CN108546078A - A kind of Cizhouyao porcelain formula and its method for cooking - Google Patents
A kind of Cizhouyao porcelain formula and its method for cooking Download PDFInfo
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- CN108546078A CN108546078A CN201810345259.8A CN201810345259A CN108546078A CN 108546078 A CN108546078 A CN 108546078A CN 201810345259 A CN201810345259 A CN 201810345259A CN 108546078 A CN108546078 A CN 108546078A
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- C04B33/00—Clay-wares
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- C04B33/00—Clay-wares
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- C04B33/13—Compounding ingredients
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- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
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- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
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- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/96—Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance
Abstract
The present invention discloses a kind of Cizhouyao porcelain formula and its method for cooking, wherein ridging is made of the raw material of following parts by weight：100 150 parts of Red Stone Ware, 10 15 parts of fire clay；The glaze is made of the raw material of following parts by weight：5 10 parts of silica flour, 0.2 0.4 parts of magnesia, 0.5 0.8 parts of titanium dioxide, 0.2 0.8 parts of prodan, 28 parts of calcium oxide, 0.02 0.03 parts of strontium chloride, 10 15 parts of blue clay, preparation method include mainly：It prepares glaze, burn biscuit body, glazing, firing, five big step of color roasting, not only color and luster is smooth, bright with stronger artistic feeling for Cizhouyao porcelain that technical solution is prepared through the invention, and has certain hardness and suppleness, it is not easy to break into pieces.
Description
Technical field
The present invention relates to Cizhouyao firing field, specifically a kind of Cizhouyao porcelain formula and its method for cooking.
Background technology
Cizhouyao its be brilliant one page in Chinese pottery history.Cizhouyao is the treasure of Chinese Han nationality's tradition technology in producing porcelain,
The maximum common cave system of Chinese ancient northern and famous civil porcelain kiln, sight platform of the kiln site in modern Hebei Handan Ci County
Pengcheng City town in town and Fengfeng Mining Area.It is key historical sites under state protection.Cizhouyao raw material originates in locality, mainly there is blue clay, white
Alkali, stoneware clay, cage soil, loess (black powder soil), camwood knag, Red Stone Ware, refractory clay, hydrometallurgy feldspar etc..Firers answer china clay
A set of unique skill has been used, has not only burnt and makes ceramic whiteware, black porcelain, yellow porcelain, green porcelain, three coloured silks, and underglaze colour is burnt on the basis of ceramic whiteware
It paints.
History trace stream is pursued, it is seen that development of the porcelain of Cizhouyao production for China's traditional lacquer industry, with
Scientific and technological progress, some row about porcelain should into patent literature, but carried out almost without the porcelain that is produced for Cizhouyao
Improve report.And Cizhouyao porcelain is not only beautiful and prolonged resistance to, the right existing Cizhouyao porcelain porcelain of heat, physicochemical property is general,
Easily fragmentation not only causes economic loss, and causes certain damage at heart to porcelain reward player.
Invention content
(1) the technical issues of solving
In view of the deficiency of the prior art, a kind of Cizhouyao porcelain formula of present invention offer and its method for cooking,
Not only color and luster is smooth, bright with stronger artistic feeling for Cizhouyao porcelain that technical solution is prepared through the invention, has
Stronger artistic feeling, and there is certain hardness and suppleness, it is not easy to it breaks into pieces.
(2) technical solution
In order to achieve the above object, the present invention is achieved by the following technical programs:
A kind of Cizhouyao porcelain formula, including ridging and glaze, the ridging are made of the raw material of following parts by weight：Boccaro
100-150 parts native, 10-15 parts of fire clay；The glaze is made of the raw material of following parts by weight：5-10 parts of silica flour, oxidation
0.2-0.4 parts of magnesium, 0.5-0.8 parts of titanium dioxide, 0.2-0.8 parts of prodan, 2-8 parts of calcium oxide, strontium chloride 0.02-0.03
Part, 10-15 parts of blue clay.
Preferably, the ridging is made of the raw material of following parts by weight：145 parts of Red Stone Ware, 12 parts of fire clay.
