CN109179991A - A kind of Yingjing sand device special-purpose high temperature transmutation glaze formula - Google Patents
A kind of Yingjing sand device special-purpose high temperature transmutation glaze formula Download PDFInfo
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- CN109179991A CN109179991A CN201811157534.XA CN201811157534A CN109179991A CN 109179991 A CN109179991 A CN 109179991A CN 201811157534 A CN201811157534 A CN 201811157534A CN 109179991 A CN109179991 A CN 109179991A
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
Abstract
The invention discloses Yingjing sand device special-purpose high temperature transmutation glaze formula, the component including following parts by weight proportion: the waste plant dregs and blast furnace waste coal ground-slag formed after straw, wheat, beans stalk, sawdust, leaf burning are mixed to form waste residue: 30-40 parts;Feldspar: 40-60 parts;Iron: 10-15 parts;Calcite: 5-8 parts;Quartz: 12-25 parts;Kaolin: 5-8 parts;1-5 parts of colouring material;According to heating curve of the ground coat enamel made from above-mentioned process recipe during firing are as follows: room temperature is lighted a fire ~ 300 DEG C;Required time 60 minutes;Two .300 DEG C ~ 600 DEG C;Required time 40 minutes;Three .600 DEG C ~ 950 DEG C;Required time 40 minutes;Four .900 DEG C ~ 1050 DEG C;Required time 80 minutes;Five .1050 DEG C ~ 1150 DEG C;Required time 40 minutes;Six .1150 DEG C ~ 1200 DEG C;Required time 60 minutes;Seven .1200 DEG C ~ 1300 DEG C, and keep the temperature at 1300 DEG C;15 ~ cease fire after twenty minutes.The present invention turns waste into wealth raw slag material, forms colorful sand device glaze, more has surface aesthetic feeling on the basis of saving black sand pottery makings, keeps the audient of sand device more extensive.
Description
Technical field
The invention belongs to become glaze formula technical field, more particularly to a kind of Yingjing sand device special-purpose high temperature transmutation glaze formula.
Background technique
The production method of sand device has a long history, and has the history of more than one thousand years according to records, and black sand device is using clay
And a kind of pottery of the sand as primary raw material, the ingredient of sand overweight other pottery classes, belong to sand pottery class, because its device root is black,
Also known as black sand pottery.Raw material is by screen, kibbling, slot is ground, adjusts mud, molding, glazing, dries, kiln burning, the processes progress such as sootiness
Production, existing black sand device has the function of high temperature resistant, acid and alkali-resistance, aqueous, ventilative, heat preservation etc., therefore is widely used in building
Decoration, tableware, tea set, health care special utensil etc., the health care for also thering is common people's modern life to stress, green ring
The actual efficacys such as guarantor.
The history of Sichuan Yingjing sand device nearly 2300, is constantly improved in succession and practice, but Yingjing sand device nearly 2300
Year is all a Color-Black, can no longer meet modern life sophistication and aesthetic diverse demand.
Why Yingjing sand device cannot colour, and not solve mainly due to following two:
1. containing a large amount of ferrotitanium vanadium in the glaze of waste residue proportion, and other composition Si-Al-K sodium calcium and magnesium compositions.Ferrovanadium titanium elements
Color development is influenced bigger by atmosphere, is in grey black in reducing atmosphere body color in oxidizing atmosphere ferrovanadium titanium body color in based on yellow
Color.
2. due to having 50% or so cinder powder or coal gangue powder and blast furnace waste coal slag in black sand mud embryo raw material ratio
Composition and organic matter are contained a large amount of impurities in the glaze of waste residue proportion after powder and straw, wheat, beans stalk, sawdust, the burning of all kinds of leaves
Composition causes that a large amount of bubble CO, CO can be generated in the case where high temperature is fired2And steam, it will lead to and occur on ceramic surface or glaze surface
A large amount of bubble or pin hole, cause the decorative effect of glaze paint to be greatly lowered, good artistic effect in traditional sense are not achieved, very
To influence pottery mold burning do not tie or burning and leak, to influence the service performance of black sand pottery, or there is a large amount of waste product.
