CN108404700A - A kind of gas-lifting type rotation circulation efficient circulation mixing arrangement of no inner draft tube - Google Patents

A kind of gas-lifting type rotation circulation efficient circulation mixing arrangement of no inner draft tube Download PDF

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Publication number
CN108404700A
CN108404700A CN201810207589.0A CN201810207589A CN108404700A CN 108404700 A CN108404700 A CN 108404700A CN 201810207589 A CN201810207589 A CN 201810207589A CN 108404700 A CN108404700 A CN 108404700A
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liquid
gas
container
fluid
nozzle
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CN108404700B (en
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尹应武
黄文峰
李大川
任毅华
尹政清
潘小勇
吐松
叶李艺
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Beijing Yingli Ecological Technology Co ltd
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TH-UNIS INSIGHT Co Ltd
Xiamen University
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/20Jet mixers, i.e. mixers using high-speed fluid streams
    • B01F25/21Jet mixers, i.e. mixers using high-speed fluid streams with submerged injectors, e.g. nozzles, for injecting high-pressure jets into a large volume or into mixing chambers
    • B01F25/212Jet mixers, i.e. mixers using high-speed fluid streams with submerged injectors, e.g. nozzles, for injecting high-pressure jets into a large volume or into mixing chambers the injectors being movable, e.g. rotating
    • B01F25/2122Rotating during jetting
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00Other mixers; Mixing plants; Combinations of mixers
    • B01F33/40Mixers using gas or liquid agitation, e.g. with air supply tubes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • B01J19/2455Stationary reactors without moving elements inside provoking a loop type movement of the reactants
    • B01J19/246Stationary reactors without moving elements inside provoking a loop type movement of the reactants internally, i.e. the mixture circulating inside the vessel such that the upward stream is separated physically from the downward stream(s)

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)

Abstract

The present invention provides a kind of gas-lifting types of no inner draft tube to revolve circulation efficient circulation mixing arrangement, it utilizes the diversion component for including stator and rotor, fluid injector is provided on rotor, fluid injector is connect with liquid guide flow pipe, liquid guide flow pipe is set to the inside of rotor and stator, gas vent is additionally provided on diversion component, gas vent is connected to gas diversion tube, and provides the mixing arrangement prepared comprising diversion component.Device pushes rotary nozzle rotating-spray liquid material to strengthen radial material and directly mixes using circulating liquid, reaction or heating or working gas are introduced near nozzle simultaneously, the fully dispersed liquid material of liquid stream and gas sprayed by rotation, simultaneously upward circulation is generated by lift of gas, strengthen axial material to be sufficiently mixed, overcomes that traditional guide shell mixing arrangement is complicated, is easy fouling, the shortcomings that outside sandwich is difficult to clean off.

Description

一种无内导流筒的气升式旋环流高效循环混合装置An air-lift high-efficiency circulation mixing device with swirling flow without inner guide tube

技术领域technical field

本发明提供了一种通过调节气液流量有效提高混合的新型旋环流式高效混合装置。The invention provides a novel swirling flow type high-efficiency mixing device which can effectively improve mixing by adjusting the gas-liquid flow rate.

背景技术Background technique

在化工、制药、水处理、冶金和食品等行业的产品生产过程中,经常涉及有混合,在传统的混合装置中,需要电动机和传动装置来驱动庞大的搅拌桨,搅拌器电机一般安装在釜体的顶部,通常采用立式布置,电动机的转速需通过减速机调节搅拌转速,再通过联轴器带动搅拌轴和搅拌桨叶转动。这种机械搅拌混合装置存在体积庞大、造价高、能耗高、放大效应显著、安装空间高和混合效果不佳等一系列缺陷。In the production process of chemical, pharmaceutical, water treatment, metallurgical and food industries, mixing is often involved. In traditional mixing devices, electric motors and transmissions are needed to drive huge stirring paddles. The stirring motors are generally installed in the kettle. The top of the body is usually arranged vertically. The speed of the motor needs to be adjusted through the reducer to adjust the stirring speed, and then the stirring shaft and the stirring blades are driven to rotate through the coupling. This mechanical stirring and mixing device has a series of defects such as bulky, high cost, high energy consumption, significant amplification effect, high installation space and poor mixing effect.

气升塔式混合器是内装圆形导流筒从筒内或筒外部通入气体产生内环流或外环流推动气液充分循环混合的新一代高效节能装备,它很好利用了气体的升力和内外环流区内的密度差实现了无搅拌的有效轴向混合和快速循环。它内部的导流筒将上升和下降流体很好地进行了分隔,但这种内装导流筒的塔式装置存在结构复杂、塔内壁与导流筒外壁间空间狭窄、易结垢难清洗检修、可能造成死区、需要较大的高径比、液位低于导流筒会导致无法环流而必须保持最低液位、对固液体系不适用等问题,需要进一步改进。The air-lift tower mixer is a new generation of high-efficiency and energy-saving equipment with a circular guide tube inside or outside the tube to generate internal circulation or external circulation to promote the full circulation and mixing of gas and liquid. It makes good use of the lift of the gas. The density difference in the inner and outer circulation zones enables effective axial mixing and rapid circulation without agitation. Its internal guide tube separates the ascending and descending fluids well, but this tower device with a built-in guide tube has a complex structure, narrow space between the inner wall of the tower and the outer wall of the guide tube, and is prone to fouling and difficult to clean and repair. , may cause a dead zone, require a large height-to-diameter ratio, and the liquid level is lower than the guide tube, which will lead to the inability to circulate and must maintain the minimum liquid level, which is not suitable for solid-liquid systems, etc., which need further improvement.

本发明针对传统带机械搅拌混合器和气升式反应器的不足,吸取了本发明团队前期利用旋转喷头作为搅拌动力源通过射流和旋转带动物料直接混合的方式强化径向混合的基础上,进一步集成了三种典型混合装置的优势,特别是在旋流混合基础上通过引进气体产生的升力和旋转喷射对气泡的分散作用,同时强化了相间、径向和轴向的混合,发明了一种无内导流筒的旋环流混合型高效新型通用混合装置。装置大大简化了现有的机械搅拌和气升塔式装置结构,克服了传统混合设备复杂、造价高、容易结垢等缺点,开创了利用径向、轴向和物料射流及多相体系间界面分散等多种手段进行混合过程强化的新型高效节能装备,这种以气体和液体协同推动的物料动力型混合模式,可以显著改善放大效应、完全替代传统机械搅拌混合器,同时优化了传统的气升塔式混合器及旋流式混合器,在釜和塔式容器中均可取得很好的混合效果。本发明对于改善非均相体系间物料混合与传质,特别是在生物发酵及污水处理中应用可以很好提升增氧效果,大幅降低爆气能耗。The present invention aims at the deficiencies of the traditional mixer with mechanical agitation and the airlift reactor, and absorbs the fact that the team of the present invention used the rotary nozzle as the stirring power source in the early stage to strengthen the radial mixing by jet flow and rotation to drive the material to directly mix, and further integrates Based on the advantages of three typical mixing devices, especially on the basis of swirl mixing, the lifting force generated by the introduction of gas and the dispersing effect of the swirling jet on the bubbles are strengthened, and the mixing between phases, radial and axial directions is strengthened, and a non-toxic mixing device is invented. The swirling flow mixing type high-efficiency new general-purpose mixing device of the inner guide tube. The device greatly simplifies the structure of the existing mechanical stirring and air-lift tower devices, overcomes the shortcomings of traditional mixing equipment such as complexity, high cost, and easy fouling, and creates the use of radial, axial and material jets and interface dispersion between multi-phase systems. It is a new type of high-efficiency and energy-saving equipment that strengthens the mixing process by various means. This material dynamic mixing mode, which is jointly promoted by gas and liquid, can significantly improve the amplification effect, completely replace the traditional mechanical stirring mixer, and optimize the traditional gas lift. Tower mixers and swirl mixers can achieve good mixing effects in kettles and tower containers. The invention can improve the mixing and mass transfer of materials between heterogeneous systems, especially in biological fermentation and sewage treatment, which can improve the oxygenation effect and greatly reduce the energy consumption of gas explosion.

