CN109081683A - A kind of big plate of environment-friendly ceramic and preparation method thereof - Google Patents
A kind of big plate of environment-friendly ceramic and preparation method thereof Download PDFInfo
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- CN109081683A CN109081683A CN201811128768.1A CN201811128768A CN109081683A CN 109081683 A CN109081683 A CN 109081683A CN 201811128768 A CN201811128768 A CN 201811128768A CN 109081683 A CN109081683 A CN 109081683A
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
- C04B33/16—Lean materials, e.g. grog, quartz
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/04—Clay; Kaolin
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
- C04B33/132—Waste materials; Refuse; Residues
- C04B33/1324—Recycled material, e.g. tile dust, stone waste, spent refractory material
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- C—CHEMISTRY; METALLURGY
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- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3217—Aluminum oxide or oxide forming salts thereof, e.g. bauxite, alpha-alumina
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- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3427—Silicates other than clay, e.g. water glass
- C04B2235/3463—Alumino-silicates other than clay, e.g. mullite
- C04B2235/3472—Alkali metal alumino-silicates other than clay, e.g. spodumene, alkali feldspars such as albite or orthoclase, micas such as muscovite, zeolites such as natrolite
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- C—CHEMISTRY; METALLURGY
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
- C04B2235/6567—Treatment time
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/96—Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/96—Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance
- C04B2235/9607—Thermal properties, e.g. thermal expansion coefficient
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/96—Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance
- C04B2235/9669—Resistance against chemicals, e.g. against molten glass or molten salts
- C04B2235/9692—Acid, alkali or halogen resistance
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/60—Production of ceramic materials or ceramic elements, e.g. substitution of clay or shale by alternative raw materials, e.g. ashes
Abstract
The invention discloses a kind of big plate of environment-friendly ceramic, green body includes following component according to the weight percentage of raw materials: potassium feldspar 20~30%, albite 20~30%, pyrophillite 5~15%, quartzy 5~15%, kaolin 20~35%, ball clay 5~15%, bentonite 5~15%, calcination of talc 2~5%, calcined alumina 2~4%, reclaimed materials 8~10%.Body recipe of the invention is different to ingredient and uncertain reclaimed materials has high usage and high suitability, make the big plate green compact of the ceramics being prepared into that there is excellent processability, to can get the high-quality finished product of the bigger specification of panel products specification bigger than existing ceramics and be able to achieve mass production.Preparation method simple process of the invention is not necessarily to polishing process, greatly reduces water consumption and polishing slag amount, and the big board finished product performance of the ceramics being prepared into is stablized, and is suitable for industrialization large-scale production.
Description
Technical field
The present invention relates to ceramic field, in particular to a kind of large size ceramic.
Background technique
Now the size of big specification ceramic tile is generally 900mm × 1800mm on the market, and thickness is in 6mm or less.This ceramics
The green compact molding of big plate is first to be pressed by material distributing machine charity base powder with Belt Conveying to great tonnage press lower section
, unlike the forming method of traditional specification architectural pottery, the no mold of molding of the big plate of ceramics, therefore to the big plate of ceramics
Blank has very high forming requirements, while four extra sizes in side to molding green compact being needed to cut, thus also can
More leftover pieces are generated, in addition in green compact transmission process, it may occur however that breakage needs to return damaged base powder
It receives and utilizes.Existing to be divided into Dry recovery and two kinds of hydrometallurgic recovery to the recovery and treatment method of base powder, Dry recovery will return
The base powder of receipts is directly added into the cloth bucket of material distributing machine cloth again, and hydrometallurgic recovery is then that base powder is entered ball mill or is stirred
System is mixed, is recycled by way of adding water and additive.Both methods all there may be with ceramic big plate blank
The problem of powder is not adapted to, and one of the raw material for preparing that base powder is recycled as ceramic big plate is even more the serious technology that is easy to appear
Defect and quality problems, as Dry recovery base powder causes dust harzard, reclaimed materials utilization rate low and ceramic big plate green compact molding
It is ineffective and cause green compact layering, intensity it is excessively low.
Summary of the invention
It is an object of the invention in view of the above shortcomings of the prior art, provide a kind of big plate of environment-friendly ceramic, mention simultaneously
For the preparation method of the big plate of the ceramics.