Preferably, the glaze is made of the raw material of following parts by weight：8 parts of silica flour, 0.3 part of magnesia, titanium dioxide
0.7 part, 0.6 part of prodan, 6 parts of calcium oxide, 0.025 part of strontium chloride, 12 parts of blue clay.
The method for cooking of Cizhouyao porcelain of above-mentioned Cizhouyao porcelain formula, includes the following steps：
S1, glaze is prepared：The each component material in glaze is placed in ball mill according to composition by weight proportioning and is crushed respectively
At fine powder, suitable water grinding 2-3h is added after fine powder mixing and is placed in crucible, after heating crucible to mud temperature is 70-80 DEG C,
Crucible is placed in micro-wave oven after microwave heating 35-40min, takes out cooling, sieving obtains glaze；
S2, biscuit body is burnt：Ridging is weighed according to composition by weight proportioning, suitable water is added after mixing, is prepared into base
Mud, base mud are fired into biscuit；
S3, glazing：By on the biscuit in the glaze glazing to step S2 in step S1, glazed body is obtained after natural air drying；
S4, firing：Glazed body after being air-dried in step S3 is placed into stove, stove is protected after being warming up to 1300-1350 DEG C
Warm 8-10h, control heating hastens as 8-10 DEG C/min, and after heat preservation is fired, for slow cooling to 850-900 DEG C, control is slow
The speed of cooling is 0.5-0.8 DEG C/min, and the mixed gas of carbon dioxide and nitrogen is led into stove, until in stove at temperature
After dropping to 550-600 DEG C, cooled to room temperature obtains sintering briquette；
S5, color roasting：Sintering briquette in step S4 is subjected to color roasting.
Preferably, it matches each component material in glaze being placed in ball mill according to composition by weight in the step S1 and divide
It is not ground into fine powder, suitable water grinding 2.5h is added after fine powder mixing and is placed in crucible, heating crucible to mud temperature is 75 DEG C
Afterwards, crucible is placed in micro-wave oven after microwave heating 38min, takes out cooling, sieving obtains glaze.
Preferably, the glazed body after being air-dried in step S3 is placed into stove in the step S4, stove is warming up to 1330
Keep the temperature 8.5h after DEG C, control heating hastens as 9 DEG C/min, and after heat preservation is fired, slow cooling controls slowly drop to 880 DEG C
The speed of temperature is 0.8 DEG C/min, and the mixed gas of carbon dioxide and nitrogen is led into stove, until temperature drops in stove
After 580 DEG C, cooled to room temperature obtains sintering briquette.
Advantageous effect
The present invention discloses a kind of Cizhouyao porcelain formula and its method for cooking component materials include ridging and glaze, wherein
Containing component materials such as prodan, titanium dioxide in glaze, glaze is interacted in calcination process as formed SiO2-TiO2-
MgO-NaSiF6, the formation of the chemical combination objects system can improve the smoothness of porcelain glaze, and the strontium chloride in component materials is being forged
The color and luster sense of ceramics can be improved during burning, porcelain surface forms pale red after being added with the ceramic roasting of strontium chloride, mainly
The reason is that the distinctive electronic structure of metallic element strontium, with certain aesthetic feeling due to distinctive pale red.
Preparation method includes preparing glaze, burning biscuit body, glazing, five big step of color roasting, toward stove wherein in sintering procedure
Interior logical nitrogen and carbon dioxide can effectively improve carbon formula and nitrogen formula in stove, improve the physicochemical property such as shock resistance of porcelain
Energy.
Specific implementation mode
In order to make the object, technical scheme and advantages of the embodiment of the invention clearer, below in conjunction with the embodiment of the present invention,
Technical scheme in the embodiment of the invention is clearly and completely described, it is clear that described embodiment is the present invention one
Divide embodiment, instead of all the embodiments.Based on the embodiments of the present invention, those of ordinary skill in the art are not making
The every other embodiment obtained under the premise of creative work, shall fall within the protection scope of the present invention.
Embodiment 1:
A kind of Cizhouyao porcelain formula, including ridging and glaze, the ridging are made of the raw material of following parts by weight：Quartz
8 parts of powder, 0.3 part of magnesia, 0.7 part of titanium dioxide, 0.6 part of prodan, 6 parts of calcium oxide, 0.025 part of strontium chloride, blue clay 12
Part.
