CN108498696A - It is a kind of to be used to treat chill pain in waist and lower extremities, the vina preparation process of muscles and bones numbness - Google Patents

It is a kind of to be used to treat chill pain in waist and lower extremities, the vina preparation process of muscles and bones numbness Download PDF

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CN108498696A
CN108498696A CN201810518990.6A CN201810518990A CN108498696A CN 108498696 A CN108498696 A CN 108498696A CN 201810518990 A CN201810518990 A CN 201810518990A CN 108498696 A CN108498696 A CN 108498696A
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parts
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rhizoma
root
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孙新平
刘中伟
杨华
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JIANGXI JIUHUA PHARMACEUTICAL CO Ltd
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JIANGXI JIUHUA PHARMACEUTICAL CO Ltd
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    • A—HUMAN NECESSITIES
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    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/67—Piperaceae (Pepper family), e.g. Jamaican pepper or kava
    • A—HUMAN NECESSITIES
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    • A61K35/00—Medicinal preparations containing materials or reaction products thereof with undetermined constitution
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    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/09—Lichens
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    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/23—Apiaceae or Umbelliferae (Carrot family), e.g. dill, chervil, coriander or cumin
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Abstract

The invention discloses a kind of for treating chill pain in waist and lower extremities, the vina preparation process of muscles and bones numbness, wherein formula includes following component：Piper wallichii (Miq.) Hand.-Mazz.：2800 2900 parts by weight, Chinese ephedra：90 100 parts by weight, Fructus Aurantii：75 80 parts by weight, cassia twig：75 80 parts by weight, silkworm excrement：24 28 parts by weight, sealwort：30 35 parts by weight, dried orange peel：50 55 parts by weight, Cortex Magnoliae Officinalis：10 15 parts by weight, semen armeniacae amarae：10 15 parts by weight, rhizoma alismatis：10 15 parts by weight, Chinese yam：10 15 parts by weight, rhizoma atractylodis：10 15 parts by weight, moutan bark：10 15 parts by weight, Rhizoma Chuanxiong：10 15 parts by weight, Rhizoma Atractylodis Macrocephalae：10 15 parts by weight, the root of Dahurain angelica：10 15 parts by weight, root of Aucklandia lappa Decne：10 15 parts by weight, lichen：10 15 parts by weight, Rhizoma Et Radix Notopterygii：10 15 parts by weight, fennel seeds：10 15 parts by weight, fructus gleditsiae：10 15 parts by weight, psoralea corylifolia：10 15 parts by weight, rhizoma cyperi：10 15 parts by weight, Semen Cuscutae：10 15 parts by weight, myrrh：10 15 parts by weight, Radix Angelicae Sinensis：10 15 parts by weight, frankincense：10 15 parts by weight.Present invention combination modern pharmaceutical is equipped, and is prepared in the way of circumfluence distillation, and the liquid for allocating completion is carried out by the way of cooling nature removal of impurities, not only increases extraction working efficiency, and improve quality standard.

Description

It is a kind of to be used to treat chill pain in waist and lower extremities, the vina preparation process of muscles and bones numbness
Technical field
The present invention relates to technical field of Chinese medicine, more particularly to a kind of wine for treating chill pain in waist and lower extremities, muscles and bones numbness Agent preparation process.
Background technology
Currently, the production technology of Chinese medicine tincture generally uses percolation or low temperatural extraction, part thermal sensitivity medicinal material is prevented Ingredient is destroyed, and is preferable extracting mode, and still, extracting cycle is long, generally needs 7-10 days production cycles, extraction efficiency It is not high, it is only extracted by the principle of " similar person mixes ", does not carry out cyto-architectural destruction, cannot fully extracted, micro- life Object is easily exceeded.
Chinese patent (application number：201710504332.7) a kind of Traditional Chinese medicinal liquor is disclosed, it is by Radix Angelicae Sinensis, Radix Astragali, three Seven, aconiti preparata,radix, wild aconite root, turpentine, rhizoma nardostachyos, Herba Cistanches, pangolin, cortex acanthopanacis, uncommon Xian grass etc. are made.The present invention is according to Chinese medicine Dialectical theory is so that qi and blood numbness is hindered since liver kidney asthenia of essence and blood, the heresy of diseases caused by external factors are taken advantage of a weak point, cause QI-blood circulation in conjunction with this disease It is unsmooth, it causes blockage of main and collateral channels or phlegm-turbidity and blood stasis blood or work and rest wound to cause hemostasis stagnation, passages through which vital energy circulates obstructed, causes muscles and bones to lose and support, channels and collaterals Numbness hinders, and with the passing of time falls ill.The medicinal liquor to rheumatism, rheumatoid arthritis, pain in waist and lower extremities, scapulohumeral periarthritis, numb limb, osteoproliferation, Protrusion of lumber intervertebral disc, cervical spondylosis, various pain chronic diseases have unique curative effect.But extracting cycle is long, extraction efficiency is not high.
Chinese patent (application number：201210056944.1) a kind of Shennong medicinal liquor and preparation method thereof is disclosed, it is by seeking Bone wind, Rhizoma Chuanxiong, Radix Angelicae Sinensis, Radix Salviae Miltiorrhizae, windproof, Cortex Eucommiae, fringed iris herb, cortex acanthopanacis, geranium wilfordii, sargentodoxa cuneata, costus root, caulis trachelospermi, safflower, The certain proportions such as chrysanthemum Radix Notoginseng, the root of bidentate achyranthes, Fructus Liquidambaris, radix bupleuri form, step：A, material prepares：It dries, is cut into 1. medicinal material is cleaned Thin slice is uniformly packed into gauze bag, tightens sack, be neatly put into container tank；2. sucrose is prepared into inverted sugar, cool to room Temperature is poured into cylinder；B, it impregnates：1. wine is poured into cylinder, stir, allow wine that can impregnate pack, seals cylinder mouth；2. impregnating, wine is observed After brown, pack taking-up is put in another wine vat, secondary immersion is carried out, seals cylinder mouth；3. after impregnating again, pack is drained It takes out, merges immersion liquid and stir evenly, seal cylinder mouth.Treat caused by wind, cold and wetness evils, cervical spondylosis, scapulohumeral periarthritis, pain in waist and lower extremities, chronic strain and rheumatism Property arthritis etc. has significant curative effect.But cannot fully extract, microorganism is easily exceeded.
It there is no a kind of high quality, production efficiency high, continuous mechanized produces for treating chill waist-leg currently on the market Bitterly, the vina preparation process of muscles and bones numbness, therefore, it is necessary to one kind ensureing mouthfeel, under the premise of improving quality standard, improve wine The production efficiency of agent realizes the preparation process of the continuous mechanized produces of vina.
Invention content
The present invention is made of 27 taste Chinese medicines, makes full use of modern pharmaceutical principle, be fully extracted drug it is effective at Point, the mode for using " circumfluence distillation " and " sub-cooled removal of impurities " carries out vina production.
