CN108410399B - A kind of left and right waist patch special glue and preparation method thereof - Google Patents

A kind of left and right waist patch special glue and preparation method thereof Download PDF

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Publication number
CN108410399B
CN108410399B CN201810266274.3A CN201810266274A CN108410399B CN 108410399 B CN108410399 B CN 108410399B CN 201810266274 A CN201810266274 A CN 201810266274A CN 108410399 B CN108410399 B CN 108410399B
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China
Prior art keywords
parts
left
right waist
special glue
styrene
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CN201810266274.3A
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Chinese (zh)
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CN108410399A (en
Inventor
史云霓
王文敏
任鹏
朱琼
陈凯
胥伟
张念装
成双
汤君
汤露
熊立平
龚飞
Original Assignee
江苏嘉好热熔胶股份有限公司
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Priority to CN201810266274.3A priority Critical patent/CN108410399B/en
Publication of CN108410399A publication Critical patent/CN108410399A/en
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIAL AS ADHESIVES
    • C09J147/00Adhesives based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, at least one having two or more carbon-to-carbon double bonds; Adhesives based on derivatives of such polymers
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIAL AS ADHESIVES
    • C09J11/00Features of adhesives not provided for in group C09J9/00, e.g. additives
    • C09J11/02Non-macromolecular additives
    • C09J11/06Non-macromolecular additives organic
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIAL AS ADHESIVES
    • C09J157/00Adhesives based on unspecified polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C09J157/02Copolymers of mineral oil hydrocarbons
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00Specific properties of additives
    • C08K2201/014Additives containing two or more different additives of the same subgroup in C08K

Abstract

A kind of left and right waist patch special glue, in parts by weight, preparing raw material includes: styrene-ethylene based compound -100 parts of diene copolymer, 100 parts of tackifying resin, 50 parts of plasticising oil.The diene is conjugated diene.The tackifying resin is selected from hydrogenated petroleum resin and/or hydrogenation phenolic resin.

Description

A kind of left and right waist patch special glue and preparation method thereof

Technical field

The present invention relates to adhesive areas more particularly to a kind of left and right waist patch special glue and preparation method thereof.

Background technique

Hot melt adhesive is a kind of adhesive of plasticity, its physical state changes with temperature and changed in certain temperature range Become, and chemical characteristic is constant, it is non-toxic and tasteless, belong to environmental-protecting chemical product.Because of its product itself system solid, convenient for packaging, fortune Defeated, storage, solvent-free, pollution-free, nontoxic type;And simple production process, high added value, it is excellent that bonding strength is big, speed is fast etc. Point and by favor.The adhesive property of left and right waist patch special glue on the market and ageing-resistant ability are not able to satisfy and want at present It asks, is easy to rub in the state of wet, not only influences comfort level, flu is also easily caused when it is cold.

Summary of the invention

In order to solve prior art problem, the first aspect of the present invention provides a kind of left and right waist patch special glue, and preparation is former Material includes: styrene-ethylene based compound-diene copolymer, tackifying resin, plasticising oil.

In some embodiments, in parts by weight, preparing raw material includes: that styrene-ethylene based compound-diene is total 100 parts of polymers, 100 parts of tackifying resin, 50 parts of plasticising oil.

In some embodiments, the diene is conjugated diene.

In some embodiments, the tackifying resin is selected from hydrogenated petroleum resin and/or hydrogenation phenolic resin.

In some embodiments, the plasticising oil is selected from Dioctyl Glutaricate, didecyl glutarate, two isodecyl of glutaric acid Ester, two fourth 2-ethoxyethyl acetate of glutaric acid, two fourth oxygen ethoxy ethyl ester of glutaric acid, Di-n-butyl Adipate, diisobutyl adipate, adipic acid Two just own esters, dioctyl adipate or adipic acid two (2- ethylhexyl), diisooctyl adipate, dinonyl adipate, oneself two Sour dinonyl, diisodecyl adipate (DIDA), two fourth 2-ethoxyethyl acetate of adipic acid, adipic acid two (Butoxyethoxy second) ester, azelaic acid Two fourth 2-ethoxyethyl acetates, dibenzyl azelate, dicyclohexyl azelate, dimethyl sebacate, n-butyl sebacate, decanedioic acid two are different Propyl ester, dioctyl sebacate, Plexol 201, decanedioic acid di-sec-octyl, di-n-nonyl sebacate, two (butoxy of decanedioic acid Second) ester, decanedioic acid two (Butoxyethoxy second) ester, dibenzyl sebacate, diethyl sebacate, in dihexyl sebacate extremely Few one kind.

