of talc, 7-10 parts of barium carbonate, 6-8 parts of kaolin, forges
Burn kaolin 4-7 parts, 6-10 parts of clear frit；
The KG-25 is prepared by the raw material of following parts by weight: potassium feldspar 20-25,18-22 parts of albite, calcines oxygen
Zinc 4-6 parts of change, 12-16 parts of wollastonite, 12-15 parts of calcination of talc, 4-6 parts of barium carbonate, 3-5 parts of strontium carbonate, 6-8 parts of kaolin,
4-7 parts of calcined kaolin, 5-8 parts of clear frit.
As an improvement of the above scheme, in step (6), the specific gravity of the overglaze glaze slip is 1.85-1.88g/ml, and flow velocity is
30-35 seconds.
As an improvement of the above scheme, in step (6), the glaze volume of the ground coat enamel is 430-460g/m2。
The invention has the following beneficial effects:
1, the present invention prepares full space of a whole page dark color ceramic tile using the technique that roller+ink-jet combines, and can effectively solve depth
Color marble pattern ink-jet bracing wire, two tone colour defect problem so that clear patterns, stereovision are strong.
2, the present invention forms the color of one layer of color 50-70% more of light color than ceramic tile using roller printing technique on ground glaze layer
Glaze layer, it is possible to reduce 25-40% ink-jet ink dosage can reduce inkjet channel gray scale by 30-40%.
Specific embodiment
To make the object, technical solutions and advantages of the present invention clearer, the present invention will be made below further detailed
Description.
A kind of preparation method of full space of a whole page dark color ceramic tile provided by the invention, comprising the following steps:
(1) color glaze is prepared, it is 4-6 parts of calcined alumina, 2-4 parts quartzy by 45-50 parts of albite, 14-18 parts of dolomite,
Talcum 3-6 parts is burnt, 1-2 parts of calcining zinc oxide, 5-8 parts of kaolin, 10-13 parts of addition ball mills of clear frit are milled to default
Color glaze glaze slip is obtained after fineness；
Ground coat enamel glaze slip of the invention is prepared by the raw material of following parts by weight: 45-50 parts of albite, dolomite 14-18
Part, 4-6 parts of calcined alumina, 2-4 parts quartzy, talcum 3-6 parts of burning, 1-2 parts of calcining zinc oxide, 5-8 parts of kaolin, clear frit
10-13 parts.
The chemical component of the color glaze glaze slip are as follows: SiO240-45%, Al2O316-19%, Fe2O30.1-0.3%,
TiO20.01-0.05%, CaO 6-8%, MgO 2-4%, K2O 1.5-3%, Na2O 2.0-3.5%, ZnO 1-2%, surplus
For impurity.
(2) green body, ground coat enamel glaze slip, overglaze glaze slip and ink-jet ink are prepared respectively；
Wherein, there is no special limitation for the raw material of the specific formula of green body and use, those skilled in the art can
It is selected according to the corresponding condition of production；Preferably, using Imitation Rock Porcelain Tiles body recipe, and green body thermal expansion coefficient and glaze of the present invention
It is adapted, the defect that glaze is split is not occurred with guarantee.
Preferably, the ground coat enamel glaze slip is mixed by 70%XKB-938A and 30%XKB-954；The XKB-938A by
The raw material of following parts by weight is prepared: 35-40 parts of potassium feldspar, 15-18 parts of calcined alumina, and 6-9 parts of kaolin, wollastonite in powder
5-8, it is 6-8 parts quartzy, 8-10 parts of calcined kaolin；The XKB-954 is prepared by the raw material of following parts by weight: albite
It is 18-22 parts, 25-30 parts of potassium feldspar, 4-7 parts of calcined alumina, 6-9 parts of kaolin, 5-8 parts of wollastonite in powder, 10-15 parts quartzy,
5-8 parts of calcined kaolin.Kaolin, zinc oxide, talcum can be effectively removed using kaolin, calcined alumina, wollastonite in powder is burnt
The glaze of good properties is prepared in impurity in powder.