Therefore, how to solve the problems of the above-mentioned prior art becomes the direction of field technical staff effort.
Summary of the invention
The object of the invention is to: a kind of suitable Yingjing sand device special-purpose high temperature transmutation glaze formula is provided, is needed in the modern life
It asks under being driven under sophistication and modern's Aesthetic, is carried out on the burning process of original Yingjing sand device surface innovative and first
Into the research and development of property, colour vision aesthetics is allowed to be able to innovative presentation on the basis of Yingjing sand device is original, gives Yingjing sand device band
Carry out new vitality, allows Yingjing sand device to move towards broader life and use field, bring more work for Yingjing sand device industry
Power and economic benefit;Solve the shortcoming that Yingjing sand device only has black.
The purpose of the present invention is realized by following technical proposals: a kind of Yingjing sand device special-purpose high temperature transmutation glaze formula,
Component including following parts by weight proportion:
The waste plant dregs and blast furnace waste coal ground-slag formed after straw, wheat, beans stalk, sawdust, leaf burning are mixed to form waste residue: 30-40
Part;Feldspar: 40-60 parts;Iron: 10-15 parts;Calcite: 5-8 parts;Quartz: 12-25 parts;Kaolin: 5-8 parts;Colouring material 1-5
Part;
According to heating curve of the ground coat enamel made from above-mentioned process recipe during firing are as follows:
One, room temperature is lighted a fire ~ 300 DEG C;Required time 55-65 minutes;
Two .300 DEG C ~ 600 DEG C;Required time 37-43 minutes;
Three .600 DEG C ~ 950 DEG C;Required time 37-43 minutes;
Four .900 DEG C ~ 1050 DEG C;Required time 35-55 minutes;
Five .1050 DEG C ~ 1150 DEG C;Required time 37-43 minutes;
Six .1150 DEG C ~ 1300 DEG C;Required time 35-60 minutes;
Seven, are kept the temperature at 1300 DEG C;Cease fire after 15-20 minutes.
One of it is preferred that, a kind of Yingjing sand device special-purpose high temperature transmutation glaze formula comprising following parts by weight are matched
The component of ratio:
The waste plant dregs that are formed and blast furnace waste coal ground-slag are mixed to form waste residue after straw, wheat, beans stalk, sawdust, leaf burning: 40 parts;
Feldspar: 45 parts;Iron: 12 parts;Calcite: 6 parts;Quartz: 22 parts;Kaolin: 7 parts;3 parts of mineral k colouring material;
According to heating curve of the ground coat enamel made from above-mentioned process recipe during firing are as follows:
One, room temperature is lighted a fire ~ 300 DEG C;Required time 65 minutes;
Two .300 DEG C ~ 600 DEG C;Required time 43 minutes;
Three .600 DEG C ~ 950 DEG C;Required time 43 minutes;
Four .900 DEG C ~ 1050 DEG C;Required time 55 minutes;
Five .1050 DEG C ~ 1150 DEG C;Required time 37 minutes;
Six .1150 DEG C ~ 1300 DEG C;Required time 50 minutes;
Seven, are kept the temperature at 1300 DEG C;Cease fire after twenty minutes.
One of it is preferred that, the waste plant dregs and blast furnace waste coal slag formed after straw, wheat, beans stalk, sawdust, leaf burning
Powder is mixed to form waste residue: 35 parts;Feldspar: 45 parts;Iron: 12 parts;Calcite: 5 parts;Quartz: 20 parts;Kaolin: 6 parts;Chromogen
4 parts of material;
According to heating curve of the ground coat enamel made from above-mentioned process recipe during firing are as follows:
One, room temperature is lighted a fire ~ 300 DEG C;Required time 60 minutes;
Two .300 DEG C ~ 600 DEG C;Required time 40 minutes;
Three .600 DEG C ~ 950 DEG C;Required time 40 minutes;
Four .900 DEG C ~ 1050 DEG C;Required time 50 minutes;
Five .1050 DEG C ~ 1150 DEG C;Required time 40 minutes;
Six .1150 DEG C ~ 1300 DEG C;Required time 50 minutes;
Seven, are kept the temperature at 1300 DEG C;Cease fire after 18 minutes.