The method for cooking of Cizhouyao porcelain of above-mentioned Cizhouyao porcelain formula includes the following steps：
S1, glaze is prepared：The each component material in glaze is placed in ball mill according to composition by weight proportioning and is crushed respectively
At fine powder, suitable water grinding 2.5h is added after fine powder mixing and is placed in crucible, after heating crucible to mud temperature is 75 DEG C, crucible
It is placed in micro-wave oven after microwave heating 38min, takes out cooling, sieving obtains glaze；
S2, biscuit body is burnt：Ridging is weighed according to composition by weight proportioning, suitable water is added after mixing, is prepared into base
Mud, base mud are fired into biscuit；
S3, glazing：By on the biscuit in the glaze glazing to step S2 in step S1, glazed body is obtained after natural air drying；
S4, firing：Glazed body after being air-dried in step S3 is placed into stove, stove is kept the temperature after being warming up to 1330 DEG C
8.5h, control heating hasten as 9 DEG C/min, and after heat preservation is fired, slow cooling controls the speed of slow cooling to 880 DEG C
For 0.8 DEG C/min, the mixed gas of carbon dioxide and nitrogen is led into stove, until after temperature drops to 580 DEG C in stove, from
It is so cooled to room temperature, obtains sintering briquette；
S5, color roasting：Sintering briquette in step S4 is subjected to color roasting.
Embodiment 2:
A kind of Cizhouyao porcelain formula, including ridging and glaze, the ridging are made of the raw material of following parts by weight：Boccaro
Native 100 parts, 10 parts of fire clay；The glaze is made of the raw material of following parts by weight：5 parts of silica flour, 0.4 part of magnesia, two
0.8 part of titanium oxide, 0.8 part of prodan, 2 parts of calcium oxide, 0.02 part of strontium chloride, 10 parts of blue clay.
The method for cooking of Cizhouyao porcelain of above-mentioned Cizhouyao porcelain formula includes the following steps：
S1, glaze is prepared：The each component material in glaze is placed in ball mill according to composition by weight proportioning and is crushed respectively
At fine powder, suitable water grinding 3h is added after fine powder mixing and is placed in crucible, after heating crucible to mud temperature is 80 DEG C, crucible is set
In micro-wave oven after microwave heating 40min, cooling is taken out, sieving obtains glaze；
S2, biscuit body is burnt：Ridging is weighed according to composition by weight proportioning, suitable water is added after mixing, is prepared into base
Mud, base mud are fired into biscuit；
S3, glazing：By on the biscuit in the glaze glazing to step S2 in step S1, glazed body is obtained after natural air drying；
S4, firing：Glazed body after being air-dried in step S3 is placed into stove, stove keeps the temperature 10h after being warming up to 1300 DEG C,
Control heating hastens as 10 DEG C/min, and after heat preservation is fired, for slow cooling to 850 DEG C, the speed for controlling slow cooling is 0.8
DEG C/min, the mixed gas of carbon dioxide and nitrogen is led into stove, until after temperature drops to 600 DEG C in stove, it is naturally cold
But to room temperature, sintering briquette is obtained；
S5, color roasting：Sintering briquette in step S4 is subjected to color roasting.
Embodiment 3:
A kind of Cizhouyao porcelain formula, including ridging and glaze, the ridging are made of the raw material of following parts by weight：Boccaro
Native 150 parts, 15 parts of fire clay；The glaze is made of the raw material of following parts by weight：10 parts of silica flour, 0.2 part of magnesia, two
0.5 part of titanium oxide, 0.2 part of prodan, 8 parts of calcium oxide, 0.03 part of strontium chloride, 15 parts of blue clay.
