CN108398362A - A kind of body refuse settling ratio and body refuse active testing instrument and test method - Google Patents

A kind of body refuse settling ratio and body refuse active testing instrument and test method Download PDF

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Publication number
CN108398362A
CN108398362A CN201810143960.1A CN201810143960A CN108398362A CN 108398362 A CN108398362 A CN 108398362A CN 201810143960 A CN201810143960 A CN 201810143960A CN 108398362 A CN108398362 A CN 108398362A
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China
Prior art keywords
body refuse
transparent container
height
settling ratio
gular transparent
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CN201810143960.1A
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Inventor
张春波
王久生
张建新
董冠良
王海军
杨雪
刘熙旸
赵维愚
周诗宇
李勐
胡婧婷
曾千会
田姝
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State Grid Corp of China SGCC
Electric Power Research Institute of State Grid Jilin Electric Power Co Ltd
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State Grid Corp of China SGCC
Electric Power Research Institute of State Grid Jilin Electric Power Co Ltd
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Priority to CN201810143960.1A priority Critical patent/CN108398362A/en
Publication of CN108398362A publication Critical patent/CN108398362A/en
Pending legal-status Critical Current

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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
    • G01N15/04Investigating sedimentation of particle suspensions
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/25Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
    • G01N21/31Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
    • G01N21/35Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light
    • G01N21/3577Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light for analysing liquids, e.g. polluted water

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  • Physics & Mathematics (AREA)
  • Chemical & Material Sciences (AREA)
  • Biochemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Spectroscopy & Molecular Physics (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Dispersion Chemistry (AREA)
  • Investigating Or Analysing Materials By Optical Means (AREA)

Abstract

A kind of body refuse settling ratio and body refuse active testing instrument and test method, belong to a kind of water quality characteristic test equipment in Treatment of Industrial Water field, more particularly to a kind of body refuse tester and test method.The present invention includes light source, condenser, collimator objective, gular transparent container, integrating sphere and computer.The present invention can bring following advantageous effect:Detection data is corrected using two parameters of intensity in transmission and scattering strength, it is ensured that the precision of instrument test result simultaneously.It is capable of the body refuse settling ratio of accurate quantitative analysis measurement coagulant precipitation processing equipment any time period;Body refuse activity that can be in qualitative test coagulant precipitation processing equipment, reliable basis is provided for combustion adjustment.Device body refuse settling ratio quantitative result, body refuse activity qualitative results favorable reproducibility.

