CN108355501A - A kind of demulsifier pipeline filling and mixing device - Google Patents

A kind of demulsifier pipeline filling and mixing device Download PDF

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Publication number
CN108355501A
CN108355501A CN201810045836.1A CN201810045836A CN108355501A CN 108355501 A CN108355501 A CN 108355501A CN 201810045836 A CN201810045836 A CN 201810045836A CN 108355501 A CN108355501 A CN 108355501A
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Prior art keywords
demulsifier
mixing
dosing
crude oil
mixing arrangement
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CN201810045836.1A
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CN108355501B (en
Inventor
苑慧莹
周志平
李琼玮
杨立华
杨会丽
奚运涛
李慧
刘爱华
王小勇
孙雨来
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Petrochina Co Ltd
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Petrochina Co Ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/40Mixing liquids with liquids; Emulsifying
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/30Injector mixers
    • B01F25/31Injector mixers in conduits or tubes through which the main component flows
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/71Feed mechanisms
    • B01F35/717Feed mechanisms characterised by the means for feeding the components to the mixer
    • B01F35/7179Feed mechanisms characterised by the means for feeding the components to the mixer using sprayers, nozzles or jets
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/71Feed mechanisms
    • B01F35/717Feed mechanisms characterised by the means for feeding the components to the mixer
    • B01F35/71805Feed mechanisms characterised by the means for feeding the components to the mixer using valves, gates, orifices or openings
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G33/00Dewatering or demulsification of hydrocarbon oils
    • C10G33/04Dewatering or demulsification of hydrocarbon oils with chemical means
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F2101/00Mixing characterised by the nature of the mixed materials or by the application field
    • B01F2101/40Mixing of ingredients for oils, fats or waxes

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)

Abstract

The invention discloses a demulsifier pipeline filling and mixing device, which consists of a medicament distributor and a mixing chamber, and comprises a cylindrical pipe body connected in a fluid pipeline through a flange, wherein an annular dosing center distribution chamber is arranged at a channel inlet of the mixer, a plurality of evenly distributed dosing branch pipes which are communicated with the dosing center distribution chamber and are provided with medicament outlet holes are arranged around the inner wall of the dosing center distribution chamber and extend towards the center of the pipe body, and the dosing branch pipes are perpendicular to the incoming liquid direction of the pipe body and point to the center of the pipe body; the medicine feeding central distribution chamber is connected with a medicine feeding main pipe communicated with a medicine source; the medicine feeding branch pipes are uniformly distributed with medicine feeding holes, and the pipe openings are covered with sealing caps. The mixing chamber is made by the steel pipe of cask shape area slot, and this device can realize demulsifier and crude oil emulsion intensive mixing, simultaneously through reducing the crude oil emulsion emulsification scheduling problem that causes because factors such as pressure reduction when getting into the centralized processing ware seriously, through field test prove, can effectively reduce more than 20% demulsifier quantity after using this medicine mixing arrangement that adds.

Description

一种破乳剂管道加注混合装置A kind of demulsifier pipeline filling and mixing device

技术领域technical field

本发明属于油田原油破乳脱水领域,涉及一种破乳剂管道加注混合装置。The invention belongs to the field of oilfield crude oil demulsification and dehydration, and relates to a demulsifier pipeline filling and mixing device.

背景技术Background technique

通过加入破乳剂实现原油破乳脱水因其具有较高的经济性而成为石油行业应用最普遍的原油脱水技术。破乳剂通过均匀分布到原油乳状液中实现乳化液滴界面膜破裂实现水滴的聚并、沉降,从而达到脱水的目的。常规的破乳剂加注工艺导致大量的破乳剂因重力和亲水性的影响,使其大部分直接融入管道底部的水相中,无法有效分散至中上部油水乳状液中,导致现场破乳剂有效利用率低。实现破乳剂在原油乳状液中均匀分散,是提高矿场破乳剂使用率的关键。Demulsification and dehydration of crude oil by adding demulsifiers has become the most common crude oil dehydration technology in the petroleum industry because of its high economic efficiency. The demulsifier achieves the purpose of dehydration by evenly distributing into the crude oil emulsion to break the interface film of the emulsified droplets to realize the coalescence and sedimentation of water droplets. The conventional demulsifier filling process results in a large amount of demulsifier being directly integrated into the water phase at the bottom of the pipeline due to the influence of gravity and hydrophilicity, and cannot be effectively dispersed into the oil-water emulsion in the middle and upper parts, resulting in the on-site demulsifier being effective. Low utilization. Realizing the uniform dispersion of the demulsifier in the crude oil emulsion is the key to improving the utilization rate of the demulsifier in the mine.

