CN109107208A - A kind of novel carbinol distilling apparatus - Google Patents
A kind of novel carbinol distilling apparatus Download PDFInfo
- Publication number
- CN109107208A CN109107208A CN201811165386.6A CN201811165386A CN109107208A CN 109107208 A CN109107208 A CN 109107208A CN 201811165386 A CN201811165386 A CN 201811165386A CN 109107208 A CN109107208 A CN 109107208A
- Authority
- CN
- China
- Prior art keywords
- conduit
- wall
- tank body
- vertical bar
- top cover
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
- C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
- C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
- C07C31/02—Monohydroxylic acyclic alcohols
- C07C31/04—Methanol
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The invention discloses a kind of novel carbinol distilling apparatus, including the second tank body and destilling tower ontology, the top of second tank body, which fastens, top cover, run through on the left of the upper surface of the top cover and is fixed with the second conduit, the outer wall top of second conduit is socketed with rubber tube, the top of the rubber tube is securely fitted in the lower surface of destilling tower ontology, runs through on the right side of the upper surface of the top cover and is fixed with third conduit, the top fixing assembling of the third conduit has adding set.The utility model is ingenious in design, it is convenient and practical, by the cooperation of the second conduit and rubber tube, by the cooperation of third conduit and adding set, to the inside sodium iodate particle of the second tank body at third conduit, acetone remaining in methanol is removed, by the cooperation of vertical bar and opening, by the cooperation of third conduit and top cover, the amount added every time is the spatial volume that opening inner wall surrounds, practical performance is strong, is conducive to promote.
Description
Technical field
The present invention relates to methanol processing technique field, specially a kind of novel carbinol distilling apparatus.
Background technique
When industrial production methanol distills methanol, crude carbinol is purified, purification process includes at distillation and chemistry
Reason, chemical treatment is mainly difficult to isolated impurity with alkali destruction in distillation process, and adjusts pH value, and distillation mainly removes easy
Volatile component such as dimethyl ether, and ethyl alcohol, the high-carbon alcohol and water of difficult volatilization, water content is dropped in the method that industrial methanol distills
To 0.01% hereinafter, being handled again with sodium iodate, acetone therein can be removed, adding in existing distilling apparatus while collecting
Sodium iodate is added to need to carry out quantitative measurement, measurement repeatedly is time-consuming and laborious, reduces working efficiency, and practical performance is poor.
Summary of the invention
The purpose of the present invention is to provide a kind of novel carbinol distilling apparatus, to solve mentioned above in the background art ask
Topic.
To achieve the above object, the invention provides the following technical scheme: a kind of novel carbinol distilling apparatus, including the second tank
Body and destilling tower ontology, the top of second tank body, which fastens, top cover, through being fixed with the on the left of the upper surface of the top cover
Two conduits, the outer wall top of second conduit are socketed with rubber tube, and the top of the rubber tube is securely fitted in destilling tower sheet
The lower surface of body, the upper surface right side of the top cover, which is run through, is fixed with third conduit, the top fixing assembling of the third conduit
There is adding set.
The outer wall top fixing sleeve of the adding set package sleeve and top plate, the third conduit is connected to sleeve, described
The upper surface of sleeve is bonded with the lower surface of top plate, and the upper surface middle position of the top plate offers through-hole, the through-hole
Inner wall is through there is vertical bar, and the top fixing assembling of the vertical bar has pressing plate, and the outer wall of the vertical bar is socketed with spring, the spring
Between pressing plate and top plate, inner wall of the bottom end sliding plug of the vertical bar to third conduit, the left side outer wall of the vertical bar
Offer opening.
Preferably, the lower surface of second tank body, which is run through, is fixed with the first conduit, the bottom end inner wall of first conduit
It is plugged with bottle stopper, the inner wall bottom end fixing assembling of second tank body has frame, and the inner wall fixing assembling of the frame has strainer,
It is plugged with block at left and right sides of the outer wall bottom end of second tank body, the outside fixing assembling of two blocks has the first tank
Body, first tank body are located at the outside of the second tank body.