In some embodiments, the conjugated diene is selected from one of 1,3- octadiene, 2,4- octadiene.

In some embodiments, the vinyl compound in 1- vinyl imidazole, 2- vinylpyridine one Kind.

In some embodiments, styrene in the styrene-ethylene based compound-diene copolymer, vinylated Close object, the weight ratio of diene is 1:1:8.

The second aspect of the present invention provides a kind of application of left and right waist as described above patch special glue in amenities.

The third aspect of the present invention provides a kind of preparation method of left and right waist patch special glue as described above, including walks as follows Suddenly, in a kettle, styrene-ethylene based compound-diene copolymer, tackifying resin, plasticising oil are mixed, heating melting, Stir 5-7h, discharge, sizing, it is cooling to get.

Specific embodiment

The detailed description for preferred implementation method of the invention below of participating in the election of and including embodiment this hair can be more easily to understand Bright content.Unless otherwise defined, all technologies used herein and scientific term have common with fields of the present invention The normally understood identical meaning of technical staff.When there is a conflict, the definition in this specification shall prevail.

As used herein term " by ... preparation " it is synonymous with "comprising".Term "comprising" used herein, " comprising ", " having ", " containing " or its any other deformation, it is intended that cover non-exclusionism includes.For example, the combination comprising listed elements Object, step, method, product or device are not necessarily limited to those elements, but may include not expressly listed other elements or Such composition, step, method, product or the intrinsic element of device.

Conjunction " Consists of " excludes any element that do not point out, step or component.If in claim, this Phrase will make claim closed, so that it is not included the material in addition to the material of those descriptions, but relative normal Except rule impurity.When being rather than immediately following after theme in the clause that phrase " Consists of " appears in claim main body, It is only limited to element described in the clause;Other elements are not excluded except the claim as a whole.

Equivalent, concentration or other values or parameter are excellent with range, preferred scope or a series of upper limit preferred values and lower limit When the Range Representation that choosing value limits, this should be understood as specifically disclosing by any range limit or preferred value and any range Any pairing of lower limit or preferred value is formed by all ranges, regardless of whether the range separately discloses.For example, when open When range " 1 to 5 ", described range should be interpreted as including range " 1 to 4 ", " 1 to 3 ", " 1 to 2 ", " 1 to 2 and 4 to 5 ", " 1 to 3 and 5 " etc..When numberical range is described herein, unless otherwise stated, otherwise the range is intended to include its end Value and all integers and score in the range.

Singular includes that plural number discusses object, unless the context clearly dictates otherwise." optional " or it is " any It is a kind of " refer to that the item described thereafter or event may or may not occur, and the description include situation that event occurs and The situation that event does not occur.

Approximate term in specification and claims is used to modify quantity, and it is specific to indicate that the present invention is not limited to this Quantity further includes the acceptable modified part without will lead to the change of dependency basis this function close with the quantity.Phase It answers, modifies a numerical value with " about ", " about " etc., mean that the present invention is not limited to the exact numericals.In some examples, approximate Term likely corresponds to the precision of the instrument of measurement numerical value.In present specification and claims, range limits can be with Combination and/or exchange, these ranges if not stated otherwise include all subranges contained therebetween.

The first aspect of the present invention provides a kind of left and right waist patch special glue, and preparing raw material includes: styrene-ethylene base Close object-diene copolymer, tackifying resin, plasticising oil.

In some embodiments, in parts by weight, preparing raw material includes: that styrene-ethylene based compound-diene is total 100 parts of polymers, 100 parts of tackifying resin, 50 parts of plasticising oil.

In some embodiments, the diene is conjugated diene.

In some embodiments, the tackifying resin is selected from hydrogenated petroleum resin and/or hydrogenation phenolic resin.

Plasticising oil is added in polymer, can increase its plasticity, improve processability, assigns product flexibility.Thermoplasticity There is interaction forces between linear macromolecule, and this physical force is from Van der Waals force (electrostatic force, induction force and color Dissipate power) and hydrogen bond, its size it is related with polymer architecture.Generally, the force ratio nonpolar molecule of polar molecule is big.Molecule Between active force not only make polymer that there is certain mechanical strength, but also many performances such as also affect its processing and forming.Heat The essence of plastic resin processing is exactly to pass through heating, increases the activity of polymer molecule, weakens active force therebetween, to make Have plasticity.But, intermolecular force strong for certain polarity is greatly and for the polymer of thermally labile, often It meets difficulty.The effect of plasticising oil is that the active force weakened between polymer molecule, to reduce softening temperature, melting temperature And glass transition temperature, reduce the viscosity of melt, increase its mobility, improves the processability and product and flexibility of polymer.