The pharmacological property of Chinese medicine used：
Caulis et Folium piperis
Nature and flavor：It is acrid in flavour and warm in nature
Effect：Wind-damp dispelling, relaxing muscles and tendons network, strong waist and knee remove numbness pain
Chinese ephedra
Nature and flavor:Pungent, slight bitter, temperature
Effect:Sweating cold dispelling, freeings lung and relieving asthma, inducing diuresis for removing edema
Fructus Aurantii
Nature and flavor：It is pungent, bitter
Effect：Relieving stagnant Qi, row phlegm, disperse accumulation
Cassia twig
Nature and flavor：Acrid, sweet, warm
Effect：Complement sun, promoting blood circulation, warming spleen and stomach
Silkworm excrement
Nature and flavor：Gan Wen
Effect：Eliminating dampness, wind-dispelling, regulating the function of the stomach to resolve the turbidity, promoting blood circulation analgesic therapy
Sealwort
Nature and flavor：It is sweet, flat
Effect：Boosting qi and nourishing yin, invigorating the spleen, moistening lung, kidney-nourishing
Dried orange peel
Nature and flavor：It is warm-natured, acrid flavour, bitter
Effect：Regulating qi-flowing for strengthening spleen, in tune, eliminating dampness, resolving sputum
Cortex Magnoliae Officinalis
Nature and flavor：It is bitter；It is pungent；It is warm-natured
Effect：Gas consumption product；Eliminating dampness except full；Relieving asthma
Semen armeniacae amarae
Effect：Sending down abnormally ascending is relieving cough and asthma, relaxes bowel
Rhizoma alismatis
Nature and flavor：It is sweet, it trembles with fear
Effect：Li Shui, excreting dampness expel the heat-evil
Chinese yam
Nature and flavor：It is sweet in flavor, it is mild-natured
Effect：Tonifying spleen nourishing the stomach, engender liquid and benefic lung, the puckery essence of kidney tonifying
Rhizoma atractylodis
Nature and flavor：Acrid flavour；It is bitter；It is warm-natured
Effect：It is drying damp and strengthening spleen；Wind-damp dispelling；Improving eyesight
Moutan bark
Nature and flavor：It is bitter, pungent, it is slightly cold
Effect：Clearing heat and cooling blood activates blood circulation and disperses blood clots, reducing the asthenic fever
Rhizoma Chuanxiong
Nature and flavor：Acrid flavour, it is warm-natured
Effect：Blood-activating and qi-promoting, wind-expelling pain-stopping
Rhizoma Atractylodis Macrocephalae
Nature and flavor：Bitter, it is sweet, it is warm-natured
Effect：Strengthening the spleen and replenishing qi, eliminate dampness and have diuretic effect, hidroschesis, tocolysis
The root of Dahurain angelica
Nature and flavor：It is warm-natured, acrid flavour, gas fragrance, slight bitter
Effect：Wind-damp dispelling, apocenosis of invigorating blood circulation, myogenic pain relieving
Root of Aucklandia lappa Decne
Nature and flavor：Acrid flavour；It is bitter；It is warm-natured
Effect：Promoting qi circulation and relieving pain；It is led in tune stagnant
Lichen
Nature and flavor：Sweet and neutral, it is nontoxic
Effect：It is Yin nourishing and lung moistening, cooling blood and hemostasis, clearing heat and detoxicating
Rhizoma Et Radix Notopterygii
Nature and flavor：Sweet and neutral, it is nontoxic
Effect：It is Yin nourishing and lung moistening, cooling blood and hemostasis, clearing heat and detoxicating
Fennel seeds
Nature and flavor：Acrid flavour, it is warm-natured
Effect：Stimulating appetite, qi-regulating cold dispelling have supporing yang road
Fructus gleditsiae
Nature and flavor：It is pungent, salty, temperature；It is slightly poisonous
Effect：Eliminating the phlegm is had one's ideas straightened out, mass dissipating and swelling eliminating
Psoralea corylifolia
Nature and flavor：It is pungent, salty, temperature；It is slightly poisonous
Effect：Tonifying kidney and strengthening yang, astringent sperm contracting urine, lumbago due to the kidney deficiency, frequent urination, infantile enuresis, kidney leakage is warming spleen and stopping diarrha, receives gas It relievings asthma
Rhizoma cyperi
Nature and flavor：Pungent slight bitter sweet and neutral
Effect：Regulating the flow of vital energy Xie Yu, menstruction regulating and pain relieving
Semen Cuscutae
Nature and flavor：It is sweet, warm
Effect：Nourishing liver and kidney, astringent sperm contracting urine, tocolysis, improving eyesight, antidiarrheal
Myrrh
Nature and flavor：Bitter is put down, nontoxic
Effect：Promoting blood circulation and stopping pain, detumescence and promoting granulation
Radix Angelicae Sinensis
Nature and flavor：Taste sweet, warm
Effect：It enriches blood；Promoting blood circulation；Menstruction regulating and pain relieving；Moisturize laxation
Frankincense
Nature and flavor：It is arduous, temperature
Effect：Regulating qi and activating blood, analgesic therapy chase after poison
Technical solution：
The present invention is achieved by the following technical solutions：
It is a kind of for treating chill pain in waist and lower extremities, the vina preparation process of muscles and bones numbness, which is characterized in that including below at Point：Piper wallichii (Miq.) Hand.-Mazz.：2800-2900 parts by weight, Chinese ephedra：90-100 parts by weight, Fructus Aurantii：75-80 parts by weight, cassia twig：75-80 weight Part, silkworm excrement：24-28 parts by weight, sealwort：30-35 parts by weight, dried orange peel：50-55 parts by weight, Cortex Magnoliae Officinalis：10-15 parts by weight, bitter apricot Benevolence：10-15 parts by weight, rhizoma alismatis：10-15 parts by weight, Chinese yam：10-15 parts by weight, rhizoma atractylodis：10-15 parts by weight, moutan bark：10- 15 parts by weight, Rhizoma Chuanxiong：10-15 parts by weight, Rhizoma Atractylodis Macrocephalae：10-15 parts by weight, the root of Dahurain angelica：10-15 parts by weight, root of Aucklandia lappa Decne：10-15 parts by weight, Lichen：10-15 parts by weight, Rhizoma Et Radix Notopterygii：10-15 parts by weight, fennel seeds：10-15 parts by weight, fructus gleditsiae：10-15 parts by weight, Psoralen Fat：10-15 parts by weight, rhizoma cyperi：10-15 parts by weight, Semen Cuscutae：10-15 parts by weight, myrrh：10-15 parts by weight, Radix Angelicae Sinensis：10- 15 parts by weight, frankincense：10-15 parts by weight.
Further, including following component：Piper wallichii (Miq.) Hand.-Mazz.：2812 parts by weight, Chinese ephedra：94 parts by weight, Fructus Aurantii：75 parts by weight, Cassia twig：75 parts by weight, silkworm excrement：24 parts by weight, sealwort：30 parts by weight, dried orange peel：50 parts by weight, Cortex Magnoliae Officinalis：11 parts by weight, semen armeniacae amarae： 11 parts by weight, rhizoma alismatis：11 parts by weight, Chinese yam：11 parts by weight, rhizoma atractylodis：11 parts by weight, moutan bark：11 parts by weight, Rhizoma Chuanxiong：11 weights Measure part, Rhizoma Atractylodis Macrocephalae：11 parts by weight, the root of Dahurain angelica：11 parts by weight, root of Aucklandia lappa Decne：11 parts by weight, lichen：11 parts by weight, Rhizoma Et Radix Notopterygii：11 parts by weight are small Fennel：11 parts by weight, fructus gleditsiae：11 parts by weight, psoralea corylifolia：11 parts by weight, rhizoma cyperi：11 parts by weight, Semen Cuscutae：11 parts by weight, Myrrh：11 parts by weight, Radix Angelicae Sinensis：11 parts by weight, frankincense：11 parts by weight.
Further, a kind of for treating chill pain in waist and lower extremities, the vina preparation process of muscles and bones numbness, which is characterized in that will Above-mentioned medicinal material by selecting, washing, drying, crushing, extracting, it is refining and edulcoration, filling, brown sugar is added, purified water is made accordingly Dosage form.
Further, the extracting method is that circumfluence distillation or sub-cooled are stood.
Further, the extraction solvent in the extracting method selects purified water or 50% ethyl alcohol.
Further, the refined, impurity-removing method is filtering or centrifugation.
Compared with prior art, the present invention having following advantageous effect：The present invention is made of 27 taste Chinese medicines, fully profit With modern pharmaceutical principle, it is fully extracted the active ingredient of drug, is used " circumfluence distillation " and " sub-cooled removal of impurities " Mode carries out vina production.