发明内容Contents of the invention

本发明主要针对现有机械混合装置结构复杂、对混合贡献小的周向运动耗能高、放大效应显著、混合效果差、物料量受到限制及气升塔式反应器内导流筒造成的一系列加工和使用等问题,在前期研发成果基础上,创新了一种结构更简单、混合效果更好、没有高径比限制和投料液位限制、放大效应小、装置结构更简单和投资运行费用更低的新型高效节能通用型混合器。通过转速、气或液体流量、压力的简单调节,可开发出适合各种体系的混合装置和工艺条件。这种依靠带压物料直接喷射和引入气体强化混合的旋环流混合体系,可有效促进对流、涡流及分子扩散。The present invention mainly aims at the complex structure of the existing mechanical mixing device, the high energy consumption of the circumferential movement which contributes little to the mixing, the significant amplification effect, the poor mixing effect, the limited amount of material and the problems caused by the guide tube in the air-lift tower reactor. Based on the previous research and development results, we have innovated a series of processing and use problems, with a simpler structure, better mixing effect, no height-to-diameter ratio restrictions and feeding liquid level restrictions, small amplification effect, simpler device structure and lower investment and operation costs. Lower new energy-efficient and universal mixer. Through simple adjustment of speed, gas or liquid flow, and pressure, mixing devices and process conditions suitable for various systems can be developed. This cyclone flow mixing system, which relies on direct injection of pressurized materials and enhanced mixing by introducing gas, can effectively promote convection, vortex and molecular diffusion.

为解决上述技术问题,本发明提供了一种导流部件,所述导流部件包括定子和转子,转子上设置有液体喷嘴,液体喷嘴与液体导流管连接,液体导流管设置于转子和定子的内部,在导流部件上还设置有气体出口,气体出口与气体导流管连通。In order to solve the above-mentioned technical problems, the present invention provides a flow guide component, the flow guide component includes a stator and a rotor, the rotor is provided with a liquid nozzle, the liquid nozzle is connected to the liquid guide pipe, and the liquid guide pipe is arranged between the rotor and the rotor. Inside the stator, a gas outlet is also provided on the guide part, and the gas outlet communicates with the gas guide pipe.

优选的,上述导流部件中,所述导流部件中的气体出口设置于液体喷嘴的上方或下方,或者,气体出口与液体喷嘴并排设置,或者,气体出口与液体喷嘴共用,或者,气体出口位于液体喷嘴上方和液体喷嘴周边,或者,气体出口位于液体喷嘴上方和下方,或者,气体出口位于液体喷嘴的周边和下方。Preferably, in the above-mentioned flow guide member, the gas outlet in the flow guide member is arranged above or below the liquid nozzle, or the gas outlet is arranged side by side with the liquid nozzle, or the gas outlet is shared with the liquid nozzle, or the gas outlet The gas outlets are located above and below the liquid nozzle, or the gas outlets are located above and below the liquid nozzle, or the gas outlets are located at the periphery and below the liquid nozzle.

优选的,上述导流部件中,所述液体喷嘴为一个或多个,喷嘴为扇形喷嘴、U型广角喷嘴、V型广角喷嘴、空化喷嘴或直接开孔或开缝的喷嘴。Preferably, in the above-mentioned flow guide member, there are one or more liquid nozzles, and the nozzles are fan-shaped nozzles, U-shaped wide-angle nozzles, V-shaped wide-angle nozzles, cavitation nozzles, or nozzles that directly open holes or slits.

优选的,上述导流部件中,所述定子位于转子的上方或定子位于转子的下方。Preferably, in the above air guiding component, the stator is located above the rotor or the stator is located below the rotor.

优选的,上述导流部件中,所述气体出口为环形出气口或孔状出气口,当气体出口为孔状出气口时,孔状出气口为一个或多个。Preferably, in the above-mentioned flow guide member, the gas outlet is an annular gas outlet or a hole-shaped gas outlet, and when the gas outlet is a hole-shaped gas outlet, there are one or more hole-shaped gas outlets.

优选的,上述导流部件中,所述液体喷嘴喷射液体的方向偏离转子轴心向液体喷嘴中心点的直线方向,液体喷嘴喷射的液体的反作用力作用在喷嘴上,推动转子旋转。Preferably, in the above-mentioned flow guiding member, the direction in which the liquid sprayed by the liquid nozzle deviates from the straight line direction from the rotor axis to the center of the liquid nozzle, the reaction force of the liquid sprayed by the liquid nozzle acts on the nozzle to push the rotor to rotate.

本发明还提供一种无内导流筒的气升式旋环流高效循环混合装置,其特征在于装置包括容器和上述导流部件,导流部件位于容器内,导流部件的液体导流管与液态流体管路连通,导流部件的气体导流管和气态流体管路连通。The present invention also provides an air-lift high-efficiency circulation mixing device for swirl flow without an inner guide tube, which is characterized in that the device includes a container and the above-mentioned guide part, the guide part is located in the container, and the liquid guide pipe of the guide part is connected to the The liquid fluid pipeline is connected, and the gas guide tube of the flow guide part is connected with the gaseous fluid pipeline.

优选的,上述气升式旋环流高效循环混合装置中,所述导流部件为多个,每个导流部件均通过液体导流管和气体导流管连接液态流体管路和气态流体管路。Preferably, in the above-mentioned air-lift swirling flow high-efficiency circulation mixing device, there are multiple guide parts, and each guide part connects the liquid fluid pipeline and the gas fluid pipeline through a liquid guide tube and a gas guide tube .

优选的,上述气升式旋环流高效循环混合装置中,所述容器为釜或塔或池或罐或需要处理的自然或人工水体。Preferably, in the above-mentioned air-lift cyclone high-efficiency circulation mixing device, the container is a kettle or a tower or a pool or a tank or a natural or artificial water body that needs to be treated.

优选的,上述气升式旋环流高效循环混合装置中,所述液态流体管路内的液体压力高于分散体系的压力,所述气态流体管路内气体的压力足以克服液体静压差。Preferably, in the air-lift high-efficiency cyclone circulation mixing device, the liquid pressure in the liquid fluid pipeline is higher than the pressure of the dispersion system, and the gas pressure in the gaseous fluid pipeline is sufficient to overcome the static pressure difference of the liquid.

优选的,上述气升式旋环流高效循环混合装置中,所述液态流体管路与液体加压装置连接,所述气态流体管路与气体加压装置连接。Preferably, in the above-mentioned air-lift high-efficiency cyclone mixing device, the liquid fluid pipeline is connected to the liquid pressurization device, and the gaseous fluid pipeline is connected to the gas pressurization device.

优选的,上述气升式旋环流高效循环混合装置中,所述液体加压装置为循环加压液体泵、循环气体压缩机,或者是具有高液位的容器或者具有高压气体的液体容器。Preferably, in the above-mentioned air-lift swirling flow high-efficiency circulation mixing device, the liquid pressurization device is a circulating pressurized liquid pump, a circulating gas compressor, or a container with a high liquid level or a liquid container with high-pressure gas.

优选的,上述气升式旋环流高效循环混合装置中,所述气体加压装置为空气压缩机,或者是具有高压气体的容器。Preferably, in the above-mentioned air-lift swirling flow high-efficiency circulation mixing device, the gas pressurization device is an air compressor, or a container with high-pressure gas.

优选的,上述气升式旋环流高效循环混合装置中,所述进入液体加压装置的液体来源于容器内的液体或者来源于非容器内液体的其他液体。Preferably, in the above-mentioned air-lift high-efficiency swirling circulation mixing device, the liquid entering the liquid pressurization device comes from the liquid in the container or from other liquids other than the liquid in the container.

优选的,上述气升式旋环流高效循环混合装置中,所述进入气体加压装置的气体来源于容器内的循环气体或者是来源于非容器内气体的其他气体。Preferably, in the above-mentioned air-lift high-efficiency cyclone circulation mixing device, the gas entering the gas pressurization device comes from the circulating gas in the container or other gases other than the gas in the container.