Preferably, running through at left and right sides of the outer wall top of first tank body has cross bar, the inside of two cross bars
Equal fixing assembling has fixture block, and the inner wall of the fixture block is mutually clamped with the ipsilateral top cover
Preferably, the outside fixing assembling of the cross bar has sphere.
Compared with prior art, convenient and practical the beneficial effects of the present invention are: the utility model is ingenious in design, pass through the second tank
Methanol solution after distilling and processing is stored in the inside of the second tank body, passes through the second conduit by the cooperation of body and top cover
With the cooperation of rubber tube, by the cooperation of third conduit and adding set, to the inside acid iodide of the second tank body at third conduit
Sodium particle is removed acetone remaining in methanol, by the cooperation of vertical bar and opening, passes through matching for third conduit and top cover
It closes, when pressing vertical bar downwards, the opening of vertical bar drives sodium iodate particle to move down, and the amount added every time is that opening inner wall encloses
At spatial volume, the amount of addition is limited, without duplicate measurements process repeatedly, to obtain the methanol of more sterling
Solution, practical performance is strong, is conducive to promote.
Detailed description of the invention
Fig. 1 is overall structure of the present invention；
Fig. 2 is structural schematic diagram at the A of Fig. 1；
Fig. 3 is structural schematic diagram at the B of Fig. 1；
Fig. 4 is third guide-tube structure sectional view of the invention.
In figure: 1, first tank body, 2, block, the 3, second tank body, the 4, first conduit, 5, frame, 6, strainer, 7, top cover, 8,
Second conduit, 9, rubber tube, 10, third conduit, 11, adding set, 111, pressing plate, 112, spring, 113, vertical bar, 114, top
Plate, 115, through-hole, 116, sleeve, 117, opening, 12, fixture block, 13, cross bar, 14, sphere, 15, bottle stopper, 16, destilling tower ontology.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete
Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on
Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other
Embodiment shall fall within the protection scope of the present invention.
Fig. 1-4 is please referred to, the present invention provides a kind of technical solution；A kind of novel carbinol distilling apparatus, including the second tank body 3
With destilling tower ontology 16, the top of the second tank body 3, which fastens, top cover 7, runs through on the left of the upper surface of top cover 7 and is fixed with the second conduit
8, the outer wall top of the second conduit 8 is socketed with rubber tube 9, and the top of rubber tube 9 is securely fitted in the following table of destilling tower ontology 16
Face, through third conduit 10 is fixed with, the top fixing assembling of third conduit 10 has adding set on the upper surface right side of top cover 7
11。
Formalin is set adequately to react, 9 sets of the rubber tube outer walls in the second conduit 8, the top of rubber tube 9 and steaming
It evaporates the condenser liquid outlet therein of tower ontology 16 to link together, so that the formalin that condenser is discharged enters the
The inside of two tank bodies 3.
The outer wall top fixing sleeve of 11 package sleeve 116 of adding set and top plate 114, third conduit 10 is connected to sleeve 116,
The upper surface of sleeve 116 is bonded with the lower surface of top plate 114, and the upper surface middle position of top plate 114 offers through-hole 115, is led to
The inner wall in hole 115 is through there is vertical bar 113, and the top fixing assembling of vertical bar 113 has pressing plate 111, and the outer wall of vertical bar 113 is socketed with bullet
Spring 112, spring 112 is between pressing plate 111 and top plate 114, the bottom end sliding plug of vertical bar 113 to the interior of third conduit 10
The left side outer wall of wall, vertical bar 113 offers opening 117.