Advantageous effect：(1) extraction efficiency improves 80%；(2) " ephedrine " rate of transform in target effective ingredient " Chinese ephedra " Improve 60%；(3) microorganism detection is qualified.Ensure mouthfeel, under the premise of improving quality standard, improves the production effect of vina Rate realizes the continuous mechanized produces of vina.
Specific implementation mode
Below by specific embodiment, the present invention is further described, it is noted that for the ordinary skill of this field For personnel, without departing from the principle of the present invention, several variations and modifications can also be made, these also should be regarded as belonging to Protection scope of the present invention.
Embodiment 1
Formula：Main ingredient：Piper wallichii (Miq.) Hand.-Mazz.：2800 grams, Chinese ephedra：90 grams, Fructus Aurantii：75 grams, cassia twig：75 grams, silkworm excrement：24 grams, sealwort： 30 grams, dried orange peel：50 grams, Cortex Magnoliae Officinalis：10 grams, semen armeniacae amarae：10 grams, rhizoma alismatis：10 grams, Chinese yam：10 grams, rhizoma atractylodis：10 grams, moutan bark：10 Gram, Rhizoma Chuanxiong：10 grams, Rhizoma Atractylodis Macrocephalae：10 grams, the root of Dahurain angelica：10 grams, root of Aucklandia lappa Decne：10 grams, lichen：10 grams, Rhizoma Et Radix Notopterygii：10 grams, fennel seeds：10 grams, pig Tooth soap：10 grams, psoralea corylifolia：10 grams, rhizoma cyperi：10 grams, Semen Cuscutae：10 grams, myrrh：10 grams, Radix Angelicae Sinensis：10 grams, frankincense：10 grams
Preparation method：By 27 taste medicinal materials, it is ground into coarse powder, is put into extraction tank, (dosage is about medicinal material amount with 50 degree of white wine 10 times) 33.44 kilograms, after infiltration 30 minutes, refluxing extraction is carried out, reflow's cycle is 2 times, and 2 hours every time, liquid crossed 100 mesh Sieve merges liquid, stands 48 hours, takes supernatant, spare.
3.344 kilograms of brown sugar is dissolved, sieved with 100 mesh sieve with 3.344 kilograms of the purified water let cool is boiled, it is spare.
Brown sugar water is added into liquid, stirs 2 hours, constant volume, total amount 150L are carried out with 50 degree of white wine.It is small to stir 1 When.By all valves, pipeline closed.Low temperature (0-7 DEG C) cooling and standings are carried out using chilled water to clean, and stand 96 hours, supernatant Liquid crosses 200 mesh sieve, and underflow turbidity liquid is centrifuged with supercentrifuge, collects centrifugate.Merge supernatant and centrifugate, carries out It is filling, contained with the vial of 500ML, 500 milliliters every bottle to get.
Embodiment 2
Formula：Main ingredient：Piper wallichii (Miq.) Hand.-Mazz.：2800 grams, Chinese ephedra：90 grams, Fructus Aurantii：75 grams, cassia twig：75 grams, silkworm excrement：24 grams, sealwort： 30 grams, dried orange peel：50 grams, Cortex Magnoliae Officinalis：10 grams, semen armeniacae amarae：10 grams, rhizoma alismatis：10 grams, Chinese yam：10 grams, rhizoma atractylodis：10 grams, moutan bark：10 Gram, Rhizoma Chuanxiong：10 grams, Rhizoma Atractylodis Macrocephalae：10 grams, the root of Dahurain angelica：10 grams, root of Aucklandia lappa Decne：10 grams, lichen：10 grams, Rhizoma Et Radix Notopterygii：10 grams, fennel seeds：10 grams, pig Tooth soap：10 grams, psoralea corylifolia：10 grams, rhizoma cyperi：10 grams, Semen Cuscutae：10 grams, myrrh：10 grams, Radix Angelicae Sinensis：10 grams, frankincense：10 grams
Preparation method：By 27 taste medicinal materials, it is ground into coarse powder, is put into extraction tank, (dosage is about medicinal material amount with 50 degree of white wine 10 times) 33.44 kilograms, after infiltration 30 minutes, refluxing extraction is carried out, reflow's cycle is 3 times, and 3 hours every time, liquid crossed 100 mesh Sieve merges liquid, stands 48 hours, takes supernatant, spare.
3.344 kilograms of brown sugar is dissolved, sieved with 100 mesh sieve with 3.344 kilograms of the purified water let cool is boiled, it is spare.
Brown sugar water is added into liquid, stirs 2 hours, constant volume, total amount 150L are carried out with 50 degree of white wine.It is small to stir 1 When.By all valves, pipeline closed.Low temperature (0-7 DEG C) cooling and standings are carried out using chilled water to clean, and stand 96 hours, supernatant Liquid crosses 200 mesh sieve, and underflow turbidity liquid is centrifuged with supercentrifuge, collects centrifugate.Merge supernatant and centrifugate, carries out It is filling, contained with the vial of 500ML, 500 milliliters every bottle to get.
Embodiment 3
Formula：Main ingredient：Piper wallichii (Miq.) Hand.-Mazz.：2800 grams, Chinese ephedra：90 grams, Fructus Aurantii：75 grams, cassia twig：75 grams, silkworm excrement：24 grams, sealwort： 30 grams, dried orange peel：50 grams, Cortex Magnoliae Officinalis：10 grams, semen armeniacae amarae：10 grams, rhizoma alismatis：10 grams, Chinese yam：10 grams, rhizoma atractylodis：10 grams, moutan bark：10 Gram, Rhizoma Chuanxiong：10 grams, Rhizoma Atractylodis Macrocephalae：10 grams, the root of Dahurain angelica：10 grams, root of Aucklandia lappa Decne：10 grams, lichen：10 grams, Rhizoma Et Radix Notopterygii：10 grams, fennel seeds：10 grams, pig Tooth soap：10 grams, psoralea corylifolia：10 grams, rhizoma cyperi：10 grams, Semen Cuscutae：10 grams, myrrh：10 grams, Radix Angelicae Sinensis：10 grams, frankincense：10 grams
Preparation method：By 27 taste medicinal materials, it is ground into coarse powder, is put into extraction tank, (dosage is about medicinal material amount with 50 degree of white wine 10 times) 33.44 kilograms, after infiltration 30 minutes, refluxing extraction is carried out, reflow's cycle is 4 times, and 4 hours every time, liquid crossed 100 mesh Sieve merges liquid, stands 48 hours, takes supernatant, spare.
3.344 kilograms of brown sugar is dissolved, sieved with 100 mesh sieve with 3.344 kilograms of the purified water let cool is boiled, it is spare.
Brown sugar water is added into liquid, stirs 2 hours, constant volume, total amount 150L are carried out with 50 degree of white wine.It is small to stir 1 When.By all valves, pipeline closed.Low temperature (0-7 DEG C) cooling and standings are carried out using chilled water to clean, and stand 96 hours, supernatant Liquid crosses 200 mesh sieve, and underflow turbidity liquid is centrifuged with supercentrifuge, collects centrifugate.Merge supernatant and centrifugate, carries out It is filling, contained with the vial of 500ML, 500 milliliters every bottle to get.
Embodiment 4
Formula：Main ingredient：Piper wallichii (Miq.) Hand.-Mazz.：2800 grams, Chinese ephedra：90 grams, Fructus Aurantii：75 grams, cassia twig：75 grams, silkworm excrement：24 grams, sealwort： 30 grams, dried orange peel：50 grams, Cortex Magnoliae Officinalis：10 grams, semen armeniacae amarae：10 grams, rhizoma alismatis：10 grams, Chinese yam：10 grams, rhizoma atractylodis：10 grams, moutan bark：10 Gram, Rhizoma Chuanxiong：10 grams, Rhizoma Atractylodis Macrocephalae：10 grams, the root of Dahurain angelica：10 grams, root of Aucklandia lappa Decne：10 grams, lichen：10 grams, Rhizoma Et Radix Notopterygii：10 grams, fennel seeds：10 grams, pig Tooth soap：10 grams, psoralea corylifolia：10 grams, rhizoma cyperi：10 grams, Semen Cuscutae：10 grams, myrrh：10 grams, Radix Angelicae Sinensis：10 grams, frankincense：10 grams
Preparation method：By 27 taste medicinal materials, it is ground into coarse powder, is put into extraction tank, (dosage is about medicinal material amount with 50 degree of white wine 10 times) 33.44 kilograms, after infiltration 30 minutes, refluxing extraction is carried out, reflow's cycle is 2 times, and 3 hours every time, liquid crossed 100 mesh Sieve merges liquid, stands 48 hours, takes supernatant, spare.
3.344 kilograms of brown sugar is dissolved, sieved with 100 mesh sieve with 3.344 kilograms of the purified water let cool is boiled, it is spare.
Brown sugar water is added into liquid, stirs 2 hours, constant volume, total amount 150L are carried out with 50 degree of white wine.It is small to stir 1 When.By all valves, pipeline closed.Low temperature (0-7 DEG C) cooling and standings are carried out using chilled water to clean, and stand 96 hours, supernatant Liquid crosses 200 mesh sieve, and underflow turbidity liquid is centrifuged with supercentrifuge, collects centrifugate.Merge supernatant and centrifugate, carries out It is filling, contained with the vial of 500ML, 500 milliliters every bottle to get.
Embodiment 5
Formula：Main ingredient：Piper wallichii (Miq.) Hand.-Mazz.：2800 grams, Chinese ephedra：90 grams, Fructus Aurantii：75 grams, cassia twig：75 grams, silkworm excrement：24 grams, sealwort： 30 grams, dried orange peel：50 grams, Cortex Magnoliae Officinalis：10 grams, semen armeniacae amarae：10 grams, rhizoma alismatis：10 grams, Chinese yam：10 grams, rhizoma atractylodis：10 grams, moutan bark：10 Gram, Rhizoma Chuanxiong：10 grams, Rhizoma Atractylodis Macrocephalae：10 grams, the root of Dahurain angelica：10 grams, root of Aucklandia lappa Decne：10 grams, lichen：10 grams, Rhizoma Et Radix Notopterygii：10 grams, fennel seeds：10 grams, pig Tooth soap：10 grams, psoralea corylifolia：10 grams, rhizoma cyperi：10 grams, Semen Cuscutae：10 grams, myrrh：10 grams, Radix Angelicae Sinensis：10 grams, frankincense：10 grams
Preparation method：By 27 taste medicinal materials, it is ground into coarse powder, is put into extraction tank, (dosage is about medicinal material amount with 50 degree of white wine 10 times) 33.44 kilograms, after infiltration 30 minutes, refluxing extraction is carried out, reflow's cycle is 3 times, and 4 hours every time, liquid crossed 100 mesh Sieve merges liquid, stands 48 hours, takes supernatant, spare.
3.344 kilograms of brown sugar is dissolved, sieved with 100 mesh sieve with 3.344 kilograms of the purified water let cool is boiled, it is spare.
Brown sugar water is added into liquid, stirs 2 hours, constant volume, total amount 150L are carried out with 50 degree of white wine.It is small to stir 1 When.By all valves, pipeline closed.Low temperature (0-7 DEG C) cooling and standings are carried out using chilled water to clean, and stand 96 hours, supernatant Liquid crosses 200 mesh sieve, and underflow turbidity liquid is centrifuged with supercentrifuge, collects centrifugate.Merge supernatant and centrifugate, carries out It is filling, contained with the vial of 500ML, 500 milliliters every bottle to get.
Embodiment 6
Formula：Main ingredient：Piper wallichii (Miq.) Hand.-Mazz.：2800 grams, Chinese ephedra：90 grams, Fructus Aurantii：75 grams, cassia twig：75 grams, silkworm excrement：24 grams, sealwort： 30 grams, dried orange peel：50 grams, Cortex Magnoliae Officinalis：10 grams, semen armeniacae amarae：10 grams, rhizoma alismatis：10 grams, Chinese yam：10 grams, rhizoma atractylodis：10 grams, moutan bark：10 Gram, Rhizoma Chuanxiong：10 grams, Rhizoma Atractylodis Macrocephalae：10 grams, the root of Dahurain angelica：10 grams, root of Aucklandia lappa Decne：10 grams, lichen：10 grams, Rhizoma Et Radix Notopterygii：10 grams, fennel seeds：10 grams, pig Tooth soap：10 grams, psoralea corylifolia：10 grams, rhizoma cyperi：10 grams, Semen Cuscutae：10 grams, myrrh：10 grams, Radix Angelicae Sinensis：10 grams, frankincense：10 grams
Preparation method：By 27 taste medicinal materials, it is ground into coarse powder, is put into extraction tank, (dosage is about medicinal material amount with 50 degree of white wine 10 times) 33.44 kilograms, after infiltration 30 minutes, refluxing extraction is carried out, reflow's cycle is 4 times, and 2 hours every time, liquid crossed 100 mesh Sieve merges liquid, stands 48 hours, takes supernatant, spare.
3.344 kilograms of brown sugar is dissolved, sieved with 100 mesh sieve with 3.344 kilograms of the purified water let cool is boiled, it is spare.
Brown sugar water is added into liquid, stirs 2 hours, constant volume, total amount 150L are carried out with 50 degree of white wine.It is small to stir 1 When.By all valves, pipeline closed.Low temperature (0-7 DEG C) cooling and standings are carried out using chilled water to clean, and stand 96 hours, supernatant Liquid crosses 200 mesh sieve, and underflow turbidity liquid is centrifuged with supercentrifuge, collects centrifugate.Merge supernatant and centrifugate, carries out It is filling, contained with the vial of 500ML, 500 milliliters every bottle to get.
Embodiment 7
Formula：Main ingredient：Piper wallichii (Miq.) Hand.-Mazz.：2800 grams, Chinese ephedra：90 grams, Fructus Aurantii：75 grams, cassia twig：75 grams, silkworm excrement：24 grams, sealwort： 30 grams, dried orange peel：50 grams, Cortex Magnoliae Officinalis：10 grams, semen armeniacae amarae：10 grams, rhizoma alismatis：10 grams, Chinese yam：10 grams, rhizoma atractylodis：10 grams, moutan bark：10 Gram, Rhizoma Chuanxiong：10 grams, Rhizoma Atractylodis Macrocephalae：10 grams, the root of Dahurain angelica：10 grams, root of Aucklandia lappa Decne：10 grams, lichen：10 grams, Rhizoma Et Radix Notopterygii：10 grams, fennel seeds：10 grams, pig Tooth soap：10 grams, psoralea corylifolia：10 grams, rhizoma cyperi：10 grams, Semen Cuscutae：10 grams, myrrh：10 grams, Radix Angelicae Sinensis：10 grams, frankincense：10 grams
Preparation method：By 27 taste medicinal materials, it is ground into coarse powder, is put into extraction tank, (dosage is about medicinal material amount with 50 degree of white wine 10 times) 33.44 kilograms, after infiltration 30 minutes, refluxing extraction is carried out, reflow's cycle is 2 times, and 4 hours every time, liquid crossed 100 mesh Sieve merges liquid, stands 48 hours, takes supernatant, spare.
3.344 kilograms of brown sugar is dissolved, sieved with 100 mesh sieve with 3.344 kilograms of the purified water let cool is boiled, it is spare.
Brown sugar water is added into liquid, stirs 2 hours, constant volume, total amount 150L are carried out with 50 degree of white wine.It is small to stir 1 When.By all valves, pipeline closed.Low temperature (0-7 DEG C) cooling and standings are carried out using chilled water to clean, and stand 96 hours, supernatant Liquid crosses 200 mesh sieve, and underflow turbidity liquid is centrifuged with supercentrifuge, collects centrifugate.Merge supernatant and centrifugate, carries out It is filling, contained with the vial of 500ML, 500 milliliters every bottle to get.