One of it is preferred that, the component including following parts by weight proportion:
The waste plant dregs that are formed and blast furnace waste coal ground-slag are mixed to form waste residue after straw, wheat, beans stalk, sawdust, leaf burning: 32 parts;
Feldspar: 60 parts;Iron: 15 parts;Calcite: 5 parts;Quartz: 16 parts;Kaolin: 7 parts;3 parts of colouring material;
According to heating curve of the ground coat enamel made from above-mentioned process recipe during firing are as follows:
One, room temperature is lighted a fire ~ 300 DEG C;Required time 55 minutes;
Two .300 DEG C ~ 600 DEG C;Required time 39 minutes;
Three .600 DEG C ~ 950 DEG C;Required time 39 minutes;
Four .900 DEG C ~ 1050 DEG C;Required time 39 minutes;
Five .1050 DEG C ~ 1150 DEG C;Required time 39 minutes;
Six .1150 DEG C ~ 1300 DEG C;Required time 60 minutes;
Seven, are kept the temperature at 1300 DEG C;Cease fire after twenty minutes.
One of it is preferred that, the colouring material is mineral coloring element.
One of it is preferred that, the colouring material is colorant.
The feldspar be it is a kind of containing calcium, sodium, potassium aluminium silicate mineral.There are many kinds of it, as albite, anorthite,
Baryta fledspar, baryta feldspar, microcline, orthoclase, glassy feldspar etc..They all have glassy lustre, and color is varied.Whether there is or not
Color, have white, yellow, pink, green, grey, black etc..Some are transparent, some are translucent.What the present invention selected is nothing
The albite of color.
The calcite is a kind of calcium carbonate mineral, and the present invention selects granular, blocky, fibrous, stalactitic, earthy equal
It can.
The quartz is low quartz (alpha-quartz), and main component is SiO2, it is colorless and transparent, it is translucent or opaque
Crystal, quality are hard.
The kaolin is a kind of nonmetallic minerals, is a kind of clay and clay based on kaolinite race clay mineral
Rock.Because white and fine and smooth, also known as white clouds are native.The pure kaolin of its matter in pure white fine and smooth, soft earthy, have it is good can
The physicochemical properties such as plasticity and fire resistance.Its mineralogical composition mainly by kaolinite, galapectite, hydromica, illite, montmorillonite and
The mineral compositions such as quartz, feldspar.
The colorant refers to the pigment that can be coloured or color material, is that the powdery being configured to color base and flux or additive has
Color ceramics ornament materials.As under-glaze pigment will be through high-temperature calcination, it is desirable that higher stability, but it is of less types, it uses earliest
Be blue and white, under-glaze red, in recent years again be made it is red, yellow, green, green, black, grey, brown etc..Over-glaze pigment need only be subjected to 600~800
DEG C temperature, thus it is various in style, it is rich in color.In addition, being to use as overglaze color decorations there are also liquid pigment, such as Jinsui River
Metal and organic matter are combined to vulcanization balm, then are made added with solvent.
Mineral coloring element refers to that crystal etc. has the minerals of different colours, can be used as the decoration material of coloured ceramics
Material.
Compared with prior art, the beneficial effects of the present invention are Yingjing sand device special-purpose high temperature transmutation of the present invention
Glaze formula turns waste into wealth raw slag material on the basis of existing Yingjing sand device, comprehensive to use, and matches in conjunction with of the present invention
Side, is added different mineral coloring element or colorant, forms colorful high temperature sand device glaze, not only solve asking for environmental pollution
Topic, and more have surface aesthetic feeling on the basis of saving black sand pottery makings, so that the audient of sand device is more extensive, it is suitble to big
The popularization and application of area.
Specific embodiment
The present invention is further illustrated combined with specific embodiments below.