优选的,上述气升式旋环流高效循环混合装置中,所述容器为多个,每个容器中设置一个或多个导流部件,每个容器中的导流部件与液态流体管路和气态流体管路连接。Preferably, in the above-mentioned air-lift swirling flow high-efficiency circulation mixing device, there are multiple containers, and one or more flow guiding parts are arranged in each container, and the flow guiding parts in each container are connected with the liquid fluid pipeline and the gaseous state. Fluid line connections.

优选的,上述气升式旋环流高效循环混合装置中,所述每个容器为封闭容器,每个封闭容器通过设置在容器上部的气体管路将气体输送入气体加压装置,每个容器通过设置于容器底部的液体管路将液体输送入液体加压装置。Preferably, in the above-mentioned air-lift swirling flow high-efficiency circulation mixing device, each of the containers is a closed container, and each closed container sends gas into the gas pressurization device through a gas pipeline arranged on the upper part of the container, and each container passes The liquid pipeline arranged at the bottom of the container transports the liquid into the liquid pressurizing device.

优选的,上述气升式旋环流高效循环混合装置中,所述装置还包括加热装置或者是冷却装置,所述加热装置或冷却设置于容器的外部或内部,对容器进行加热和冷却,或者是对将要进入液体加压装置的液体进行加热或冷却,或者对进入气体压缩装置的气体进行加热或者是冷却。Preferably, in the above-mentioned air-lift swirling flow high-efficiency circulation mixing device, the device also includes a heating device or a cooling device, and the heating device or cooling device is arranged on the outside or inside of the container to heat and cool the container, or To heat or cool a liquid entering a liquid pressurization device, or to heat or cool a gas entering a gas compression device.

优选的,上述气升式旋环流高效循环混合装置中,所述装置还包括检测装置,所述检测装置包括体系内液体或和气体检测器中的一种或多种。Preferably, in the above-mentioned air-lift high-efficiency cyclone circulation mixing device, the device further includes a detection device, and the detection device includes one or more of liquid or gas detectors in the system.

优选的,上述气升式旋环流高效循环混合装置中,所述装置还包括控制装置,所述控制装置与液体流体管路阀门、气态流体管路阀门、容器的气体排放出口阀门、容器的液体排放出口阀门中的一个或多个连接。Preferably, in the above-mentioned air-lift swirling flow high-efficiency circulation mixing device, the device also includes a control device, which is connected with the liquid fluid pipeline valve, the gaseous fluid pipeline valve, the gas discharge outlet valve of the container, and the liquid of the container. One or more connections in the discharge outlet valve.

本发明还提供了一种应用上述气升式旋环流高效循环混合装置进行溶液混合或气液混合的方法,所述方法包括如下步骤:The present invention also provides a method for mixing solutions or mixing gas and liquid by using the above-mentioned air-lift high-efficiency circulation mixing device, and the method includes the following steps:

步骤1)将液体A加入到合适的容器中,使得液体平面高于液体喷嘴和气体出口,将液体B进行加压输入到液态流体管路;Step 1) Add liquid A to a suitable container so that the liquid level is higher than the liquid nozzle and the gas outlet, and pressurize liquid B into the liquid fluid pipeline;

步骤2)将液体B通过液体喷嘴喷射入容器中液体A的液面以下,将气体压缩然后通过气态流体管路输送到气体出口,将气体喷射到容器中的液体A的液面以下。Step 2) The liquid B is sprayed into the container below the liquid level of the liquid A through the liquid nozzle, the gas is compressed and then transported to the gas outlet through the gaseous fluid pipeline, and the gas is sprayed below the liquid level of the liquid A in the container.

优选的,上述方法中,所述液体A和液体B为相同液体或者是不同液体。Preferably, in the above method, the liquid A and the liquid B are the same liquid or different liquids.

优选的,上述方法中,所述气体喷射到容器中的液体A的液面下旋转喷头附近。Preferably, in the above method, the gas is sprayed to the vicinity of the rotating spray head below the liquid surface of the liquid A in the container.

优选的,上述方法中,所述导入的气体可以是需要通入的反应气体或加热蒸汽或作为工作介质的空气或氮气或密闭体系循环压缩的工作介质。Preferably, in the above method, the introduced gas may be the reaction gas or heating steam that needs to be introduced, or air or nitrogen as the working medium, or the working medium compressed by the closed system cycle.

优选的,上述方法中,所述喷头旋转速度在100~300转时效果最佳。Preferably, in the above method, the rotation speed of the spray head is 100-300 rotations, and the effect is the best.

优选的,上述方法中,所述液体喷嘴产生的液旋流直径为容器直径的三分之一左右时效果最佳,气体和液体每小时循环或通入量为混合液体物料的4~5倍时效果最佳。在循环气体体积超过液体体积一半时即可产生环流。Preferably, in the above method, the effect is best when the diameter of the liquid swirl generated by the liquid nozzle is about one-third of the diameter of the container, and the gas and liquid are circulated or introduced per hour at 4 to 5 times that of the mixed liquid material works best. Circulation can be generated when the circulating gas volume exceeds half the liquid volume.

本发明具有如下优点:The present invention has the following advantages:

(1)本发明的导流部件实现了液体和气体的混合喷射,既实现了气体充分搅拌液体,同时也实现了气体作为反应介质能够充分地与液体混合,同时液体混合的方式提高了反应溶液的搅拌速度,而且液体的加入实现了液体喷嘴推动自身旋转,气体出口和液体出口的设置实现了可以以所需要的气液混合方式进行混合。提高了气液混合效率,实现气体反应介质或气体反应介质不仅能够作为反应原料,还能够作为反应体系搅拌的工具。(1) The flow guide part of the present invention realizes the mixed injection of liquid and gas, which not only realizes that the gas can fully stir the liquid, but also realizes that the gas can be fully mixed with the liquid as a reaction medium, and the way of liquid mixing improves the reaction solution. The stirring speed is high, and the addition of the liquid realizes the liquid nozzle to push itself to rotate, and the setting of the gas outlet and the liquid outlet realizes the mixing in the required gas-liquid mixing mode. The gas-liquid mixing efficiency is improved, and the gas reaction medium or the gas reaction medium can not only be used as a reaction raw material, but also can be used as a tool for stirring the reaction system.

(2)本发明借助带压流体从转子液体喷嘴喷出时的射流和动力喷嘴产生的反作用力推动喷头旋转,以物料直接混合的方式提供径向混合和物料旋转混合动能,向外喷射旋转的液流同时将通入的气体分散和向周边推送,形成中心气液均匀混合区,气体向上的升力可强化轴向混合力和物流的环流,产生类似电炉“烧开水”沸腾状态的内循环。这种持续喷入的旋转液流和同时通入气体的混合模式不但强化了径向混合和扩散,而且有效促进了气体的分散和向周边旋转扩散。通过气液压力和流量的调节,可以形成高效旋环流体系,大大强化对流、涡流及分子扩散,可适应各种实际体系的混合。(2) The present invention pushes the nozzle to rotate by means of the jet flow and the reaction force produced by the power nozzle when the pressurized fluid is ejected from the rotor liquid nozzle, and provides radial mixing and material rotation mixing kinetic energy in the form of direct mixing of materials, and sprays and rotates outwards. At the same time, the liquid flow disperses and pushes the incoming gas to the periphery to form a central gas-liquid uniform mixing zone. The upward lift of the gas can strengthen the axial mixing force and the circulation of the material flow, creating an internal circulation similar to the boiling state of "boiling water" in an electric furnace. The mixing mode of continuously injecting rotating liquid flow and feeding gas not only strengthens the radial mixing and diffusion, but also effectively promotes the dispersion of gas and the rotating diffusion to the periphery. Through the adjustment of gas-liquid pressure and flow rate, a high-efficiency cyclone flow system can be formed, which greatly strengthens convection, eddy current and molecular diffusion, and can adapt to the mixing of various actual systems.

(3)新装置对均匀曝气和增加气体分散性和溶解度非常有效,无论是否存在导流筒都能够实现反应体系的旋环流体的高效运转,而且,即使在无需导流筒的情况下也可形成更高的旋环流体系,很好克服了传统气升塔式混合装置的不足。(3) The new device is very effective for uniform aeration and increasing gas dispersion and solubility, regardless of whether there is a draft tube, it can realize the efficient operation of the swirling fluid of the reaction system, and even without a draft tube It can form a higher cyclone flow system, which overcomes the shortcomings of the traditional air-lift tower mixing device.