Description

A kind of body refuse settling ratio and body refuse active testing instrument and test method
Technical field
The invention belongs to a kind of water quality characteristic test equipment in Treatment of Industrial Water field, more particularly to a kind of body refuse tester And test method.
Background technology
Treatment of Industrial Water technological process is a process for gradually removing impurities in water, and the removal of impurity follows removal grain size Rule from big to small, and diameter is referred to as colloid in 0.1 μm or more of substance in water, colloid is made of different-diameter particle A stabilising system, the removing of colloidal substance then relies primarily on industrial coagulant precipitation equipment, therefore, is set as pretreatment key Standby coagulant precipitation device is the equipment that water treatment field is most widely used, and coagulant precipitation process is a complicated mass transfer mistake Journey, the hydrodynamics and kinetic theory for also including complexity mainly disperse including electrolyte mixing, electrolyte hydrolyzes, flocculation, wads a quilt with cotton Processes, the factors for influencing coagulant precipitation such as solidifying body growth, sedimentation include mainly:Source quality (salt content, basicity), water temperature, water PH value, electrolytes (being determined by small-scale test), body refuse concentration and activity, coagulation time, equipment size and structure distribution, Run flow velocity (under predetermined processing), coagulation agent dose etc..It is many for a fixed coagulant precipitation equipment and design water source In more influence factors water temperature (can be controlled by heater), body refuse concentration and activity, coagulation agent dose can taking human as control, Wherein, the suspended matter of coagulation agent dose and water, colloidal content and sludge volume determine body refuse concentration and activity, therefore, coagulation There are certain relevances with coagulation agent dose for agent dose.In actual operation, body refuse concentration and activity, coagulation agent dose usually The case where being to be controlled by experience, being usually present control lag.
The key of coagulant precipitation equipment operation control is body refuse amount and the active adjustment of body refuse.But currently, without such The test equipment of type can only use the settling ratio of artificial qualitative test body refuse, and cannot carry out body refuse active testing.Therefore, The operation of current coagulant precipitation equipment control be it is extensive, there are the problem of mainly have:1) anti-load impact ability is small, far reaches Less than design requirement;System equipment operation stability is not high, and effluent quality fluctuation is big, occurs the exceeded feelings of delivery turbidity often Condition;2) dosage adjustment is inappropriate, and dosing dosage is low, and coagulant precipitation effect is poor, and the substances removal effect such as colloid declines, after causing Continuous system dirt is stifled;Dosing dosage is high, not only increases cost, has also resulted in unreacted coagulant and occurred in follow-up system Coagulating when especially handling low temperature and low turbidity water, easily causes product (colloid) pollution (ultrafiltration etc. of follow-up system coagulant Membranous system occurs serious dirty stifled);3) body refuse discharge is inappropriate, and body refuse discharge capacity is more than actual emission, and effluent quality deteriorates, and is Nominal output is not achieved in system, and body refuse water content is big, and desliming workload increases, and discharge capacity is less than actual emission, on the one hand meeting The mixing of activated sludge and water is hindered, on the other hand, can cause to be discharged a large amount of alumen ustum risings, effluent quality can also deteriorate;4) place When managing municipal middle water, the hardness that may cause in water exceeded in short-term, basicity and ammonia nitrogen, total phosphorus are exceeded, are generated to membranous system Irreversible harmful effect.
In conclusion the industrial coagulant precipitation processing of water is the key that Treatment of Industrial Water, and body refuse amount and activity control are Industrial coagulant precipitation handles the key well run, and body refuse amount is more or can all directly affect body refuse activity and waterpower flow less, most Water quality is caused to deteriorate eventually.Therefore, accurately controlling for coagulant precipitation processing is exactly to get hold of " as soon as degree ", this degree the moment Be body refuse amount how much.Currently, coagulant precipitation extensive style control, adjustment be influence entire Treatment of Industrial Water effect principal element it One, it is necessary to be improved.Control accuracy is run in order to improve coagulant precipitation equipment, the operation level of further lifting means has Effect control effluent quality fluctuation, finally avoids effluent quality from deteriorating and generates harmful effect to subsequent processing device, settled to body refuse The quantitative determination of ratio and the active qualitative test of body refuse just seem very practical significance.