The method for cooking of Cizhouyao porcelain of above-mentioned Cizhouyao porcelain formula includes the following steps：
S1, glaze is prepared：The each component material in glaze is placed in ball mill according to composition by weight proportioning and is crushed respectively
At fine powder, suitable water grinding 2h is added after fine powder mixing and is placed in crucible, after heating crucible to mud temperature is 70 DEG C, crucible is set
In micro-wave oven after microwave heating 35min, cooling is taken out, sieving obtains glaze；
S2, biscuit body is burnt：Ridging is weighed according to composition by weight proportioning, suitable water is added after mixing, is prepared into base
Mud, base mud are fired into biscuit；
S3, glazing：By on the biscuit in the glaze glazing to step S2 in step S1, glazed body is obtained after natural air drying；
S4, firing：Glazed body after being air-dried in step S3 is placed into stove, stove keeps the temperature 10h after being warming up to 1350 DEG C,
Control heating hastens as 10 DEG C/min, and after heat preservation is fired, for slow cooling to 850 DEG C, the speed for controlling slow cooling is 0.5
DEG C/min, the mixed gas of carbon dioxide and nitrogen is led into stove, until after temperature drops to 550 DEG C in stove, it is naturally cold
But to room temperature, sintering briquette is obtained；
S5, color roasting：Sintering briquette in step S4 is subjected to color roasting.
Embodiment 4:
A kind of Cizhouyao porcelain formula, including ridging and glaze, the ridging are made of the raw material of following parts by weight：Boccaro
Native 110 parts, 11 parts of fire clay；The glaze is made of the raw material of following parts by weight：7 parts of silica flour, 0.3 part of magnesia, two
0.6 part of titanium oxide, 0.4 part of prodan, 3 parts of calcium oxide, 0.02 part of strontium chloride, 11 parts of blue clay.
The method for cooking of Cizhouyao porcelain of above-mentioned Cizhouyao porcelain formula such as embodiment 1.
Embodiment 5:
A kind of Cizhouyao porcelain formula, including ridging and glaze, the ridging are made of the raw material of following parts by weight：Boccaro
Native 145 parts, 14 parts of fire clay；The glaze is made of the raw material of following parts by weight：8 parts of silica flour, 0.3 part of magnesia, two
0.7 part of titanium oxide, 0.7 part of prodan, 7 parts of calcium oxide, 0.025 part of strontium chloride, 14 parts of blue clay.
The method for cooking of Cizhouyao porcelain of above-mentioned Cizhouyao porcelain formula such as embodiment 2.
Embodiment 6:
A kind of Cizhouyao porcelain formula, including ridging and glaze, the ridging are made of the raw material of following parts by weight：Boccaro
Native 135 parts, 13 parts of fire clay；The glaze is made of the raw material of following parts by weight：7 parts of silica flour, 0.3 part of magnesia, two
0.6 part of titanium oxide, 0.7 part of prodan, 5 parts of calcium oxide, 0.025 part of strontium chloride, 12 parts of blue clay.
The method for cooking of Cizhouyao porcelain of above-mentioned Cizhouyao porcelain formula such as embodiment 3.
Performance test：
Following performance test is carried out to the preparation-obtained composite materials of 1-6 of the embodiment of the present invention：
Hardness and wear rate test:Experimental group：Experimental group is the porcelain that 1-6 of the embodiment of the present invention is fired；Control group：
Same size porcelain is sold in the market.Wherein each 30 of the experiment ceramics of experimental group and control group.To experimental group and control component
It carry out not hardness test and antidetonation test.Hardness test is the measuring and calculating hardness level of porcelain, and antidetonation test is to be placed into porcelain
It under the conditions of 800 DEG C, is vibrated, calculates and the number that tile bursts apart or cracks occurs.
Table 1
| Experimental group | Hardness/HRC | Burst apart or crack number/ |
| Embodiment 1 | 110 | 0 |
| Embodiment 2 | 108 | 1 |
| Embodiment 3 | 109 | 0 |
| Embodiment 4 | 107 | 0 |
| Embodiment 5 | 109 | 1 |
| Embodiment 6 | 109 | 0 |
| Control group | 84 | 4 |
As shown in Table 1, the porcelain that the present invention obtains has preferable physical strength and shock strength.
It should be noted that herein, relational terms such as first and second and the like are used merely to a reality
Body or operation are distinguished with another entity or operation, are deposited without necessarily requiring or implying between these entities or operation
In any actual relationship or order or sequence.Moreover, the terms "include", "comprise" or its any other variant are intended to
Non-exclusive inclusion, so that the process, method, article or equipment including a series of elements is not only wanted including those
Element, but also include other elements that are not explicitly listed, or further include for this process, method, article or equipment
Intrinsic element.In the absence of more restrictions, the element limited including sentence "including a ...", it is not excluded that
There is also other identical elements in the process, method, article or apparatus that includes the element.