Embodiment 8
Formula：Main ingredient：Piper wallichii (Miq.) Hand.-Mazz.：2800 grams, Chinese ephedra：90 grams, Fructus Aurantii：75 grams, cassia twig：75 grams, silkworm excrement：24 grams, sealwort： 30 grams, dried orange peel：50 grams, Cortex Magnoliae Officinalis：10 grams, semen armeniacae amarae：10 grams, rhizoma alismatis：10 grams, Chinese yam：10 grams, rhizoma atractylodis：10 grams, moutan bark：10 Gram, Rhizoma Chuanxiong：10 grams, Rhizoma Atractylodis Macrocephalae：10 grams, the root of Dahurain angelica：10 grams, root of Aucklandia lappa Decne：10 grams, lichen：10 grams, Rhizoma Et Radix Notopterygii：10 grams, fennel seeds：10 grams, pig Tooth soap：10 grams, psoralea corylifolia：10 grams, rhizoma cyperi：10 grams, Semen Cuscutae：10 grams, myrrh：10 grams, Radix Angelicae Sinensis：10 grams, frankincense：10 grams
Preparation method：By 27 taste medicinal materials, it is ground into coarse powder, is put into extraction tank, (dosage is about medicinal material amount with 50 degree of white wine 10 times) 33.44 kilograms, after infiltration 30 minutes, refluxing extraction is carried out, reflow's cycle is 3 times, and 2 hours every time, liquid crossed 100 mesh Sieve merges liquid, stands 48 hours, takes supernatant, spare.
3.344 kilograms of brown sugar is dissolved, sieved with 100 mesh sieve with 3.344 kilograms of the purified water let cool is boiled, it is spare.
Brown sugar water is added into liquid, stirs 2 hours, constant volume, total amount 150L are carried out with 50 degree of white wine.It is small to stir 1 When.By all valves, pipeline closed.Low temperature (0-7 DEG C) cooling and standings are carried out using chilled water to clean, and stand 96 hours, supernatant Liquid crosses 200 mesh sieve, and underflow turbidity liquid is centrifuged with supercentrifuge, collects centrifugate.Merge supernatant and centrifugate, carries out It is filling, contained with the vial of 500ML, 500 milliliters every bottle to get.
Embodiment 9
Formula：Main ingredient：Piper wallichii (Miq.) Hand.-Mazz.：2800 grams, Chinese ephedra：90 grams, Fructus Aurantii：75 grams, cassia twig：75 grams, silkworm excrement：24 grams, sealwort： 30 grams, dried orange peel：50 grams, Cortex Magnoliae Officinalis：10 grams, semen armeniacae amarae：10 grams, rhizoma alismatis：10 grams, Chinese yam：10 grams, rhizoma atractylodis：10 grams, moutan bark：10 Gram, Rhizoma Chuanxiong：10 grams, Rhizoma Atractylodis Macrocephalae：10 grams, the root of Dahurain angelica：10 grams, root of Aucklandia lappa Decne：10 grams, lichen：10 grams, Rhizoma Et Radix Notopterygii：10 grams, fennel seeds：10 grams, pig Tooth soap：10 grams, psoralea corylifolia：10 grams, rhizoma cyperi：10 grams, Semen Cuscutae：10 grams, myrrh：10 grams, Radix Angelicae Sinensis：10 grams, frankincense：10 grams
Preparation method：By 27 taste medicinal materials, it is ground into coarse powder, is put into extraction tank, (dosage is about medicinal material amount with 50 degree of white wine 10 times) 33.44 kilograms, after infiltration 30 minutes, refluxing extraction is carried out, reflow's cycle is 4 times, and 3 hours every time, liquid crossed 100 mesh Sieve merges liquid, stands 48 hours, takes supernatant, spare.
3.344 kilograms of brown sugar is dissolved, sieved with 100 mesh sieve with 3.344 kilograms of the purified water let cool is boiled, it is spare.
Brown sugar water is added into liquid, stirs 2 hours, constant volume, total amount 150L are carried out with 50 degree of white wine.It is small to stir 1 When.By all valves, pipeline closed.Low temperature (0-7 DEG C) cooling and standings are carried out using chilled water to clean, and stand 96 hours, supernatant Liquid crosses 200 mesh sieve, and underflow turbidity liquid is centrifuged with supercentrifuge, collects centrifugate.Merge supernatant and centrifugate, carries out It is filling, contained with the vial of 500ML, 500 milliliters every bottle to get.
Embodiment 10
Formula：Main ingredient：Piper wallichii (Miq.) Hand.-Mazz.：2900 grams, Chinese ephedra：100 grams, Fructus Aurantii：80 grams, cassia twig：80 grams, silkworm excrement：It is 28 grams, yellow Essence：35 grams, dried orange peel：55 grams, Cortex Magnoliae Officinalis：15 grams, semen armeniacae amarae：15 grams, rhizoma alismatis：15 grams, Chinese yam：15 grams, rhizoma atractylodis：15 grams, moutan bark： 15 grams, Rhizoma Chuanxiong：15 grams, Rhizoma Atractylodis Macrocephalae：15 grams, the root of Dahurain angelica：15 grams, root of Aucklandia lappa Decne：15 grams, lichen：15 grams, Rhizoma Et Radix Notopterygii：15 grams, fennel seeds：15 grams, Fructus gleditsiae：15 grams, psoralea corylifolia：15 grams, rhizoma cyperi：15 grams, Semen Cuscutae：15 grams, myrrh：15 grams, Radix Angelicae Sinensis：15 grams, frankincense：15 grams
Preparation method：By 27 taste medicinal materials, it is ground into coarse powder, is put into extraction tank, (dosage is about medicinal material amount with 50 degree of white wine 10 times) 33.44 kilograms, after infiltration 30 minutes, refluxing extraction is carried out, reflow's cycle is 2 times, and 2 hours every time, liquid crossed 100 mesh Sieve merges liquid, stands 48 hours, takes supernatant, spare.
3.344 kilograms of brown sugar is dissolved, sieved with 100 mesh sieve with 3.344 kilograms of the purified water let cool is boiled, it is spare.
Brown sugar water is added into liquid, stirs 2 hours, constant volume, total amount 150L are carried out with 50 degree of white wine.It is small to stir 1 When.By all valves, pipeline closed.Low temperature (0-7 DEG C) cooling and standings are carried out using chilled water to clean, and stand 96 hours, supernatant Liquid crosses 200 mesh sieve, and underflow turbidity liquid is centrifuged with supercentrifuge, collects centrifugate.Merge supernatant and centrifugate, carries out It is filling, contained with the vial of 500ML, 500 milliliters every bottle to get.
Embodiment 11
Formula：Main ingredient：Piper wallichii (Miq.) Hand.-Mazz.：2900 grams, Chinese ephedra：100 grams, Fructus Aurantii：80 grams, cassia twig：80 grams, silkworm excrement：It is 28 grams, yellow Essence：35 grams, dried orange peel：55 grams, Cortex Magnoliae Officinalis：15 grams, semen armeniacae amarae：15 grams, rhizoma alismatis：15 grams, Chinese yam：15 grams, rhizoma atractylodis：15 grams, moutan bark： 15 grams, Rhizoma Chuanxiong：15 grams, Rhizoma Atractylodis Macrocephalae：15 grams, the root of Dahurain angelica：15 grams, root of Aucklandia lappa Decne：15 grams, lichen：15 grams, Rhizoma Et Radix Notopterygii：15 grams, fennel seeds：15 grams, Fructus gleditsiae：15 grams, psoralea corylifolia：15 grams, rhizoma cyperi：15 grams, Semen Cuscutae：15 grams, myrrh：15 grams, Radix Angelicae Sinensis：15 grams, frankincense：15 grams
Preparation method：By 27 taste medicinal materials, it is ground into coarse powder, is put into extraction tank, (dosage is about medicinal material amount with 50 degree of white wine 10 times) 33.44 kilograms, after infiltration 30 minutes, refluxing extraction is carried out, reflow's cycle is 3 times, and 3 hours every time, liquid crossed 100 mesh Sieve merges liquid, stands 48 hours, takes supernatant, spare.