发明内容Contents of the invention

本发明的目的在于克服上述现有技术的缺点,提供一种破乳剂管道加注混合装置,该装置可以保证破乳剂与原油乳状液充分混合的同时,降低由于流体进入脱水装置前受压降变化影响,产生非均匀的剪切而导致乳状液与脱出水的二次混合乳化。The purpose of the present invention is to overcome the above-mentioned shortcomings of the prior art, and provide a demulsifier pipeline filling and mixing device, which can ensure that the demulsifier and the crude oil emulsion are fully mixed, and at the same time reduce the pressure drop change due to the fluid entering the dehydration device Influenced by non-uniform shearing, resulting in the secondary mixing and emulsification of the emulsion and the extracted water.

为达到上述目的,本发明采用以下技术方案予以实现:In order to achieve the above object, the present invention adopts the following technical solutions to achieve:

一种破乳剂管道加注混合装置,包括安装于原油脱水系统前端的混合筒,混合室的前端为原油流入口,后端为原油流出口;混合筒的中部设置有混合室,混合室与原油流入口之间筒壁上开设有破乳剂加注口,筒壁内为加药室,加药室与破乳剂加注口相连通。A demulsifier pipeline filling and mixing device, including a mixing cylinder installed at the front end of the crude oil dehydration system, the front end of the mixing chamber is the crude oil inflow inlet, and the rear end is the crude oil outflow outlet; the middle part of the mixing cylinder is provided with a mixing chamber, which is connected with the crude oil A demulsifier filling port is opened on the cylinder wall between the inflow ports, and a dosing chamber is inside the cylinder wall, and the dosing chamber communicates with the demulsifier filling port.

本发明进一步的改进在于:The further improvement of the present invention is:

加药室为围绕筒壁向中心呈辐射状分布的若干喷淋管。The dosing chamber is a number of spray pipes radially distributed around the cylinder wall to the center.

喷淋管的直径为8mm,长度为24mm,且表面均匀分布有若干直径为0.8mm的圆孔。The diameter of the spray pipe is 8mm, the length is 24mm, and a number of circular holes with a diameter of 0.8mm are evenly distributed on the surface.

喷淋管的管口设置有密封帽。The nozzle of the spray pipe is provided with a sealing cap.

喷淋管的数量为8个。The number of spray pipes is 8.

混合室为垂直于混合筒的中空圆柱体。The mixing chamber is a hollow cylinder perpendicular to the mixing cylinder.

中空圆柱体上开设有若干缝隙。Several gaps are opened on the hollow cylinder.

圆柱体的长度为154mm,直径为137mm,壁厚为7.1mm。The cylinder has a length of 154 mm, a diameter of 137 mm and a wall thickness of 7.1 mm.

缝隙的宽度为3mm,长度为110mm。The slot has a width of 3 mm and a length of 110 mm.

缝隙为割缝,共开设有六组;其中,四组由5个割缝组成;二组由16个割缝组成。The gaps are slits, and there are six groups in total; among them, the fourth group is composed of 5 slits; the second group is composed of 16 slits.

与现有技术相比,本发明具有以下有益效果:Compared with the prior art, the present invention has the following beneficial effects:

本发明通过法兰连接在流体管道中的圆筒形管体,在混合器的通道入口处设有环形加药中心分配室,环绕所述加药中心分配室内壁向管体中心延伸并均布的多根与加药中心分配室连通的设有出药孔的加药支管,加药支管垂直于管体的来液方向指向管体中心;加药中心分配室连有连通药源的供药总管;加药支管均匀分布加药孔,同时管口盖有密封帽。混合室由圆桶形带割缝钢管制成,本装置可以实现破乳剂与原油乳状液充分混合,同时通过减少进入集中处理器时由于压力降低等因素引起的原油乳状液乳化严重等问题,通过现场试验证明,应用该加药混合装置后可以有效降低破乳剂用量20%以上。The present invention connects the cylindrical pipe body in the fluid pipeline through the flange, and an annular dosing center distribution chamber is arranged at the channel entrance of the mixer, and the inner wall of the dosing center distribution chamber extends to the center of the pipe body and is uniformly distributed around the dosing center distribution chamber. There are multiple dosing branch pipes with drug outlet holes connected to the distribution room of the dosing center. The dosing branch pipes are perpendicular to the direction of the incoming liquid of the pipe body and point to the center of the pipe body; the distribution room of the dosing center is connected to the drug supply connected to the drug source The main pipe; the dosing branch pipe evenly distributes the dosing holes, and the nozzle is covered with a sealing cap. The mixing chamber is made of a barrel-shaped steel pipe with slots. This device can realize the full mixing of the demulsifier and the crude oil emulsion. At the same time, it can reduce the serious emulsification of the crude oil emulsion caused by factors such as pressure drop when entering the centralized processor. The field test proves that the dosage of the demulsifier can be effectively reduced by more than 20% after the application of the dosing and mixing device.

附图说明Description of drawings

图1为破乳剂管道加注混合装置结构示意图;Fig. 1 is a structural schematic diagram of a demulsifier pipeline filling and mixing device;

图2为破乳剂加注系统左视图。Figure 2 is a left view of the demulsifier filling system.

其中,1-破乳剂加注口;2-破乳剂加注系统;3-混合室;4-混合筒。Among them, 1-demulsifier filling port; 2-demulsifier filling system; 3-mixing chamber; 4-mixing cylinder.

具体实施方式Detailed ways

下面结合附图对本发明做进一步详细描述:The present invention is described in further detail below in conjunction with accompanying drawing:

参见图1和图2,本发明破乳剂管道加注混合装置,包括安装于原油管道上的混合筒4,混合室3的前端为原油流入口,后端为原油流出口;混合筒4的中部设置有混合室3;混合室3为垂直于混合筒4的中空圆柱体。中空圆柱体上开设有若干缝隙。加药室为围绕管道外壁向管道中心呈辐射状分布的加药喷淋管;加药喷淋管垂直于轴向延伸至管体中心均匀分布;混合室外形为与管道垂直连接的圆柱形管体;混合室由割缝钢制管体构成,该钢制管体安设计分布着宽度一定的割缝。有8根加药喷淋管围绕管道外壁向管道中心呈辐射状分布,每根喷淋管长24mm,直径8mm,上面均匀分布有10个直径为0.8mm的圆孔,同时管口盖有密封帽。加药喷淋管垂直于轴向延伸至管体中心均匀分布。该圆柱体长度为154mm,直径为137mm,壁厚为10mm。混合室内设计有可以按照管道流体压力手动调节的稳压混合装置,该混合装置由一个管柱型钢管制成,钢管外径127mm,壁厚7.1mm,管体分布有特定宽度和长度的缝隙。混合装置分布的割缝宽度为3mm,长度为110mm。混合装置共有6组割缝,其中有4组割缝由5个宽为3mm,长度为110mm的割缝组成,2组割缝由16个宽为3mm,长度为110mm的割缝组成。Referring to Fig. 1 and Fig. 2, the demulsifier pipeline filling and mixing device of the present invention includes a mixing cylinder 4 installed on the crude oil pipeline, the front end of the mixing chamber 3 is the crude oil inflow inlet, and the rear end is the crude oil outflow outlet; the middle part of the mixing cylinder 4 A mixing chamber 3 is provided; the mixing chamber 3 is a hollow cylinder perpendicular to the mixing cylinder 4 . Several gaps are opened on the hollow cylinder. The dosing chamber is a dosing spray pipe radially distributed around the outer wall of the pipe to the center of the pipe; the dosing spray pipe extends perpendicular to the axial direction to the center of the pipe body and is evenly distributed; the shape of the mixing chamber is a cylindrical pipe vertically connected to the pipe body; the mixing chamber is composed of a slotted steel pipe body, and the steel pipe body is designed with slots of a certain width. There are 8 dosing spray pipes distributed radially around the outer wall of the pipe to the center of the pipe. Each spray pipe is 24mm long and 8mm in diameter. There are 10 round holes with a diameter of 0.8mm evenly distributed on it. At the same time, the nozzle cover is sealed. cap. The dosing spray pipe extends vertically to the center of the pipe body and distributes evenly. The cylinder has a length of 154 mm, a diameter of 137 mm and a wall thickness of 10 mm. The mixing chamber is designed with a pressure-stabilizing mixing device that can be manually adjusted according to the fluid pressure in the pipeline. The mixing device is made of a cylindrical steel pipe with an outer diameter of 127mm and a wall thickness of 7.1mm. The pipe body is distributed with gaps of specific width and length. The slits distributed by the mixing device have a width of 3 mm and a length of 110 mm. There are 6 groups of slots in the mixing device, of which 4 groups of slots are composed of 5 slots with a width of 3 mm and a length of 110 mm, and two groups of slots are composed of 16 slots with a width of 3 mm and a length of 110 mm.

本发明的原理:Principle of the present invention:

本发明围绕管道外壁向管道中心呈辐射状分布有8根加药喷淋管,每根喷淋管长24mm,直径8mm,上面均匀分布有10个直径为0.8mm的圆孔,同时管口盖有密封帽。混合室为圆柱体,该圆柱体长度为154mm,直径为137mm,壁厚为10mm。混合室内设计有可以按照管道流体压力手动调节的稳压混合装置,该混合装置由一个管柱型钢管制成,钢管外径127mm,壁厚7.1mm,管体分布有特定宽度和长度的缝隙。混合装置共有6组割缝,其中有4组割缝由5个宽为3mm,长度为110mm的割缝组成,2组割缝由16个宽为3mm,长度为110mm的割缝组成。In the present invention, 8 dosing spray pipes are radially distributed around the outer wall of the pipe to the center of the pipe. Each spray pipe is 24mm long and 8mm in diameter, and 10 round holes with a diameter of 0.8mm are evenly distributed on it. With sealing cap. The mixing chamber is a cylinder with a length of 154 mm, a diameter of 137 mm and a wall thickness of 10 mm. The mixing chamber is designed with a pressure-stabilizing mixing device that can be manually adjusted according to the fluid pressure in the pipeline. The mixing device is made of a cylindrical steel pipe with an outer diameter of 127mm and a wall thickness of 7.1mm. The pipe body is distributed with gaps of specific width and length. There are 6 groups of slots in the mixing device, of which 4 groups of slots are composed of 5 slots with a width of 3 mm and a length of 110 mm, and two groups of slots are composed of 16 slots with a width of 3 mm and a length of 110 mm.

本发明的工作过程:Working process of the present invention:

工作时将本发明通过法兰安装在原油脱水系统前端,破乳剂加注系统设计有围绕管道外壁向管道中心呈辐射状分布有8根加药喷淋管,这样生成的射流可以使破乳剂尽量均匀的分散到管道内的原油乳状液中,加注破乳剂后的流体随后进入混合室,混合室入口通过设计实现高剪切流条件,从而达到较低或中度压力下降的目的。在混合室出口,设计的出口渠道使多相流混合物的均匀分布于管道,从而避免新的油水乳状液液滴的产生。When working, the invention is installed on the front end of the crude oil dehydration system through the flange. The demulsifier filling system is designed with 8 dosing spray pipes radially distributed around the outer wall of the pipeline to the center of the pipeline, so that the generated jet can make the demulsifier as much as possible. Evenly dispersed into the crude oil emulsion in the pipeline, the fluid filled with demulsifier then enters the mixing chamber, and the inlet of the mixing chamber is designed to achieve high shear flow conditions, so as to achieve the purpose of low or moderate pressure drop. At the outlet of the mixing chamber, the outlet channel is designed so that the multiphase flow mixture is evenly distributed in the pipeline, thereby avoiding the generation of new oil-water emulsion droplets.

以上内容仅为说明本发明的技术思想,不能以此限定本发明的保护范围,凡是按照本发明提出的技术思想,在技术方案基础上所做的任何改动,均落入本发明权利要求书的保护范围之内。The above content is only to illustrate the technical ideas of the present invention, and cannot limit the protection scope of the present invention. Any changes made on the basis of the technical solutions according to the technical ideas proposed in the present invention shall fall within the scope of the claims of the present invention. within the scope of protection.

Claims (10)

1. a kind of demulsifier pipeline fills mixing arrangement, which is characterized in that the mixing including being installed on crude oil dehydrating system front end The front end of cylinder (4), mixing chamber (3) is crude oil inflow entrance, and rear end is crude oil outflux;Mixing drum is provided with mixing in the middle part of (4) Room (3) offers demulsifier filler (1) on barrel between mixing chamber (3) and crude oil inflow entrance, be dosing room (2) in barrel, Dosing room (2) is connected with demulsifier filler (1).
2. demulsifier pipeline according to claim 1 fills mixing arrangement, which is characterized in that dosing room (2) are around cylinder Wall is to the radially distributed several spray tubes (6) in center.
3. demulsifier pipeline according to claim 2 fills mixing arrangement, which is characterized in that spray tube (6) it is a diameter of 8mm, length 24mm, and surface is evenly distributed with the circular hole of several a diameter of 0.8mm.
4. demulsifier pipeline according to claim 2 or 3 fills mixing arrangement, which is characterized in that the nozzle of spray tube (6) It is provided with seal cap.
5. demulsifier pipeline according to claim 2 or 3 fills mixing arrangement, which is characterized in that the quantity of spray tube (6) It is 8.
6. demulsifier pipeline according to claim 1 fills mixing arrangement, which is characterized in that mixing chamber (3) be perpendicular to The hollow cylinder of mixing drum (4).
7. demulsifier pipeline according to claim 1 fills mixing arrangement, which is characterized in that offered on hollow cylinder Several gaps.
8. demulsifier pipeline described according to claim 6 or 7 fills mixing arrangement, which is characterized in that the length of cylinder is 154mm, a diameter of 137mm, wall thickness 7.1mm.
9. demulsifier pipeline according to claim 7 fills mixing arrangement, which is characterized in that the width in gap is 3mm, long Degree is 110mm.
10. the demulsifier pipeline according to claim 7 or 9 fills mixing arrangement, which is characterized in that gap is slot, altogether Offer six groups;Wherein, it is made of 5 slots for four groups;Two groups are made of 16 slots.
CN201810045836.1A 2018-01-17 2018-01-17 Demulsifier pipeline filling and mixing device Active CN108355501B (en)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112899010A (en) * 2021-01-12 2021-06-04 森诺技术有限公司 Circular solution liquid injection device

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