In some embodiments, the plasticising oil is selected from Dioctyl Glutaricate, didecyl glutarate, two isodecyl of glutaric acid Ester, two fourth 2-ethoxyethyl acetate of glutaric acid, two fourth oxygen ethoxy ethyl ester of glutaric acid, Di-n-butyl Adipate, diisobutyl adipate, adipic acid Two just own esters, dioctyl adipate or adipic acid two (2- ethylhexyl), diisooctyl adipate, dinonyl adipate, oneself two Sour dinonyl, diisodecyl adipate (DIDA), two fourth 2-ethoxyethyl acetate of adipic acid, adipic acid two (Butoxyethoxy second) ester, azelaic acid Two fourth 2-ethoxyethyl acetates, dibenzyl azelate, dicyclohexyl azelate, dimethyl sebacate, n-butyl sebacate, decanedioic acid two are different Propyl ester, dioctyl sebacate, Plexol 201, decanedioic acid di-sec-octyl, di-n-nonyl sebacate, two (butoxy of decanedioic acid Second) ester, decanedioic acid two (Butoxyethoxy second) ester, dibenzyl sebacate, diethyl sebacate, in dihexyl sebacate extremely Few one kind.

In some embodiments, the conjugated diene is selected from one of 1,3- octadiene, 2,4- octadiene.

No. CAS of 1,3- octadiene is 1002-33-1, and No. CAS of 2,4- octadienes is 13643-08-8.

In some embodiments, the vinyl compound in 1- vinyl imidazole, 2- vinylpyridine one Kind.

No. CAS of 1- vinyl imidazole is 1072-63-5, and No. CAS of 2- vinylpyridine is 100-69-6.

In some embodiments, styrene in the styrene-ethylene based compound-diene copolymer, vinylated Close object, the weight ratio of diene is 1:1:8.

The second aspect of the present invention provides a kind of application of left and right waist as described above patch special glue in amenities.

The third aspect of the present invention provides a kind of preparation method of left and right waist patch special glue as described above, including walks as follows Suddenly, in a kettle, styrene-ethylene based compound-diene copolymer, tackifying resin, plasticising oil are mixed, heating melting, Stir 5-7h, discharge, sizing, it is cooling to get.

Left and right waist provided by the invention pastes special glue, peel strength with higher, styrene-ethylene based compound-bis- Main body of the alkene copolymer as adhesive improves the water resistance of adhesive, the especially performance of salt tolerant aqueous corrosion, is being used for It is not easily to fall off when in amenities.Left and right waist patch special glue provided by the invention has good cryogenic property simultaneously, in temperature The case where degumming and cracking will not occur in storage and use under the conditions of lower.

The present invention is further explained combined with specific embodiments below.

Embodiment 1

Left and right waist pastes special glue, and in parts by weight, preparing raw material includes: styrene-ethylene based compound-diene copolymerization 100 parts of object, 100 parts of hydrogenated petroleum resin, 30 parts of diisodecyl glutarate, 20 parts of Plexol 201.

The preparation method of the styrene-ethylene based compound-diene copolymer is, by styrene, 1- vinyl imidazole, The mixing of 1,3- octadiene, is heated to 150 DEG C, cumyl peroxide is then added, persistently stir 15h, discharging to get.It is described Styrene, 1- vinyl imidazole, 1,3- octadiene, cumyl peroxide weight ratio be 1:1:8:0.04.

Preparation method includes the following steps, in a kettle, by styrene-ethylene based compound-diene copolymer 100 Part, 100 parts of hydrogenated petroleum resin, 30 parts of diisodecyl glutarate, 20 parts of Plexol 201 mixing, heating melting, stirring 6h discharges, sizing, it is cooling to get.

Embodiment 2

Left and right waist pastes special glue, and in parts by weight, preparing raw material includes: styrene-ethylene based compound-diene copolymerization 100 parts of object, 100 parts of hydrogenated petroleum resin, 30 parts of diisodecyl glutarate, 20 parts of Plexol 201.

The preparation method of the styrene-ethylene based compound-diene copolymer is, by styrene, 1- vinyl imidazole, The mixing of 2,4- octadienes, is heated to 150 DEG C, cumyl peroxide is then added, persistently stir 15h, discharging to get.It is described Styrene, 1- vinyl imidazole, 2,4- octadiene, cumyl peroxide weight ratio be 1:1:8:0.04.

Preparation method includes the following steps, in a kettle, by styrene-ethylene based compound-diene copolymer 100 Part, 100 parts of hydrogenated petroleum resin, 30 parts of diisodecyl glutarate, 20 parts of Plexol 201 mixing, heating melting, stirring 6h discharges, sizing, it is cooling to get.