A kind of embodiment 1: Yingjing sand device special-purpose high temperature transmutation glaze formula comprising the component of following parts by weight proportion:
The waste plant dregs that are formed and blast furnace waste coal ground-slag are mixed to form waste residue after straw, wheat, beans stalk, sawdust, leaf burning: 40 parts;Feldspar:
45 parts;Iron: 12 parts;Calcite: 6 parts;Quartz: 22 parts;Kaolin: 7 parts;3 parts of colouring material, the colouring material is colorant.
According to heating curve of the ground coat enamel made from above-mentioned process recipe during firing are as follows:
One, room temperature is lighted a fire ~ 300 DEG C;Required time 65 minutes;
Two .300 DEG C ~ 600 DEG C;Required time 43 minutes;
Three .600 DEG C ~ 950 DEG C;Required time 43 minutes;
Four .900 DEG C ~ 1050 DEG C;Required time 55 minutes;
Five .1050 DEG C ~ 1150 DEG C;Required time 37 minutes;
Six .1150 DEG C ~ 1300 DEG C;Required time 50 minutes;
Seven, are kept the temperature at 1300 DEG C;Cease fire after twenty minutes.
Application Example:
Due to present invention is directed to the dedicated high temperature transmutation glaze formula of Ya'an Sichuan province Yingjing sand device, it gathers materials on the spot, will become
Waste be changed into values.
Straw, wheat, beans stalk, sawdust, all kinds of leaves etc. are forbidden burning due to the requirement of environmental protection, and therefore, pile up like a mountain, along
Affect environment.
Waste residue used in the present invention is Yaan Prefecture's blast furnace waste coal ground-slag and straw, wheat, beans stalk, sawdust, the combustion of all kinds of leaves
Waste residue after burning, is turned waste into wealth, comprehensive to use, and manufactures distinctive Yingjing sand device glaze, has epoch-making innovative significance, both
It solves problem of environmental pollution, so that traditional sand device the colorful artistic effect of tool is occurred and rise in value again return, kill two birds with one stone.
The present invention will take raw material classification to use, and by rational formula, green body takes heating system different in heating curve
Degree, drains organic matter and foreign gas all before the initial melting temperature of base glaze starts, and produces to avoid the gases affect of generation
The performance attractive in appearance on product surface.In addition, keeping black sand pottery base by optimization of C/C composites and reasonable control furnace atmosphere and heating curve
Magically change goes out to meet the surface aesthetic feeling of black sand pottery makings while eigen.
Specifically, firstly, changing heating curve and the time of firing to improve the resistance to burning temperature of glaze, so as to sintering procedure
In make glaze after a large amount of bubble drains, glaze just starts to melt, and does not just cause that glaze paint generates a large amount of bubbles or pin hole, glaze paint are smooth
Degree greatly improves and meets the material characteristic aesthetic feeling of Yingjing sand device, has mixed the sand for the thawing that can be rapidly heated in a short time
Device high-temperature glaze imparts traditional sand device new makings and imposing manner, presents peculiar aesthetic feeling.
Then, the heating curve of firing is adjusted, then hydrogen reduction burning and anaerobic is taken to burn different firing atmosphere modes, most
A variety of unique colors and skin texture are being presented on black sand idiosome eventually.
A kind of embodiment 2: Yingjing sand device special-purpose high temperature transmutation glaze formula comprising the component of following parts by weight proportion:
The waste plant dregs that are formed and blast furnace waste coal ground-slag are mixed to form waste residue after straw, wheat, beans stalk, sawdust, leaf burning: 35 parts;Feldspar:
45 parts;Iron: 12 parts;Calcite: 5 parts;Quartz: 20 parts;Kaolin: 6 parts;4 parts of colouring material;The colouring material is mineral
Color element.