3.344 kilograms of brown sugar is dissolved, sieved with 100 mesh sieve with 3.344 kilograms of the purified water let cool is boiled, it is spare.
Brown sugar water is added into liquid, stirs 2 hours, constant volume, total amount 150L are carried out with 50 degree of white wine.It is small to stir 1 When.By all valves, pipeline closed.Low temperature (0-7 DEG C) cooling and standings are carried out using chilled water to clean, and stand 96 hours, supernatant Liquid crosses 200 mesh sieve, and underflow turbidity liquid is centrifuged with supercentrifuge, collects centrifugate.Merge supernatant and centrifugate, carries out It is filling, contained with the vial of 500ML, 500 milliliters every bottle to get.
Embodiment 12
Formula：Main ingredient：Piper wallichii (Miq.) Hand.-Mazz.：2900 grams, Chinese ephedra：100 grams, Fructus Aurantii：80 grams, cassia twig：80 grams, silkworm excrement：It is 28 grams, yellow Essence：35 grams, dried orange peel：55 grams, Cortex Magnoliae Officinalis：15 grams, semen armeniacae amarae：15 grams, rhizoma alismatis：15 grams, Chinese yam：15 grams, rhizoma atractylodis：15 grams, moutan bark： 15 grams, Rhizoma Chuanxiong：15 grams, Rhizoma Atractylodis Macrocephalae：15 grams, the root of Dahurain angelica：15 grams, root of Aucklandia lappa Decne：15 grams, lichen：15 grams, Rhizoma Et Radix Notopterygii：15 grams, fennel seeds：15 grams, Fructus gleditsiae：15 grams, psoralea corylifolia：15 grams, rhizoma cyperi：15 grams, Semen Cuscutae：15 grams, myrrh：15 grams, Radix Angelicae Sinensis：15 grams, frankincense：15 grams
Preparation method：By 27 taste medicinal materials, it is ground into coarse powder, is put into extraction tank, (dosage is about medicinal material amount with 50 degree of white wine 10 times) 33.44 kilograms, after infiltration 30 minutes, refluxing extraction is carried out, reflow's cycle is 4 times, and 4 hours every time, liquid crossed 100 mesh Sieve merges liquid, stands 48 hours, takes supernatant, spare.
3.344 kilograms of brown sugar is dissolved, sieved with 100 mesh sieve with 3.344 kilograms of the purified water let cool is boiled, it is spare.
Brown sugar water is added into liquid, stirs 2 hours, constant volume, total amount 150L are carried out with 50 degree of white wine.It is small to stir 1 When.By all valves, pipeline closed.Low temperature (0-7 DEG C) cooling and standings are carried out using chilled water to clean, and stand 96 hours, supernatant Liquid crosses 200 mesh sieve, and underflow turbidity liquid is centrifuged with supercentrifuge, collects centrifugate.Merge supernatant and centrifugate, carries out It is filling, contained with the vial of 500ML, 500 milliliters every bottle to get.
Embodiment 13
Formula：Main ingredient：Piper wallichii (Miq.) Hand.-Mazz.：2900 grams, Chinese ephedra：100 grams, Fructus Aurantii：80 grams, cassia twig：80 grams, silkworm excrement：It is 28 grams, yellow Essence：35 grams, dried orange peel：55 grams, Cortex Magnoliae Officinalis：15 grams, semen armeniacae amarae：15 grams, rhizoma alismatis：15 grams, Chinese yam：15 grams, rhizoma atractylodis：15 grams, moutan bark： 15 grams, Rhizoma Chuanxiong：15 grams, Rhizoma Atractylodis Macrocephalae：15 grams, the root of Dahurain angelica：15 grams, root of Aucklandia lappa Decne：15 grams, lichen：15 grams, Rhizoma Et Radix Notopterygii：15 grams, fennel seeds：15 grams, Fructus gleditsiae：15 grams, psoralea corylifolia：15 grams, rhizoma cyperi：15 grams, Semen Cuscutae：15 grams, myrrh：15 grams, Radix Angelicae Sinensis：15 grams, frankincense：15 grams
Preparation method：By 27 taste medicinal materials, it is ground into coarse powder, is put into extraction tank, (dosage is about medicinal material amount with 50 degree of white wine 10 times) 33.44 kilograms, after infiltration 30 minutes, refluxing extraction is carried out, reflow's cycle is 2 times, and 3 hours every time, liquid crossed 100 mesh Sieve merges liquid, stands 48 hours, takes supernatant, spare.
3.344 kilograms of brown sugar is dissolved, sieved with 100 mesh sieve with 3.344 kilograms of the purified water let cool is boiled, it is spare.
Brown sugar water is added into liquid, stirs 2 hours, constant volume, total amount 150L are carried out with 50 degree of white wine.It is small to stir 1 When.By all valves, pipeline closed.Low temperature (0-7 DEG C) cooling and standings are carried out using chilled water to clean, and stand 96 hours, supernatant Liquid crosses 200 mesh sieve, and underflow turbidity liquid is centrifuged with supercentrifuge, collects centrifugate.Merge supernatant and centrifugate, carries out It is filling, contained with the vial of 500ML, 500 milliliters every bottle to get.
Embodiment 14
Formula：Main ingredient：Piper wallichii (Miq.) Hand.-Mazz.：2900 grams, Chinese ephedra：100 grams, Fructus Aurantii：80 grams, cassia twig：80 grams, silkworm excrement：It is 28 grams, yellow Essence：35 grams, dried orange peel：55 grams, Cortex Magnoliae Officinalis：15 grams, semen armeniacae amarae：15 grams, rhizoma alismatis：15 grams, Chinese yam：15 grams, rhizoma atractylodis：15 grams, moutan bark： 15 grams, Rhizoma Chuanxiong：15 grams, Rhizoma Atractylodis Macrocephalae：15 grams, the root of Dahurain angelica：15 grams, root of Aucklandia lappa Decne：15 grams, lichen：15 grams, Rhizoma Et Radix Notopterygii：15 grams, fennel seeds：15 grams, Fructus gleditsiae：15 grams, psoralea corylifolia：15 grams, rhizoma cyperi：15 grams, Semen Cuscutae：15 grams, myrrh：15 grams, Radix Angelicae Sinensis：15 grams, frankincense：15 grams
Preparation method：By 27 taste medicinal materials, it is ground into coarse powder, is put into extraction tank, (dosage is about medicinal material amount with 50 degree of white wine 10 times) 33.44 kilograms, after infiltration 30 minutes, refluxing extraction is carried out, reflow's cycle is 3 times, and 4 hours every time, liquid crossed 100 mesh Sieve merges liquid, stands 48 hours, takes supernatant, spare.
3.344 kilograms of brown sugar is dissolved, sieved with 100 mesh sieve with 3.344 kilograms of the purified water let cool is boiled, it is spare.
Brown sugar water is added into liquid, stirs 2 hours, constant volume, total amount 150L are carried out with 50 degree of white wine.It is small to stir 1 When.By all valves, pipeline closed.Low temperature (0-7 DEG C) cooling and standings are carried out using chilled water to clean, and stand 96 hours, supernatant Liquid crosses 200 mesh sieve, and underflow turbidity liquid is centrifuged with supercentrifuge, collects centrifugate.Merge supernatant and centrifugate, carries out It is filling, contained with the vial of 500ML, 500 milliliters every bottle to get.