Embodiment 3

Left and right waist pastes special glue, and in parts by weight, preparing raw material includes: styrene-ethylene based compound-diene copolymerization 100 parts of object, 100 parts of hydrogenated petroleum resin, 30 parts of diisodecyl glutarate, 20 parts of Plexol 201.

The preparation method of the styrene-ethylene based compound-diene copolymer is, by styrene, 2- vinylpyridine, The mixing of 1,3- octadiene, is heated to 150 DEG C, cumyl peroxide is then added, persistently stir 15h, discharging to get.It is described Styrene, 2- vinylpyridine, 1,3- octadiene, cumyl peroxide weight ratio be 1:1:8:0.04.

Preparation method includes the following steps, in a kettle, by styrene-ethylene based compound-diene copolymer 100 Part, 100 parts of hydrogenated petroleum resin, 30 parts of diisodecyl glutarate, 20 parts of Plexol 201 mixing, heating melting, stirring 6h discharges, sizing, it is cooling to get.

Embodiment 4

Adhesive, in parts by weight, prepare raw material include: styrene-ethylene based compound -00 part of monoene copolymer 1, 100 parts of hydrogenated petroleum resin, 30 parts of diisodecyl glutarate, 20 parts of Plexol 201.

The preparation method of the styrene-ethylene based compound-monoene copolymer is, by styrene, 1- vinyl imidazole, The mixing of 2- octene, is heated to 150 DEG C, cumyl peroxide is then added, persistently stir 15h, discharging to get.The benzene second Alkene, 1- vinyl imidazole, 2- octene, cumyl peroxide weight ratio be 1:1:8:0.04.

Preparation method includes the following steps, in a kettle, by styrene-ethylene based compound-monoene copolymer 1 00 Part, 100 parts of hydrogenated petroleum resin, 30 parts of diisodecyl glutarate, 20 parts of Plexol 201 mixing, heating melting, stirring 6h discharges, sizing, it is cooling to get.

Embodiment 5

Adhesive, in parts by weight, prepare raw material include: styrene-ethylene based compound -100 parts of diene copolymer, 100 parts of hydrogenated petroleum resin, 30 parts of diisodecyl glutarate, 20 parts of Plexol 201.

The preparation method of the styrene-ethylene based compound-diene copolymer is, by styrene, 1- vinyl imidazole, The mixing of 1,3- octadiene, is heated to 150 DEG C, cumyl peroxide is then added, persistently stir 15h, discharging to get.It is described Styrene, 1- vinyl imidazole, 1,3- octadiene, cumyl peroxide weight ratio be 1:0.1:8:0.04.

Preparation method includes the following steps, in a kettle, by styrene-ethylene based compound-diene copolymer 100 Part, 100 parts of hydrogenated petroleum resin, 30 parts of diisodecyl glutarate, 20 parts of Plexol 201 mixing, heating melting, stirring 6h discharges, sizing, it is cooling to get.

Embodiment 6

Adhesive, in parts by weight, preparing raw material includes: 100 parts of styrene-diene copolymer, hydrogenated petroleum resin 100 parts, 30 parts of diisodecyl glutarate, 20 parts of Plexol 201.

The preparation method of the styrene-diene copolymer is to mix styrene, 1,3- octadiene, be heated to 150 DEG C, cumyl peroxide is then added, persistently stirs 15h, discharging to get.The styrene, 1,3- octadiene, peroxidating The weight ratio of diisopropylbenzene (DIPB) is 1:4:0.02.

Preparation method includes the following steps, in a kettle, by 100 parts of styrene-diene copolymer, non-hydrogenated petroleum tree 100 parts of rouge, 30 parts of diisodecyl glutarate, 20 parts of Plexol 201 mixing, heating melting stir 6h, discharge, sizing, It is cooling to get.

Test method

1. water resistance test

By embodiment 1-6 in nonwoven cloth proofing, rubberised layer measures peel strength with a thickness of 2mm, according to GB/T 2791, It is denoted as A0, unit N/cm.Then the non-woven fabrics for being pasted with embodiment 1-6 is washed, washing times are 90 times, then measure stripping From intensity, it is denoted as A1, unit N/cm.

2. cryogenic property is tested

By embodiment 1-6 in nonwoven cloth proofing, then rubberised layer stores 90 days with a thickness of 2mm in -18 DEG C, then Peel strength is measured, A is denoted as2, unit N/cm.

Test result is listed in the table below.

Example above-mentioned is merely illustrative, for explaining some features of this patent.The attached claims are intended to The range as wide as possible being contemplated that is sought, and embodiments as presented herein is only the combination according to all possible embodiment Selection embodiment explanation.Therefore, the purpose of applicant is that the attached claims are not illustrated feature of the invention Exemplary selectional restriction.And the progress in science and technology will be formed language express it is inaccurate due to and it is not current The possible equivalent considered or son replacement, and these variations should also be interpreted to be wanted by appended right in the conceived case Ask covering.

Claims (8)

1. a kind of left and right waist pastes special glue, which is characterized in that it includes: that styrene-ethylene based compound-diene is total that it, which prepares raw material, 100 parts of polymers, 100 parts of tackifying resin, 50 parts of plasticising oil, the vinyl compound are selected from 1- vinyl imidazole, 2- vinyl One of pyridine.
2. left and right waist as described in claim 1 pastes special glue, which is characterized in that the diene is conjugated diene.
3. left and right waist as described in claim 1 pastes special glue, which is characterized in that the tackifying resin is selected from hydrogenated petroleum resin And/or hydrogenation phenolic resin.
4. left and right waist as described in claim 1 pastes special glue, which is characterized in that the plasticising oil be selected from Dioctyl Glutaricate, Didecyl glutarate, diisodecyl glutarate, two fourth 2-ethoxyethyl acetate of glutaric acid, two fourth oxygen ethoxy ethyl ester of glutaric acid, adipic acid-di-n Butyl ester, diisobutyl adipate, di-n-hexyl adipate, dioctyl adipate or adipic acid two (2- ethylhexyl), adipic acid Di-isooctyl, dinonyl adipate, diisononyl adipate, diisodecyl adipate (DIDA), two fourth 2-ethoxyethyl acetate of adipic acid, adipic acid two (Butoxyethoxy second) ester, two fourth 2-ethoxyethyl acetate of azelaic acid, dibenzyl azelate, dicyclohexyl azelate, dimethyl sebacate, N-butyl sebacate, diisopropyl sebacate, dioctyl sebacate, Plexol 201, decanedioic acid di-sec-octyl, the last of the ten Heavenly stems two Sour two nonyl esters, decanedioic acid two (butoxy second) ester, decanedioic acid two (Butoxyethoxy second) ester, dibenzyl sebacate, decanedioic acid At least one of diethylester, dihexyl sebacate.
5. left and right waist as claimed in claim 2 pastes special glue, which is characterized in that the conjugated diene be selected from 1,3- octadiene, One of 2,4- octadiene.
6. left and right waist as described in claim 1 pastes special glue, which is characterized in that the styrene-ethylene based compound-diene Styrene in copolymer, vinyl compound, diene weight ratio be 1:1:8.
7. a kind of left and right waist as described in any one of claim 1-6 claim pastes special glue answering in amenities With.
8. a kind of preparation method of the left and right waist patch special glue as described in any one of claim 1-6 claim, including such as Lower step mixes styrene-ethylene based compound-diene copolymer, tackifying resin, plasticising oil, heating is molten in a kettle Melt, stir 5-7h, discharge, sizing, it is cooling to get.
CN201810266274.3A 2018-03-28 2018-03-28 A kind of left and right waist patch special glue and preparation method thereof CN108410399B (en)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1664043A (en) * 2005-02-25 2005-09-07 苏州市丛岭胶粘剂有限公司 Sealing adhesive
CN102702990A (en) * 2012-05-31 2012-10-03 苏州联科合成材料有限公司 Removable hot-melt pressure-sensitive adhesive tape for temporary fixation
CN103540281A (en) * 2013-10-21 2014-01-29 广东东方树脂有限公司 Quickly-cured rubber-type hot melt adhesive
CN107603538A (en) * 2017-09-25 2018-01-19 常州中翔科技有限公司 A kind of epoxidized block copolymer adhesive and preparation method thereof

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6379791B1 (en) * 2000-02-08 2002-04-30 3M Innovative Properties Company Compatibilized pressure-sensitive adhesives

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1664043A (en) * 2005-02-25 2005-09-07 苏州市丛岭胶粘剂有限公司 Sealing adhesive
CN102702990A (en) * 2012-05-31 2012-10-03 苏州联科合成材料有限公司 Removable hot-melt pressure-sensitive adhesive tape for temporary fixation
CN103540281A (en) * 2013-10-21 2014-01-29 广东东方树脂有限公司 Quickly-cured rubber-type hot melt adhesive
CN107603538A (en) * 2017-09-25 2018-01-19 常州中翔科技有限公司 A kind of epoxidized block copolymer adhesive and preparation method thereof

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