According to heating curve of the ground coat enamel made from above-mentioned process recipe during firing are as follows:
One, room temperature is lighted a fire ~ 300 DEG C;Required time 60 minutes;
Two .300 DEG C ~ 600 DEG C;Required time 40 minutes;
Three .600 DEG C ~ 950 DEG C;Required time 40 minutes;
Four .900 DEG C ~ 1050 DEG C;Required time 50 minutes;
Five .1050 DEG C ~ 1150 DEG C;Required time 40 minutes;
Six .1150 DEG C ~ 1300 DEG C;Required time 50 minutes;
Seven, are kept the temperature at 1300 DEG C;Cease fire after 18 minutes.
A kind of embodiment 3: Yingjing sand device special-purpose high temperature transmutation glaze formula comprising the component of following parts by weight proportion:
The waste plant dregs that are formed and blast furnace waste coal ground-slag are mixed to form waste residue after straw, wheat, beans stalk, sawdust, leaf burning: 32 parts;
Feldspar: 60 parts;Iron: 15 parts;Calcite: 5 parts;Quartz: 16 parts;Kaolin: 7 parts;3 parts of colouring material;The colouring material
For mineral coloring element.The optional blue of color, green, red etc..
According to heating curve of the ground coat enamel made from above-mentioned process recipe during firing are as follows:
One, room temperature is lighted a fire ~ 300 DEG C;Required time 55 minutes;
Two .300 DEG C ~ 600 DEG C;Required time 39 minutes;
Three .600 DEG C ~ 950 DEG C;Required time 39 minutes;
Four .900 DEG C ~ 1050 DEG C;Required time 39 minutes;
Five .1050 DEG C ~ 1150 DEG C;Required time 39 minutes;
Six .1150 DEG C ~ 1300 DEG C;Required time 60 minutes;
Seven, are kept the temperature at 1300 DEG C;Cease fire after twenty minutes.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all in essence of the invention
Made any modifications, equivalent replacements, and improvements etc., should all be included in the protection scope of the present invention within mind and principle.
Claims (6)
1. a kind of Yingjing sand device special-purpose high temperature transmutation glaze formula, it is characterised in that: the component including following parts by weight proportion:
The waste plant dregs and blast furnace waste coal ground-slag formed after straw, wheat, beans stalk, sawdust, leaf burning are mixed to form waste residue: 30-40
Part;Feldspar: 40-60 parts;Iron: 10-15 parts;Calcite: 5-8 parts;Quartz: 12-25 parts;Kaolin: 5-8 parts;Colouring material 1-5
Part;
According to heating curve of the ground coat enamel made from above-mentioned process recipe during firing are as follows:
One, room temperature is lighted a fire ~ 300 DEG C;Required time 55-65 minutes;
Two .300 DEG C ~ 600 DEG C;Required time 37-43 minutes;
Three .600 DEG C ~ 950 DEG C;Required time 37-43 minutes;
Four .900 DEG C ~ 1050 DEG C;Required time 35-55 minutes;
Five .1050 DEG C ~ 1150 DEG C;Required time 37-43 minutes;
Six .1150 DEG C ~ 1300 DEG C;Required time 35-60 minutes;
Seven, are kept the temperature at 1300 DEG C;Cease fire after 15-20 minutes.
2. Yingjing sand device special-purpose high temperature transmutation glaze formula according to claim 1, it is characterised in that: including following parts by weight
The component of number proportion:
The waste plant dregs that are formed and blast furnace waste coal ground-slag are mixed to form waste residue after straw, wheat, beans stalk, sawdust, leaf burning: 40 parts;
Feldspar: 45 parts;Iron: 12 parts;Calcite: 6 parts;Quartz: 22 parts;Kaolin: 7 parts;3 parts of raw mineral materials of coloring;
According to heating curve of the ground coat enamel made from above-mentioned process recipe during firing are as follows:
One, room temperature is lighted a fire ~ 300 DEG C;Required time 65 minutes;
Two .300 DEG C ~ 600 DEG C;Required time 43 minutes;
Three .600 DEG C ~ 950 DEG C;Required time 43 minutes;
Four .900 DEG C ~ 1050 DEG C;Required time 55 minutes;
Five .1050 DEG C ~ 1150 DEG C;Required time 37 minutes;
Six .1150 DEG C ~ 1300 DEG C;Required time 50 minutes;
Seven, are kept the temperature at 1300 DEG C;Cease fire after twenty minutes.