Therefore there is an urgent need for a kind of novel technical solutions to solve the problems, such as this in the prior art.
Invention content
The technical problem to be solved by the present invention is to:A kind of body refuse settling ratio and body refuse active testing instrument and test side are provided Method runs control accuracy to improve coagulant precipitation equipment, and the operation level of further lifting means effectively controls effluent quality wave It is dynamic, it finally avoids effluent quality from deteriorating and harmful effect is generated to subsequent processing device.
A kind of body refuse settling ratio and body refuse active testing instrument, including light source, condenser, collimator objective, gular transparent container, Integrating sphere and computer;
Water inlet pipe is provided at the top of the gular transparent container, water inlet pipe lower section is provided with overflow pipe;
The integrating sphere is connected with the computer communication;
The light source, condenser, collimator objective, gular transparent container and integrating sphere are sequentially arranged.
The light source, the condenser, the collimator objective, the gular transparent container and the integrating sphere cloth successively It sets on pedestal.
The light source is infrared light supply.
A kind of body refuse settling ratio and body refuse activity test method use a kind of foregoing body refuse settling ratio and body refuse to live Property tester, it is characterized in that:Include the following steps,
Step 1: water to be measured is poured into gular transparent container, static -100 minutes 30 minutes;
Step 2: open the light source, gular transparent container obtains the irradiation light that intensity is Tr, at the same obtain by water sample and The luminous intensity Tx of gular transparent holder absorption, the luminous intensity Ts scattered and the luminous intensity for penetrating water sample and gular transparent container Tt, i.e.,:
Tr=Tt+Tx+Ts, wherein Tr is the intensity of incident light, Tt be penetrate luminous intensity, Tx be absorb luminous intensity, Ts is the luminous intensity of scattering;
Step 3: obtaining the transmittivity Д t, i.e. Д t=100% × Tt/ (Tt+Tx+Ts) of light;The scattering ratio Д of light S, i.e. Д s=100% × Ts/ (Tt+Tx+Ts);
Step 4: the total height for obtaining liquid in gular transparent container is L, then there is L=Ls+Ln=Ls+Lns+Lnc+ Lnj, wherein L is liquid total height, Ls is water layer height, Lns is weaker zone body refuse height, Lnc is sublevel body refuse height, Lnj For close layer body refuse height;
Step 5: computer obtains body refuse settling ratio:Ct=100% × (Lnc+Lnj)/L, body refuse activity:H=100% ×(Lns+Lnc)/(Lns+Lnc+Lnj);
Step 6: the computer obtains body refuse settling ratio quantitative identification foundation, when Д t 3% or 2%≤Д of > t≤ 3%, when Д s/ Д t < 60, the corresponding optical len of integrating sphere is divided into water layer height Ls;
When the corresponding optical len of 2%≤Д t≤3% and t >=60 Д s/ Д is divided into weaker zone body refuse height Lns.
As 1%≤Д t < 2%, 100 corresponding optical lens of Д s/ Д t < are divided into sublevel body refuse height Lnc.
As 1%≤Д t < 2%, t >=100 s/ Д Д or 1% corresponding optical lens of Д t < are divided into close layer body refuse Height Lnj;
Step 7: the computer obtains body refuse activity qualitative discrimination foundation, as h > 80%, body refuse characteristic is lived for height Property body refuse;When 60%≤h≤80%, body refuse characteristic is moderate activity body refuse;As 40%≤h < 60%, body refuse characteristic is minuent Active sludge;As h < 40%, body refuse characteristic is ultralow degree active sludge.
By above-mentioned design scheme, the present invention can bring following advantageous effect:It is strong using intensity in transmission and scattering simultaneously Two parameters are spent to correct detection data, it is ensured that the precision of instrument test result.Can accurate quantitative analysis measure coagulant precipitation at Manage the body refuse settling ratio of equipment any time period;Body refuse activity that can be in qualitative test coagulant precipitation processing equipment, for operation Adjustment provides reliable basis.Device body refuse settling ratio quantitative result, body refuse activity qualitative results favorable reproducibility.By adjusting in time Body refuse height, greatly improves body refuse activity, lifting means effluent quality, and the glutinous dirt that can avoid or substantially slow down follow-up equipment is blocked up Phenomenon.The use of device can effectively improve the operation stability of coagulant precipitation equipment and anti-load impact ability, can effectively drop Secondary pollution caused by low coagulant delay sedimentation.