The technical solution used in the present invention is: a kind of big plate of environment-friendly ceramic, green body is according to the weight percentage of raw materials
Including following component:
Wherein, potassium feldspar, albite play congruent melting in ceramic sheet slab body formula of the invention as spectra
Effect.Specific effect are as follows: be 1. filled in generated gap in sintering procedure；2. promoting the growth of mullite crystal；3. obtaining
The green body of densified sintering product.The preferred potassium feldspar of the present invention, albite total content between 40~60%, can stable prod matter
Amount.If potassium albite total content is too low, it is difficult to fill up all gaps in green body, the porosity improves, to the mechanical strength of product,
Transparency is unfavorable；If potassium albite total content is excessively high, product skeleton is caused to die down, has the tendency that increasing deformation.Pyrophillite category
In phyllosilicate, most of pyrophillite powder are white, and general whiteness is 80% or more.The biggish leaf of the preferred fineness of the present invention
Cured stone powder end, whiteness effectively improves adobe whiteness up to 93% or more, to enhance the brightness and colour developing of product surface decorative pattern
Effect.Quartzy main component is SiO2, a part of SiO2With Al2O3Mullite crystal is generated at high temperature；Remaining part is with molten
Melt in violent graininess remaining and base, be largely converted into half stable cristobalite, it and mullite crystal are formed together base
The skeleton of body, increases the ability of product resistance to deformation, while increasing green body whiteness.Ball clay and bentonite belong to clay, because of two
Person's plasticity is good, for improving the processability of blank in ceramic sheet slab body formula of the invention, in the present invention ball clay and
Bentonitic appropriate addition can guarantee that after the reclaimed materials that formula gross mass 8~10% is added, base powder remains to stablize logical
Cross compression moulding.Calcination of talc primary aqueous closes magnesium silicate, and quality is very soft, has satiny feel, for the present invention
Ceramic sheet slab body formula in not only reduce the firing temperature of green body, but also improve the mobility of base powder.Due to reclaimed materials
Physical and chemical properties by certain destruction, need to increase a small amount of talcum, stablize the mobility of base powder, avoid because of base powder
Expect poor fluidity, causes the flatness of charity and compacting green compact not up to standard.Calcined alumina is the aluminium oxide after high-temperature calcination,
Wherein Al2O3Content not only improves green body whiteness up to 90~95% or more, but also expands the firing range of green body, guarantees be added
It is formulated after the reclaimed materials of gross mass 8~10%, the high temperature that base powder still adapts to roller way kiln is fired.
As a further improvement of the foregoing solution, the reclaimed materials cuts remaining corner base during being selected from Production of Ceramics
The base powder that the cause breakage of powder and ceramics into roller way kiln firing generates.
As a further improvement of the foregoing solution, the chemical component of the reclaimed materials mainly includes SiO2And Al2O3, also wrap
Include a small amount of K2O、Na2O and micro Fe2O3, CaO, MgO etc..
As a further improvement of the foregoing solution, in the kaolin containing 5~10% calcined kaolin.In kaolin
Main component is Al2O3, it is the primary chemical composition of green body, and the introducing of appropriate calcined kaolin can expand the firing of green body
Range improves the stability of firing.
A kind of preparation method of the big plate of environment-friendly ceramic as described above comprising following processing step:
1) it mixes by other components investment ball mill in addition to reclaimed materials according to the weight percentage of raw materials, obtains magma
Material；
2) recycling slurry is made by wet process automatic recycling device in reclaimed materials according to the weight percentage of raw materials, then by magma
Material with recycling slurry with 100:(8~10) ratio mix, be made mixed slurry, by sieving, it is aging, remove iron, ink-jet drying,
Obtain ceramic sheet slab powder；
3) ceramic sheet slab powder compression moulding after press cloth, it is dry by dry kiln, obtain ceramic big plate green compact；
4) ceramic big plate green compact are applied ground coat enamel, ink-jet decoration, apply overglaze by Belt Conveying, into height in roller kilns
Temperature firing, firing temperature are 1185~1215 DEG C, and firing time is 110~180min, through cooling, edging, packaging to get ceramics
Big board finished product.
The beneficial effects of the present invention are:
Body recipe of the invention is different to ingredient and uncertain reclaimed materials has high usage and high suitability, makes to make
Standby the big plate green compact of ceramics have excellent processability, to can get the bigger specification of panel products specification bigger than existing ceramics
High-quality finished product and be able to achieve mass production.