The bottom end of vertical bar 113 is plugged into the inner wall of the third conduit 10 of 116 bottom end of sleeve, pushes up top plate 114,
The inside of sleeve 116 installs sodium iodate particle, and top plate 114 is placed in the top of sleeve 116, presses dynamic pressure plate 111, pressing plate 111 downwards
Vertical bar 113 is pushed to move down, pressing plate 111 applies pressure to spring 112, and because of the elastic property of itself elasticity occurs for spring 112
Deformation, sodium iodate particle enter the inside of opening 117,117 length that is open and the equal length of third conduit 10, vertical bar
The inner wall of 113 outer walls and third conduit 10 closely fits together, and vertical bar 113 drives opening 117 to be moved downward to opening 117
Lower end when being in the bottom end of third conduit 10, be open 117 top just completely into the inside for arriving third conduit 10 when, set
Sodium iodate inside cylinder 116 no longer enters the inside of opening 117, continues to push down on pressing plate 111, so that vertical bar 113 drives
Be open the inner walls of 117 fully extended third conduits 10, sodium iodate particle fallen to from opening 117 inside of second tank body 3 with
Methanol solution reaction.
Specifically, the lower surface of the second tank body 3, which is run through, is fixed with the first conduit 4, the bottom end inner wall grafting of the first conduit 4
There is bottle stopper 15, the inner wall bottom end fixing assembling of the second tank body 3 has frame 5, and the inner wall fixing assembling of frame 5 has strainer 6, the second tank
It is plugged with block 2 at left and right sides of the outer wall bottom end of body 3, the outside fixing assembling of two blocks 2 has the first tank body 1, the first tank
Body 1 is located at the outside of the second tank body 3.
The lower surface of block 2 cannot be exceeded by being housed in the formalin liquid level inside the first tank body 1, and bottle stopper 15 is rubber material
Matter, plug are sealed in the inside of the first conduit 4, take out the second tank body 3, bottle stopper 15 is taken out, is again put into the second tank body 3
Onto the block 2 of the inside of the first tank body 1, methanol solution is entered by the strainer 6 of 5 inner wall of frame flowing through the first conduit 4
The collection to methanol solution is completed in the inside of first tank body 1, takes out the second tank body 3, then methanol solution is poured out.
Specifically, the inside of two cross bars 13 is equal through there is cross bar 13 at left and right sides of the outer wall top of the first tank body 1
Fixing assembling has fixture block 12, and the inner wall of fixture block 12 is connected to the left and right sides of top cover 7, and top cover 7 is covered the top in the second tank body 3
End pushes cross bar 13 inwardly, and cross bar 13 moves inward through the first tank body 1, until cross bar 13 pushes fixture block 12 to be stuck in top
On the outer wall of lid 7, top cover 7 is limited, as shown in figure 3, the upper and lower ends of fixture block 12 will be pushed up to the interior lateral bend of top cover 7
Lid 7 blocks.
Specifically, the outside fixing assembling of cross bar 13 has sphere 14, increase the contact area between cross bar 13, it is convenient
Pull cross bar 13.
Working principle: when being distilled to methanol mixed solution, by condenser in the top of rubber tube 9 and destilling tower
Outlet end links together, and top cover 7 is buckled in the top of the second tank body 3, and the methanol solution obtained after distillation is processed is from rubber tube 9
Inside flow through the inside that the second conduit 8 enters the second tank body 3, at adding set 11 add additive sodium iodate particle,
Sodium iodate particle is reacted by the inside that third conduit 10 enters the second tank body 3 with acetone remaining in methanol solution, will be erected
The bottom end of bar 113 is plugged into the inner wall of the third conduit 10 of 116 bottom end of sleeve, pushes up top plate 114, in sleeve 116
Portion installs sodium iodate particle, and top plate 114 is placed in the top of sleeve 116, presses dynamic pressure plate 111 downwards, and pressing plate 111 pushes vertical bar 113
It moves down, pressing plate 111 applies pressure to spring 112, and because of the elastic property of itself elastic deformation, sodium iodate occur for spring 112
Particle enters the inside of opening 117, and the lower end that vertical bar 113 drives opening 117 to be moved downward to opening 117 is in third conduit
When 10 bottom end, be open 117 top just completely into the inside for arriving third conduit 10 when, the sodium iodate inside sleeve 116
The inside for no longer entering opening 117, continues to push down on pressing plate 111, so that vertical bar 113 drives opening 117 fully extended the
The inner wall of three conduits 10, the inside that sodium iodate particle falls to the second tank body 3 from opening 117 are reacted with methanol solution, every time
The volume that the amount of addition sodium iodate is surrounded by 117 inner wall of opening.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Benefit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent elements of the claims
Variation is included within the present invention.Any reference signs in the claims should not be construed as limiting the involved claims.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiments being understood that.
