CN108969393A - It is a kind of containing light oil without silicon cleaning-free hair conditioner and preparation method thereof - Google Patents
It is a kind of containing light oil without silicon cleaning-free hair conditioner and preparation method thereof Download PDFInfo
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- CN108969393A CN108969393A CN201811072900.1A CN201811072900A CN108969393A CN 108969393 A CN108969393 A CN 108969393A CN 201811072900 A CN201811072900 A CN 201811072900A CN 108969393 A CN108969393 A CN 108969393A
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- light oil
- hair conditioner
- containing light
- free hair
- oil
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
- A61K2800/34—Free of silicones
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Abstract
This application involves a kind of containing light oil without silicon cleaning-free hair conditioner, it is counted on the basis of weight percent, being made of following raw materials without silicon cleaning-free hair conditioner containing light oil: stearamidopropyl dimethylamine 1%-2%, cetostearyl alcohol 4%-5%, light oil 0.3%-3%, lactic acid 0.45%-1%, first moisturizer 1%-10%, second moisturizer 1%-5%, vegetable oil 0.1%-3%, vitamin E 0.1%-1%, disodium ethylene diamine tetraacetate 0.05%-0.1%, essence 0.5%-1%, the water of preservative 0.7%-0.8% and surplus.The application further relates to a kind of prepare the method without silicon cleaning-free hair conditioner containing light oil as described above.The beneficial effects of the present application are as follows substitute silicone oil using light oil such as benzyl carbinol benzoic ether, can make cleaning-free hair conditioner using it is rear it is salubrious, comfortable, without greasy feeling and make hair that there is apparent reflecting feel.
Description
Technical field
This application involves washing product technical fields.Specifically, it is disposable without silicon containing light oil that this application involves a kind of
Hair conditioner and preparation method thereof.
Background technique
There is many meanings for a people for hair, are far longer than male to the meaning of women.Dense healthy hair maid
Oomph multiplication.The Classical Design of beauty is long hair fluttering, but today's society is ubiquitous for the damage of hair, if
Schoolgirl's hair dries up bifurcated, just influences whether that women's is refined.Therefore, it is necessary to use hair conditioner hair is made to keep gloss bright
It is beautiful.
Hair conditioner is also referred to as Rinsing, usually uses in pairs with shampoo.It has been generally acknowledged that hair has negative electrical charge, shampoo washing hair is used
Afterwards, hair can be made to cause the hair after washing to be difficult to comb to generate electrostatic with more negative electrical charges.Shampoo usually contains
Based on anionic surfactant and nonionic surfactant, it can be neutralized using hair conditioner and remain in band yin in hair surface
The molecule of ion forms monomolecular film, and keeps the hair to tangle submissive, is easy to comb.But currently used in the market is mostly punching
Type hair conditioner is washed, needs to wash using clear water after use, this had both easily caused the hair scale piece surface of hair to come to harm, can also wave
Take a large amount of water.
In view of the deficiency of above-mentioned washing hair conditioner, cleaning-free hair conditioner is this can to make hair keep gloss beautiful whenever and wherever possible
Favor of the product by numerous women.Most of traditional cleaning-free hair conditioner all adds silicone oil, although silicone oil itself is to scalp
Hair is not done harm to, but can be deposited in root of hair with being difficult to avoid that during use, and scalp and hair-care is enabled to be easy to appear greasy, hair
The not fluffy phenomenon of collapsing.
For this purpose, there is an urgent need in the art to develop after a kind of use it is salubrious, comfortable, have without greasy feeling and to hair apparent
Reflecting feel without silicon cleaning-free hair conditioner and preparation method thereof.
Summary of the invention
The application be designed to provide it is a kind of containing light oil without silicon cleaning-free hair conditioner, to solve the above-mentioned prior art
In technical problem.The application innovatively uses light oil such as benzyl carbinol benzoic ether substitution silicone oil, and selects suitably
Moisturizing agent composition and vegetable oil as raw material, can make cleaning-free hair conditioner using it is rear it is salubrious, comfortable, without greasy feeling and have hair
There is apparent reflecting feel.
The purpose of the application, which also resides in provide, a kind of prepares the side without silicon cleaning-free hair conditioner containing light oil as described above
Method.
To achieve the goals above, the application provides following technical proposals.
