CN109207339A - A kind of vinegar powder piece and preparation method thereof - Google Patents

A kind of vinegar powder piece and preparation method thereof Download PDF

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Publication number
CN109207339A
CN109207339A CN201811447619.1A CN201811447619A CN109207339A CN 109207339 A CN109207339 A CN 109207339A CN 201811447619 A CN201811447619 A CN 201811447619A CN 109207339 A CN109207339 A CN 109207339A
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China
Prior art keywords
parts
vinegar
extract
vinegar powder
powder
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CN201811447619.1A
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Chinese (zh)
Inventor
孔维海
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Nanjing Royal Plaque Biotechnology Co Ltd
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Nanjing Royal Plaque Biotechnology Co Ltd
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Priority to CN201811447619.1A priority Critical patent/CN109207339A/en
Publication of CN109207339A publication Critical patent/CN109207339A/en
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    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12JVINEGAR; PREPARATION OR PURIFICATION THEREOF
    • C12J1/00Vinegar; Preparation or purification thereof
    • C12J1/08Addition of flavouring ingredients
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12JVINEGAR; PREPARATION OR PURIFICATION THEREOF
    • C12J1/00Vinegar; Preparation or purification thereof
    • C12J1/02Vinegar; Preparation or purification thereof from wine

Abstract

The invention belongs to health medicine technical fields, and in particular to a kind of vinegar powder piece and preparation method thereof.The vinegar powder includes following content of component: 80-100 parts of vinegar powder, 20-30 parts of wax gourd extract, 20-30 parts of haw thorn extract, 20-30 parts of Thallus Laminariae (Thallus Eckloniae) extract, 12-16 parts of spirulina extract, 10-15 parts of pregelatinized starch, 7-8 parts of microcrystalline cellulose, 1-2 parts of magnesium stearate.Vinegar powder piece of the invention not only has the function of reducing blood lipid, and can provide multi-faceted nutritional support to be edible, and the vinegar powder tablet quality is stablized, and effective component content improves, and preparation method is simple, is suitble to industrialized production.

