CN108926875A - A kind of quick sinking cooling device of tyrosine processing - Google Patents
A kind of quick sinking cooling device of tyrosine processing Download PDFInfo
- Publication number
- CN108926875A CN108926875A CN201810518746.XA CN201810518746A CN108926875A CN 108926875 A CN108926875 A CN 108926875A CN 201810518746 A CN201810518746 A CN 201810518746A CN 108926875 A CN108926875 A CN 108926875A
- Authority
- CN
- China
- Prior art keywords
- fixedly mounted
- cooling
- cabinet
- slot
- sinking
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000001816 cooling Methods 0.000 title claims abstract description 59
- OUYCCCASQSFEME-QMMMGPOBSA-N L-tyrosine Chemical compound OC(=O)[C@@H](N)CC1=CC=C(O)C=C1 OUYCCCASQSFEME-QMMMGPOBSA-N 0.000 title claims abstract description 19
- OUYCCCASQSFEME-UHFFFAOYSA-N tyrosine Natural products OC(=O)C(N)CC1=CC=C(O)C=C1 OUYCCCASQSFEME-UHFFFAOYSA-N 0.000 title claims abstract description 19
- 239000000498 cooling water Substances 0.000 claims abstract description 41
- 230000003472 neutralizing effect Effects 0.000 claims abstract description 25
- 239000007788 liquid Substances 0.000 claims abstract description 18
- NJPPVKZQTLUDBO-UHFFFAOYSA-N novaluron Chemical compound C1=C(Cl)C(OC(F)(F)C(OC(F)(F)F)F)=CC=C1NC(=O)NC(=O)C1=C(F)C=CC=C1F NJPPVKZQTLUDBO-UHFFFAOYSA-N 0.000 claims abstract description 18
- 238000000034 method Methods 0.000 claims abstract description 15
- 238000005192 partition Methods 0.000 claims abstract description 13
- 238000002347 injection Methods 0.000 claims abstract description 9
- 239000007924 injection Substances 0.000 claims abstract description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 16
- 239000000706 filtrate Substances 0.000 claims description 10
- 239000010802 sludge Substances 0.000 claims description 9
- 239000007921 spray Substances 0.000 claims description 9
- 238000009434 installation Methods 0.000 claims description 5
- 230000017525 heat dissipation Effects 0.000 claims description 4
- 238000005119 centrifugation Methods 0.000 claims 1
- 239000013049 sediment Substances 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- 239000002893 slag Substances 0.000 description 3
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 2
- 239000000908 ammonium hydroxide Substances 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 239000012530 fluid Substances 0.000 description 2
- 239000012452 mother liquor Substances 0.000 description 2
- 238000006386 neutralization reaction Methods 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000013003 hot bending Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D21/00—Separation of suspended solid particles from liquids by sedimentation
- B01D21/009—Heating or cooling mechanisms specially adapted for settling tanks
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D21/00—Separation of suspended solid particles from liquids by sedimentation
- B01D21/003—Sedimentation tanks provided with a plurality of compartments separated by a partition wall
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D21/00—Separation of suspended solid particles from liquids by sedimentation
- B01D21/0039—Settling tanks provided with contact surfaces, e.g. baffles, particles
- B01D21/0045—Plurality of essentially parallel plates
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D21/00—Separation of suspended solid particles from liquids by sedimentation
- B01D21/02—Settling tanks with single outlets for the separated liquid
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D21/00—Separation of suspended solid particles from liquids by sedimentation
- B01D21/24—Feed or discharge mechanisms for settling tanks
- B01D21/2405—Feed mechanisms for settling tanks
Abstract
The invention discloses a kind of tyrosine to process quick sinking cooling device,Including cooling water tank,Cabinet,Exchange heat bend pipe,Centrifugal pump,Neutralizing tank and pedestal,Neutralizing tank is fixedly mounted in the top left side of the pedestal,Cabinet is fixedly mounted in the top right side of pedestal,Centrifugal pump is fixedly mounted in the top of pedestal,Centrifugal pump is between neutralizing tank and cabinet,Liquid injection port is fixedly mounted in the top of neutralizing tank,Liquid outlet is fixedly mounted in the bottom outer wall of neutralizing tank,Circulating pump and cooling water tank is fixedly mounted in the top of cabinet,Circulating pump is located at the left side of cooling water tank,Cabinet is seal case,Partition is fixedly mounted in the inside of cabinet,Cabinet is separated into cooling heat transferring slot and reservoir by partition,And cooling heat transferring slot position is in the top of reservoir,The tyrosine processing is simple with quick sinking cooling device structure,It is easy to use,Mixed liquor cooling velocity is fast,It is high-efficient to be classified sediment,To reduce the process-cycle.
Description
Technical field
The present invention relates to chemical field, specifically a kind of tyrosine processes quick sinking cooling device.
Background technique
It needs that Guang refinement mother liquor is mixed and neutralized with ammonium hydroxide in the process of tyrosine, Guang refinement mother liquor and ammonium hydroxide
Heat can be generated during neutralization reaction, needs to carry out sinking cooling to mixed liquor after neutralization reaction, simultaneously using plate-frame filtering
Junket fine work is separated with filtered fluid, under normal circumstances, for the cooling of mixed liquor sinking using the method for quiet system, concrete mode is will
Mixed liquor injection stands cooling tank or stands in cooling bath, cools down to its natural sedimentation, and this mode cooling rate is slow, sinking
Time is long, substantially prolongs tyrosine production cycle, inefficiency.
Summary of the invention
The purpose of the present invention is to provide a kind of tyrosine to process quick sinking cooling device, to solve above-mentioned background skill
The problem of being proposed in art.
To achieve the above object, the present invention provides the following technical solutions：
A kind of quick sinking cooling device of tyrosine processing, including cooling water tank, cabinet, heat exchange bend pipe, centrifugal pump, neutralizing tank
And neutralizing tank is fixedly mounted in pedestal, the top left side of the pedestal, cabinet, the top of pedestal is fixedly mounted in the top right side of pedestal
Centrifugal pump is fixedly mounted, centrifugal pump is between neutralizing tank and cabinet, and liquid injection port is fixedly mounted in the top of neutralizing tank, neutralizing tank
Liquid outlet is fixedly mounted in bottom outer wall, circulating pump is fixedly mounted for the top of cabinet and cooling water tank, circulating pump are located at cooling water
The left side of case, cabinet are seal case, and partition is fixedly mounted in the inside of cabinet, and cabinet is separated into cooling heat transferring slot and storage by partition
Liquid bath, and cooling heat transferring slot position is in the top of reservoir.
As a further solution of the present invention：Fixed installation heat exchange bend pipe in the cooling heat transferring slot, the one of the bend pipe that exchanges heat
End is connected by the water outlet of conduit and centrifugal pump, and the water inlet end of centrifugal pump is connect by conduit with pot bottom liquid outlet is neutralized,
The other end of heat exchange bend pipe installs straight tube, and straight tube is through in reservoir, and straight tube is fixedly mounted on partition by support of pipelines
Top, and the nozzle of straight tube is located at the left side of reservoir.
As further scheme of the invention：Four pieces of sinking slot plate washers of bottom fixed installation of the reservoir, every piece
Sinking slot plate washer spaced set forms sinking slot between every piece of sinking slot plate washer, and the bottom right of reservoir, which is fixedly mounted, to overflow
Flowing plate, the outer right wall bottom of reservoir are fixedly mounted with valvular filtrate (liquid, are fixedly mounted on the front bulkhead of reservoir
Four with valvular sludge outlet, and each sludge outlet is respectively positioned on the front bulkhead of corresponding sinking slot.
As further scheme of the invention：The height of the overflow plate is higher than sinking slot plate washer.
As further scheme of the invention：Shower plate, shower plate is fixedly mounted in the inner tip of the cooling water tank
Bottom several spray heads are fixedly mounted, arc heat sink is fixedly mounted in the inside of cooling water tank, and arc heat sink is located at shower plate
Underface, the water inlet end of circulating pump is connected to by conduit with the left bottom of cooling heat transferring slot, the water outlet of circulating pump and spray
The water inlet end connection of plate is drenched, return pipe, the top of return pipe and cooling heat transferring slot is fixedly mounted in the right side wall bottom of cooling water tank
Connection.
As further scheme of the invention：The front and back end of the arc heat sink is through to the outside of cooling water tank,
And arc heat sink is located at the outer end portion fixed installation radiating fin of cooling water tank.
Compared with prior art, the beneficial effects of the invention are as follows：
This utility structure is simple, easy to use, and the mixed liquor in neutralizing tank is pumped into heat exchange bend pipe by centrifugal pump, then via changing
Hot bending pipe end straight tube injects in reservoir, and mixed liquor successively fills up sinking slot from left to right, extends the sinking time, and make filtrate
It is sufficiently separated with filter residue, exchanges heat when mixed liquor flows through heat exchange bend pipe with cooling water, thus accelerate mixed liquor cooling velocity,
Cooling water is pumped into shower plate by circulating pump out of cooling heat transferring slot simultaneously, and is sprayed on arc heat sink by spray head, after cooling
Cooling water be back in cooling heat transferring slot through return pipe, to form circulating water, the external fixed peace of arc heat sink
Radiating fin is filled, the heat dissipation area of arc heat sink is increased, further increases cooling velocity, to reduce the production cycle.
Detailed description of the invention
Fig. 1 is the structural schematic diagram that tyrosine processes quick sinking cooling device.
Fig. 2 is the cross-sectional view that tyrosine processes quick sinking cooling device.
Fig. 3 is the structural schematic diagram that tyrosine processes arc heat sink in quick sinking cooling device.
In figure：Liquid injection port 1, cooling water tank 2, shower plate 3, circulating pump 4, spray head 5, arc heat sink 6, cooling heat transferring slot 7,
Cabinet 8, heat exchange bend pipe 9, support of pipelines 10, partition 11, overflow plate 12, sinking slot plate washer 13, reservoir 14, filtrate (liquid 15,
Sinking slot 16, centrifugal pump 17, neutralizing tank 18, radiating fin 19, sludge outlet 20, pedestal 21.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete
Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on
Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other
Embodiment shall fall within the protection scope of the present invention.
Please refer to Fig. 1~3, in the embodiment of the present invention, a kind of tyrosine processing quick sinking cooling device, including fluid injection
Mouthful 1, cooling water tank 2, shower plate 3, circulating pump 4, spray head 5, arc heat sink 6, cooling heat transferring slot 7, cabinet 8, heat exchange bend pipe 9,
Support of pipelines 10, partition 11, overflow plate 12, sinking slot plate washer 13, reservoir 14, filtrate (liquid 15, sinking slot 16, centrifugal pump
17, neutralizing tank is fixedly mounted in the top left side of neutralizing tank 18, radiating fin 19, sludge outlet 20 and pedestal 21, the pedestal 21
18, cabinet 8 is fixedly mounted in the top right side of pedestal 21, and centrifugal pump 17 is fixedly mounted in the top of pedestal 21, during centrifugal pump 17 is located at
Between tank 18 and cabinet 8, liquid injection port 1 is fixedly mounted in the top of neutralizing tank 18, is fixedly mounted in the bottom outer wall of neutralizing tank 18
Circulating pump 4 is fixedly mounted for the top of liquid outlet, cabinet 8 and cooling water tank 2, circulating pump 4 are located at the left side of cooling water tank 2, cabinet 8
Partition 11 is fixedly mounted in inside for seal case, cabinet 8, and cabinet 8 is separated into cooling heat transferring slot 7 and reservoir by partition 11
14, and cooling heat transferring slot 7 is located at the top of reservoir 14, and heat exchange bend pipe 9 is fixedly mounted in the cooling heat transferring slot 7, exchanges heat curved
One end of pipe 9 is connect by conduit with the water outlet of centrifugal pump 17, and the water inlet end of centrifugal pump 17 passes through conduit and 18 bottom of neutralizing tank
The other end of the connection of portion's liquid outlet, heat exchange bend pipe 9 installs straight tube, and straight tube is through in reservoir 14, and straight tube passes through support of pipelines
10 are fixedly mounted on the top of partition 11, and the nozzle of straight tube is located at the left side of reservoir 14；The bottom of the reservoir 14 is solid
Dingan County fills four pieces of sinking slot plate washers 13, every piece of 13 spaced set of sinking slot plate washer, and it is heavy to be formed between every piece of sinking slot plate washer 13
Slot 16 is put, overflow plate 12 is fixedly mounted in the bottom right of reservoir 14, and the outer right wall bottom of reservoir 14, which is fixedly mounted, to be had
Four are fixedly mounted on the front bulkhead of reservoir 14 with valvular sludge outlet 20 for the filtrate (liquid 15 of valve, and each filter
Slag outlet 20 is respectively positioned on the front bulkhead of corresponding sinking slot 16；The height of the overflow plate 12 is higher than sinking slot plate washer 13；It is described
Shower plate 3 is fixedly mounted in the inner tip of cooling water tank 2, and several spray heads 5 are fixedly mounted in the bottom of shower plate 3, cooling water tank 2
Arc heat sink 6 is fixedly mounted in inside, and arc heat sink 6 is located at the underface of shower plate 3, and the water inlet end of circulating pump 4 is by leading
Pipe is connected to the left bottom of cooling heat transferring slot 7, and the water outlet of circulating pump 4 is connect with the water inlet end of shower plate 3, cooling water tank 2
Right side wall bottom return pipe is fixedly mounted, return pipe is connected to the top of cooling heat transferring slot 7；Before the arc heat sink 6
Rear end is through to the outside of cooling water tank 2, and arc heat sink 6 is located at the outer end portion fixed installation radiating fin of cooling water tank 2
Piece 19；In use, the mixed liquor in neutralizing tank 18 is pumped into heat exchange bend pipe 9 by centrifugal pump 17, then via 9 end of heat exchange bend pipe
It holds in straight tube injection reservoir 14, mixed liquor successively fills up sinking slot 16 from left to right, extends the sinking time, and make filtrate and filter
Slag is sufficiently separated, and filter residue is deposited in the slot bottom of sinking slot 16, and filtrate can cross the spilling of overflow plate 12, and filter residue passes through 20 row of sludge outlet
Out, cooling water is stored in cooling heat transferring slot 7, exchanged heat when mixed liquor flows through heat exchange bend pipe 9 with cooling water, to accelerate
Mixed liquor cooling velocity, while cooling water is pumped into shower plate 3 by circulating pump 4 from cooling heat transferring slot 7, and is sprayed on by spray head 5
On arc heat sink 6, to cool down to cooling water, the cooling water after cooling is back in cooling heat transferring slot 7 through return pipe,
To improve radiating efficiency, the external of arc heat sink 6 is fixedly mounted radiating fin 19, increases the heat dissipation of arc heat sink 6
Area further increases cooling velocity, to reduce the production cycle.
The working principle of the invention is：
In use, the mixed liquor in neutralizing tank 18 is pumped into heat exchange bend pipe 9 by centrifugal pump 17, then via 9 end of heat exchange bend pipe
It holds in straight tube injection reservoir 14, mixed liquor successively fills up sinking slot 16 from left to right, extends the sinking time, and make filtrate and filter
Slag is sufficiently separated, and filter residue is deposited in the slot bottom of sinking slot 16, and filtrate can cross the spilling of overflow plate 12, and filter residue passes through 20 row of sludge outlet
Out, cooling water is stored in cooling heat transferring slot 7, exchanged heat when mixed liquor flows through heat exchange bend pipe 9 with cooling water, to accelerate
Mixed liquor cooling velocity, while cooling water is pumped into shower plate 3 by circulating pump 4 from cooling heat transferring slot 7, and is sprayed on by spray head 5
On arc heat sink 6, to cool down to cooling water, the cooling water after cooling is back in cooling heat transferring slot 7 through return pipe,
To improve radiating efficiency, the external of arc heat sink 6 is fixedly mounted radiating fin 19, increases the heat dissipation of arc heat sink 6
Area further increases cooling velocity, to reduce the production cycle.
Although the present invention is described in detail referring to the foregoing embodiments, for those skilled in the art,
It is still possible to modify the technical solutions described in the foregoing embodiments, or part of technical characteristic is carried out etc.
With replacement, all within the spirits and principles of the present invention, any modification, equivalent replacement, improvement and so on should be included in this
Within the protection scope of invention.
Claims (6)
1. a kind of tyrosine processes quick sinking cooling device, including cooling water tank (2), cabinet (8), exchange heat bend pipe (9), from
Heart pump (17), neutralizing tank (18) and pedestal (21), which is characterized in that neutralizing tank is fixedly mounted in the top left side of the pedestal (21)
(18), cabinet (8) are fixedly mounted in the top right side of pedestal (21), and centrifugal pump (17) are fixedly mounted in the top of pedestal (21), centrifugation
Pump (17) is located between neutralizing tank (18) and cabinet (8), and liquid injection port (1) is fixedly mounted in the top of neutralizing tank (18), neutralizing tank
(18) liquid outlet is fixedly mounted in bottom outer wall, the top of cabinet (8) is fixedly mounted circulating pump (4) and cooling water tank (2), follows
Ring pump (4) is located at the left side of cooling water tank (2), and cabinet (8) is seal case, and partition (11) are fixedly mounted in the inside of cabinet (8),
Cabinet (8) is separated into cooling heat transferring slot (7) and reservoir (14) by partition (11), and cooling heat transferring slot (7) is located at reservoir
(14) top.
2. tyrosine according to claim 1 processes quick sinking cooling device, which is characterized in that the cooling heat transferring
Heat exchange bend pipe (9) is fixedly mounted in slot (7), one end of heat exchange bend pipe (9) is connect by conduit with the water outlet of centrifugal pump (17),
The water inlet end of centrifugal pump (17) is connect by conduit with neutralizing tank (18) bottom liquid outlet, the other end installation of heat exchange bend pipe (9)
Straight tube, straight tube are through in reservoir (14), and straight tube is fixedly mounted on the top of partition (11) by support of pipelines (10), and straight
The nozzle of pipe is located at the left side of reservoir (14).
3. tyrosine according to claim 1 processes quick sinking cooling device, which is characterized in that the reservoir
(14) four pieces of sinking slot plate washers (13), every piece of sinking slot plate washer (13) spaced set, every piece of sinking slot is fixedly mounted in bottom
Sinking slot (16) are formed between plate washer (13), overflow plate (12) are fixedly mounted in the bottom right of reservoir (14), reservoir (14)
Outer right wall bottom be fixedly mounted with valvular filtrate (liquid (15), four are fixedly mounted on the front bulkhead of reservoir (14)
With valvular sludge outlet (20), and each sludge outlet (20) is respectively positioned on the front bulkhead of corresponding sinking slot (16).
4. tyrosine according to claim 3 processes quick sinking cooling device, which is characterized in that the overflow plate
(12) height is higher than sinking slot plate washer (13).
5. tyrosine according to claim 1 processes quick sinking cooling device, which is characterized in that the cooling water tank
(2) shower plate (3) are fixedly mounted in inner tip, and several spray heads (5), cooling water tank (2) is fixedly mounted in the bottom of shower plate (3)
Inside arc heat sink (6) are fixedly mounted, arc heat sink (6) is located at the underface of shower plate (3), circulating pump (4) into
Water end (W.E.) is connected to by conduit with the left bottom of cooling heat transferring slot (7), the water inlet of the water outlet and shower plate (3) of circulating pump (4)
Return pipe is fixedly mounted in the right side wall bottom of end connection, cooling water tank (2), and return pipe is connected to the top of cooling heat transferring slot (7).
6. tyrosine according to claim 5 processes quick sinking cooling device, which is characterized in that the arc heat dissipation
The front and back end of plate (6) is through to the outside of cooling water tank (2), and arc heat sink (6) is located at the outer end portion of cooling water tank (2)
It is fixedly mounted radiating fin (19).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810518746.XA CN108926875A (en) | 2018-05-25 | 2018-05-25 | A kind of quick sinking cooling device of tyrosine processing |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810518746.XA CN108926875A (en) | 2018-05-25 | 2018-05-25 | A kind of quick sinking cooling device of tyrosine processing |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108926875A true CN108926875A (en) | 2018-12-04 |
Family
ID=64449187
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810518746.XA Pending CN108926875A (en) | 2018-05-25 | 2018-05-25 | A kind of quick sinking cooling device of tyrosine processing |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112619207A (en) * | 2020-11-24 | 2021-04-09 | 郑锦锦 | Environment-friendly water conservancy sediment device of easily clearing up |
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Application publication date: 20181204 |