The overglaze glaze slip is mixed by 35%KG-14,40%KG-32 and 25%KG-25；The KG-14 is by following
The raw material of parts by weight is prepared: 20-25 parts of potassium feldspar 20-25 albite, 2-4 parts of calcining zinc oxide, 5-8 parts of wollastonite, white
8-13 parts of marble, 4-8 parts of calcination of talc, 6-9 parts of barium carbonate, 5-8 parts of kaolin, 4-7 parts of calcined kaolin, clear frit 8-12
Part；The KG-32 is prepared by the raw material of following parts by weight: potassium feldspar 20-25, and 18-22 parts of albite, calcining zinc oxide 4-
6 parts, 8-12 parts of wollastonite, 8-10 parts of dolomite, 6-8 parts of calcination of talc, 7-10 parts of barium carbonate, 6-8 parts of kaolin, calcine kaolinite
It is 4-7 parts native, 6-10 parts of clear frit；The KG-25 is prepared by the raw material of following parts by weight: potassium feldspar 20-25, albite
18-22 parts, 4-6 parts of calcining zinc oxide, 12-16 parts of wollastonite, 12-15 parts of calcination of talc, 4-6 parts of barium carbonate, strontium carbonate 3-5
Part, 6-8 parts of kaolin, 4-7 parts of calcined kaolin, 5-8 parts of clear frit.
The present invention is used using albite, talcum as the glaze formula system of main fluxing, can be melted at a lower temperature
Change, good glaze paint is prepared；And the glaze paint in the present invention is transparent glaze paint, can preferably show the effect of decoration.
Preferably, the chemical component of the overglaze glaze slip are as follows: SiO245.6-52.7%, Al2O312-17%, Fe2O3
0.1-0.2%, TiO20.2-0.5%, CaO 5-7.5%, MgO 0.3-0.7%, K2O 2.7-5.8%, Na2O 3.6-
5.3%, ZnO 3-5%, SrO 7-9%, ZrO23-5%, surplus are impurity.It can be seen that from the chemical component of overglaze glaze slip
Na in the present invention2O, the alkali metal oxide contents such as ZnO, SrO are higher, therefore it can be melted at a lower temperature.Simultaneously originally
Also contain a small amount of MgO in the glaze of invention, the melting temperature of glaze paint, but the MgO or work of too high amount can be significantly reduced
The zirconium for being for mineralizer is precipitated, and forms opacifying effect, therefore the additional amount of talcum is controlled in the present invention.Preferably, the overglaze
The fineness of glaze slip is that 325 meshes tail over 0.4-0.7%, specific gravity 1.88-1.93g/ml, and flow velocity is 30-38 seconds.This fineness range
There is interior glaze slip relatively good mobility can be dispersed in ceramic tile blank surface during glazing；Tool is prepared
There is the glaze paint of superperformance.
Wherein, the ink-jet ink is using ink common in the market, if Caro is than the TSG-40001 type that sub- company produces
Number ink-jet ink etc., those skilled in the art can select adaptable ink according to the color effect of brick mask body.
(3) ground coat enamel glaze slip is applied to form ground glaze layer in the billet surface of drying；
The present invention is not particularly limited the technique for applying ground coat enamel to billet surface, can be used and the side such as drenches glaze, glaze spraying, gets rid of glaze
Formula carries out.Preferably, using the glazing mode of leaching glaze, leaching glaze is specifically carried out using bell jar.Bell jar leaching glaze can effectively ensure glaze
Material is uniformly distributed, and can recycle extra glaze slip, saves cost.
Preferably, the specific gravity of ground coat enamel glaze slip is 1.85-1.88g/ml, and flow velocity is 30-35 seconds, and the glaze volume of the ground coat enamel is
500-530g/m2.Suitable glaze slip specific gravity, flow velocity and glaze volume can to form color in process of osmosis in color glaze slurry equal
Even color glaze layer.