(4)新装置借助体系输入或循环物料的动能产生喷射及旋流场强制形成射流和漩涡流,可强化传质传热。(4) The new device uses the kinetic energy of system input or circulating materials to generate jets and swirl fields to form jets and vortex flows, which can enhance mass and heat transfer.

(5)该新型混合模式可以广泛应用,开发的新型装置可大可小,可高可矮,物料可多可少、可串联或并联,可一泵多套,可开放可密闭,釜、塔、池、槽、罐等容器或人工或自然水体都可因地制宜改造。是结构简单、适应各种空间、混合分散效果好的新一代高效节能混合装备系统。在气相、液相、气液、气固两相和气液固三相体系中及混合、反应及分离过程中可以广泛应用。(5) The new mixing mode can be widely used. The new device developed can be large or small, high or short, with more or less materials, can be connected in series or in parallel, can have multiple sets of one pump, can be opened or sealed, kettles, towers Containers or artificial or natural water bodies such as pools, tanks, tanks, etc. can be transformed according to local conditions. It is a new generation of high-efficiency energy-saving hybrid equipment system with simple structure, adaptable to various spaces, and good mixing and dispersing effects. It can be widely used in gas phase, liquid phase, gas-liquid, gas-solid two-phase and gas-liquid-solid three-phase system and in the process of mixing, reaction and separation.

附图说明Description of drawings

图1为本发明第一种实施方式提供旋流混合装置的结构示意图;Fig. 1 is a schematic structural view of a swirl mixing device provided by a first embodiment of the present invention;

图2为本发明第二种实施方式提供旋流混合装置的结构示意图;Fig. 2 is a schematic structural diagram of a swirl mixing device provided in a second embodiment of the present invention;

图3为本发明第三种实施方式提供旋流混合装置的结构示意图;FIG. 3 is a schematic structural view of a swirl mixing device provided in a third embodiment of the present invention;

图4为本发明第四种实施方式提供旋流混合装置的结构示意图;Fig. 4 is a schematic structural diagram of a swirl mixing device provided in a fourth embodiment of the present invention;

图5为本发明实施方式提供的混合装置中的导流部件结构示意图;Fig. 5 is a schematic structural diagram of a flow guide member in a mixing device according to an embodiment of the present invention;

图6为本发明实施方式提供的旋流混合装置的混合原理示意图;6 is a schematic diagram of the mixing principle of the swirl mixing device provided by the embodiment of the present invention;

图7为本发明实施方式提供的旋流混合装置中,不同鼓泡直径下混合效果对比图;Fig. 7 is a comparison diagram of mixing effects under different bubbling diameters in the swirl mixing device provided by the embodiment of the present invention;

图8为本发明实施方式提供的旋流混合装置中,不同气体流量下混合效果对比图;Fig. 8 is a comparison diagram of mixing effects under different gas flow rates in the swirl mixing device provided by the embodiment of the present invention;

图9为本发明实施方式提供的旋流混合装置中,不同液体流量下混合效果对比图;Fig. 9 is a comparison diagram of mixing effects under different liquid flow rates in the swirl mixing device provided by the embodiment of the present invention;

图10为本发明实施方式提供的旋流混合装置中,压强和转速关系图;Fig. 10 is a diagram showing the relationship between pressure and rotational speed in the swirl mixing device provided by the embodiment of the present invention;

图11为本发明实施方式提供的旋流混合装置中,液体流量和转速关系图;Fig. 11 is a diagram of the relationship between liquid flow and rotational speed in the swirl mixing device provided by the embodiment of the present invention;

图12为本发明实施方式提供的旋流混合装置中,扇形喷嘴数量和转速的关系图;图13为本发明实施方式提供的旋流混合装置中,溶解氧量和时间的关系图;Fig. 12 is a diagram showing the relationship between the number of fan nozzles and the rotational speed in the swirl mixing device provided by the embodiment of the present invention; Fig. 13 is a diagram showing the relationship between the amount of dissolved oxygen and time in the swirl mixing device provided by the embodiment of the present invention;

1-导流装置;2-流体运输部分;3-容器部分;4-检测部分;5-导流部件;6-气态动力部件;7-液态动力部件;8-液态流体管路;9-气态流体管路;10-液体流量计;11-气体流量计;12-探头;13-检测仪;14-记录仪;15-外部容器;16-定子;17-液体导流管;18-气体导流管;19-环形布气口;20-液体喷嘴;21-转子。1-guiding device; 2-fluid transport part; 3-container part; 4-detection part; 5-guiding part; 6-gas power part; 7-liquid power part; 8-liquid fluid pipeline; Fluid pipeline; 10-liquid flowmeter; 11-gas flowmeter; 12-probe; 13-detector; 14-recorder; 15-external container; 16-stator; Flow tube; 19-annular air distribution port; 20-liquid nozzle; 21-rotor.

具体实施方式Detailed ways

下面将结合附图对本发明的技术方案进行清楚、完整地描述。显然,所描述的实施例是本发明一部分实施例,而不是全部的实施例。基于本发明中的实施例,本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例,都属于本发明保护的范围。The technical solutions of the present invention will be clearly and completely described below in conjunction with the accompanying drawings. Apparently, the described embodiments are some, but not all, embodiments of the present invention. Based on the embodiments of the present invention, all other embodiments obtained by persons of ordinary skill in the art without making creative efforts belong to the protection scope of the present invention.

在本发明的描述中,需要说明的是,术语“中心”、“上”、“下”、“左”、“右”、“竖直”、“水平”、“内”、“外”等指示的方位或位置关系为基于附图所示的方位或位置关系,仅是为了便于描述本发明和简化描述,而不是指示或暗示所指的装置或元件必须具有特定的方位、以特定的方位构造和操作,因此不能理解为对本发明的限制。此外,术语“第一”、“第二”、“第三”仅用于描述目的,而不能理解为指示或暗示相对重要性。In the description of the present invention, it should be noted that the terms "center", "upper", "lower", "left", "right", "vertical", "horizontal", "inner", "outer" etc. The indicated orientation or positional relationship is based on the orientation or positional relationship shown in the drawings, and is only for the convenience of describing the present invention and simplifying the description, rather than indicating or implying that the referred device or element must have a specific orientation, or in a specific orientation. construction and operation, therefore, should not be construed as limiting the invention. In addition, the terms "first", "second", and "third" are used for descriptive purposes only, and should not be construed as indicating or implying relative importance.

实施例1Example 1

如图1-6所示,本实施例提供了一种无内导流筒的气升式旋环流高效循环混合装置,装置包括导流装置1;液体循环泵或直接带压液体物料与液体输送管道组成的液体循环系统和空气压缩机或带压反应或加热气体物料或作为工作介质的气体循环压缩系统构成的流体运输部分2;釜或塔为主体的容器部分3;检测器和物料调控阀门构成的检测部分4。导流装置1位于反应容器3内部,通过液态流体管路8连接液体动力部件7,通过气态流体管路9连接气态动力部件6,液态流体管路8上设置液体流量计10,气态流体管路9上设置气体流量计11,液体动力部件7将流体通过管路8从导流部件5的液体喷嘴20中喷出,从而提供动力使流体旋转,气态动力部件6将气体通过管路从导流装置1的导流部件的环形布气口19中喷出,从而形成循环流动。总体上是以带压液体提供旋转动力,气体提供升力,从而形成旋转循环混合体系。As shown in Figures 1-6, this embodiment provides an air-lift high-efficiency circulation mixing device for swirl flow without an inner guide tube, the device includes a guide device 1; a liquid circulation pump or a direct pressurized liquid material and liquid transport Fluid transportation part 2 composed of liquid circulation system composed of pipelines and air compressor or pressure reaction or heating gas material or gas circulation compression system as working medium; container part 3 with kettle or tower as the main body; detector and material control valve Constitute the detection part 4. The flow guiding device 1 is located inside the reaction vessel 3, and is connected to the liquid power component 7 through the liquid fluid pipeline 8, and connected to the gaseous power component 6 through the gaseous fluid pipeline 9. The liquid flow meter 10 is arranged on the liquid fluid pipeline 8, and the gaseous fluid pipeline 9 is provided with a gas flow meter 11, and the liquid power part 7 sprays the fluid through the pipeline 8 from the liquid nozzle 20 of the flow guide part 5, thereby providing power to make the fluid rotate, and the gaseous power part 6 passes the gas through the pipeline from the flow guide The air is sprayed out from the annular air distribution port 19 of the flow guiding part of the device 1, thereby forming a circulating flow. Generally speaking, pressurized liquid provides rotational power, and gas provides lift, thus forming a rotational circulation mixing system.

流体运输部件2,用于将待混合流体输送至所述导流装置1中进行混合;其中,所述导流装置1包括导流部件5和向导流部件输送气体和液体的部分管路,所述导流部件包括定子16、液体导流管17、气体导流管18、环形布气口19;液体喷嘴20和转子21,所述转子21内部设置流体腔和液体喷嘴20,所述液体喷嘴20用于通过来自于所述流体腔内的一部分流体带动所述转子21相对所述定子16旋转,所述流体腔内的另一部分流体从所述其他喷嘴20中喷出,所述环形布气口19用于通过来自于所述气体导流管18内的气体喷出,形成环形气流,并带动所述容器3内部的流体形成循环流动。The fluid transportation part 2 is used to deliver the fluid to be mixed to the flow guide device 1 for mixing; wherein, the flow guide device 1 includes a flow guide part 5 and a part of the pipeline for delivering gas and liquid to the guide part, so The flow guiding part comprises a stator 16, a liquid guide pipe 17, a gas guide pipe 18, an annular gas distribution port 19; a liquid nozzle 20 and a rotor 21, and the inside of the rotor 21 is provided with a fluid cavity and a liquid nozzle 20, and the liquid nozzle 20 The rotor 21 is used to drive the rotor 21 to rotate relative to the stator 16 through a part of the fluid from the fluid chamber, and another part of the fluid in the fluid chamber is sprayed from the other nozzles 20. The annular air distribution port 19 It is used to form a ring-shaped air flow through the jetting of gas from the gas guide pipe 18, and drive the fluid inside the container 3 to form a circular flow.

需要说明的是,喷嘴包括动力喷嘴和直流喷嘴,动力喷嘴是指出口具有拐角的喷嘴。动力喷嘴中喷出的流体的反作用力作用在动力喷嘴上,推动整个转子旋转。It should be noted that the nozzle includes a power nozzle and a straight-line nozzle, and the power nozzle refers to a nozzle with an outlet having a corner. The reaction force of the fluid sprayed from the power nozzle acts on the power nozzle, pushing the entire rotor to rotate.

混合容器3,设为一个或多个,且各所述混合容器3中设置有一个或多个所述导流装置1。One or more mixing containers 3 are provided, and each mixing container 3 is provided with one or more flow guiding devices 1 .

还需要说明的是,待混合流体从导流装置1中喷出后,导流装置1可以盛放于任何容器中,例如池子、溶液罐等。It should also be noted that, after the mixed fluid is ejected from the flow guiding device 1 , the flow guiding device 1 can be contained in any container, such as a pool, a solution tank, and the like.

实施例2Example 2

图1至4为混合装置的不同实施方式。其中,图1给出了旋流混合装置的第一种实施方式,其中导流装置1的一端伸入至混合容器3中部;图2给出了混合装置的第二种实施方式,其中导流装置1在容器3的底部向上喷射;图3给出了混合装置的第三种实施方式,混合流体来自于反应容器3外的外部容器15;图4给出了混合装置的第四种实施方式,容器密闭,有多个容器串联,气体为容器内部循坏。Figures 1 to 4 show different embodiments of mixing devices. Wherein, Fig. 1 has provided the first embodiment of the swirl mixing device, wherein one end of the flow guide device 1 extends into the middle of the mixing container 3; Fig. 2 has provided the second embodiment of the mixing device, wherein the flow guide The device 1 is sprayed upwards at the bottom of the container 3; Fig. 3 shows a third embodiment of the mixing device, and the mixed fluid comes from an external container 15 outside the reaction vessel 3; Fig. 4 shows a fourth embodiment of the mixing device , the container is airtight, there are multiple containers connected in series, and the gas circulates inside the container.

实施例3Example 3

图5为本发明实施方式提供的旋流混合装置中导流部件的结构示意图。导流装置主要由导流部件5构成,导流部件5的基本原理就是由五部分组成,即定子16、液体导流管17、气体导流管18、环形布气口19、转子21和液体喷头20,气体通过气体导流管18由环形布气口19喷出,液体通过液体导流管17和转子21上的液体喷嘴20喷出,定子16由液体喷嘴20推动着转动。Fig. 5 is a schematic structural diagram of a flow guiding component in a swirl mixing device provided by an embodiment of the present invention. The flow guide device is mainly composed of the flow guide part 5, and the basic principle of the flow guide part 5 is composed of five parts, namely the stator 16, the liquid guide tube 17, the gas guide tube 18, the annular gas distribution port 19, the rotor 21 and the liquid nozzle 20. The gas is ejected through the gas guide pipe 18 from the annular gas distribution port 19, the liquid is ejected through the liquid guide pipe 17 and the liquid nozzle 20 on the rotor 21, and the stator 16 is driven to rotate by the liquid nozzle 20.

具体而言,其中液体喷嘴20设置在转子上,通过轴承与定子16连接,轴承连接定子16和转子21,转子21与轴承的连接方式可以采用螺纹连接、焊接等各种固定形式,旋转头内腔可根据需要确定尺寸,开出的螺纹孔用于连接液体喷嘴20,轴承可以采用一个或者多个深沟球轴承组合使用,也可以采用一个或者多个深沟球轴承和轴向推力轴承组合使用,其中气体导流管和液体导流管直径可根据需要调整,环形布气口19的大小开口位置也可根据需要调整。Specifically, the liquid nozzle 20 is arranged on the rotor, and is connected with the stator 16 through a bearing, and the bearing is connected with the stator 16 and the rotor 21, and the connection mode between the rotor 21 and the bearing can adopt various fixing methods such as screw connection, welding, etc., inside the rotating head The size of the cavity can be determined according to the needs, and the threaded hole is used to connect the liquid nozzle 20. The bearing can be used in combination with one or more deep groove ball bearings, or a combination of one or more deep groove ball bearings and axial thrust bearings can be used. In use, the diameters of the gas guide tube and the liquid guide tube can be adjusted as required, and the size and opening position of the annular gas distribution port 19 can also be adjusted as required.

导流部件5可以是子弹头形、橄榄形、圆形、方形、长柱形、横管形等多种结构形式。导流部件5的液体喷嘴20可以是单独提供旋转的液体喷嘴20,也可以是一个或多个提供旋转的液体喷嘴20和一个或多个顶部液体喷嘴20的组合,液体喷嘴20可以设置喷射孔,喷射孔不限制数量,但原则上开孔面积总和不超过连接管的横截面积;液体喷嘴20安装角度和喷射方向可以是任意角度,喷射形式可以是细孔喷雾、雾化喷嘴、小液流喷射或其组合,可根据旋转速度和体系的具体要求合理确定喷射角度。The flow guide member 5 can be in various structural forms such as bullet-shaped, olive-shaped, circular, square, elongated column, and horizontal tube. The liquid nozzle 20 of the flow guide part 5 can be a liquid nozzle 20 that provides rotation alone, or a combination of one or more liquid nozzles 20 that provide rotation and one or more top liquid nozzles 20, and the liquid nozzle 20 can be provided with spray holes , the number of injection holes is not limited, but in principle the sum of the opening areas does not exceed the cross-sectional area of the connecting pipe; the installation angle of the liquid nozzle 20 and the injection direction can be any angle, and the injection form can be fine-hole spray, atomizing nozzle, small liquid Stream injection or its combination, the injection angle can be reasonably determined according to the rotation speed and the specific requirements of the system.

需要说明的是,导流部件5中的液体喷嘴20可以采用现有技术中任何型号。例如,导流部件5为九嘴导流部件或五嘴导流部件,液体喷嘴20为U型广角喷嘴、V型广角喷嘴、扇形喷嘴、空化喷嘴。但是导流部件5和液体喷嘴20的结构和型号并不限于上述例子。液体喷嘴20可以分布在转子的四周,液体喷嘴20安装的角度也是可以根据需要进行设计,液体喷嘴20也可以安装在导流部件5底部,而且液体喷嘴20的角度也是可调的,比如45℃。液体喷嘴20的形状也是多种多样,液体喷嘴20可长可短,孔径可大可小,出口拐角角度等等也千变万化。需要说明的是,形状一样的液体喷嘴20,市面上不同厂家的命名方式可能是不一样的。It should be noted that, the liquid nozzle 20 in the flow guide member 5 can adopt any type in the prior art. For example, the guide part 5 is a nine-nozzle guide part or a five-nozzle guide part, and the liquid nozzle 20 is a U-shaped wide-angle nozzle, a V-shaped wide-angle nozzle, a fan-shaped nozzle, or a cavitation nozzle. However, the structure and type of the flow guide member 5 and the liquid nozzle 20 are not limited to the above examples. The liquid nozzles 20 can be distributed around the rotor, and the installation angle of the liquid nozzles 20 can also be designed according to the needs. The liquid nozzles 20 can also be installed at the bottom of the guide member 5, and the angle of the liquid nozzles 20 is also adjustable, such as 45°C . The shape of the liquid nozzle 20 is also various. The liquid nozzle 20 can be long or short, the aperture can be large or small, and the angle of the outlet corner is also ever-changing. It should be noted that the liquid nozzles 20 with the same shape may be named differently by different manufacturers on the market.

从安装的角度看,液体喷嘴20的安装和组成是多样的,导流部件5在一个混合体系中的安装位置也是多变的;从进料的角度看,就有向下、向上、侧向进料取决于导流部件的安装方向,可以泵加压进料、泵循环进料、带压液体经管道直接进料混合等,可以单个体系、可以串联体系、可以并联体系等;从物料的角度看,可以使单纯气体、单纯液体、气液、液固如溶解、气液固等物料体系,可以作为物料自身搅拌器,也可以作为多种流体的混合装置;从装备的角度不仅仅是搅拌釜圆桶状,可以使常见的搅拌釜、圆桶、塔设备、方形的污水池等等,也可以是自然界的湖泊河流等等场合,可以单独导流部件作为混合设备,也可以是导流部件与传统的机械搅拌等设备耦合使用,甚至与换热器耦合使用等多种形式。From the perspective of installation, the installation and composition of the liquid nozzle 20 are various, and the installation position of the guide member 5 in a mixing system is also changeable; from the perspective of feeding, there are downward, upward, sideways The feeding depends on the installation direction of the diversion parts. It can be pump pressurized feeding, pump circulating feeding, pressurized liquid directly feeding and mixing through pipelines, etc. It can be a single system, a series system, a parallel system, etc.; from the material From a perspective, it can make pure gas, simple liquid, gas-liquid, liquid-solid such as dissolved, gas-liquid-solid and other material systems, which can be used as a mixer for the material itself, or as a mixing device for various fluids; from the perspective of equipment, it is not only The stirred tank is in the shape of a barrel, which can be used in common stirred tanks, drums, tower equipment, square sewage pools, etc., or it can be used in natural lakes and rivers, etc., and can be used as a mixing device alone or as a guide Flow components are coupled with traditional mechanical stirring and other equipment, and even coupled with heat exchangers and other forms.

实施例4Example 4

图6示出了具有旋流混合装置的混合原理示意图。如图6所示,在液体喷嘴20作用下,一方面搅拌釜内部流体有一个自中心向周边循环流动的效果,另一方面有一个中间往下旋流效果,复杂的多重旋流可满足提升混合效果的要求。导流部件5沿所述容器的竖直方向伸至所述待混合流体中。该设置方式使得喷出的气体和液体产生强烈的翻滚、湍流、摩擦等旋流混合形式,促进物料直接接触并均匀混合,利用加入物料或蒸汽或压缩空气的动力或借助泵推动的循环物料的动力实现了物料间的直接混合,可大大强化传热、传质或反应效率,通过对底部的喷射可防止沉降和堵塞出料口。需要说明的是,导流部件5的设置方式并不仅限于上述优选例。作为可选的实施方式,所述导流部件5与所述待混合流体间隔设置。Figure 6 shows a schematic diagram of the mixing principle with a swirl mixing device. As shown in Figure 6, under the action of the liquid nozzle 20, on the one hand, the fluid inside the stirred tank has the effect of circulating from the center to the periphery; Mixed effect requirements. The flow guide member 5 extends into the fluid to be mixed along the vertical direction of the container. This setting method makes the sprayed gas and liquid produce strong tumbling, turbulent flow, friction and other swirl mixing forms, promotes direct contact and uniform mixing of materials, and uses the power of adding materials or steam or compressed air or the circulation of materials driven by pumps. The power realizes direct mixing between materials, which can greatly enhance heat transfer, mass transfer or reaction efficiency, and prevent sedimentation and blockage of the discharge port by spraying the bottom. It should be noted that, the arrangement manner of the flow guide member 5 is not limited to the above preferred examples. As an optional implementation manner, the flow guide member 5 is spaced apart from the fluid to be mixed.

作为可供优选的实施方式,所述导流部件5设为一个,且所述导流部件5设置于所述混合容器的中心轴线上,所述中心轴线平行于所述混合容器3的竖直方向;或者,所述导流部件5设为多个,沿所述中心轴线对称设置。As an alternative preferred embodiment, one guide member 5 is provided, and the guide member 5 is arranged on the central axis of the mixing container, and the central axis is parallel to the vertical direction of the mixing container 3. direction; or, the flow guide member 5 is provided in multiples, symmetrically arranged along the central axis.

作为优选的实施方式,所述旋流混合装置还包括检测部分4,设有检测探头12,且所述检测探头12伸入任一个或多个所述混合容器3中,并伸至所述待混合流体中。检测探头12与检测仪13连接,检测仪13与记录仪14连接,形成对检测结果的记录。As a preferred embodiment, the swirl mixing device also includes a detection part 4, which is provided with a detection probe 12, and the detection probe 12 extends into any one or more of the mixing containers 3, and extends to the to-be-treated in the mixed fluid. The detection probe 12 is connected to the detector 13, and the detector 13 is connected to the recorder 14 to form a record of the detection result.

检测部分4用于检测流体中的各项理化参数,例如电导率等。检测部分4可以采用现有的任何检测类设备。例如,可选的,检测部分4包括电导率仪和无纸记录仪。The detection part 4 is used to detect various physical and chemical parameters in the fluid, such as electrical conductivity and the like. The detection part 4 can adopt any existing detection equipment. For example, optionally, the detection part 4 includes a conductivity meter and a paperless recorder.

需要说明的是,本实施例提供的混合装置可以应用在各种需对流体进行搅拌的领域。待混合流体可以为液体混合或气液混合体系。It should be noted that the mixing device provided in this embodiment can be applied in various fields where fluids need to be stirred. The fluid to be mixed can be a liquid mixture or a gas-liquid mixture system.

实施例5Example 5

应用图1所述的装置,对旋流混合装置的功率进行测量时,在直径1200mm,高度1500mm的反应容器3中装入清水1500L,采用2扇形喷嘴2广角喷嘴,在最大循坏液体6.6m3/h,反应釜内液体为1.5m3液体,一小时内反应釜液体可以循环4.4次,在实际体系中可根据实际情况调节循环量。在最大液体流量6.6m3/h、最大气体流量10m3/h下运行一小时,实际体系消耗电量为4Kw,小于一般搅拌电机功率7.5Kw。Using the device described in Figure 1, when measuring the power of the swirl mixing device, put 1500L of clear water into the reaction vessel 3 with a diameter of 1200mm and a height of 1500mm, and use 2 fan-shaped nozzles and 2 wide-angle nozzles to achieve a maximum circulation rate of 6.6m. 3 /h, the liquid in the reactor is 1.5m 3 liquid, and the liquid in the reactor can be circulated 4.4 times within one hour, and the circulation amount can be adjusted according to the actual situation in the actual system. Running for one hour under the maximum liquid flow rate of 6.6m 3 /h and the maximum gas flow rate of 10m 3 /h, the actual power consumption of the system is 4Kw, which is less than the general stirring motor power of 7.5Kw.