Preparation method simple process of the invention is not necessarily to polishing process, greatly reduces water consumption and polishing slag amount,
The big board finished product performance of the ceramics being prepared into is stablized, and industrialization large-scale production is suitable for.
Specific embodiment
The present invention is specifically described below with reference to embodiment, in order to technical field personnel to of the invention
Understand.It is necessary to it is emphasized that embodiment is only intended to, the present invention will be further described herein, should not be understood as to this
The limitation of invention protection scope, fields person skilled in the art, the non-intrinsically safe that the present invention is made according to foregoing invention content
The modifications and adaptations of property, should still fall within protection scope of the present invention.Mentioned raw materials following simultaneously are unspecified, are
Commercial product；The processing step or preparation method not referred in detail be processing step known to a person skilled in the art or
Preparation method.
Embodiment 1
A kind of big plate of environment-friendly ceramic, green body includes following component according to the weight percentage of raw materials:
Wherein, the reclaimed materials cuts remaining corner base powder and ceramics into roller way kiln during being selected from Production of Ceramics
The base powder that the cause breakage of firing generates.
Preparation method:
1) it mixes by other components investment ball mill in addition to reclaimed materials according to the weight percentage of raw materials, obtains magma
Material；
2) recycling slurry is made by wet process automatic recycling device in reclaimed materials according to the weight percentage of raw materials, then by magma
Material mix with recycling slurry with the ratio of 100:8, and mixed slurry is made, by sieving, it is aging, remove iron, ink-jet drying, obtain ceramic
Sheet slab powder；
3) ceramic sheet slab powder compression moulding after press cloth, molding specification are 1600mm × 3200mm, thickness
It is dry by dry kiln for 6mm, obtain ceramic big plate green compact；
4) ceramic big plate green compact are applied ground coat enamel, ink-jet decoration, apply overglaze by Belt Conveying, into height in roller kilns
Temperature firing, firing temperature are 1185 DEG C, firing time 180min, through cooling, edging, packaging to get the 1 big plate of ceramics of embodiment
Finished product.
Embodiment 2
A kind of big plate of environment-friendly ceramic, green body includes following component according to the weight percentage of raw materials:
Wherein, the reclaimed materials cuts remaining corner base powder and ceramics into roller way kiln during being selected from Production of Ceramics
The base powder that the cause breakage of firing generates.
Preparation method:
1) it mixes by other components investment ball mill in addition to reclaimed materials according to the weight percentage of raw materials, obtains magma
Material；
2) recycling slurry is made by wet process automatic recycling device in reclaimed materials according to the weight percentage of raw materials, then by magma
Material with recycling slurry with 100:(8~10) ratio mix, be made mixed slurry, by sieving, it is aging, remove iron, ink-jet drying,
Obtain ceramic sheet slab powder；
3) ceramic sheet slab powder compression moulding after press cloth, molding specification are 1600mm × 3200mm, thickness
It is dry by dry kiln for 6mm, obtain ceramic big plate green compact；
4) ceramic big plate green compact are applied ground coat enamel, ink-jet decoration, apply overglaze by Belt Conveying, into height in roller kilns
Temperature firing, firing temperature are 1185~1215 DEG C, and firing time is 110~180min, through cooling, edging, packaging to get implementation
The 2 big board finished product of ceramics of example.
Embodiment 3
A kind of big plate of environment-friendly ceramic, green body includes following component according to the weight percentage of raw materials:
Wherein, the reclaimed materials cuts remaining corner base powder and ceramics into roller way kiln during being selected from Production of Ceramics
The base powder that the cause breakage of firing generates.
Preparation method:
1) it mixes by other components investment ball mill in addition to reclaimed materials according to the weight percentage of raw materials, obtains magma
Material；
2) recycling slurry is made by wet process automatic recycling device in reclaimed materials according to the weight percentage of raw materials, then by magma
Material with recycling slurry with 100:(8~10) ratio mix, be made mixed slurry, by sieving, it is aging, remove iron, ink-jet drying,
Obtain ceramic sheet slab powder；
3) ceramic sheet slab powder compression moulding after press cloth, molding specification are 1600mm × 3200mm, thickness
It is dry by dry kiln for 6mm, obtain ceramic big plate green compact；
4) ceramic big plate green compact are applied ground coat enamel, ink-jet decoration, apply overglaze by Belt Conveying, into height in roller kilns
Temperature firing, firing temperature are 1185~1215 DEG C, and firing time is 110~180min, through cooling, edging, packaging to get implementation
The 3 big board finished product of ceramics of example.