More preferably, the specific gravity of ground coat enamel glaze slip is 1.86-1.87g/ml, and flow velocity is 32-34 seconds, and the glaze volume of the ground coat enamel is
505-520g/m2。
(4) roller printing technique is used to print color glaze glaze slip on the ground glaze layer to form color glaze layer, the face of color glaze layer
The 50-70% of light color of color ratio ceramic tile.
Preferably, the specific gravity of color glaze is 1.4-1.55g/ml, and flow velocity is 18-25 seconds, and the glaze volume of the color glaze is 110-
130g/m2.In roller printing technique, the effect of the flow velocity lifting key of color glaze, when the flow velocity of color glaze exceeds above range,
The glaze slip performance that will affect color glaze makes glaze slip precipitating or network blocking, pattern two tone colour occur.Further, suitable glaze volume energy
So that forming the uniform color glaze layer of color in process of osmosis in color glaze slurry, guarantee that the color of color glaze layer is more of light color than ceramic tile
50-70%.
More preferably, the specific gravity of color glaze is 1.45-1.50g/ml, and flow velocity is 19-23 seconds, and the glaze volume of the color glaze is 115-
125g/m2。
The present invention prints the color glaze of one layer of color 50-70% more of light color than ceramic tile using roller printing technique on ground glaze layer
Layer, it is possible to reduce the dosage of subsequent i alphakjet ink prevents occurring bracing wire between spray head.Preferably, the color of the color glaze compares porcelain
Brick 55-65% of light color.More preferably, the color of the color glaze more of light color than ceramic tile 60%.
(5) ink-jet ink is printed on the color glaze layer using ink-jetting process, to form pattern；
Wherein, the ink-jet ink is using ink common in the market, if Crow is than the TSG-40001 type that sub- company produces
Number ink-jet ink etc., those skilled in the art can select adaptable ink according to the color effect of brick mask body.
Preferably, ink jet printing is carried out between 40-60 DEG C；It is further preferred that carrying out ink-jet print at 40-50 DEG C
Brush, the temperature for controlling ink jet printing can accelerate the infiltration rate that brick faces ink-jet ink, reduce ink dizzy dye effect, so that
It is more life-like to permeate lines.
The green body that step (4) is obtained places preset time so that decorative pattern penetrates into color glaze layer；
Preferably, green body is placed 1-3 minutes, so that ink-jet ink penetrates sufficiently into color glaze layer；Further preferably
, green body is placed 1-2 minutes, too long standing time will affect production efficiency.
(6) apply overglaze in billet surface, to form cover coat；
Wherein, the technique for applying overglaze to billet surface is not particularly limited, leaching glaze, glaze spraying can be used, get rid of glaze, silk screen
The modes such as printing carry out.Preferably, in this step, using the glazing mode of leaching glaze, leaching glaze is specifically carried out using bell jar.Clock
Cover leaching glaze can effectively ensure being uniformly distributed for glaze, and can recycle extra glaze slip, save cost.
Preferably, the specific gravity of overglaze is 1.85-1.88g/ml, and flow velocity is 30-35 seconds, and the glaze volume of the overglaze is 430-
460g/m2, suitable glaze volume can form the suitable cover coat of thickness, provide good polishing condition；It will not cover simultaneously
Wire falling wire mark scopiform at micro concavo-convex structure, guarantee sheen brick non-skid property.
It should be noted that between step (5) and (6), it is further comprising the steps of:
(5.1) water spray step (5) resulting green body is used, the dosage of water is 112g/m2；
(5.2) the resulting green body of step 5.1 is delivered to step (6).
(7) green body for obtaining step (6) is dried；
Preferably, after drying, moisture content≤1% of the green body, it is further preferred that moisture content≤0.8%；Due to this
The glaze paint of ceramic tile in invention is thicker, therefore before entering kiln firing, needs sufficiently to dry it, to prevent brick face from cracking
The defects of.
(8) green body for obtaining step (7) is burnt into, and obtains full space of a whole page dark color ceramic tile.