The above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations, although with reference to the foregoing embodiments
Invention is explained in detail, it will be understood by those of ordinary skill in the art that:It still can be to aforementioned each implementation
Technical solution recorded in example is modified or equivalent replacement of some of the technical features；And these modification or
It replaces, the spirit and scope for various embodiments of the present invention technical solution that it does not separate the essence of the corresponding technical solution.
Claims (6)
1. a kind of Cizhouyao porcelain formula, which is characterized in that including ridging and glaze, the raw material earthed up by following parts by weight
It is made：100-150 parts of Red Stone Ware, 10-15 parts of fire clay；The glaze is made of the raw material of following parts by weight：Silica flour 5-
10 parts, 0.2-0.4 parts of magnesia, 0.5-0.8 parts of titanium dioxide, 0.2-0.8 parts of prodan, 2-8 parts of calcium oxide, strontium chloride
0.02-0.03 parts, 10-15 parts of blue clay.
2. porcelain formula in Cizhouyao according to claim 1, which is characterized in that the raw material earthed up by following parts by weight
It is made：145 parts of Red Stone Ware, 12 parts of fire clay.
3. porcelain formula in Cizhouyao according to claim 1, which is characterized in that the glaze by following parts by weight raw material
It is made：8 parts of silica flour, 0.3 part of magnesia, 0.7 part of titanium dioxide, 0.6 part of prodan, 6 parts of calcium oxide, strontium chloride 0.025
Part, 12 parts of blue clay.
4. according to the method for cooking of Cizhouyao porcelain of any Cizhouyao porcelain formulas of claim 1-3, feature exists
In including the following steps：
S1, glaze is prepared：It matches each component material in glaze being placed in ball mill according to composition by weight and be respectively crushed into carefully
Powder is added suitable water grinding 2-3h and is placed in crucible after fine powder mixing, after heating crucible to mud temperature is 70-80 DEG C, crucible
It is placed in micro-wave oven after microwave heating 35-40min, takes out cooling, sieving obtains glaze；
S2, biscuit body is burnt：Ridging is weighed according to composition by weight proportioning, suitable water is added after mixing, is prepared into base mud, base
Mud is fired into biscuit；
S3, glazing：By on the biscuit in the glaze glazing to step S2 in step S1, glazed body is obtained after natural air drying；
S4, firing：Glazed body after being air-dried in step S3 is placed into stove, stove keeps the temperature 8- after being warming up to 1300-1350 DEG C
10h, control heating hastens as 8-10 DEG C/min, and after heat preservation is fired, slow cooling controls slow cooling to 850-900 DEG C
Speed be 0.5-0.8 DEG C/min, the mixed gas of carbon dioxide and nitrogen is led into stove, temperature drops in the stove
After 550-600 DEG C, cooled to room temperature obtains sintering briquette；
S5, color roasting：Sintering briquette in step S4 is subjected to color roasting.
5. the method for cooking of Cizhouyao porcelain of porcelain formula in Cizhouyao according to claim 3, which is characterized in that described
The each component material in glaze is placed in ball mill according to composition by weight proportioning in step S1 and is respectively crushed into fine powder, fine powder is mixed
Suitable water grinding 2.5h is added after conjunction to be placed in crucible, after heating crucible to mud temperature is 75 DEG C, crucible is placed in micro-wave oven
After microwave heating 38min, cooling is taken out, sieving obtains glaze.
6. the method for cooking of Cizhouyao porcelain of porcelain formula in Cizhouyao according to claim 3, which is characterized in that described
The glazed body after being air-dried in step S3 is placed into stove in step S4, stove keeps the temperature 8.5h after being warming up to 1330 DEG C, control rises
Temperature hastens as 9 DEG C/min, and after heat preservation is fired, for slow cooling to 880 DEG C, the speed for controlling slow cooling is 0.8 DEG C/min,
The mixed gas for leading to carbon dioxide and nitrogen into stove naturally cools to room until after temperature drops to 580 DEG C in stove
Temperature obtains sintering briquette.
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