CN108341648A - A kind of wall waterproof fireproofing thermal insulation material and preparation method thereof - Google Patents

A kind of wall waterproof fireproofing thermal insulation material and preparation method thereof Download PDF

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Publication number
CN108341648A
CN108341648A CN201810388416.3A CN201810388416A CN108341648A CN 108341648 A CN108341648 A CN 108341648A CN 201810388416 A CN201810388416 A CN 201810388416A CN 108341648 A CN108341648 A CN 108341648A
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Prior art keywords
parts
thermal insulation
insulation material
waterproof fireproofing
fireproofing thermal
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CN201810388416.3A
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Chinese (zh)
Inventor
谭群英
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Hefei Jin Yunxin Materials Co Ltd
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Hefei Jin Yunxin Materials Co Ltd
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Priority to CN201810388416.3A priority Critical patent/CN108341648A/en
Publication of CN108341648A publication Critical patent/CN108341648A/en
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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B28/00Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
    • C04B28/02Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
    • C04B28/06Aluminous cements
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/20Resistance against chemical, physical or biological attack
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/20Resistance against chemical, physical or biological attack
    • C04B2111/27Water resistance, i.e. waterproof or water-repellent materials
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/20Resistance against chemical, physical or biological attack
    • C04B2111/28Fire resistance, i.e. materials resistant to accidental fires or high temperatures
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/40Porous or lightweight materials

Abstract

The invention discloses the raw material compositions of a kind of wall waterproof fireproofing thermal insulation material and preparation method thereof, including following parts by weight:12 18 parts of 10 20 parts of cement, 30 50 parts of expanded perlite, 15 25 parts of porous ceramic grain, 7 15 parts of composite reinforcing fiber, 6 14 parts of sepiolite powder, 4 10 parts of mica powder, 15 parts of waterproofing agent, 25 parts of dispersant, 0.5 3.5 parts of thickener and water.The present invention selects natural inorganic material, tasteless, pollution-free nonirritant, and good waterproof performance, thermal coefficient are small, and coefficient of heat insulation is big, adhesion strength height not only energy conservation and environmental protection but also safe and applicable.

Description

A kind of wall waterproof fireproofing thermal insulation material and preparation method thereof
Technical field
The present invention relates to building material technical fields, and in particular to a kind of wall waterproof fireproofing thermal insulation material and its preparation Method.
Background technology
With the continuous change of people's living environment, heat-insulated, the warming effect in house is also continuously improved in people, and shows The materials for wall occurred on the market is all made of the materials such as the materials such as polyphenyl, polyurethane, foam glass and is made, the heat preservation of these materials Effect is poor, and heat insulation is low, and heat preservation and energy-saving effect are poor, in addition to insulative effectiveness is low also not environmentally, and with less fire protecting performance, The easily aging of manufactured product, and materials for wall is expensive, increases the consumption standard of people, the technique in production process Also complicated.Single insulating wall material does not have fireproof performance, the raising with China to wall fire-protection standard, wall material The fire protecting performance of material closes the life and health of people especially, and it is that current China's building is gone in the material of one to solve wall fire prevention with heat preservation Industry technical problem urgently to be resolved hurrily.
Invention content
Technical problem to be solved by the invention is to provide a kind of energy saving, waterproof, heat preservation, heat-insulated wall waterproof fireproofings Thermal insulation material.
In order to achieve the above object, the present invention is achieved through the following technical solutions:
A kind of wall waterproof fireproofing thermal insulation material includes the raw material composition of following parts by weight:10-20 parts of cement, expansion are precious 30-50 parts of pearl rock, 7-15 parts of composite reinforcing fiber, 6-14 parts of sepiolite powder, 4-10 parts of mica powder, is prevented 15-25 parts of porous ceramic grain 12-18 parts of 1-5 parts of aqua, 2-5 parts of dispersant, 0.5-3.5 parts of thickener and water.
Preferably, including the raw material of following parts by weight forms:15 parts of cement, 40 parts of expanded perlite, porous ceramic grain 20 Part, 11 parts of composite reinforcing fiber, 10 parts of sepiolite powder, 7 parts of mica powder, 3 parts of waterproofing agent, 3.5 parts of dispersant, 2 parts of thickener and 15 parts of water.
Preferably, the cement is aluminosilicate cement.
Preferably, the expanded perlite is water-proof charing closed-cell expanded perlite, and grain size 0.6-1.2mm, unit weight is 100-200kg/m3, 9-14 times of expansion multiple.
Preferably, the porous ceramic grain is using flyash as the porous ceramic grain of main material, grain size 10-15mm.
Preferably, it is 2-4 that the composite reinforcing fiber, which is weight ratio,:1 carbon fiber and the composition of polyimide fiber.
Preferably, the waterproofing agent is calcium stearate, aluminum stearate or sodium methyl silicate.
Preferably, the dispersant is calgon.
Preferably, the thickener is cellulose ether.
The present invention also provides the above-mentioned wall preparation methods of waterproof fireproofing thermal insulation material, include the following steps:
(1)In parts by weight, 10- is mixed in the expanded perlite weighed up, porous ceramic grain, sepiolite powder, mica powder first Then 20min adds water and waterproofing agent to stir 3-5min, add cement, thickener stirring 3-5min, obtain mixture slurry;
(2)Above-mentioned mixture slurry is heated to 60-70 degree and keeps the temperature 20-30min, composite strengthening is added after being then cooled to room temperature Fiber and dispersant, continue stirring until fiber dispersity it is good, without conglomeration, obtain fibrous mixture slurry;
(3)By step(2)Gained mixture slurry pours into die for molding, is demoulded after standing 4-6h, and it is 25 degree, humidity to be put into temperature 90% or more fog room carries out standard curing 28d to get wall waterproof fireproofing thermal insulation material.
Compared with prior art, the present invention having following advantageous effect:
(1)Wall provided by the invention waterproof fireproofing thermal insulation material selects natural inorganic material, tasteless, pollution-free stingless Swash property, and good permeability, thermal coefficient are small, and coefficient of heat insulation is big, adhesion strength height not only energy conservation and environmental protection but also safe and applicable.
(2)The wall provided in the present invention waterproof fireproofing thermal insulation material, energy saving, insulation good flame retardation effect, Ageing-resistant intensity is good, resistance to compression coefficient is high, anti crack performance is good, cheap, applied widely, saves production cost.
(3)The wall provided in the present invention waterproof fireproofing thermal insulation material, preparation method is simple, easily operated, convenient for applying Work, do not need binder directly can be applied to all kinds of base course walls by insulating wall material, be firmly bonded, do not crack, extend The service life of wall.
Specific implementation mode
Form by the following examples is described in further detail the above of the present invention again, but should not be by this The range for being interpreted as the above-mentioned theme of the present invention is only limitted to following embodiment, all based on the technology realized belonging to the above of the present invention It all belongs to the scope of the present invention.
Embodiment 1
A kind of wall waterproof fireproofing thermal insulation material includes the raw material composition of following parts by weight:10 parts of cement, expanded perlite 30 parts, 15 parts of porous ceramic grain, 7 parts of composite reinforcing fiber, 6 parts of sepiolite powder, 4 parts of mica powder, 1 part of waterproofing agent, 2 parts of dispersant, 12 parts of 0.5 part of thickener and water.
Wherein, the cement is aluminosilicate cement.
Wherein, the expanded perlite is water-proof charing closed-cell expanded perlite, and grain size 0.6-1.2mm, unit weight is 100-200kg/m3, 9-14 times of expansion multiple.
Wherein, the porous ceramic grain is using flyash as the porous ceramic grain of main material, grain size 10-15mm.
Wherein, it is 2 that the composite reinforcing fiber, which is weight ratio,:1 carbon fiber and the composition of polyimide fiber.
Wherein, the waterproofing agent is calcium stearate.
Wherein, the dispersant is calgon.
Wherein, the thickener is cellulose ether.
The present invention also provides the above-mentioned wall preparation methods of waterproof fireproofing thermal insulation material, include the following steps:
(1)In parts by weight, the expanded perlite weighed up, porous ceramic grain, sepiolite powder, mica powder are mixed first Then 10min adds water and waterproofing agent to stir 3min, add cement, thickener stirring 3min, obtain mixture slurry;
(2)Above-mentioned mixture slurry is heated to 60 degree and keeps the temperature 20min, be then cooled to after room temperature be added composite reinforcing fiber and Dispersant, continue stirring until fiber dispersity it is good, without conglomeration, obtain fibrous mixture slurry;
(3)By step(2)Gained mixture slurry pours into die for molding, is demoulded after standing 4h, and it is 25 degree, humidity to be put into temperature 90% or more fog room carries out standard curing 28d to get wall waterproof fireproofing thermal insulation material.
Embodiment 2
A kind of wall waterproof fireproofing thermal insulation material includes the raw material composition of following parts by weight:20 parts of cement, expanded perlite 50 parts, 25 parts of porous ceramic grain, 15 parts of composite reinforcing fiber, 14 parts of sepiolite powder, 10 parts of mica powder, 5 parts of waterproofing agent, dispersant 5 18 parts of part, 3.5 parts of thickener and water.
Wherein, the cement is aluminosilicate cement.
Wherein, the expanded perlite is water-proof charing closed-cell expanded perlite, and grain size 0.6-1.2mm, unit weight is 100-200kg/m3, 9-14 times of expansion multiple.
Wherein, the porous ceramic grain is using flyash as the porous ceramic grain of main material, grain size 10-15mm.
Wherein, it is 4 that the composite reinforcing fiber, which is weight ratio,:1 carbon fiber and the composition of polyimide fiber.
Wherein, the waterproofing agent is aluminum stearate.
Wherein, the dispersant is calgon.
Preferably, the thickener is cellulose ether.
The present invention also provides the above-mentioned wall preparation methods of waterproof fireproofing thermal insulation material, include the following steps:
(1)In parts by weight, the expanded perlite weighed up, porous ceramic grain, sepiolite powder, mica powder are mixed first Then 20min adds water and waterproofing agent to stir 5min, add cement, thickener stirring 5min, obtain mixture slurry;
(2)Above-mentioned mixture slurry is heated to 70 degree and keeps the temperature 30min, be then cooled to after room temperature be added composite reinforcing fiber and Dispersant, continue stirring until fiber dispersity it is good, without conglomeration, obtain fibrous mixture slurry;
(3)By step(2)Gained mixture slurry pours into die for molding, is demoulded after standing 6h, and it is 25 degree, humidity to be put into temperature 90% or more fog room carries out standard curing 28d to get wall waterproof fireproofing thermal insulation material.
Embodiment 3
A kind of wall waterproof fireproofing thermal insulation material includes the raw material composition of following parts by weight:15 parts of cement, expanded perlite 40 parts, 20 parts of porous ceramic grain, 11 parts of composite reinforcing fiber, 10 parts of sepiolite powder, 7 parts of mica powder, 3 parts of waterproofing agent, dispersant 3.5 15 parts of part, 2 parts of thickener and water.
Wherein, the cement is aluminosilicate cement.
Wherein, the expanded perlite is water-proof charing closed-cell expanded perlite, and grain size 0.6-1.2mm, unit weight is 100-200kg/m3, 9-14 times of expansion multiple.
Wherein, the porous ceramic grain is using flyash as the porous ceramic grain of main material, grain size 10-15mm.
Wherein, it is 2.5 that the composite reinforcing fiber, which is weight ratio,:1 carbon fiber and the composition of polyimide fiber.
Wherein, the waterproofing agent is sodium methyl silicate.
Wherein, the dispersant is calgon.
Preferably, the thickener is cellulose ether.