Description

A kind of vinegar powder piece and preparation method thereof
Technical field
The invention belongs to health medicine technical fields, and in particular to a kind of vinegar powder piece and preparation method thereof.
Background technique
Vinegar not only can be used as flavouring, but also be ideal health food.Existing a large amount of clinical practice proves, eats Vinegar have it is antifatigue, prevention of arterial hardening, hypertension, improve a poor appetite, promote digestion, skin maintenance and cosmetic benefits, anti-cancer and cancer-preventing, prevent sclerotin It is loose, treat calculus, relieve the effect of alcohol, diuresis the effects of.
Vinegar can be prepared by spray drying with the lesser solid vinegar powder of full of nutrition, irritation.With vinegar phase Than, lack that some irritations are strong, organic acid of high volatility in vinegar powder, and the weaker organic acid of volatility, ligustrazine, outer ring two The nutritional ingredients such as peptide and minerals are retained, and become a kind of novel healthy food material.For example, apple vinegar powder is just It has become the weight-reducing in the fashionable world, reduce the health product raw material of cholesterol.U.S. FDA is in approval apple vinegar powder in 1994 as battalion Support replenishers.
The application for a patent for invention document of application publication number CN102250747A discloses a kind of making aloe juice glutinous rice nutrition vinegar The preparation method of powder, this method include raw material cleaning, slice, it is dry, crush, fermentation, sterilizing, spray drying;It improves The depth of the utilization rate and processing of aloe and glutinous rice, avoids the loss of aloe Oryza glutinosa vinegar nutritional ingredient, it is glutinous to improve aloe The nutritive value of rice vinegar is conducive to shorten fermentation time, and body digests and assimilates it, improves its bioavilability.
The application for a patent for invention document of application publication number CN105112275A discloses a kind of mixed greens vinegar powder and its system Preparation Method, this method is using tremella powder, celery powder, spinach powder, sweet potato powder as raw material;Wine is carried out with other raw materials after sweet potato powder curing Then essence fermentation accesses acetic acid bacteria and carries out acetic fermentation, obtains vinegar liquid;Vinegar liquid is spray-dried to obtain vinegar powder.Wherein, tremella and spinach The viscosity for improving prepared vinegar liquid is added according to the proportion, so that vinegar liquid is in semifluid shape, is not necessarily in spray-drying process It is further added by thickener and stabilizer;And wall sticking phenomenon can be mitigated while improving viscosity.The product vinegar powder has color It is vivid, slightly sweet taste, delicate mouthfeel, fragrance is mellow, advantage of long shelf-life.
But the above-mentioned published patent vinegar powder is common vinegar powder, contained nutriment is single.
Summary of the invention
In order to solve the deficiencies in the prior art, the purpose of the present invention is to provide a kind of vinegar powder pieces and preparation method thereof, originally Inventing vinegar powder piece obtained not only has the function of reducing blood lipid, and multi-faceted nutritional support can be provided for eater.
To achieve the goals above, the invention adopts the following technical scheme:
A kind of vinegar powder piece, including following content of component: 80-100 parts of vinegar powder, 20-30 parts of wax gourd extract, haw thorn extract 20-30 parts, 20-30 parts of Thallus Laminariae (Thallus Eckloniae) extract, 12-16 parts of spirulina extract, 10-15 parts of pregelatinized starch, microcrystalline cellulose 7-8 Part, 1-2 parts of magnesium stearate.
As a preferred solution of the present invention, the vinegar powder piece, including following content of component: 90 parts of vinegar powder, wax gourd are extracted 25 parts of object, 25 parts of haw thorn extract, 25 parts of Thallus Laminariae (Thallus Eckloniae) extract, 14 parts of spirulina extract, 13 parts of pregelatinized starch, microcrystalline cellulose 7 parts, 2 parts of magnesium stearate of element.
As a preferred solution of the present invention, the vinegar powder is apple vinegar powder.
As a preferred solution of the present invention, the vinegar powder the preparation method is as follows:
(1) preparation of apple vinegar: choosing full apple and be put into sterile workshop fermentation 10-15 days, the apple after obtaining fermentation mildew Fruit is inoculated with and handles rear venting culture, aerlbic culture 50 days at 28 DEG C -39 DEG C, daily timing agitation, after aerlbic culture, Foam is cleared up, song is made into;It will be placed in watt cylinder at song, sealing fermentation;Mature fermented grain is made after fermentation;Mature fermented grain Filtering is added edible salt, is first put into outdoor watt cylinder and is exposed to the sun after stirring evenly, when ferment unstrained spirits temperature reaches 70 DEG C -80 DEG C, then by turning over Unstrained spirits is kept for 48-52 DEG C of temperature of ferment unstrained spirits, until acetic acid content reaches 6-9 grams/100 milliliters, color becomes natural yellow, obtains into Ripe vinegar fermented grain;Mature vinegar fermented grain sterilization treatment is obtained into apple vinegar;
(2) compound fill out will be added in apple vinegar to deposit agent and obtain mixed liquor, be spray-dried, obtain the apple vinegar powder;Wherein, described multiple It is maltose, starch and the gruel essence that mass ratio is 1:1:2 that conjunction, which fills out and deposits agent,.
A kind of preparation method of vinegar powder piece, comprising the following steps: the first step weighs raw material;Second step, by vinegar powder, wax gourd Extract, haw thorn extract, Thallus Laminariae (Thallus Eckloniae) extract part, spirulina extract are uniformly mixed to obtain mixture, third step, by the mixing After object is dissolved in distilled water and is ultrasonically treated 10-15 minutes;Microcrystalline cellulose is added, twice ultrasonic is handled 10-15 minutes To clear cream;The clear cream is spray dried to fine powder by the 4th step;5th step, by the fine powder and pregelatinized starch, magnesium stearate Mixed powder one-step palletizing, obtain vinegar powder piece.
Think in Compendium of Material Medica: vinegar energy subduing inflammation, aproll gas, pathogenic toxin killing, all medicines of reason.Existing a large amount of clinical practice Prove, vinegar have it is antifatigue, prevention of arterial hardening, hypertension, improve a poor appetite, promote digestion, skin maintenance and cosmetic benefits, anticancer, prevention Sclerotin is loose, treats the effects of calculus, rescue, diuresis.Main functional component in vinegar includes: r- aminobutyric acid, ligustrazine And Lovastatin etc., they all have preferable effect for reducing blood fat.
Compared with prior art, the present invention has the advantages that: vinegar powder piece of the invention not only has the function of reducing blood lipid, And multi-faceted nutritional support can be provided to be edible, and the vinegar powder tablet quality is stablized, effective component content improves, and it is made Preparation Method is simple, is suitble to industrialized production.
Specific embodiment
Below by specific embodiment, invention is further described in detail.But those skilled in the art will manage Solution, the following example is merely to illustrate the present invention, and should not be taken as limiting the scope of the invention.Specific skill is not specified in embodiment Art or condition person, described technology or conditions carry out to specifications according to the literature in the art.Agents useful for same or instrument Production firm person is not specified, being can be with conventional products that are commercially available.
Embodiment 1
A kind of vinegar powder piece, including following content of component: 80 parts of vinegar powder, 20 parts of wax gourd extract, 20 parts of haw thorn extract, kelp 20 parts of extract, 12 parts of spirulina extract, 10 parts of pregelatinized starch, 7 parts of microcrystalline cellulose, 1 part of magnesium stearate.
Wherein, the vinegar powder be apple vinegar powder, the apple vinegar powder the preparation method is as follows:
(1) preparation of apple vinegar: choosing full apple and be put into sterile workshop fermentation 10 days, the apple after obtaining fermentation mildew, Inoculation processing rear venting culture, aerlbic culture 50 days at 28 DEG C, daily timing agitation after aerlbic culture, clear up foam, Song is made into;It will be placed in watt cylinder at song, sealing fermentation;Mature fermented grain is made after fermentation;Mature fermented grain filtering, it is added Edible salt is first put into outdoor watt cylinder after stirring evenly and is exposed to the sun, and when ferment unstrained spirits temperature reaches 70 DEG C, then by turning over unstrained spirits, keeps ferment unstrained spirits temperature 48 DEG C of degree, until acetic acid content reaches 6 grams/100 milliliters, color becomes natural yellow, obtains mature vinegar fermented grain;Mature vinegar fermented grain is gone out Bacterium handles to obtain apple vinegar;
(2) compound fill out will be added in apple vinegar to deposit agent and obtain mixed liquor, be spray-dried, obtain the apple vinegar powder;Wherein, described multiple It is maltose, starch and the gruel essence that mass ratio is 1:1:2 that conjunction, which fills out and deposits agent,.
A kind of preparation method of vinegar powder piece, comprising the following steps: the first step weighs raw material;Second step, by vinegar powder, wax gourd Extract, haw thorn extract, Thallus Laminariae (Thallus Eckloniae) extract part, spirulina extract are uniformly mixed to obtain mixture, third step, by the mixing Object is dissolved in distilled water and is ultrasonically treated after ten minutes;Microcrystalline cellulose is added, twice ultrasonic handles 10 minutes and obtains clear cream; The clear cream is spray dried to fine powder by the 4th step;5th step, by the mixing of the fine powder and pregelatinized starch, magnesium stearate Powder one-step palletizing obtains vinegar powder piece.
Embodiment 2
A kind of vinegar powder piece, including following content of component: 100 parts of vinegar powder, 30 parts of wax gourd extract, 30 parts of haw thorn extract, sea Band 30 parts of extract, 16 parts of spirulina extract, 15 parts of pregelatinized starch, 8 parts of microcrystalline cellulose, 2 parts of magnesium stearate.
Wherein, the vinegar powder be apple vinegar powder, the vinegar powder the preparation method is as follows:
(1) preparation of apple vinegar: choosing full apple and be put into sterile workshop fermentation 15 days, the apple after obtaining fermentation mildew, Inoculation processing rear venting culture, aerlbic culture 50 days at 39 DEG C, daily timing agitation after aerlbic culture, clear up foam, Song is made into;It will be placed in watt cylinder at song, sealing fermentation;Mature fermented grain is made after fermentation;Mature fermented grain filtering, it is added Edible salt is first put into outdoor watt cylinder after stirring evenly and is exposed to the sun, and when ferment unstrained spirits temperature reaches 80 DEG C, then by turning over unstrained spirits, keeps ferment unstrained spirits temperature 52 DEG C of degree, until acetic acid content reaches 9 grams/100 milliliters, color becomes natural yellow, obtains mature vinegar fermented grain;Mature vinegar fermented grain is gone out Bacterium handles to obtain apple vinegar;
(2) compound fill out will be added in apple vinegar to deposit agent and obtain mixed liquor, be spray-dried, obtain the apple vinegar powder;Wherein, described multiple It is maltose, starch and the gruel essence that mass ratio is 1:1:2 that conjunction, which fills out and deposits agent,.
A kind of preparation method of vinegar powder piece, comprising the following steps: the first step weighs raw material;Second step, by vinegar powder, wax gourd Extract, haw thorn extract, Thallus Laminariae (Thallus Eckloniae) extract part, spirulina extract are uniformly mixed to obtain mixture, third step, by the mixing After object is dissolved in distilled water and is ultrasonically treated 15 minutes;Microcrystalline cellulose is added, twice ultrasonic handles 15 minutes and obtains clear cream; The clear cream is spray dried to fine powder by the 4th step;5th step, by the mixing of the fine powder and pregelatinized starch, magnesium stearate Powder one-step palletizing obtains vinegar powder piece.
Embodiment 3
A kind of vinegar powder piece, including following content of component: 90 parts of vinegar powder, 25 parts of wax gourd extract, 25 parts of haw thorn extract, kelp 25 parts of extract, 14 parts of spirulina extract, 13 parts of pregelatinized starch, 7 parts of microcrystalline cellulose, 2 parts of magnesium stearate.
Wherein, the vinegar powder be apple vinegar powder, the vinegar powder the preparation method is as follows:
(1) preparation of apple vinegar: choosing full apple and be put into sterile workshop fermentation 12 days, the apple after obtaining fermentation mildew, Inoculation processing rear venting culture, aerlbic culture 50 days at 39 DEG C, daily timing agitation after aerlbic culture, clear up foam, Song is made into;It will be placed in watt cylinder at song, sealing fermentation;Mature fermented grain is made after fermentation;Mature fermented grain filtering, it is added Edible salt is first put into outdoor watt cylinder after stirring evenly and is exposed to the sun, and when ferment unstrained spirits temperature reaches 78 DEG C, then by turning over unstrained spirits, keeps ferment unstrained spirits temperature 50 DEG C of degree, until acetic acid content reaches 8 grams/100 milliliters, color becomes natural yellow, obtains mature vinegar fermented grain;Mature vinegar fermented grain is gone out Bacterium handles to obtain apple vinegar;
(2) compound fill out will be added in apple vinegar to deposit agent and obtain mixed liquor, be spray-dried, obtain the apple vinegar powder;Wherein, described multiple It is maltose, starch and the gruel essence that mass ratio is 1:1:2 that conjunction, which fills out and deposits agent,.
A kind of preparation method of vinegar powder piece, comprising the following steps: the first step weighs raw material;Second step, by vinegar powder, wax gourd Extract, haw thorn extract, Thallus Laminariae (Thallus Eckloniae) extract part, spirulina extract are uniformly mixed to obtain mixture, third step, by the mixing After object is dissolved in distilled water and is ultrasonically treated 14 minutes;Microcrystalline cellulose is added, twice ultrasonic handles 13 minutes and obtains clear cream; The clear cream is spray dried to fine powder by the 4th step;5th step, by the mixing of the fine powder and pregelatinized starch, magnesium stearate Powder one-step palletizing obtains vinegar powder piece.
Toxicologic study
Toxicology test is carried out using the vinegar powder piece sample of embodiment 1-3, the toxicological safety of compound preparation of the invention is commented Valence test result is as follows:
(1) acute oral toxicity test: after giving intragastric administration on mice with the sample of 20000mg/kg BW dosage, have no that animal has Animal, gross examination of skeletal muscle no abnormality seen, acute oral poison of the sample to mouse are dissected in toxication shape, no animal dead, off-test Property LD50 be greater than 20000mg/kg BW, acute oral toxicity belongs to nontoxic grade.
(2) genetic toxicity test: three genetic toxicity tests (Salmonella reversion test, mouse marrow cell micro nuclear test, mouse essences Sub- deformity test) result is feminine gender.
The above is only preferred embodiments of the present invention, is not intended to limit the scope of the present invention, Therefore any trickle amendment, equivalent variations and modification made to the above embodiment according to the technical essence of the invention, belong to In the range of technical solution of the present invention.

Claims (5)

1. a kind of vinegar powder piece, which is characterized in that including following content of component: 80-100 parts of vinegar powder, wax gourd extract 20-30 Part, 20-30 parts of haw thorn extract, 20-30 parts of Thallus Laminariae (Thallus Eckloniae) extract, 12-16 parts of spirulina extract, 10-15 parts of pregelatinized starch, 7-8 parts of microcrystalline cellulose, 1-2 parts of magnesium stearate.
2. a kind of vinegar powder piece according to claim 1, which is characterized in that including following content of component: 90 parts of vinegar powder, winter It is 25 parts of melon extract, 25 parts of haw thorn extract, 25 parts of Thallus Laminariae (Thallus Eckloniae) extract, 14 parts of spirulina extract, 13 parts of pregelatinized starch, micro- 7 parts of crystalline cellulose, 2 parts of magnesium stearate.
3. a kind of vinegar powder piece according to claim 1, which is characterized in that the vinegar powder is apple vinegar powder.
4. a kind of vinegar powder piece according to claim 1, which is characterized in that the vinegar powder the preparation method is as follows:
The preparation of apple vinegar: choosing full apple and be put into sterile workshop fermentation 10-15 days, the apple after obtaining fermentation mildew, Inoculation processing rear venting culture, aerlbic culture 50 days at 28 DEG C -39 DEG C, daily timing agitation, after aerlbic culture, cleaning Song is made into foam;It will be placed in watt cylinder at song, sealing fermentation;Mature fermented grain is made after fermentation;Mature fermented grain mistake Filter is added edible salt, is first put into outdoor watt cylinder and is exposed to the sun after stirring evenly, when ferment unstrained spirits temperature reaches 70 DEG C -80 DEG C, then by turning over Unstrained spirits is kept for 48-52 DEG C of temperature of ferment unstrained spirits, until acetic acid content reaches 6-9 grams/100 milliliters, color becomes natural yellow, obtains into Ripe vinegar fermented grain;Mature vinegar fermented grain sterilization treatment is obtained into apple vinegar;
Compound fill out will be added in apple vinegar to deposit agent and obtain mixed liquor, be spray-dried, obtain the apple vinegar powder;Wherein, described compound Filling out and depositing agent is maltose, starch and the gruel essence that mass ratio is 1:1:2.
5. a kind of preparation method of vinegar powder piece described in claim 1, which comprises the following steps: the first step weighs Raw material;Vinegar powder, wax gourd extract, haw thorn extract, Thallus Laminariae (Thallus Eckloniae) extract part, spirulina extract are uniformly mixed by second step Mixture, third step, after the mixture is dissolved in distilled water and is ultrasonically treated 10-15 minutes;Microcrystalline cellulose is added, Twice ultrasonic handles 10-15 minutes and obtains clear cream;The clear cream is spray dried to fine powder by the 4th step;5th step, will be described thin The mixed powder one-step palletizing of powder and pregelatinized starch, magnesium stearate obtains vinegar powder piece.
CN201811447619.1A 2018-11-29 2018-11-29 A kind of vinegar powder piece and preparation method thereof Pending CN109207339A (en)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1687378A (en) * 2005-04-01 2005-10-26 王浩贵 Wax gourd vinegar
JP2006087389A (en) * 2004-09-27 2006-04-06 Seiwa Kk Powdery brewed vinegar and method for producing the same
CN102228303A (en) * 2011-07-13 2011-11-02 佛山市海天调味食品股份有限公司 Solid preparation of fruit vinegar effervescent tablets and processing technology thereof
CN105733918A (en) * 2016-02-29 2016-07-06 南京益生健生物技术有限公司 Method for preparing blood-fat-reducing vinegar powder
CN106119066A (en) * 2016-08-28 2016-11-16 北海生巴达生物科技有限公司 A kind of former vinegar of spirulina and brewing method
CN106554898A (en) * 2016-12-02 2017-04-05 南京御匾国健生物科技有限公司 A kind of preparation method of vinegar powder
CN106929376A (en) * 2015-12-29 2017-07-07 青岛智通四海家具设计研发有限公司 Hypoglycemic fruit vinegar
CN108707532A (en) * 2018-07-20 2018-10-26 三原县甘露池醋厂 A kind of apple vinegar and preparation method thereof
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
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CN1687378A (en) * 2005-04-01 2005-10-26 王浩贵 Wax gourd vinegar
CN102228303A (en) * 2011-07-13 2011-11-02 佛山市海天调味食品股份有限公司 Solid preparation of fruit vinegar effervescent tablets and processing technology thereof
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CN106119066A (en) * 2016-08-28 2016-11-16 北海生巴达生物科技有限公司 A kind of former vinegar of spirulina and brewing method
CN106554898A (en) * 2016-12-02 2017-04-05 南京御匾国健生物科技有限公司 A kind of preparation method of vinegar powder
CN108707532A (en) * 2018-07-20 2018-10-26 三原县甘露池醋厂 A kind of apple vinegar and preparation method thereof
CN108865631A (en) * 2018-08-06 2018-11-23 陈永顺 A kind of preparation method of health-care vinegar

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