In the first aspect, the application provide it is a kind of containing light oil without silicon cleaning-free hair conditioner, using weight percent as base
Quasi- meter, being made of following raw materials without silicon cleaning-free hair conditioner containing light oil:
Stearamidopropyl dimethylamine 1%-2%,
Cetostearyl alcohol 4%-5%,
Light oil 0.3%-3%,
Lactic acid 0.45%-1%,
First moisturizer 1%-10%,
Second moisturizer 1%-5%,
Vegetable oil 0.1%-3%,
Vitamin E 0.1%-1%,
Disodium ethylene diamine tetraacetate 0.05%-0.1%,
Essence 0.5%-1%,
Preservative 0.7%-0.8%, and
The water of surplus.
In a kind of embodiment of first aspect, the light oil includes benzyl carbinol benzoic ether.
In a kind of embodiment of first aspect, first moisturizer includes glycerol and/or panthenol.
In a kind of embodiment of first aspect, second moisturizer includes Miglyol 812N.
In a kind of embodiment of first aspect, the vegetable oil includes camellia seed oil.
In a kind of embodiment of first aspect, counted on the basis of weight percent, it is described to exempt from containing light oil without silicon
Hair conditioner is washed to be made of following raw materials:
Stearamidopropyl dimethylamine 1.3%,
Cetostearyl alcohol 5%,
Benzyl carbinol benzoic ether 3%,
Lactic acid 0.45%,
Glycerol 3%,
Miglyol 812N 3%,
Camellia seed oil 1%,
Vitamin E 0.3%,
Disodium ethylene diamine tetraacetate 0.05%,
Essence 0.6%,
Preservative 0.73%,
With the water of surplus.
In a kind of embodiment of first aspect, counted on the basis of weight percent, it is described to exempt from containing light oil without silicon
Hair conditioner is washed to be made of following raw materials:
Stearamidopropyl dimethylamine 1.6%,
Cetostearyl alcohol 4.5%,
Benzyl carbinol benzoic ether 2%,
Lactic acid 0.72%,
Glycerol 6%,
Miglyol 812N 2%,
Camellia seed oil 2%,
Vitamin E 0.7%,
Disodium ethylene diamine tetraacetate 0.1%,
Essence 0.8%,
Preservative 0.76%,
With the water of surplus.
In a kind of embodiment of first aspect, counted on the basis of weight percent, it is described to exempt from containing light oil without silicon
Hair conditioner is washed to be made of following raw materials:
Stearamidopropyl dimethylamine 2%,
Cetostearyl alcohol 4%,
Benzyl carbinol benzoic ether 1%,
Lactic acid 0.9%,
Glycerol 10%,
Miglyol 812N 1%,
Camellia seed oil 3%,
Vitamin E 0.1%,
Disodium ethylene diamine tetraacetate 0.1%,
Essence 1%,
Preservative 0.8%,
With the water of surplus.
In second aspect, the application provide it is a kind of prepare as described in relation to the first aspect containing light oil without silicon washing-free hair
The method of element, the method includes the following steps:
(1) disodium ethylene diamine tetraacetate, the first moisturizer and lactic acid are mixed in water, and stirring is warming up to the first temperature, obtains
To the first reaction mixture；
(2) cetostearyl alcohol, stearamidopropyl dimethylamine, light oil, vegetable oil and the second moisturizer are mixed, stirring is simultaneously
Second temperature is warming up to being completely dissolved, obtains the second reaction mixture；
(3) the first reaction mixture and second mixture is mixed to be cooled to third temperature after stirring 10-15 minutes, obtain
To third reaction mixture；
(4) vitamin E, preservative and essence are added into third reaction mixture, stirs evenly, it is mixed to obtain the 4th reaction
Close object；And
(5) when the 4th reaction mixture is cooled to four temperature, blowing, obtain it is described containing light oil without the disposable shield of silicon
Hair element.
In a kind of embodiment of second aspect, the step (1) carries out in emulsion pot.
In a kind of embodiment of second aspect, first temperature is 80-90 DEG C；And/or the second temperature is
90-95℃；And/or the third temperature is 40-45 DEG C；And/or the 4th temperature is 35-38 DEG C.
Compared with prior art, the beneficial effects of the present application are as follows using light oil such as benzyl carbinol benzoic ether substituted for silicon
Oil, can make cleaning-free hair conditioner using it is rear it is salubrious, comfortable, without greasy feeling and make hair that there is apparent reflecting feel.
Detailed description of the invention
Fig. 1 shows the dry comb drop in resistance rate according to embodiment and comparative example.
Fig. 2 shows the smoothness test result according to embodiment and comparative example.
Fig. 3 shows the glossiness test result according to embodiment and comparative example.
Fig. 4 shows the moistening test result according to embodiment and comparative example.
Specific embodiment
Term "comprising", " comprising ", " having " and their derivative are not excluded for any other component, step or mistake
The presence of journey, and whether disclose in this application with these other components, step or process unrelated.To eliminate any query,
Unless expressly stated, otherwise in the application it is all use term "comprising"s, " comprising ", or " having " composition may include appoint
What additional additive, auxiliary material or compound.On the contrary, in addition to necessary to operating characteristics those, term " substantially by ...
Composition " excludes any other component, step or process except the hereinafter described range of any term.Term " by ...
Composition " does not include any component, step or the process for not specifically describing or listing.Unless expressly stated, otherwise term "or" refers to
Separate member listed or any combination thereof.
Embodiment
Below in conjunction with the embodiment of the present invention, clear and complete description is carried out to technical solution of the present invention.Such as nothing
It illustrates, reagent used and raw material can all be bought by commercial sources.
Synthetic example 1-4
The formula of synthetic example 1-4 is as follows:
Synthetic example 1-4 without silicon cleaning-free hair conditioner the preparation method is as follows:
(1) water, EDETATE SODIUM, glycerol, lactic acid are added in emulsion pot, stirring is warming up to 90 DEG C, for use.
(2) in oil cauldron be added cetostearyl alcohol, stearamidopropyl dimethylamine, benzyl carbinol benzoic ether, camellia seed oil,
Miglyol 812N stirs and is warming up to 90 DEG C to being completely dissolved, for use.
(3) raw material dissolved in oil cauldron is poured into emulsion pot, it is cooling after stirring 10-15 minutes.
(4) when Material is cooled to 45 DEG C, vitamin E, preservative and essence is added, stirs evenly.
(5) when Material is cooled to 38 DEG C, blowing, obtain each embodiment without silicon cleaning-free hair conditioner.
Comparative example
Comparative example is containing silicone oil but without benzyl carbinol benzoic ether without silicon cleaning-free hair conditioner.
Comparative formulation is as follows:
| Stearamidopropyl dimethylamine | 1 |
| Cetostearyl alcohol | 4.5 |
| Dimethyl silicone polymer | 0.5 |
| Lactic acid | 0.45 |
| Glycerol | 1 |
| Camellia seed oil | 0.1 |
| Miglyol 812N | 5 |
| Vitamin E | 1 |
| EDETATE SODIUM | 0.05 |
| Essence | 0.5 |
| Preservative | 0.7 |
Comparative example without silicon cleaning-free hair conditioner the preparation method is as follows:
(1) water, EDETATE SODIUM, glycerol, lactic acid are added in emulsion pot, stirring is warming up to 90 DEG C, for use.
(2) in oil cauldron be added cetostearyl alcohol, stearamidopropyl dimethylamine, dimethyl silicone polymer, camellia seed oil,
Miglyol 812N stirs and is warming up to 90 DEG C to being completely dissolved, for use.
(3) raw material dissolved in oil cauldron is poured into emulsion pot, it is cooling after stirring 10-15 minutes.
(4) when Material is cooled to 45 DEG C, vitamin E, preservative and essence is added, stirs evenly.
(5) when Material is cooled to 38 DEG C, blowing, obtain comparative example without silicon cleaning-free hair conditioner.
Efficacy test:
1. instrument test
Using standard shampooing (melissa shampoo), by 6 beams, naturally untreated Asia topknot is cleaned to non-foam, to topknot
Under conditions of 25 DEG C of room temperature, humidity 60% after natural drying, the cleaning-free hair conditioner of 0.5g embodiment and comparative example is weighed respectively,
It is uniformly applied on topknot, dry comb test is carried out on JC45B (model) combing instrument, while hair conditioner will be not used after cleaning
Topknot is compared as blank sample, shown in result table 1 as follows and Fig. 1.
The dry comb test result of the hair conditioner of table 1. embodiment 1-4 and comparative example 1-2
From table 1 and Fig. 1: the dry comb resistance without silicon cleaning-free hair conditioner of embodiment 4 is minimum, is slightly better than comparative example.
2. organoleptic detection
60 triers are selected, after washing hair using standard shampooing and drying up, 6 groups are randomly divided into, respectively using real
Apply example 1 without silicon cleaning-free hair conditioner, the hair conditioner of embodiment 2, the hair conditioner of embodiment 3, the hair conditioner of embodiment 4, comparative example
Cleaning-free hair conditioner, by expert group to the smoothness of hair conditioner, brightness, moistening carry out various aspects marking (1 assigns to 5
Point), and be averaged.Test result is as follows text table 2 and Fig. 2-4 shown in, wherein Fig. 2 is shown according to embodiment and comparative example
Smoothness test result；Fig. 3 shows the glossiness test result according to embodiment and comparative example；Fig. 4 show according to embodiment and
The moistening test result of comparative example.
The hair conditioner sensory test result of table 2. embodiment 1-4 and comparative example
| Sample | Smoothness | Glossiness | Moistening |
| Case 1 | 4.3 | 3.6 | 3.8 |
| Case 2 | 4.6 | 4.8 | 4.2 |
| Case 3 | 4.2 | 4.2 | 4.5 |
| Case 4 | 4.5 | 3.8 | 4.8 |
| Comparative example | 4.3 | 4.1 | 3.6 |
By table 2, Fig. 2, Fig. 3 and Fig. 4 it is found that in terms of smoothness, embodiment 2 is preferably and better than comparative example；In glossiness
Aspect, embodiment 2 preferably, and are better than comparative example；In terms of moistening, embodiment 4 preferably, and is better than comparative example.
Conclusion: described herein without containing silicone oil and to joined light oil benzene second without silicon cleaning-free hair conditioner containing light oil
Alcohol benzoic ether obviously feels salubrious, comfortable, no greasy feeling after use, have apparent reflecting feel to hair, can reach addition
The product of silicone oil is same or better effect.
The above-mentioned description to embodiment is that this Shen can be understood and applied for the ease of those skilled in the art
Please.Person skilled in the art obviously easily can make various modifications to these embodiments, and described herein
General Principle is applied in other embodiments without paying creative labor.Therefore, the application is not limited to implementation here
Example, those skilled in the art make according to herein disclosed content in the case where not departing from the application scope and spirit
It improves and modifies within all scope of the present application.
Claims (10)
1. it is a kind of containing light oil without silicon cleaning-free hair conditioner, counted on the basis of weight percent, it is described to exempt from containing light oil without silicon
Hair conditioner is washed to be made of following raw materials:
Stearamidopropyl dimethylamine 1%-2%,
Cetostearyl alcohol 4%-5%,
Light oil 0.3%-3%,
Lactic acid 0.45%-1%,
First moisturizer 1%-10%,
Second moisturizer 1%-5%,
Vegetable oil 0.1%-3%,
Vitamin E 0.1%-1%,
Disodium ethylene diamine tetraacetate 0.05%-0.1%,
Essence 0.5%-1%,
Preservative 0.7%-0.8%, and
The water of surplus.
2. as described in claim 1 containing light oil without silicon cleaning-free hair conditioner, which is characterized in that the light oil includes benzene second
Alcohol benzoic ether.
3. as described in claim 1 containing light oil without silicon cleaning-free hair conditioner, which is characterized in that first moisturizer includes
Glycerol and/or panthenol；And/or second moisturizer includes Miglyol 812N.
4. as described in claim 1 containing light oil without silicon cleaning-free hair conditioner, which is characterized in that the vegetable oil includes camellia
Seed oil.
5. as described in claim 1 containing light oil without silicon cleaning-free hair conditioner, which is characterized in that on the basis of weight percent
Meter, being made of following raw materials without silicon cleaning-free hair conditioner containing light oil:
Stearamidopropyl dimethylamine 1.3%,
Cetostearyl alcohol 5%,
Benzyl carbinol benzoic ether 3%,
Lactic acid 0.45%,
Glycerol 3%,
Miglyol 812N 3%,
Camellia seed oil 1%,
Vitamin E 0.3%,
Disodium ethylene diamine tetraacetate 0.05%,
Essence 0.6%,
Preservative 0.73%,
With the water of surplus.
6. as described in claim 1 containing light oil without silicon cleaning-free hair conditioner, which is characterized in that on the basis of weight percent
Meter, being made of following raw materials without silicon cleaning-free hair conditioner containing light oil:
Stearamidopropyl dimethylamine 1.6%,
Cetostearyl alcohol 4.5%,
Benzyl carbinol benzoic ether 2%,
Lactic acid 0.72%,
Glycerol 6%,
Miglyol 812N 2%,
Camellia seed oil 2%,
Vitamin E 0.7%,
Disodium ethylene diamine tetraacetate 0.1%,
Essence 0.8%,
Preservative 0.76%,
With the water of surplus.
7. as described in claim 1 containing light oil without silicon cleaning-free hair conditioner, which is characterized in that on the basis of weight percent
Meter, being made of following raw materials without silicon cleaning-free hair conditioner containing light oil:
Stearamidopropyl dimethylamine 2%,
Cetostearyl alcohol 4%,
Benzyl carbinol benzoic ether 1%,
Lactic acid 0.9%,
Glycerol 10%,
Miglyol 812N 1%,
Camellia seed oil 3%,
Vitamin E 0.1%,
Disodium ethylene diamine tetraacetate 0.1%,
Essence 1%,
Preservative 0.8%,
With the water of surplus.
8. a kind of method without silicon cleaning-free hair conditioner prepared as of any of claims 1-7 containing light oil, described
Method includes the following steps:
(1) disodium ethylene diamine tetraacetate, the first moisturizer and lactic acid are mixed in water, and stirring is warming up to the first temperature, obtains the
One reaction mixture；
(2) cetostearyl alcohol, stearamidopropyl dimethylamine, light oil, vegetable oil and the second moisturizer are mixed, stirs and heats up
To second temperature to being completely dissolved, the second reaction mixture is obtained；
(3) the first reaction mixture and second mixture are mixed and is cooled to third temperature after stirring 10-15 minutes, obtains the
Three reaction mixtures；
(4) vitamin E, preservative and essence are added into third reaction mixture, stirs evenly, obtains the 4th reaction mixing
Object；And
(5) when the 4th reaction mixture is cooled to four temperature, blowing, obtain it is described containing light oil without silicon washing-free hair
Element.
9. method according to claim 8, which is characterized in that the step (1) carries out in emulsion pot.
10. method as claimed in claim 8 or 9, which is characterized in that first temperature is 80-90 DEG C；And/or described
Two temperature are 90-95 DEG C；And/or the third temperature is 40-45 DEG C；And/or the 4th temperature is 35-38 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811072900.1A CN108969393B (en) | 2018-09-14 | 2018-09-14 | Light oil-containing silicon-free wash-free hair conditioner and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811072900.1A CN108969393B (en) | 2018-09-14 | 2018-09-14 | Light oil-containing silicon-free wash-free hair conditioner and preparation method thereof |
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| Publication Number | Publication Date |
|---|---|
| CN108969393A true CN108969393A (en) | 2018-12-11 |
| CN108969393B CN108969393B (en) | 2021-02-19 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111195220A (en) * | 2020-02-12 | 2020-05-26 | 中国热带农业科学院海口实验站 | Hair conditioner with repairing function and preparation method and application thereof |
Citations (3)
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|---|---|---|---|---|
| WO2005069822A2 (en) * | 2004-01-14 | 2005-08-04 | Finetex, Inc. | Phenylethyl benzoate for use in cosmetics, toiletries and personal care products |
| CN101427986A (en) * | 2008-12-17 | 2009-05-13 | 广东名臣有限公司 | Cleaning-free hair conditioner and method of producing the same |
| US20170252279A1 (en) * | 2006-04-10 | 2017-09-07 | Inolex Investment Corporation | Hair Conditioning Cosmetic Compositions Containing a Mixture of Amidoamines |
-
2018
- 2018-09-14 CN CN201811072900.1A patent/CN108969393B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2005069822A2 (en) * | 2004-01-14 | 2005-08-04 | Finetex, Inc. | Phenylethyl benzoate for use in cosmetics, toiletries and personal care products |
| US20170252279A1 (en) * | 2006-04-10 | 2017-09-07 | Inolex Investment Corporation | Hair Conditioning Cosmetic Compositions Containing a Mixture of Amidoamines |
| CN101427986A (en) * | 2008-12-17 | 2009-05-13 | 广东名臣有限公司 | Cleaning-free hair conditioner and method of producing the same |
Non-Patent Citations (1)
| Title |
|---|
| 上海华银日用品有限公司: "《国产非特殊用途化妆品备案》", 29 April 2018 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111195220A (en) * | 2020-02-12 | 2020-05-26 | 中国热带农业科学院海口实验站 | Hair conditioner with repairing function and preparation method and application thereof |
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