Embodiment 4: performance test
Above-described embodiment 1~3 is prepared into the big board finished product of resulting ceramics and carries out correlated performance test, test result respectively
As shown in table 1 below.
The big board finished product correlated performance test result of table 1 Examples 1 to 3 ceramics
Above-described embodiment is the preferred embodiment of the present invention, all with similar technique of the invention and made equivalence changes,
It should belong to protection category of the invention.
Claims (5)
1. a kind of big plate of environment-friendly ceramic, it is characterised in that green body includes following component according to the weight percentage of raw materials:
2. the big plate of a kind of environment-friendly ceramic according to claim 1, it is characterised in that: the reclaimed materials is selected from Production of Ceramics
The base powder that the cause breakage for cutting remaining corner base powder and ceramics into roller way kiln firing in the process generates.
3. the big plate of a kind of environment-friendly ceramic according to claim 1, it is characterised in that: the chemical component master of the reclaimed materials
It to include SiO2And Al2O3。
4. the big plate of a kind of environment-friendly ceramic according to claim 1, it is characterised in that: in the kaolin containing 5~
10% calcined kaolin.
5. a kind of preparation method of such as big plate of the described in any item environment-friendly ceramics of Claims 1 to 4, it is characterised in that including such as
Lower processing step:
1) it mixes by other components investment ball mill in addition to reclaimed materials according to the weight percentage of raw materials, obtains original slurry material；
2) recycling slurry is made by wet process automatic recycling device in reclaimed materials according to the weight percentage of raw materials, then by original slurry material with
Slurry is recycled with 100:(8~10) ratio mixing, mixed slurry is made, by sieving, it is aging, except iron, ink-jet it is dry, must make pottery
Porcelain sheet slab powder；
3) ceramic sheet slab powder compression moulding after press cloth, it is dry by dry kiln, obtain ceramic big plate green compact；
4) ceramic big plate green compact are applied ground coat enamel, ink-jet decoration, apply overglaze, burnt into roller kilns high temperature by Belt Conveying
At firing temperature is 1185~1215 DEG C, and firing time is 110~180min, through cooling, edging, packaging to get the big plate of ceramics
Finished product.
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| CN201811128768.1A CN109081683A (en) | 2018-09-26 | 2018-09-26 | A kind of big plate of environment-friendly ceramic and preparation method thereof |
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Cited By (9)
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| CN109626975A (en) * | 2019-02-27 | 2019-04-16 | 佛山石湾鹰牌陶瓷有限公司 | A kind of firing process of the big plate of ceramics |
| CN109665826A (en) * | 2018-12-27 | 2019-04-23 | 广州美和成厨卫科技有限公司 | A kind of high-strength ceramic plate and preparation method thereof |
| CN110066163A (en) * | 2019-05-24 | 2019-07-30 | 佛山市东鹏陶瓷有限公司 | A kind of preparation method and the big plate of ceramics of the big plate of stone multi-panel ceramics |
| CN110483010A (en) * | 2019-08-21 | 2019-11-22 | 蒙娜丽莎集团股份有限公司 | A kind of processability is good, high-strength large size ceramic plate and preparation method thereof |
| CN111704450A (en) * | 2020-05-22 | 2020-09-25 | 福建德胜新建材有限公司 | Preparation method of ceramic rock plate and ceramic rock plate |
| CN112250430A (en) * | 2020-08-31 | 2021-01-22 | 杨纲雄 | Porcelain clay, porcelain and preparation method thereof |
| CN115246735A (en) * | 2022-08-01 | 2022-10-28 | 河北浩锐陶瓷制品有限公司 | Production process of energy-saving environment-friendly ceramic tile |
| CN115838274A (en) * | 2022-09-19 | 2023-03-24 | 杭州诺贝尔陶瓷有限公司 | High-toughness and high-strength building ceramic rock slab blank and preparation method thereof |
| CN116835960A (en) * | 2023-07-11 | 2023-10-03 | 广东家美陶瓷有限公司 | Coated body preparation device and preparation method, coated body blank and preparation method |
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Application publication date: 20181225 |