Claims (4)
1. a kind of novel carbinol distilling apparatus, it is characterised in that: including the second tank body (3) and destilling tower ontology (16), described
The top of two tank bodies (3), which fastens, to be had top cover (7), is run through on the left of the upper surface of the top cover (7) and is fixed with the second conduit (8), institute
The outer wall top for stating the second conduit (8) is socketed with rubber tube (9), and the top of the rubber tube (9) is securely fitted in destilling tower sheet
The lower surface of body (16), the upper surface right side of the top cover (7), which is run through, to be fixed with third conduit (10), the third conduit (10)
Top fixing assembling have adding set (11).
Adding set (11) package sleeve (116) and top plate (114), the outer wall top fixing sleeve of the third conduit (10)
Be connected to sleeve (116), the upper surface of the sleeve (116) is bonded with the lower surface of top plate (114), the top plate (114) it is upper
Surface middle position offers through-hole (115), and the inner wall of the through-hole (115), which runs through, to be had vertical bar (113), the vertical bar (113)
Top fixing assembling have pressing plate (111), the outer wall of the vertical bar (113) is socketed with spring (112), spring (112) position
Between pressing plate (111) and top plate (114), inner wall of the bottom end sliding plug of the vertical bar (113) to third conduit (10), institute
The left side outer wall for stating vertical bar (113) offers opening (117).
2. a kind of novel carbinol distilling apparatus according to claim 1, it is characterised in that: under second tank body (3)
Surface is through being fixed with the first conduit (4), and the bottom end inner wall of first conduit (4) is plugged with bottle stopper (15), second tank
The inner wall bottom end fixing assembling of body (3) has frame (5), and the inner wall fixing assembling of the frame (5) has strainer (6), and described second
It is plugged with block (2) at left and right sides of the outer wall bottom end of tank body (3), the outside fixing assembling of two blocks (2) has first
Tank body (1), first tank body (1) are located at the outside of the second tank body (3).
3. a kind of novel carbinol distilling apparatus according to claim 1, it is characterised in that: outside first tank body (1)
Through having cross bar (13) at left and right sides of wall top, the equal fixing assembling in inside of two cross bars (13) has fixture block (12), institute
The inner wall and the ipsilateral top cover (7) for stating fixture block (12) are mutually clamped.
4. a kind of novel carbinol distilling apparatus according to claim 3, it is characterised in that: the outside of the cross bar (13) is solid
Surely sphere (14) are equipped with.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811165386.6A CN109107208B (en) | 2018-10-08 | 2018-10-08 | Methanol distillation device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811165386.6A CN109107208B (en) | 2018-10-08 | 2018-10-08 | Methanol distillation device |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN109107208A true CN109107208A (en) | 2019-01-01 |
| CN109107208B CN109107208B (en) | 2023-09-26 |
Family
ID=64857519
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811165386.6A Active CN109107208B (en) | 2018-10-08 | 2018-10-08 | Methanol distillation device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109107208B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112973169A (en) * | 2021-02-23 | 2021-06-18 | 陆鹤霄 | Combined type methanol evaporator |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2923571Y (en) * | 2006-05-23 | 2007-07-18 | 彭实 | Powder quantitative taking device |
| CN102428354A (en) * | 2009-05-15 | 2012-04-25 | 巴斯夫欧洲公司 | Automatic analysis of fine-particle solids |