Description of the drawings
Below in conjunction with the drawings and specific embodiments, the present invention is further illustrated:
Fig. 1 is a kind of structural schematic diagram of body refuse settling ratio and body refuse active testing instrument of the present invention.
Fig. 2 is liquid layered signal in the gular transparent container of a kind of body refuse settling ratio of the present invention and body refuse active testing instrument Figure.
In figure, 1- light sources, 2- spotlights, 3- collimator objectives, 4- gular transparents container, 5- integrating spheres, 6- computers, 41- Water inlet pipe, 42- overflow pipes, 7- pedestals.
Specific implementation mode
A kind of body refuse settling ratio and body refuse active testing instrument, as shown in Fig. 1 Fig. 2:Including light source 1, condenser 2, collimation object Mirror 3, gular transparent container 4, integrating sphere 5 and computer 6;
The top of the gular transparent container 4 is provided with water inlet pipe 41,41 lower section of the water inlet pipe is provided with overflow pipe 42;
The integrating sphere 5 and the communication connection of the computer 6;
The light source 1, condenser 2, collimator objective 3, gular transparent container 4 and integrating sphere 5 are sequentially arranged.
The light source 1, the condenser 2, the collimator objective 3, the gular transparent container 4 and the integrating sphere 5 according to It is secondary to be arranged on pedestal 7.
The light source 1 is infrared light supply.
Light is sent out from light source 1, and through condenser 2 and 3 parallel radiation of collimator objective on gular transparent container 4, rectangle is saturating Sewage natural layering after being stood in bright container 4, gradually muddy from top to bottom, integrating sphere 5 will transmit through the light of gular transparent container 4 Line acquires and is transferred to computer and calculated, and the body refuse settling ratio and body refuse activity of sewage are obtained by data analysis.
A kind of body refuse settling ratio and body refuse activity test method use a kind of foregoing body refuse settling ratio and body refuse to live Property tester, it is characterized in that:Include the following steps,
Step 1: water to be measured is poured into gular transparent container 4, static -100 minutes 30 minutes;
Step 2: opening the light source 1, gular transparent container 4 obtains the irradiation light that intensity is Tr, while obtaining by water sample The light intensity of the luminous intensity Tx, the luminous intensity Ts and transmission water sample and gular transparent container 4 that are scattered that are absorbed with gular transparent container 4 Tt is spent, i.e.,:
Tr=Tt+Tx+Ts, wherein Tr is the intensity of incident light, Tt be penetrate luminous intensity, Tx be absorb luminous intensity, Ts is the luminous intensity of scattering;
Step 3: obtaining the transmittivity Д t, i.e. Д t=100% × Tt/ (Tt+Tx+Ts) of light;The scattering ratio Д of light S, i.e. Д s=100% × Ts/ (Tt+Tx+Ts);
Step 4: the total height for obtaining gular transparent container (4) interior liquid is L, then there is L=Ls+Ln=Ls+Lns+Lnc+ Lnj, wherein L is liquid total height, Ls is water layer height, Lns is weaker zone body refuse height, Lnc is sublevel body refuse height, Lnj For close layer body refuse height;
Step 5: computer obtains body refuse settling ratio:Ct=100% × (Lnc+Lnj)/L, body refuse activity:H=100% ×(Lns+Lnc)/(Lns+Lnc+Lnj);
Step 6: the computer 6 obtain body refuse settling ratio quantitative identification foundation, when Д t 3% or 2%≤Д of > t≤ 3%, when Д s/ Д t < 60,5 corresponding optical len of integrating sphere is divided into water layer height Ls;
When the corresponding optical len of 2%≤Д t≤3% and t >=60 Д s/ Д is divided into weaker zone body refuse height Lns.
As 1%≤Д t < 2%, 100 corresponding optical lens of Д s/ Д t < are divided into sublevel body refuse height Lnc.
As 1%≤Д t < 2%, t >=100 s/ Д Д or 1% corresponding optical lens of Д t < are divided into close layer body refuse Height Lnj;
Step 7: the computer 6 obtains body refuse activity qualitative discrimination foundation, as h > 80%, body refuse characteristic is lived for height Property body refuse;When 60%≤h≤80%, body refuse characteristic is moderate activity body refuse;As 40%≤h < 60%, body refuse characteristic is minuent Active sludge;As h < 40%, body refuse characteristic is ultralow degree active sludge.

Claims (4)

1. a kind of body refuse settling ratio and body refuse active testing instrument, it is characterized in that:Including light source (1), condenser (2), collimator objective (3), gular transparent container (4), integrating sphere (5) and computer (6);
Water inlet pipe (41) is provided at the top of the gular transparent container (4), the water inlet pipe (41) lower section is provided with overflow pipe (42);
The integrating sphere (5) and the computer (6) communication connection;
The light source (1), condenser (2), collimator objective (3), gular transparent container (4) and integrating sphere (5) are sequentially arranged.
2. a kind of body refuse settling ratio according to claim 1 and body refuse active testing instrument, it is characterized in that:The light source (1), The condenser (2), the collimator objective (3), the gular transparent container (4) and the integrating sphere (5) are sequentially arranged in bottom On seat (7).
3. a kind of body refuse settling ratio according to claim 1 and body refuse active testing instrument, it is characterized in that:The light source (1) For infrared light supply.
4. a kind of body refuse settling ratio and body refuse activity test method, using a kind of body refuse settling ratio as described in claim 1 and Body refuse active testing instrument, it is characterized in that:Include the following steps,
Step 1: water to be measured is poured into gular transparent container (4), static -100 minutes 30 minutes;
Step 2: opening the light source (1), gular transparent container (4) obtains the irradiation light that intensity is Tr, while obtaining by water sample The luminous intensity Tx absorbed with gular transparent container (4), the luminous intensity Ts that is scattered and through water sample and gular transparent container (4) Luminous intensity Tt, i.e.,:
Tr=Tt+Tx+Ts, wherein Tr is the intensity of incident light, Tt is the luminous intensity penetrated, Tx is the luminous intensity absorbed, Ts is The luminous intensity of scattering;
Step 3: obtaining the transmittivity Д t, i.e. Д t=100% × Tt/ (Tt+Tx+Ts) of light;The scattering ratio Д s of light, i.e., Д s=100% × Ts/ (Tt+Tx+Ts);
Step 4: the total height for obtaining gular transparent container (4) interior liquid is L, then there is L=Ls+Ln=Ls+Lns+Lnc+Lnj, Wherein, L is liquid total height, Ls is water layer height, Lns is weaker zone body refuse height, Lnc is sublevel body refuse height, Lnj is tight Close layer body refuse height;
Step 5: computer obtains body refuse settling ratio:Ct=100% × (Lnc+Lnj)/L, body refuse activity:H=100% × (Lns+Lnc)/(Lns+Lnc+Lnj);
Step 6: the computer (6) obtains body refuse settling ratio quantitative identification foundation, when Д t 3% or 2%≤Д of > t≤ 3%, when Д s/ Д t < 60, the corresponding optical len of integrating sphere (5) is divided into water layer height Ls;
When the corresponding optical len of 2%≤Д t≤3% and t >=60 Д s/ Д is divided into weaker zone body refuse height Lns.
As 1%≤Д t < 2%, 100 corresponding optical lens of Д s/ Д t < are divided into sublevel body refuse height Lnc.
As 1%≤Д t < 2%, t >=100 s/ Д Д or 1% corresponding optical lens of Д t < are divided into close layer body refuse height Lnj;
Step 7: the computer (6) obtains body refuse activity qualitative discrimination foundation, as h > 80%, body refuse characteristic is high activity Body refuse;When 60%≤h≤80%, body refuse characteristic is moderate activity body refuse;As 40%≤h < 60%, body refuse characteristic is low living Property body refuse;As h < 40%, body refuse characteristic is ultralow degree active sludge.
CN201810143960.1A 2018-02-12 2018-02-12 A kind of body refuse settling ratio and body refuse active testing instrument and test method Pending CN108398362A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114088592A (en) * 2021-11-24 2022-02-25 西安西热水务环保有限公司 Automatic correction device and method for floc sedimentation ratio measuring device

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103528797A (en) * 2013-10-22 2014-01-22 长春四叶之义科技有限公司 Novel system for detecting transmittance and reflectivity of lens of optical system

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103528797A (en) * 2013-10-22 2014-01-22 长春四叶之义科技有限公司 Novel system for detecting transmittance and reflectivity of lens of optical system

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114088592A (en) * 2021-11-24 2022-02-25 西安西热水务环保有限公司 Automatic correction device and method for floc sedimentation ratio measuring device
CN114088592B (en) * 2021-11-24 2024-05-07 西安西热水务环保有限公司 Automatic correction device and method for floc sedimentation ratio measuring device

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