实施例6Example 6

对不同液体流量下喷头在空气中的转速进行测量时,在直径1200mm,高度1500mm的反应容器中装入清水1500L,采用2扇形喷嘴2广角喷嘴,结果如表1所示。When measuring the rotational speed of the nozzle in the air under different liquid flow rates, 1500L of clean water was filled in a reaction vessel with a diameter of 1200mm and a height of 1500mm, and 2 fan-shaped nozzles and 2 wide-angle nozzles were used. The results are shown in Table 1.

表1Table 1

实施例7Example 7

对不同液体流量下喷头在水中的转速进行测量时,在直径1200mm,高度1500mm的反应容器中装入清水1500L,采用2扇形喷嘴2广角喷嘴,结果如表2所示。When measuring the rotational speed of the nozzle in water under different liquid flow rates, 1500L of clean water was filled in a reaction vessel with a diameter of 1200mm and a height of 1500mm, and 2 fan-shaped nozzles and 2 wide-angle nozzles were used. The results are shown in Table 2.

表2Table 2

气流量(m3/h)Air flow(m 3 /h) 气压(MPa)air pressure (MPa) 液流量(m3/h)Liquid flow(m 3 /h) 液压(MPa)Hydraulic pressure (MPa) 转速(r/min)Speed(r/min) 00 00 1.21.2 0.180.18 7171 00 00 1.81.8 0.160.16 109109 00 00 2.42.4 0.120.12 139139 00 00 3.03.0 0.080.08 157157 00 00 3.63.6 0.060.06 179179 00 00 4.24.2 0.040.04 215215 00 00 4.84.8 0.030.03 258258 00 00 5.45.4 0.020.02 303303 00 00 6.06.0 0.020.02 343343 00 00 6.66.6 0.010.01 358358

实施例8Example 8

在测量不同液气比对循环流动效果的影响时,在直径1200mm,高度1500mm的反应容器中装入清水1500L,采用2扇形喷嘴2广角喷嘴,分别在液气比3:1、3:2、3:3、3:4、3:5、3:6、3:7、3:8、3:9、3:10下待鼓泡稳定后测量气泡分布区直径、转速以及液体流动形式,结果如表3所示。When measuring the influence of different liquid-gas ratios on the effect of circulating flow, 1500L of clean water was filled in a reaction vessel with a diameter of 1200mm and a height of 1500mm, and 2 fan-shaped nozzles and 2 wide-angle nozzles were used, respectively, at liquid-gas ratios of 3:1, 3:2, 3:3, 3:4, 3:5, 3:6, 3:7, 3:8, 3:9, 3:10 After the bubbling is stable, measure the diameter of the bubble distribution area, rotational speed and liquid flow form, and the result as shown in Table 3.

表3table 3

实施例9Example 9

在测量不同鼓泡直径下新型装置的混合效果时,在直径1200mm,高度1500mm的反应容器中装入清水1500L,采用2扇形喷嘴2广角喷嘴,结果如图7所示,当鼓泡直径为450mm的时候混合效果最好。When measuring the mixing effect of the new device under different bubbling diameters, put 1500L of clean water into a reaction vessel with a diameter of 1200mm and a height of 1500mm, and use 2 fan-shaped nozzles and 2 wide-angle nozzles. The results are shown in Figure 7. When the bubbling diameter is 450mm It works best when mixed.

实施例10Example 10

在测量不同气流量下新型装置的混合效果时,在直径1200mm,高度1500mm的反应容器中装入清水1500L,采用2扇形喷嘴2广角喷嘴,液流量为6m3/h下,结果如图8所示,当气流量在7m3/h时混合效果最好。When measuring the mixing effect of the new device under different air flow rates, 1500L of clean water was filled in a reaction vessel with a diameter of 1200mm and a height of 1500mm, using 2 fan-shaped nozzles and 2 wide-angle nozzles, and the liquid flow rate was 6m 3 /h. The results are shown in Figure 8 It shows that the mixing effect is best when the air flow rate is 7m 3 /h.

实施例11Example 11

在测量不同液流量下新型装置的混合效果时,在直径1200mm,高度1500mm的反应容器中装入清水1500L,采用2扇形喷嘴2广角喷嘴,气流量为8m3/h下,结果如图9所示,当液流量在6m3/h时混合效果最好。When measuring the mixing effect of the new device under different liquid flow rates, 1500L of clean water was filled in a reaction vessel with a diameter of 1200mm and a height of 1500mm, using 2 fan-shaped nozzles and 2 wide-angle nozzles, and the air flow rate was 8m 3 /h. The results are shown in Figure 9. It shows that the mixing effect is best when the liquid flow rate is 6m 3 /h.

实施例12Example 12

在测量液体压力和喷头转速的关系时,在直径1200mm,高度1500mm的反应容器中装入清水1500L,采用2扇形喷嘴2广角喷嘴,无气流量下,结果如图10所示,无气流量下液体压力和喷头转速呈现一定的线性关系,可以根据此关系来通过液体压力来控制喷头转速。When measuring the relationship between the liquid pressure and the speed of the nozzle, put 1500L of clean water into a reaction vessel with a diameter of 1200mm and a height of 1500mm, and use 2 fan-shaped nozzles and 2 wide-angle nozzles without air flow. The results are shown in Figure 10. There is a certain linear relationship between the liquid pressure and the speed of the nozzle, and the speed of the nozzle can be controlled by the liquid pressure according to this relationship.

实施例13Example 13

在测量液体流量和喷头转速的关系时,在直径1200mm,高度1500mm的反应容器中装入清水1500L,采用2扇形喷嘴2广角喷嘴,无气流量下,结果如图11所示,无气流量下液体流量和喷头转速呈现一定的线性关系,可以根据此关系来通过液体流量来控制喷头转速。When measuring the relationship between the liquid flow rate and the speed of the nozzle, put 1500L of clean water into a reaction vessel with a diameter of 1200mm and a height of 1500mm, using 2 fan-shaped nozzles and 2 wide-angle nozzles, and the results are shown in Figure 11 under no air flow. There is a certain linear relationship between the liquid flow and the speed of the nozzle, and the speed of the nozzle can be controlled by the liquid flow according to this relationship.

实施例14Example 14

在测量扇形喷嘴数量和喷头转速的关系时,在直径1200mm,高度1500mm的反应容器中装入清水1500L,在液流量6m3/h,气流量8m3/h下,结果如图12所示,扇形喷嘴数量和喷头转速呈现一定的线性关系,可以根据此关系来通过扇形喷嘴数量来控制喷头转速。When measuring the relationship between the number of fan-shaped nozzles and the speed of the nozzle, 1500L of clean water was filled in a reaction vessel with a diameter of 1200mm and a height of 1500mm, and the liquid flow rate was 6m 3 /h and the air flow rate was 8m 3 /h. The results are shown in Figure 12. There is a certain linear relationship between the number of fan-shaped nozzles and the speed of the nozzle. According to this relationship, the number of fan-shaped nozzles can be used to control the speed of the nozzle.

实施例15Example 15

在测量新型装置溶解氧量和时间的关系时,在直径120cm,高度150cm的反应容器中装入清水1500L,采用2扇形喷嘴2广角喷嘴,在液流量6m3/h,气流量3m3/h下,结果如图13所示。When measuring the relationship between dissolved oxygen and time in the new device, put 1500L of clean water into a reaction vessel with a diameter of 120cm and a height of 150cm, using 2 fan-shaped nozzles and 2 wide-angle nozzles, with a liquid flow rate of 6m 3 /h and an air flow rate of 3m 3 /h Next, the result is shown in Figure 13.