3. Yingjing sand device special-purpose high temperature transmutation glaze formula according to claim 1, it is characterised in that: including following parts by weight
The component of number proportion:
The waste plant dregs that are formed and blast furnace waste coal ground-slag are mixed to form waste residue after straw, wheat, beans stalk, sawdust, leaf burning: 35 parts;
Feldspar: 45 parts;Iron: 12 parts;Calcite: 5 parts;Quartz: 20 parts;Kaolin: 6 parts;4 parts of colouring material;
According to heating curve of the ground coat enamel made from above-mentioned process recipe during firing are as follows:
One, room temperature is lighted a fire ~ 300 DEG C;Required time 60 minutes;
Two .300 DEG C ~ 600 DEG C;Required time 40 minutes;
Three .600 DEG C ~ 950 DEG C;Required time 40 minutes;
Four .900 DEG C ~ 1050 DEG C;Required time 50 minutes;
Five .1050 DEG C ~ 1150 DEG C;Required time 40 minutes;
Six .1150 DEG C ~ 1300 DEG C;Required time 50 minutes;
Seven, are kept the temperature at 1300 DEG C;Cease fire after 18 minutes.
4. Yingjing sand device special-purpose high temperature transmutation glaze formula according to claim 1, it is characterised in that: including following parts by weight
The component of number proportion:
The waste plant dregs that are formed and blast furnace waste coal ground-slag are mixed to form waste residue after straw, wheat, beans stalk, sawdust, leaf burning: 32 parts;
Feldspar: 60 parts;Iron: 15 parts;Calcite: 5 parts;Quartz: 16 parts;Kaolin: 7 parts;3 parts of colouring material;
According to heating curve of the ground coat enamel made from above-mentioned process recipe during firing are as follows:
One, room temperature is lighted a fire ~ 300 DEG C;Required time 55 minutes;
Two .300 DEG C ~ 600 DEG C;Required time 39 minutes;
Three .600 DEG C ~ 950 DEG C;Required time 39 minutes;
Four .900 DEG C ~ 1050 DEG C;Required time 39 minutes;
Five .1050 DEG C ~ 1150 DEG C;Required time 39 minutes;
Six .1150 DEG C ~ 1300 DEG C;Required time 60 minutes;
Seven, are kept the temperature at 1300 DEG C;Cease fire after twenty minutes.
5. Yingjing sand device special-purpose high temperature transmutation glaze formula according to claim 1, it is characterised in that: the colouring material is
Mineral coloring element.
6. Yingjing sand device special-purpose high temperature transmutation glaze formula according to claim 1, it is characterised in that: the colouring material is
Colorant.
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CN1962557A (en) * | 2006-12-06 | 2007-05-16 | 江苏高淳陶瓷股份有限公司 | Ceramic scarlet-variable glaze and its application method |
CN106365448A (en) * | 2016-08-26 | 2017-02-01 | 福建泉州顺美集团有限责任公司 | Multi-void imitated stone glaze porcelain and preparation process |
CN107651941A (en) * | 2017-11-02 | 2018-02-02 | 张韶璞 | A kind of porcelain and its method for cooking |
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2018
- 2018-09-30 CN CN201811157534.XA patent/CN109179991A/en active Pending
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
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CN1724477A (en) * | 2005-05-25 | 2006-01-25 | 广东全福陶瓷实业有限公司 | Manufacturing method of redyohen tenmoku ceramic and ceramic glaze used therefor |
CN1962557A (en) * | 2006-12-06 | 2007-05-16 | 江苏高淳陶瓷股份有限公司 | Ceramic scarlet-variable glaze and its application method |
CN106365448A (en) * | 2016-08-26 | 2017-02-01 | 福建泉州顺美集团有限责任公司 | Multi-void imitated stone glaze porcelain and preparation process |
CN107651941A (en) * | 2017-11-02 | 2018-02-02 | 张韶璞 | A kind of porcelain and its method for cooking |
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