Preferably, firing temperature is 1155-1200 DEG C, and firing period is 55-65 minutes, and heating rate is 5-15 DEG C/minute
Clock.It is burnt at this temperature, green body, glaze paint is enabled to sufficiently to be sintered, obtain the stable Imitation Rock Porcelain Tiles of performance.
It should be noted that flower technology is seeped in existing ink-jet, directly ink-jet ink is sprayed on ground glaze layer, for depth
The ceramic tile of the pattern of the full space of a whole page of color, the ink-jet ink of big dosage cause ceramic tile to be easy to appear bracing wire between spray head, influence ceramic tile
Overall quality.The present invention prepares full space of a whole page dark color ceramic tile using the technique that roller+ink-jet combines, and can effectively solve depth
Color marble pattern ink-jet bracing wire, two tone colour defect problem so that clear patterns, stereovision are strong.
Wherein, the technique that the present invention is combined using roller+ink-jet, it is possible to reduce 25-40% ink-jet ink dosage, ink-jet are logical
Road gray scale can reduce 30-40%.
Correspondingly, using the above method to be prepared the invention also discloses a kind of full space of a whole page dark color ceramic tile.It is described complete
Space of a whole page dark color ceramic tile includes green body and is sequentially arranged in the ground glaze layer of billet surface, color glaze layer and cover coat, in the color glaze layer
Infiltration has decorative pattern, and the color of the color glaze layer is 50-70% more of light color than ceramic tile.
Above disclosed is only a preferred embodiment of the present invention, cannot limit the power of the present invention with this certainly
Sharp range, therefore equivalent changes made in accordance with the claims of the present invention, are still within the scope of the present invention.
Claims (10)
1. a kind of preparation method of full space of a whole page dark color ceramic tile characterized by comprising
(1) color glaze is prepared, it is 4-6 parts of calcined alumina, 2-4 parts quartzy by 45-50 parts of albite, 14-18 parts of dolomite, it burns and slides
3-6 parts of stone, 1-2 parts of calcining zinc oxide, 5-8 parts of kaolin, 10-13 parts of addition ball mills of clear frit are milled to default fineness
After obtain color glaze glaze slip；
(2) green body, ground coat enamel glaze slip, overglaze glaze slip and ink-jet ink are prepared respectively；
(3) ground coat enamel glaze slip is applied to form ground glaze layer in the billet surface of drying；
(4) roller printing technique is used to print color glaze glaze slip on the ground glaze layer to form color glaze layer, the color ratio of color glaze layer
The 50-70% of light color of ceramic tile；
(5) ink-jet ink is printed on the color glaze layer using ink-jetting process, to form pattern；
(6) apply overglaze glaze slip in billet surface, to form cover coat；
(7) green body for obtaining step (6) is dried；
(8) green body for obtaining step (7) is burnt into, and obtains full space of a whole page dark color ceramic tile.
2. the preparation method of full space of a whole page dark color ceramic tile as described in claim 1, which is characterized in that in step (4), the color glaze
The specific gravity of glaze slip is 1.4-1.55g/ml, and flow velocity is 18-25 seconds.
3. the preparation method of full space of a whole page dark color ceramic tile as claimed in claim 2, which is characterized in that in step (4), the color glaze
The glaze volume of glaze slip is 110-130g/m2。
4. the preparation method of full space of a whole page dark color ceramic tile as claimed in claim 3, which is characterized in that the chemistry of the color glaze glaze slip
Ingredient are as follows: SiO240-45%, Al2O316-19%, Fe2O30.1-0.3%, TiO20.01-0.05%, CaO 6-8%,
MgO 2-4%, K2O 1.5-3%, Na2O 2.0-3.5%, ZnO 1-2%, surplus are impurity.
5. the preparation method of full space of a whole page dark color ceramic tile as described in claim 1, which is characterized in that the ground coat enamel glaze slip is by 70%
XKB-938A and 30%XKB-954 are mixed；
The XKB-938A is prepared by the raw material of following parts by weight: 35-40 parts of potassium feldspar, 15-18 parts of calcined alumina, high
Soil 6-9 parts of ridge, wollastonite in powder 5-8 is 6-8 parts quartzy, and 8-10 parts of calcined kaolin；
The XKB-954 is prepared by the raw material of following parts by weight: 18-22 parts of albite, 25-30 parts of potassium feldspar, calcining oxygen
Aluminium 4-7 parts of change, it is 6-9 parts of kaolin, 5-8 parts of wollastonite in powder, 10-15 parts quartzy, 5-8 parts of calcined kaolin.
6. the preparation method of full space of a whole page dark color ceramic tile as claimed in claim 5, which is characterized in that in step (3), the ground coat enamel
The specific gravity of glaze slip is 1.85-1.88g/ml, and flow velocity is 30-35 seconds.
7. the preparation method of full space of a whole page dark color ceramic tile as claimed in claim 6, which is characterized in that in step (3), the ground coat enamel
Glaze volume be 500-530g/m2。
8. the preparation method of full space of a whole page dark color ceramic tile as described in claim 1, which is characterized in that the overglaze glaze slip is by 35%
KG-14,40%KG-32 and 25%KG-25 are mixed；
The KG-14 is prepared by the raw material of following parts by weight: 20-25 parts of potassium feldspar 20-25 albite, calcining zinc oxide 2-
4 parts, 5-8 parts of wollastonite, 8-13 parts of dolomite, 4-8 parts of calcination of talc, 6-9 parts of barium carbonate, 5-8 parts of kaolin, calcined kaolin
4-7 parts, 8-12 parts of clear frit；
The KG-32 is prepared by the raw material of following parts by weight: potassium feldspar 20-25, and 18-22 parts of albite, calcining zinc oxide
4-6 parts, 8-12 parts of wollastonite, 8-10 parts of dolomite, 6-8 parts of calcination of talc, 7-10 parts of barium carbonate, 6-8 parts of kaolin, calcining is high
Soil 4-7 parts of ridge, 6-10 parts of clear frit；
The KG-25 is prepared by the raw material of following parts by weight: potassium feldspar 20-25, and 18-22 parts of albite, calcining zinc oxide
4-6 parts, 12-16 parts of wollastonite, 12-15 parts of calcination of talc, 4-6 parts of barium carbonate, 3-5 parts of strontium carbonate, 6-8 parts of kaolin, calcining
4-7 parts of kaolin, 5-8 parts of clear frit.
9. the preparation method of full space of a whole page dark color ceramic tile as claimed in claim 8, which is characterized in that in step (6), the overglaze
The specific gravity of glaze slip is 1.85-1.88g/ml, and flow velocity is 30-35 seconds.
10. the preparation method of full space of a whole page dark color ceramic tile as claimed in claim 9, which is characterized in that in step (6), the bottom
The glaze volume of glaze is 430-460g/m2。
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| CN111943727A (en) * | 2020-08-11 | 2020-11-17 | 佛山市三水新明珠建陶工业有限公司 | Method for manufacturing micro-marble polished ceramic chip |
| CN112592061A (en) * | 2020-12-30 | 2021-04-02 | 广西欧神诺陶瓷有限公司 | Polished glaze, ceramic tile and preparation method |
| CN113845307A (en) * | 2021-11-30 | 2021-12-28 | 佛山科海意诺陶瓷科技有限公司 | High-simulation digital mold ceramic tile and preparation method thereof |
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Effective date of registration: 20221123 Address after: 526200 Longwan Ceramic City, Xiamao Town, Sihui City, Zhaoqing City, Guangdong Province Patentee after: ZHAOQING LEHUA CERAMIC SANITARY WARE Co.,Ltd. Patentee after: Wrigley Furniture Group Co.,Ltd. Address before: 526200 Longwan Ceramic City, Xiamao Town, Sihui City, Zhaoqing City, Guangdong Province Patentee before: ZHAOQING LEHUA CERAMIC SANITARY WARE Co.,Ltd. |