显然,上述实例仅仅是为清楚的说明而举例,而并非对实施方式的限定。对于所属领域的普通技术人员来说,在上述说明的基础上还可以做出其它不同形式的变化或变动。这里无需也无法对所有的实施方式予以穷举。而由此所引伸出的显而易见的变化或变动仍处于本发明创造的保护范围之中。Apparently, the above examples are only examples for clear description, rather than limiting the implementation. For those of ordinary skill in the art, other changes or changes in different forms can be made on the basis of the above description. It is not necessary and impossible to exhaustively list all the implementation manners here. And the obvious changes or changes derived therefrom are still within the scope of protection of the present invention.

Claims (22)

1. a kind of diversion component, the diversion component includes stator and rotor, is provided with fluid injector on rotor, fluid injector with Liquid guide flow pipe connects, and liquid guide flow pipe is set to the inside of rotor and stator, gas vent is additionally provided on diversion component, Gas vent is connected to gas diversion tube.
2. diversion component according to claim 1, it is characterised in that the gas vent in the diversion component is set to liquid Above or below body nozzle, alternatively, gas vent is arranged side by side with fluid injector, alternatively, gas vent is total with fluid injector With alternatively, gas vent is located above fluid injector and fluid injector periphery, alternatively, gas vent is located above fluid injector And lower section, alternatively, gas vent is located at the periphery and lower section of fluid injector.
3. diversion component according to claim 1 or 2, it is characterised in that the fluid injector is one or more, nozzle For fan nozzle, U-shaped wide-angle nozzle, V-type wide-angle nozzle, cavitating nozzle or direct trepanning or the nozzle to crack.
4. diversion component according to claim 3, it is characterised in that the stator is located at the top of rotor or stator is located at The lower section of rotor.
5. diversion component according to claim 2, it is characterised in that the gas vent be annular air outlet or it is poroid go out Gas port, when gas vent is poroid gas outlet, poroid gas outlet is one or more.
6. according to claim 1-5 any one of them diversion components, it is characterised in that the side of the fluid injector injection liquid To rectilinear direction of the rotor axis to fluid injector central point is deviateed, the reaction force acts of the liquid of fluid injector injection are being sprayed On mouth, drive rotor rotation.
7. a kind of gas-lifting type of no inner draft tube revolves circulation efficient circulation mixing arrangement, it is characterised in that device includes container and power Profit requires 1-6 any one of them diversion components, diversion component to be located in container, liquid guide flow pipe and the liquid stream of diversion component The gas diversion tube of body pipeline connection, diversion component is connected to gaseous state fluid circuit.
8. device according to claim 8, it is characterised in that the diversion component is multiple, and each diversion component passes through Liquid guide flow pipe connects fluid liquid pipeline and gaseous state fluid circuit with gas diversion tube.
9. according to claim 7-8 any one of them devices, it is characterised in that the container is kettle or tower or pond or tank or needs Nature or artificial water to be processed.
10. according to claim 7-9 any one of them devices, it is characterised in that the fluid pressure in the fluid liquid pipeline Higher than the pressure of dispersion, the pressure of gas is enough to overcome fluid pressure poor in the gaseous fluid pipeline.
11. according to claim 7-10 any one of them devices, it is characterised in that the fluid liquid pipeline and liquid pressing Device connects, and the gaseous fluid pipeline is connect with gas pressurized device.
12. according to the devices described in claim 11, it is characterised in that the liquid pressing device is cycle fluid under pressure pump, follows Ring gas compressor, or the container with high liquid level or the liquid container with high pressure gas.
13. device according to claim 12, it is characterised in that the gas pressurized device is air compressor, either Container with high pressure gas.
14. according to the devices described in claim 11, it is characterised in that the liquid source into liquid pressing device is in appearance Liquid in device or in non-container liquid other liquid.
15. according to the devices described in claim 11, it is characterised in that the gas source into gas pressurized device is in appearance Recyclegas in device is either from other gases of non-gas in container.
16. according to claim 7-15 any one of them devices, it is characterised in that the container is multiple, is set in each container One or more diversion components are set, the diversion component in each container is connect with fluid liquid pipeline and gaseous state fluid circuit.
17. according to claim 7-16 any one of them devices, it is characterised in that each container is closed container, each Gas is conveyed into gas pressurized device by closed container by the gas piping for being arranged in upper vessel portion, and each container passes through setting Liquid is conveyed into liquid pressing device in the liquid line of container bottom.
18. according to claim 7-17 any one of them devices, it is characterised in that described device further include heating device or It is cooling device, the heating device or cooling settings heat container and are cooled down in the outside or inside of container, or It is that the liquid that will enter liquid pressing device is heated or cooled, or is carried out to the gas for entering gas compressing apparatus Heating is either cooling.
19. according to claim 7-18 any one of them devices, it is characterised in that described device further includes detection device, described Detection device include in system liquid or with it is one or more in detector.
20. according to claim 7-19 any one of them devices, it is characterised in that described device further includes control device, described Control device and liquid fluid pipe valve, the liquid of gaseous fluid pipe valve, the gas discharge outlet valve of container, container One or more of exhaust outlet valve connects.
21. a kind of method carrying out solution mixing or gas-liquid mixed using any one of claim 7-20 described devices, the side Method includes the following steps:
Liquid A is added in suitable container by step 1) so that fluid level is higher than fluid injector and gas vent, by liquid B carries out pressurization and is input to fluid liquid pipeline;
Liquid B is spurted into the liquid level of liquid in containers A hereinafter, then gas compression is passed through gas by step 2) by fluid injector State fluid circuit is transported to gas vent, below the liquid level of the liquid A in gas injection to container.
22. according to the method for claim 21, it is characterised in that liquid A and liquid B in the method are same liquid Either different liquids.
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111302508A (en) * 2020-02-26 2020-06-19 厦门大学 Efficient rotary-circulation oxygen-increasing and air-distributing device
CN113289537A (en) * 2021-06-07 2021-08-24 浙江天奇新材料科技股份有限公司 Modified furan resin fixed-ratio production processing system and production method

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH04266698A (en) * 1990-11-17 1992-09-22 Boc Group Plc:The Gas cylinder
WO1995027557A1 (en) * 1994-04-12 1995-10-19 Ekokehitys Oy Method of generating gas bubbles in a liquid and apparatus for the implementation of the method
CN101857303A (en) * 2010-06-18 2010-10-13 江苏金山环保工程集团有限公司 Novel quick-installation aeration connector for membrane bioreactor
CN106607004A (en) * 2015-10-21 2017-05-03 中国石油化工股份有限公司 Circulation mixer and application thereof
CN206535447U (en) * 2017-01-22 2017-10-03 杭州中泰深冷技术股份有限公司 A kind of novel gas-liquid mixing fluid-filling structure
CN107537338A (en) * 2016-06-28 2018-01-05 厦门大学 A kind of efficiently hybrid technology is equipped with energy-conservation

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH04266698A (en) * 1990-11-17 1992-09-22 Boc Group Plc:The Gas cylinder
WO1995027557A1 (en) * 1994-04-12 1995-10-19 Ekokehitys Oy Method of generating gas bubbles in a liquid and apparatus for the implementation of the method
CN101857303A (en) * 2010-06-18 2010-10-13 江苏金山环保工程集团有限公司 Novel quick-installation aeration connector for membrane bioreactor
CN106607004A (en) * 2015-10-21 2017-05-03 中国石油化工股份有限公司 Circulation mixer and application thereof
CN107537338A (en) * 2016-06-28 2018-01-05 厦门大学 A kind of efficiently hybrid technology is equipped with energy-conservation
CN206535447U (en) * 2017-01-22 2017-10-03 杭州中泰深冷技术股份有限公司 A kind of novel gas-liquid mixing fluid-filling structure

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111302508A (en) * 2020-02-26 2020-06-19 厦门大学 Efficient rotary-circulation oxygen-increasing and air-distributing device
CN113289537A (en) * 2021-06-07 2021-08-24 浙江天奇新材料科技股份有限公司 Modified furan resin fixed-ratio production processing system and production method
CN113289537B (en) * 2021-06-07 2022-05-31 浙江天奇新材料科技股份有限公司 Modified furan resin fixed-ratio production processing system and production method

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