Embodiment 15
Formula：Main ingredient：Piper wallichii (Miq.) Hand.-Mazz.：2900 grams, Chinese ephedra：100 grams, Fructus Aurantii：80 grams, cassia twig：80 grams, silkworm excrement：It is 28 grams, yellow Essence：35 grams, dried orange peel：55 grams, Cortex Magnoliae Officinalis：15 grams, semen armeniacae amarae：15 grams, rhizoma alismatis：15 grams, Chinese yam：15 grams, rhizoma atractylodis：15 grams, moutan bark： 15 grams, Rhizoma Chuanxiong：15 grams, Rhizoma Atractylodis Macrocephalae：15 grams, the root of Dahurain angelica：15 grams, root of Aucklandia lappa Decne：15 grams, lichen：15 grams, Rhizoma Et Radix Notopterygii：15 grams, fennel seeds：15 grams, Fructus gleditsiae：15 grams, psoralea corylifolia：15 grams, rhizoma cyperi：15 grams, Semen Cuscutae：15 grams, myrrh：15 grams, Radix Angelicae Sinensis：15 grams, frankincense：15 grams
Preparation method：By 27 taste medicinal materials, it is ground into coarse powder, is put into extraction tank, (dosage is about medicinal material amount with 50 degree of white wine 10 times) 33.44 kilograms, after infiltration 30 minutes, refluxing extraction is carried out, reflow's cycle is 4 times, and 2 hours every time, liquid crossed 100 mesh Sieve merges liquid, stands 48 hours, takes supernatant, spare.
3.344 kilograms of brown sugar is dissolved, sieved with 100 mesh sieve with 3.344 kilograms of the purified water let cool is boiled, it is spare.
Brown sugar water is added into liquid, stirs 2 hours, constant volume, total amount 150L are carried out with 50 degree of white wine.It is small to stir 1 When.By all valves, pipeline closed.Low temperature (0-7 DEG C) cooling and standings are carried out using chilled water to clean, and stand 96 hours, supernatant Liquid crosses 200 mesh sieve, and underflow turbidity liquid is centrifuged with supercentrifuge, collects centrifugate.Merge supernatant and centrifugate, carries out It is filling, contained with the vial of 500ML, 500 milliliters every bottle to get.
Embodiment 16
Formula：Main ingredient：Piper wallichii (Miq.) Hand.-Mazz.：2900 grams, Chinese ephedra：100 grams, Fructus Aurantii：80 grams, cassia twig：80 grams, silkworm excrement：It is 28 grams, yellow Essence：35 grams, dried orange peel：55 grams, Cortex Magnoliae Officinalis：15 grams, semen armeniacae amarae：15 grams, rhizoma alismatis：15 grams, Chinese yam：15 grams, rhizoma atractylodis：15 grams, moutan bark： 15 grams, Rhizoma Chuanxiong：15 grams, Rhizoma Atractylodis Macrocephalae：15 grams, the root of Dahurain angelica：15 grams, root of Aucklandia lappa Decne：15 grams, lichen：15 grams, Rhizoma Et Radix Notopterygii：15 grams, fennel seeds：15 grams, Fructus gleditsiae：15 grams, psoralea corylifolia：15 grams, rhizoma cyperi：15 grams, Semen Cuscutae：15 grams, myrrh：15 grams, Radix Angelicae Sinensis：15 grams, frankincense：15 grams
Preparation method：By 27 taste medicinal materials, it is ground into coarse powder, is put into extraction tank, (dosage is about medicinal material amount with 50 degree of white wine 10 times) 33.44 kilograms, after infiltration 30 minutes, refluxing extraction is carried out, reflow's cycle is 3 times, and 2 hours every time, liquid crossed 100 mesh Sieve merges liquid, stands 48 hours, takes supernatant, spare.
3.344 kilograms of brown sugar is dissolved, sieved with 100 mesh sieve with 3.344 kilograms of the purified water let cool is boiled, it is spare.
Brown sugar water is added into liquid, stirs 2 hours, constant volume, total amount 150L are carried out with 50 degree of white wine.It is small to stir 1 When.By all valves, pipeline closed.Low temperature (0-7 DEG C) cooling and standings are carried out using chilled water to clean, and stand 96 hours, supernatant Liquid crosses 200 mesh sieve, and underflow turbidity liquid is centrifuged with supercentrifuge, collects centrifugate.Merge supernatant and centrifugate, carries out It is filling, contained with the vial of 500ML, 500 milliliters every bottle to get.
Embodiment 17
Formula：Main ingredient：Piper wallichii (Miq.) Hand.-Mazz.：2900 grams, Chinese ephedra：100 grams, Fructus Aurantii：80 grams, cassia twig：80 grams, silkworm excrement：It is 28 grams, yellow Essence：35 grams, dried orange peel：55 grams, Cortex Magnoliae Officinalis：15 grams, semen armeniacae amarae：15 grams, rhizoma alismatis：15 grams, Chinese yam：15 grams, rhizoma atractylodis：15 grams, moutan bark： 15 grams, Rhizoma Chuanxiong：15 grams, Rhizoma Atractylodis Macrocephalae：15 grams, the root of Dahurain angelica：15 grams, root of Aucklandia lappa Decne：15 grams, lichen：15 grams, Rhizoma Et Radix Notopterygii：15 grams, fennel seeds：15 grams, Fructus gleditsiae：15 grams, psoralea corylifolia：15 grams, rhizoma cyperi：15 grams, Semen Cuscutae：15 grams, myrrh：15 grams, Radix Angelicae Sinensis：15 grams, frankincense：15 grams
Preparation method：By 27 taste medicinal materials, it is ground into coarse powder, is put into extraction tank, (dosage is about medicinal material amount with 50 degree of white wine 10 times) 33.44 kilograms, after infiltration 30 minutes, refluxing extraction is carried out, reflow's cycle is 2 times, and 4 hours every time, liquid crossed 100 mesh Sieve merges liquid, stands 48 hours, takes supernatant, spare.
3.344 kilograms of brown sugar is dissolved, sieved with 100 mesh sieve with 3.344 kilograms of the purified water let cool is boiled, it is spare.
Brown sugar water is added into liquid, stirs 2 hours, constant volume, total amount 150L are carried out with 50 degree of white wine.It is small to stir 1 When.By all valves, pipeline closed.Low temperature (0-7 DEG C) cooling and standings are carried out using chilled water to clean, and stand 96 hours, supernatant Liquid crosses 200 mesh sieve, and underflow turbidity liquid is centrifuged with supercentrifuge, collects centrifugate.Merge supernatant and centrifugate, carries out It is filling, contained with the vial of 500ML, 500 milliliters every bottle to get.
Embodiment 18
Formula：Main ingredient：Piper wallichii (Miq.) Hand.-Mazz.：2900 grams, Chinese ephedra：100 grams, Fructus Aurantii：80 grams, cassia twig：80 grams, silkworm excrement：It is 28 grams, yellow Essence：35 grams, dried orange peel：55 grams, Cortex Magnoliae Officinalis：15 grams, semen armeniacae amarae：15 grams, rhizoma alismatis：15 grams, Chinese yam：15 grams, rhizoma atractylodis：15 grams, moutan bark： 15 grams, Rhizoma Chuanxiong：15 grams, Rhizoma Atractylodis Macrocephalae：15 grams, the root of Dahurain angelica：15 grams, root of Aucklandia lappa Decne：15 grams, lichen：15 grams, Rhizoma Et Radix Notopterygii：15 grams, fennel seeds：15 grams, Fructus gleditsiae：15 grams, psoralea corylifolia：15 grams, rhizoma cyperi：15 grams, Semen Cuscutae：15 grams, myrrh：15 grams, Radix Angelicae Sinensis：15 grams, frankincense：15 grams
Preparation method：By 27 taste medicinal materials, it is ground into coarse powder, is put into extraction tank, (dosage is about medicinal material amount with 50 degree of white wine 10 times) 33.44 kilograms, after infiltration 30 minutes, refluxing extraction is carried out, reflow's cycle is 4 times, and 3 hours every time, liquid crossed 100 mesh Sieve merges liquid, stands 48 hours, takes supernatant, spare.
3.344 kilograms of brown sugar is dissolved, sieved with 100 mesh sieve with 3.344 kilograms of the purified water let cool is boiled, it is spare.
Brown sugar water is added into liquid, stirs 2 hours, constant volume, total amount 150L are carried out with 50 degree of white wine.It is small to stir 1 When.By all valves, pipeline closed.Low temperature (0-7 DEG C) cooling and standings are carried out using chilled water to clean, and stand 96 hours, supernatant Liquid crosses 200 mesh sieve, and underflow turbidity liquid is centrifuged with supercentrifuge, collects centrifugate.Merge supernatant and centrifugate, carries out It is filling, contained with the vial of 500ML, 500 milliliters every bottle to get.
Comparative example 1
With reference to Chinese patent (application number：201710504332.7) a kind of medicinal liquor for being prepared of embodiment.
Comparative example 2
With reference to Chinese patent (application number：201210056944.1) a kind of medicinal liquor for being prepared of embodiment.
Comparative example 3
In addition to no Piper wallichii (Miq.) Hand.-Mazz., material content and step are consistent with embodiment 1.
Comparative example 4
In addition to no Chinese ephedra, material content and step are consistent with embodiment 1.
Test example 1
Clinical trial is divided into two parts：
(1) animal acute toxicity and chronic toxicity experiment：
1, animal acute toxicity test
Drug：Vina obtained in 1-18 of the embodiment of the present invention.
Experimental animal：Regular grade NIH mouse, weight 18g ± 2g, half male and half female.
Method and result：
Experiment mice is randomly divided into 18 groups of half male and half females, 18 parts of vina of feeding, 20 hours or so hungry respectively, by every Feed 5ml 3 times per natural gift, it is continuous to feed one week, observe 10 days, mouse activity normally, non-toxic reaction, no death.Show the medicine Object is without acute toxicity, clinical medicine dose safety.
2, long-term toxicity test for animals
Drug：Vina obtained in 1-18 of the embodiment of the present invention.
Animal：Regular grade SD rats, weight 200g ± 10g, half male and half female.
Method and result：
Experiment mice is randomly divided into 18 groups of half male and half females, 18 parts of vina of feeding, feed, often 2 times a day by every respectively Secondary 5ml is continuously fed 90 days, survey weight, in last time be administered after 24 hours sacrificed by decapitation, survey blood, routine urinalysis, liver function, The effect of dosage is observed in renal function, the internal organ such as coring, kidney, the variation of tissues observed form, and observation diet, movable variation are real Bright non-toxic reaction is verified, is a kind of safe vina.
Pass through two above toxicity test, it was demonstrated that the present invention is safe, nontoxic pair by vina made from embodiment 1-18 Effect, it can be used for carrying out clinical test to clinical patients.
Test example 2
Effect research of the embodiment of the present invention:
220 pain in the back patients are chosen, wherein adult human male 112, adult female 108 is randomly divided into 22 groups, every group 10 People.
(2) investigation result
Investigation result is shown in Table 1
Initial investigation results show that significant therapeutic effect can be played by taking vina prepared by the present invention.

Claims (6)

1. a kind of for treating chill pain in waist and lower extremities, the vina preparation process of muscles and bones numbness, which is characterized in that including following component： Piper wallichii (Miq.) Hand.-Mazz.：2800-2900 parts by weight, Chinese ephedra：90-100 parts by weight, Fructus Aurantii：75-80 parts by weight, cassia twig：75-80 parts by weight, silkworm Sand：24-28 parts by weight, sealwort：30-35 parts by weight, dried orange peel：50-55 parts by weight, Cortex Magnoliae Officinalis：10-15 parts by weight, semen armeniacae amarae：10- 15 parts by weight, rhizoma alismatis：10-15 parts by weight, Chinese yam：10-15 parts by weight, rhizoma atractylodis：10-15 parts by weight, moutan bark：10-15 weight Part, Rhizoma Chuanxiong：10-15 parts by weight, Rhizoma Atractylodis Macrocephalae：10-15 parts by weight, the root of Dahurain angelica：10-15 parts by weight, root of Aucklandia lappa Decne：10-15 parts by weight, lichen： 10-15 parts by weight, Rhizoma Et Radix Notopterygii：10-15 parts by weight, fennel seeds：10-15 parts by weight, fructus gleditsiae：10-15 parts by weight, psoralea corylifolia：10- 15 parts by weight, rhizoma cyperi：10-15 parts by weight, Semen Cuscutae：10-15 parts by weight, myrrh：10-15 parts by weight, Radix Angelicae Sinensis：10-15 weight Part, frankincense：10-15 parts by weight.
2. it is according to claim 1 or 2 a kind of for treating chill pain in waist and lower extremities, the vina preparation process of muscles and bones numbness, It is characterized in that, including following component：Piper wallichii (Miq.) Hand.-Mazz.：2812 parts by weight, Chinese ephedra：94 parts by weight, Fructus Aurantii：75 parts by weight, cassia twig：75 weights Measure part, silkworm excrement：24 parts by weight, sealwort：30 parts by weight, dried orange peel：50 parts by weight, Cortex Magnoliae Officinalis：11 parts by weight, semen armeniacae amarae：11 parts by weight, Rhizoma alismatis：11 parts by weight, Chinese yam：11 parts by weight, rhizoma atractylodis：11 parts by weight, moutan bark：11 parts by weight, Rhizoma Chuanxiong：11 parts by weight, Rhizoma Atractylodis Macrocephalae： 11 parts by weight, the root of Dahurain angelica：11 parts by weight, root of Aucklandia lappa Decne：11 parts by weight, lichen：11 parts by weight, Rhizoma Et Radix Notopterygii：11 parts by weight, fennel seeds：11 weights Measure part, fructus gleditsiae：11 parts by weight, psoralea corylifolia：11 parts by weight, rhizoma cyperi：11 parts by weight, Semen Cuscutae：11 parts by weight, myrrh：11 weights Measure part, Radix Angelicae Sinensis：11 parts by weight, frankincense：11 parts by weight.
3. it is according to claim 1 or 2 a kind of for treating chill pain in waist and lower extremities, the vina preparation process of muscles and bones numbness, Be characterized in that, by above-mentioned medicinal material by selecting, washing, drying, crushing, extracting, it is refining and edulcoration, filling, brown sugar, purified water is added Corresponding dosage form is made.
4. according to claim 3 a kind of for treating chill pain in waist and lower extremities, the vina preparation process of muscles and bones numbness, feature It is, the extracting method is that circumfluence distillation or sub-cooled are stood.
5. according to claim 3 a kind of for treating chill pain in waist and lower extremities, the vina preparation process of muscles and bones numbness, feature It is, the extraction solvent in the extracting method selects purified water or 50% ethyl alcohol.
6. according to claim 3 a kind of for treating chill pain in waist and lower extremities, the vina preparation process of muscles and bones numbness, feature It is, the refined, impurity-removing method is filtering or centrifugation.
CN201810518990.6A 2018-05-28 2018-05-28 It is a kind of to be used to treat chill pain in waist and lower extremities, the vina preparation process of muscles and bones numbness Pending CN108498696A (en)

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Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104189463A (en) * 2014-08-07 2014-12-10 江西九华药业有限公司 Rheumatism pain medicinal liquor and preparation method thereof
CN105168736A (en) * 2015-09-13 2015-12-23 登封市科技企业孵化服务中心 Traditional Chinese medicine wine for relieving pains in treatment of rheumatism

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104189463A (en) * 2014-08-07 2014-12-10 江西九华药业有限公司 Rheumatism pain medicinal liquor and preparation method thereof
CN105168736A (en) * 2015-09-13 2015-12-23 登封市科技企业孵化服务中心 Traditional Chinese medicine wine for relieving pains in treatment of rheumatism

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