| CN204453352U (en) * | 2014-12-22 | 2015-07-08 | 杨健 | A kind of Intelligent rice-storing case quantifying rice |
| CN207856893U (en) * | 2017-12-28 | 2018-09-14 | 怀化学院 | A kind of detachable reactor |
| CN108522318A (en) * | 2018-04-13 | 2018-09-14 | 合肥图腾龙机械设计有限公司 | A kind of quantitative feeding and the device for feeding with spice function |
| CN207856688U (en) * | 2017-12-29 | 2018-09-14 | 广州途富香料科技有限公司 | A kind of automatic gauge equipment dissolved by heating for menthol |
| CN209270861U (en) * | 2018-10-08 | 2019-08-20 | 南京理工大学连云港研究院 | A kind of novel carbinol distilling apparatus |
-
2018
- 2018-10-08 CN CN201811165386.6A patent/CN109107208B/en active Active
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2923571Y (en) * | 2006-05-23 | 2007-07-18 | 彭实 | Powder quantitative taking device |
| CN102428354A (en) * | 2009-05-15 | 2012-04-25 | 巴斯夫欧洲公司 | Automatic analysis of fine-particle solids |
| CN204453352U (en) * | 2014-12-22 | 2015-07-08 | 杨健 | A kind of Intelligent rice-storing case quantifying rice |
| CN207856893U (en) * | 2017-12-28 | 2018-09-14 | 怀化学院 | A kind of detachable reactor |
| CN207856688U (en) * | 2017-12-29 | 2018-09-14 | 广州途富香料科技有限公司 | A kind of automatic gauge equipment dissolved by heating for menthol |
| CN108522318A (en) * | 2018-04-13 | 2018-09-14 | 合肥图腾龙机械设计有限公司 | A kind of quantitative feeding and the device for feeding with spice function |
| CN209270861U (en) * | 2018-10-08 | 2019-08-20 | 南京理工大学连云港研究院 | A kind of novel carbinol distilling apparatus |
Non-Patent Citations (1)
| Title |
|---|
| 段长强等: "《现代化学试剂手册 第一分册 通用试剂》", 北京：化学工业出版社 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112973169A (en) * | 2021-02-23 | 2021-06-18 | 陆鹤霄 | Combined type methanol evaporator |
Also Published As
| Publication number | Publication date |
|---|---|
| CN109107208B (en) | 2023-09-26 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN209270861U (en) | A kind of novel carbinol distilling apparatus | |
| CN109107208A (en) | A kind of novel carbinol distilling apparatus | |
| CN203281546U (en) | Silicon wafer bubble washing device | |
| CN104277067A (en) | Device and method for reducing chlorine ion content in dimethyldichlorosilance hydrolysate | |
| CN201770478U (en) | Ultraclean high-purity sulfuric acid extraction device | |
| CN206262339U (en) | One kind is used for organic silicon monomer synthesis tail gas absorption plant | |
| CN208648927U (en) | Wastewater treatment equipment is used in a kind of processing of bamboo product | |
| CN204147736U (en) | The spray recovery system of tail gas | |
| CN201908057U (en) | Corn starch milk cyclone device | |
| CN201962178U (en) | Novel reaction device for anaerobic methane tank | |
| CN201799186U (en) | Air filter | |
| CN216704403U (en) | Intermittent type formula is desorption device behind silica gel adsorption against current | |
| CN205095495U (en) | Filter -pressing jar for phosphorus removal pool | |
| CN210782798U (en) | Edible compressed fiber rehydration device | |
| CN104673502A (en) | Continuous esterification technique for producing biodiesel from waste grease | |
| CN201530787U (en) | Device for removing calcium formate in neopentyl glycol by calcium method | |
| CN218674606U (en) | Measuring device for granular fuel production | |
| CN201815148U (en) | Oil-water separator in neutralization procedure | |
| CN211586502U (en) | Organic matter production environment-friendly device | |
| CN203177592U (en) | Liquid crystal dehumidification device | |
| CN201842787U (en) | Methanol separator | |
| CN203264303U (en) | Vacuum decompression concentrator | |
| CN208711364U (en) | A kind of concentrated sulfuric acid multi-level gas purification system | |
| CN209116009U (en) | Steam drainage recovery device | |
| CN203568900U (en) | Anaerobic biological wastewater treatment device |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |