CN108905284A - A kind of extraction and separation tank and its application method - Google Patents

A kind of extraction and separation tank and its application method Download PDF

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Publication number
CN108905284A
CN108905284A CN201811005914.1A CN201811005914A CN108905284A CN 108905284 A CN108905284 A CN 108905284A CN 201811005914 A CN201811005914 A CN 201811005914A CN 108905284 A CN108905284 A CN 108905284A
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China
Prior art keywords
tank body
extraction
tank
material guide
stirring plate
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CN201811005914.1A
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Chinese (zh)
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CN108905284B (en
Inventor
朱峰
郭俊
范翠玲
朱金龙
王瑞
张培岭
王婷婷
朱梅
朱林
朱小梅
班文洁
邱玉礼
张霞
朱方敏
王洒洒
尹佳君
张松
罗海荣
王峰
张婷
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Baotou Xintiandi Environmental Protection Anticorrosion Engineering Co ltd
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Anhui Mount Everest Bio Tech Ltd
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Priority to CN201811005914.1A priority Critical patent/CN108905284B/en
Publication of CN108905284A publication Critical patent/CN108905284A/en
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Extraction Or Liquid Replacement (AREA)

Abstract

本发明公开了一种萃取分离罐及其使用方法，涉及萃取装置技术领域技术领域。本发明包括罐体，罐体内设有空腔，罐体上设有多个进料管，每个进料管上均嵌入安装有液体流量计，罐体内设有搅拌装置，罐体的内壁上嵌入安装有螺旋加热管，罐体的下端转动连接有旋转导料台，罐体的周侧面设有多个出料管，出料管的下端设有排污嘴。本发明通过设置搅拌装置、螺旋加热管、出料管和旋转导料台，通过搅拌装置对罐体内部的混合萃取物进行搅拌提高萃取效率，同时螺旋加热管也能提高萃取效率，再控制旋转导料台转动到合适的出料管，实现萃取液层的分开流出，不受残留物的污染，提高了萃取精度。

The invention discloses an extraction and separation tank and a use method thereof, and relates to the technical field of extraction devices. The invention comprises a tank body, a cavity is arranged in the tank body, a plurality of feeding pipes are arranged on the tank body, a liquid flowmeter is embedded and installed on each feeding pipe, a stirring device is arranged in the tank body, and a stirring device is arranged on the inner wall of the tank body A spiral heating tube is embedded and installed, and the lower end of the tank body is rotatably connected with a rotary material guide platform. A plurality of discharge pipes are arranged on the peripheral side of the tank body, and a sewage nozzle is provided at the lower end of the discharge pipe. In the present invention, by setting a stirring device, a spiral heating tube, a discharge pipe and a rotating material guide table, the stirring device can stir the mixed extract inside the tank to improve the extraction efficiency, and the spiral heating tube can also improve the extraction efficiency, and then control the rotation The material guide table is rotated to the appropriate discharge pipe to realize the separate outflow of the extraction liquid layer, without being polluted by residues, and improving the extraction accuracy.

Description

A kind of extraction and separation tank and its application method
Technical field
The invention belongs to extraction equipment technical fields, more particularly to a kind of extraction and separation tank and its application method.
Background technique
Extraction refers to using compound solubility or the difference of distribution coefficient in the solvent of two kinds immiscible (or slightly soluble), It is transferred to compound in another solvent from a kind of solvent.By repeated multiple times extraction, by the compound of the overwhelming majority The method extracted.
Existing extraction equipment is mostly that small device is extracted, and production efficiency is low, and extraction time is long, and not It is easy to control, when being easy to generate in the same discharge hole for discharge, remaining extraction feed liquid is blended in next layered material liquid, and one As extracted after need to clean equipment, with remove discharge port adherency clout, be not able to satisfy society it is growing Demand does not improve production efficiency and precision.
Summary of the invention
The purpose of the present invention is to provide a kind of extraction and separation tank and its application methods, by the way that agitating device, spiral is arranged Heating tube, discharge nozzle and rotation guide platform are stirred raising extraction by mixed extracts of the agitating device to tank interior Efficiency, while helical heating pipe can also improve extraction efficiency, then control rotation guide platform and turn to suitable discharge nozzle, realize extraction The separated outflow of liquid layer is taken, not by the pollution of residue, improves extraction precision, solves existing extraction equipment production efficiency It is low, the low problem of precision.
The purpose of the present invention can be achieved through the following technical solutions：
A kind of extraction and separation tank, including tank body, the tank body is interior to be equipped with cavity, and the tank body is equipped with multiple feed pipes, Insertion is equipped with fluid flowmeter on each feed pipe；
The upper end of the tank body is fixedly installed with rotation telescopic cylinder, and rotation telescopic cylinder is equipped with telescopic rod, telescopic rod One end be fixedly connected on rotation telescopic cylinder on, the other end pass through tank body be connected with agitating device；
Insertion is equipped with helical heating pipe on the inner wall of the tank body, and agitating device is in the inner ring of helical heating pipe；
The lower end of the tank body is rotatably connected to rotation guide platform, and the upper surface of rotation guide platform is equipped with deflector chute, guide Slot is in ramped shaped；
All sides of the tank body are equipped with multiple discharge nozzles, and the lower end of discharge nozzle is equipped with blowdown mouth, and discharge nozzle is equipped with the One electrically operated valve.
Further, the agitating device includes the first storage frame, and the middle part of the first storage frame is equipped with the first accommodating groove, the One end of one accommodating groove is rotatably connected to the first agitating plate, and the length and width of the first agitating plate is respectively smaller than the first accommodating groove Length and width, the first agitating plate other end are rotatably connected to the second storage frame, and the middle part of the second storage frame is equipped with the second storage Slot, the length and width of the second accommodating groove are respectively smaller than the length and width of the first accommodating groove, and the first agitating plate is rotatably connected on One end of second accommodating groove, the other end of the second accommodating groove are rotatably connected to the second agitating plate, the length and width of the second agitating plate Degree is respectively smaller than the length and width of the second accommodating groove, the first storage frame, the first agitating plate, the second storage frame and the second agitating plate Line is in " W " shape；
The outer wall of the first storage frame is equipped with fixed block, and one end of telescopic rod is fixedly connected on fixed block, and second Shaft is rotatably connected on agitating plate, the other end of shaft is fixedly connected with the shaft of telescopic rod；
Array has multiple through-holes on the first storage frame, the first agitating plate, the second storage frame and the second agitating plate.
Further, the discharge nozzle is between deflector chute upper end horizontal plane and deflector chute least significant end horizontal plane.
Further, the edge of the guide platform is equipped with rotating seal ring, and the inner ring of rotating seal ring, which is fixedly mounted on, to be led Expect that the edge of platform, the outer ring of rotating seal ring fit closely the inner wall of tank body；
Rotation cylinder is fixedly installed on the bottom wall of the tank body, rotation cylinder is equipped with shaft, and one end of shaft is fixed It is mounted on the output end of rotation cylinder, the other end is fixedly connected with guide platform.
Further, the inner wall of the tank body is equipped with bearing, and the horizontal plane of bearing is under the horizontal plane of discharge nozzle Side, the inner ring of bearing are fixedly connected with the edge of guide platform, and the outer ring of bearing is fixedly connected with the inner wall of tank body.
Further, the blowdown mouth and discharge nozzle interface are equipped with the second electrically operated valve.
Further, the application method carries out as steps described below：
Step 1: raw material is added separately in tank body by feed pipe, various raw materials are added by fluid flowmeter control Amount；
Step 2: starting helical heating pipe carries out the best temperature for being heated to be conducive to extraction to the intracorporal mixing liquid of tank Degree；
Step 3: starting rotation telescopic cylinder, drives the first storage frame on agitating device to move down by telescopic rod, The first agitating plate is pushed, the second storage frame and the second agitating plate spread apart on telescopic rod is rotated, to the intracorporal mixing of tank Liquid, which is stirred, comes into full contact with it, is conducive to the progress of extraction process；
Step 4: after the completion of stirring, starting rotation telescopic cylinder drives the first storage on agitating device by telescopic rod Frame up moves, and pulls the first agitating plate, and the second storage frame and the second agitating plate are retracted to together on telescopic rod, leaves mixing Liquid layer；
Step 5: control rotation cylinder drives the rotation guide platform rotation on shaft, turn to out the lower end of deflector chute Expects pipe is in the position of tank body, opens the first electrically operated valve and realizes that the material of tank body is transferred out by discharge nozzle；
Step 5: the first electrically operated valve of control is closed when the layering material of tank body lower layer has soon flowed, the second electricity is opened The mixed liquor at layering is discharged by blowdown mouth in movable valve, and it is next to the progress of next discharge nozzle to be rotated further by rotation guide platform The extract liquor blowing of layer, while rotating guide platform and blocking the nozzle of a upper discharge nozzle, then by disassembly discharge nozzle, by past First electrically operated valve is added cleaning solution and cleans to discharge nozzle, prepares blowing next time, prevents from polluting.
Beneficial effects of the present invention：
1, the present invention passes through agitating device pair by setting agitating device, helical heating pipe, discharge nozzle and rotation guide platform The mixed extracts of tank interior are stirred raising extraction efficiency, while helical heating pipe can also improve extraction efficiency, then control System rotation guide platform turns to suitable discharge nozzle, realizes that the separated outflow of extraction liquid layer improves not by the pollution of residue Extract precision；
2, the present invention makes agitating device spread apart in stirring, makes stirring amplitude by setting in the agitating device of " W " shape It is bigger, so that agitating device is relaxed at the end of stirring and be retracted to above liquid layer, prevents from having an impact extraction and lower liquid, and due to setting Multiple through-holes comb extraction feed liquid by through-hole, refine feed liquid, and it is agglomerating to avoid feed liquid, accelerate extraction efficiency；
3, the present invention is convenient for people daily batch by setting fluid flowmeter convenient for controlling the amount for the extraction feed liquid being added Control when amount production, it is time saving and energy saving；
4, the present invention is by setting blowdown mouth, the first electrically operated valve and the second electrically operated valve, when the layering object of tank body lower layer When material has soon flowed, the first electrically operated valve of control is closed, and the second electrically operated valve is opened, and the mixed liquor at layering is made to pass through blowdown mouth Discharge is rotated further by rotation guide platform and carries out next layer of extract liquor blowing to next discharge nozzle, while rotating guide platform will be upper The nozzle of one discharge nozzle is blocked, then by disassembly discharge nozzle, by toward the first electrically operated valve be added cleaning solution to discharge nozzle and Blowdown mouth is cleaned, and is prepared blowing next time, is prevented from polluting, and extraction precision is improved.
Detailed description of the invention
In order to illustrate the technical solution of the embodiments of the present invention more clearly, will be described below to embodiment required Attached drawing is briefly described, it should be apparent that, drawings in the following description are only some embodiments of the invention, for ability For the those of ordinary skill of domain, without creative efforts, it can also be obtained according to these attached drawings other attached Figure.
Fig. 1 is structural schematic diagram of the invention；
Fig. 2 is the structural schematic diagram of the liquid-dividing head in the present invention；
Fig. 3 is apparatus of the present invention schematic diagram of internal structure；
Fig. 4 is agitating device structural schematic diagram.
In attached drawing, parts list represented by the reference numerals are as follows：
1- tank body, 2- feed pipe, 3- fluid flowmeter, 4- rotation telescopic cylinder, 5- agitating device, 6- helical heating pipe, 7- rotation guide platform, 8- discharge nozzle, 9- bearing, 11- cavity, 41- telescopic rod, the storage frame of 51- first, the first agitating plate of 52-, The storage frame of 53- second, the second agitating plate of 54-, 55- through-hole, 71- deflector chute, 72- rotating seal ring, 73- rotation cylinder, 74- turn Axis, 81- blowdown mouth, the first electrically operated valve of 82-, the first accommodating groove of 511-, 512- fixed block, the second accommodating groove of 531-, 541- axis Bar.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts all other Embodiment shall fall within the protection scope of the present invention.
In the description of the present invention, it is to be understood that, term " on ", "lower", "bottom", " in ", "vertical", "inner" etc. refer to Show orientation or positional relationship, is merely for convenience of description of the present invention and simplification of the description, rather than the component of indication or suggestion meaning Or element must have a particular orientation, and be constructed and operated in a specific orientation, therefore be not considered as limiting the invention.
Also referring to Fig. 1 and 2, a kind of extraction and separation tank, including tank body 1 is equipped with cavity 11 in tank body 1, on tank body 1 Equipped with multiple feed pipes 2, insertion is equipped with fluid flowmeter 3 on each feed pipe 2, for monitoring the additional amount of feed liquid；
The upper end of tank body 1 is fixedly installed with rotation telescopic cylinder 4, and rotation telescopic cylinder 4 is equipped with telescopic rod 41, stretches One end of bar 41 is fixedly connected on rotation telescopic cylinder 4, and the other end passes through tank body 1 and is connected with agitating device 5, for feed liquid It is stirred, accelerates extraction efficiency；
Insertion is equipped with helical heating pipe 6 on the inner wall of tank body 1, and agitating device 5 is in the inner ring of helical heating pipe 6, For being heated to extraction feed liquid, extraction efficiency is improved；
The lower end of tank body 1 is rotatably connected to rotation guide platform 7, and the upper surface of rotation guide platform 7 is equipped with deflector chute 71, leads Hopper 71 is in ramped shaped, is flowed completely out convenient for extraction feed liquid；
All sides of tank body 1 are equipped with multiple discharge nozzles 8, and the lower end of discharge nozzle 8 is equipped with blowdown mouth 81, for back to be discharged Residual liquid, discharge nozzle 8 are equipped with the first electrically operated valve 82, clean for controlling the outflow of liquid, and convenient for the later period.
Also referring to Fig. 3 and Fig. 4, agitating device 5 includes the first storage frame 51, and the middle part of the first storage frame 51 is equipped with the One accommodating groove 511, one end of the first accommodating groove 511 are rotatably connected to the first agitating plate 52, the length and width of the first agitating plate 52 Degree is respectively smaller than the length and width of the first accommodating groove 511, and 52 other end of the first agitating plate is rotatably connected to the second storage frame 53, The middle part of second storage frame 53 is equipped with the second accommodating groove 531, and the length and width of the second accommodating groove 531 is respectively smaller than the first receipts Receive the length and width of slot 511, the first agitating plate 52 is rotatably connected on one end of the second accommodating groove 531, the second accommodating groove 531 The other end is rotatably connected to the second agitating plate 54, and rotation connection mode is to be rotatablely connected by shaft, the second agitating plate 54 Length and width is respectively smaller than the length and width of the second accommodating groove 531, and the first storage frame 51, the first agitating plate 52, second are received Frame 53 and 54 line of the second agitating plate are received in " W " shape；
The outer wall of first storage frame 51 is equipped with fixed block 512, and one end of telescopic rod 41 is fixedly connected on fixed block 512 On, shaft 541 is rotatably connected on the second agitating plate 54, the other end of shaft 541 is fixedly connected with the shaft of telescopic rod 41, passes through Telescopic cylinder 4 drives the first storage frame 51, the first agitating plate 52, second storage frame 53 and the second agitating plate 54 on telescopic rod 41 It is rotated after being stretched, the liquid in tank body 1 is stirred, control, which is realized, shrinks, and agitating device 5 is retracted on extract liquor Side avoids influencing to extract；
Array has multiple lead on first storage frame 51, the first agitating plate 52, second storage frame 53 and the second agitating plate 54 Hole 55 is combed by 55 pairs of extraction feed liquids of through-hole, refines feed liquid, and it is agglomerating to avoid feed liquid, accelerates extraction efficiency.
Discharge nozzle 8 is between 71 least significant end horizontal plane of 71 upper end horizontal plane of deflector chute and deflector chute, when deflector chute 71 Realize discharging when least significant end goes to one end that discharge nozzle 8 is in tank body 1, remaining discharge nozzle 8 remains unchanged seal closure.
The edge of guide platform 7 is equipped with rotating seal ring 72, and the inner ring of rotating seal ring 72 is fixedly mounted on the side of guide platform 7 Edge, the outer ring of rotating seal ring 72 fit closely the inner wall of tank body 1, prevent liquid from leaking out；
Rotation cylinder 73 is fixedly installed on the bottom wall of tank body 1, rotation cylinder 73 is equipped with shaft 74, one end of shaft 74 It is fixedly mounted on the output end of rotation cylinder 73, the other end is fixedly connected with guide platform 7, realizes the rotation of guide platform 7；
The inner wall of tank body 1 is equipped with bearing 9, and the horizontal plane of bearing 9 is in the lower section of the horizontal plane of discharge nozzle 8, bearing 9 Inner ring is fixedly connected with the edge of guide platform 7, and the outer ring of bearing 9 is fixedly connected with the inner wall of tank body 1.
Blowdown mouth 81 and 8 interface of discharge nozzle are equipped with the second electrically operated valve.
Application method carries out as steps described below：
Step 1: raw material is added separately in tank body 1 by feed pipe 2, various originals are added by 3 control of fluid flowmeter The amount of material；
Step 2: starting helical heating pipe 6 carries out the best temperature for being heated to be conducive to extraction to the mixing liquid in tank body 1 Degree；
Step 3: starting rotation telescopic cylinder 4, drives the first storage frame 51 on agitating device 5 past by telescopic rod 41 Lower movement, pushes the first agitating plate 52, and the second storage frame 53 and the second agitating plate 54 spread apart on telescopic rod 41 is turned Dynamic, being stirred to the mixing liquid in tank body 1 comes into full contact with it, is conducive to the progress of extraction process；
Step 4: after the completion of stirring, starting rotation telescopic cylinder 4 drives first on agitating device 5 by telescopic rod 41 Storage frame 51 up moves, and pulls the first agitating plate 52, and the second storage frame 53 and the second agitating plate 54 are shunk on telescopic rod 41 To together, leaving mixing liquid layer；
Step 5: control rotation cylinder 73 drives the rotation guide platform 7 on shaft 74 to rotate, make the lower end of deflector chute 71 The position that discharge nozzle 8 is in tank body 1 is turned to, the first electrically operated valve 82 is opened and realizes that the material of tank body 1 is passed by discharge nozzle 8 Output is gone；
Step 6: when the layering material of 1 lower layer of tank body has soon flowed, the first electrically operated valve 82 of control is closed, and opens the The mixed liquor at layering is discharged by blowdown mouth 81 in two electrically operated valves, is rotated further by rotation guide platform 7 to next discharge nozzle 8 Next layer of extract liquor blowing is carried out, while rotating guide platform 7 and blocking the nozzle of a upper discharge nozzle 8, then by removing Expects pipe 8 cleans discharge nozzle 8 and blowdown mouth 81 by the way that cleaning solution is added toward the first electrically operated valve 82, and preparation is put next time Material, prevents from polluting.
Present invention disclosed above preferred embodiment is only intended to help to illustrate the present invention.There is no detailed for preferred embodiment All details are described, are not limited the invention to the specific embodiments described.Obviously, according to the content of this specification, It can make many modifications and variations.These embodiments are chosen and specifically described to this specification, is in order to better explain the present invention Principle and practical application, so that skilled artisan be enable to better understand and utilize the present invention.The present invention is only It is limited by claims and its full scope and equivalent.

Claims (7)

1.一种萃取分离罐，包括罐体(1)，所述罐体(1)内设有空腔(11)，其特征在于，所述罐体(1)上设有多个进料管(2)，每个进料管(2)上均嵌入安装有液体流量计(3)；1. an extraction and separation tank, comprising a tank body (1), the tank body (1) is provided with a cavity (11), it is characterized in that, the tank body (1) is provided with a plurality of feed pipes (2), each feed pipe (2) is embedded with a liquid flow meter (3); 所述罐体(1)的上端固定安装有转动伸缩气缸(4)，转动伸缩气缸(4)上设有伸缩杆(41)，伸缩杆(41)的一端固定连接在转动伸缩气缸(4)上，另一端穿过罐体(1)连接有搅拌装置(5)；The upper end of the tank body (1) is fixedly equipped with a rotating telescopic cylinder (4), the rotating telescopic cylinder (4) is provided with a telescopic rod (41), and one end of the telescopic rod (41) is fixedly connected to the rotating telescopic cylinder (4) , the other end passes through the tank body (1) and is connected with a stirring device (5); 所述罐体(1)的内壁上嵌入安装有螺旋加热管(6)，搅拌装置(5)处于螺旋加热管(6)的内圈中；A spiral heating tube (6) is embedded on the inner wall of the tank body (1), and the stirring device (5) is located in the inner ring of the spiral heating tube (6); 所述罐体(1)的下端转动连接有旋转导料台(7)，旋转导料台(7)的上端面设有导料槽(71)，导料槽(71)呈斜坡状；The lower end of the tank body (1) is rotatably connected with a rotary material guide platform (7), and the upper surface of the rotary material guide platform (7) is provided with a material guide groove (71), and the material guide groove (71) is slope-shaped; 所述罐体(1)的周侧面设有多个出料管(8)，出料管(8)的下端设有排污嘴(81)，出料管(8)上设有第一电动阀门(82)。The surrounding side of the tank body (1) is provided with a plurality of discharge pipes (8), the lower end of the discharge pipe (8) is provided with a sewage nozzle (81), and the discharge pipe (8) is provided with a first electric valve (82). 2.根据权利要求1所述的一种萃取分离罐,其特征在于，所述搅拌装置(5)包括第一收纳框(51)，第一收纳框(51)的中部设有第一收纳槽(511)，第一收纳槽(511)的一端转动连接有第一搅拌板(52)，第一搅拌板(52)的长度和宽度分别小于第一收纳槽(511)的长度和宽度，第一搅拌板(52)另一端转动连接有第二收纳框(53)，第二收纳框(53)的中部设有第二收纳槽(531)，第二收纳槽(531)的长度和宽度分别小于第一收纳槽(511)的长度和宽度，第一搅拌板(52)转动连接在第二收纳槽(531)的一端，第二收纳槽(531)的另一端转动连接有第二搅拌板(54)，第二搅拌板(54)的长度和宽度分别小于第二收纳槽(531)的长度和宽度，第一收纳框(51)、第一搅拌板(52)、第二收纳框(53)和第二搅拌板(54)连线呈“W”形；2. An extraction and separation tank according to claim 1, characterized in that, the stirring device (5) comprises a first storage frame (51), and a first storage tank is provided in the middle of the first storage frame (51) (511), one end of the first storage tank (511) is rotatably connected with a first stirring plate (52), and the length and width of the first stirring plate (52) are respectively less than the length and width of the first storage tank (511). The other end of a stirring plate (52) is rotatably connected with a second storage frame (53), the middle part of the second storage frame (53) is provided with a second storage groove (531), and the length and width of the second storage groove (531) are respectively Less than the length and width of the first storage tank (511), the first stirring plate (52) is rotatably connected to one end of the second storage tank (531), and the other end of the second storage tank (531) is rotatably connected to the second stirring plate (54), the length and the width of the second stirring plate (54) are less than the length and the width of the second storage tank (531) respectively, the first storage frame (51), the first stirring plate (52), the second storage frame ( 53) and the second stirring plate (54) are connected in a "W" shape; 所述第一收纳框(51)的外壁上设有固定块(512)，伸缩杆(41)的一端固定连接在固定块(512)上，第二搅拌板(54)上转动连接有轴杆(541)，轴杆(541)的另一端固定连接伸缩杆(41)的杆身；The outer wall of the first storage frame (51) is provided with a fixed block (512), one end of the telescopic rod (41) is fixedly connected to the fixed block (512), and the second stirring plate (54) is rotatably connected with a shaft (541), the other end of shaft rod (541) is fixedly connected to the shaft of telescopic rod (41); 所述第一收纳框(51)、第一搅拌板(52)、第二收纳框(53)和第二搅拌板(54)上均阵列有多个通孔(55)。A plurality of through holes (55) are arrayed on the first receiving frame (51), the first stirring plate (52), the second receiving frame (53) and the second stirring plate (54). 3.根据权利要求1所述的一种萃取分离罐,其特征在于，所述出料管(8)处于导料槽(71)上端水平面和导料槽(71)最低端水平面之间。3. An extraction and separation tank according to claim 1, characterized in that the discharge pipe (8) is located between the upper end level of the material guide trough (71) and the lowest end level of the material guide trough (71). 4.根据权利要求1所述的一种萃取分离罐,其特征在于，所述导料台(7)的边缘设有旋转密封圈(72)，旋转密封圈(72)的内环固定安装在导料台(7)的边缘，旋转密封圈(72)的外环紧密贴合罐体(1)的内壁；4. A kind of extraction and separation tank according to claim 1, characterized in that, the edge of the guide table (7) is provided with a rotary sealing ring (72), and the inner ring of the rotary sealing ring (72) is fixedly mounted on The edge of the material guide table (7), the outer ring of the rotary sealing ring (72) is closely attached to the inner wall of the tank body (1); 所述罐体(1)的底壁上固定安装有转动气缸(73)，转动气缸(73)上设有转轴(74)，转轴(74)的一端固定安装在转动气缸(73)的输出端上，另一端固定连接导料台(7)。A rotary cylinder (73) is fixedly installed on the bottom wall of the tank body (1), and a rotary shaft (74) is arranged on the rotary cylinder (73), and one end of the rotary shaft (74) is fixedly mounted on the output end of the rotary cylinder (73) The other end is fixedly connected to the material guide table (7). 5.根据权利要求1所述的一种萃取分离罐,其特征在于，所述罐体(1)的内壁上设有轴承(9)，轴承(9)的水平面处于出料管(8)的水平面的下方，轴承(9)的内环固定连接导料台(7)的边缘，轴承(9)的外环固定连接罐体(1)的内壁。5. A kind of extraction and separation tank according to claim 1, characterized in that, the inner wall of the tank body (1) is provided with a bearing (9), and the horizontal plane of the bearing (9) is at the bottom of the discharge pipe (8). Below the horizontal plane, the inner ring of the bearing (9) is fixedly connected to the edge of the material guide platform (7), and the outer ring of the bearing (9) is fixedly connected to the inner wall of the tank body (1). 6.根据权利要求1所述的一种萃取分离罐,其特征在于，所述排污嘴(81)与出料管(8)接口处设有第二电动阀门。6. An extraction and separation tank according to claim 1, characterized in that a second electric valve is provided at the interface between the sewage nozzle (81) and the discharge pipe (8). 7.根据权利要求1所述的一种萃取分离罐的使用方法,其特征在于：包括权利要求1-6任一项权利要求所述的萃取分离罐，所述使用方法按照下述步骤进行：7. The method of using an extraction and separation tank according to claim 1, characterized in that: it comprises the extraction and separation tank according to any one of claims 1-6, and the method of use is carried out according to the following steps: 步骤一、将原料由进料管(2)分别加入到罐体(1)内，通过液体流量计(3)把控加入各种原料的量；Step 1. Add the raw materials into the tank (1) respectively through the feed pipe (2), and control the amount of various raw materials added through the liquid flow meter (3); 步骤二、启动螺旋加热管(6)对罐体(1)内的混合液体进行加热到有利于萃取的最佳温度；Step 2, start the spiral heating tube (6) to heat the mixed liquid in the tank (1) to an optimum temperature for extraction; 步骤三、启动转动伸缩气缸(4)，通过伸缩杆(41)带动搅拌装置(5)上的第一收纳框(51)往下运动，推动第一搅拌板(52)，第二收纳框(53)和第二搅拌板(54)在伸缩杆(41)上舒展开，进行转动，对罐体(1)内的混合液体进行搅拌使其充分接触，有利于萃取工序的进行；Step 3, start and rotate the telescopic cylinder (4), drive the first storage frame (51) on the stirring device (5) to move downward through the telescopic rod (41), push the first stirring plate (52), and the second storage frame ( 53) and the second stirring plate (54) are stretched out on the telescopic rod (41) and rotated to stir the mixed liquid in the tank body (1) to make it fully contact, which is beneficial to the extraction process; 步骤四、搅拌完成后，启动转动伸缩气缸(4)，通过伸缩杆(41)带动搅拌装置(5)上的第一收纳框(51)往上运动，拉动第一搅拌板(52)，第二收纳框(53)和第二搅拌板(54)在伸缩杆(41)上收缩到一起，离开混合液层；Step 4: After the stirring is completed, start and rotate the telescopic cylinder (4), drive the first receiving frame (51) on the stirring device (5) to move upward through the telescopic rod (41), and pull the first stirring plate (52), the second The second storage frame (53) and the second stirring plate (54) shrink together on the telescopic rod (41), leaving the mixed liquid layer; 步骤五、控制转动气缸(73)带动轴杆(74)上的旋转导料台(7)转动，使导料槽(71)的下端转动到出料管(8)处于罐体(1)的位置，打开第一电动阀门(82)实现罐体(1)的物料通过出料管(8)传输出去；Step 5. Control the rotating cylinder (73) to drive the rotating material guide table (7) on the shaft rod (74) to rotate, so that the lower end of the material guide groove (71) is rotated until the discharge pipe (8) is at the bottom of the tank body (1). position, open the first electric valve (82) to realize that the material in the tank body (1) is transmitted through the discharge pipe (8); 步骤五、当罐体(1)下层的分层物料快要流完时，控制第一电动阀门(82)关闭，打开第二电动阀门，使分层处的混合液通过排污嘴(81)排出，再转动旋转导料台(7)到下一个出料管(8)进行下一层的萃取液放料，同时旋转导料台(7)将上一个出料管(8)的管口堵住，再通过拆卸出料管(8)，通过往第一电动阀门(82)加入清洗液对出料管(8)进行清洗，准备下一次放料，防止污染。Step 5. When the stratified material in the lower layer of the tank body (1) is about to run out, control the first electric valve (82) to close, and open the second electric valve to discharge the mixed liquid at the stratified part through the drain nozzle (81). Then turn the rotating material guide table (7) to the next discharge pipe (8) to discharge the extract of the next layer, and at the same time rotate the material guide table (7) to block the nozzle of the previous discharge pipe (8) , and then by dismantling the discharge pipe (8), the discharge pipe (8) is cleaned by adding cleaning solution to the first electric valve (82), so as to prepare for the next discharge and prevent pollution.
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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111991845A (en) * 2020-08-21 2020-11-27 昆明理工大学 Rotary ultrasonic-microwave combined microfluid extraction equipment
CN114307938A (en) * 2021-11-29 2022-04-12 武汉立刚网络科技有限公司 MnV for manufacturing potential ammonia sensor2O6Powder extraction device
CN116351101A (en) * 2023-04-23 2023-06-30 江苏东宝农化股份有限公司 Extraction equipment and application thereof in azadirachtin extraction

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2510155Y (en) * 2001-11-27 2002-09-11 中国科学院广州化学研究所 Separating funnel
CN204485855U (en) * 2015-03-06 2015-07-22 武汉亿强科技开发有限公司 A kind of ceramic reactor with easily contained agitating device
CN104841317A (en) * 2015-05-21 2015-08-19 苏州欢颜电气有限公司 Stirring device automatically adjusted along with height of liquid level
CN104984561A (en) * 2014-08-10 2015-10-21 胡刘满 Plant active component extraction device
WO2017212806A1 (en) * 2016-06-09 2017-12-14 日本軽金属株式会社 Stirring device
CN207478034U (en) * 2017-11-10 2018-06-12 贵溪市鼎邦涂料有限公司 A kind of organic extraction separator

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2510155Y (en) * 2001-11-27 2002-09-11 中国科学院广州化学研究所 Separating funnel
CN104984561A (en) * 2014-08-10 2015-10-21 胡刘满 Plant active component extraction device
CN204485855U (en) * 2015-03-06 2015-07-22 武汉亿强科技开发有限公司 A kind of ceramic reactor with easily contained agitating device
CN104841317A (en) * 2015-05-21 2015-08-19 苏州欢颜电气有限公司 Stirring device automatically adjusted along with height of liquid level
WO2017212806A1 (en) * 2016-06-09 2017-12-14 日本軽金属株式会社 Stirring device
CN207478034U (en) * 2017-11-10 2018-06-12 贵溪市鼎邦涂料有限公司 A kind of organic extraction separator

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111991845A (en) * 2020-08-21 2020-11-27 昆明理工大学 Rotary ultrasonic-microwave combined microfluid extraction equipment
CN114307938A (en) * 2021-11-29 2022-04-12 武汉立刚网络科技有限公司 MnV for manufacturing potential ammonia sensor2O6Powder extraction device
CN116351101A (en) * 2023-04-23 2023-06-30 江苏东宝农化股份有限公司 Extraction equipment and application thereof in azadirachtin extraction
CN116351101B (en) * 2023-04-23 2023-10-20 江苏东宝农化股份有限公司 Extraction equipment and application thereof in azadirachtin extraction

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