The present invention also provides the above-mentioned wall preparation methods of waterproof fireproofing thermal insulation material, include the following steps:
(1)In parts by weight, the expanded perlite weighed up, porous ceramic grain, sepiolite powder, mica powder are mixed first Then 13min adds water and waterproofing agent to stir 4.5min, add cement, thickener stirring 3.5min, obtain mixture slurry;
(2)Above-mentioned mixture slurry is heated to 62 degree and keeps the temperature 27min, be then cooled to after room temperature be added composite reinforcing fiber and Dispersant, continue stirring until fiber dispersity it is good, without conglomeration, obtain fibrous mixture slurry;
(3)By step(2)Gained mixture slurry pours into die for molding, is demoulded after standing 5.5h, and it is 25 degree, humidity to be put into temperature 90% or more fog room carries out standard curing 28d to get wall waterproof fireproofing thermal insulation material.
Embodiment 4
A kind of wall waterproof fireproofing thermal insulation material includes the raw material composition of following parts by weight:18 parts of cement, expanded perlite 45 parts, 18 parts of porous ceramic grain, 9 parts of composite reinforcing fiber, 8 parts of sepiolite powder, 8 parts of mica powder, 2 parts of waterproofing agent, 4 parts of dispersant, 14 parts of 1 part of thickener and water.
Wherein, the cement is aluminosilicate cement.
Wherein, the expanded perlite is water-proof charing closed-cell expanded perlite, and grain size 0.6-1.2mm, unit weight is 100-200kg/m3, 9-14 times of expansion multiple.
Wherein, the porous ceramic grain is using flyash as the porous ceramic grain of main material, grain size 10-15mm.
Wherein, it is 3 that the composite reinforcing fiber, which is weight ratio,:1 carbon fiber and the composition of polyimide fiber.
Wherein, the waterproofing agent is calcium stearate.
Wherein, the dispersant is calgon.
Wherein, the thickener is cellulose ether.
The present invention also provides the above-mentioned wall preparation methods of waterproof fireproofing thermal insulation material, include the following steps:
(1)In parts by weight, the expanded perlite weighed up, porous ceramic grain, sepiolite powder, mica powder are mixed first Then 15min adds water and waterproofing agent to stir 4min, add cement, thickener stirring 4min, obtain mixture slurry;
(2)Above-mentioned mixture slurry is heated 65 degree and keeps the temperature 25min, composite reinforcing fiber is added after being then cooled to room temperature and is divided Powder, continue stirring until fiber dispersity it is good, without conglomeration, obtain fibrous mixture slurry;
(3)By step(2)Gained mixture slurry pours into die for molding, is demoulded after standing 5h, and it is 25 degree, humidity to be put into temperature 90% or more fog room carries out standard curing 28d to get wall waterproof fireproofing thermal insulation material.
Embodiment 5
A kind of wall waterproof fireproofing thermal insulation material includes the raw material composition of following parts by weight:12 parts of cement, expanded perlite 35 parts, 22 parts of porous ceramic grain, 12 parts of composite reinforcing fiber, 8 parts of sepiolite powder, 7 parts of mica powder, 2 parts of waterproofing agent, 3 parts of dispersant, 16 parts of 2 parts of thickener and water.
Wherein, the cement is aluminosilicate cement.
Wherein, the expanded perlite is water-proof charing closed-cell expanded perlite, and grain size 0.6-1.2mm, unit weight is 100-200kg/m3, 9-14 times of expansion multiple.
Wherein, the porous ceramic grain is using flyash as the porous ceramic grain of main material, grain size 10-15mm.
Wherein, it is 2-4 that the composite reinforcing fiber, which is weight ratio,:1 carbon fiber and the composition of polyimide fiber.
Wherein, the waterproofing agent is sodium methyl silicate.
Wherein, the dispersant is calgon.
Wherein, the thickener is cellulose ether.
The present invention also provides the above-mentioned wall preparation methods of waterproof fireproofing thermal insulation material, include the following steps:
(1)In parts by weight, the expanded perlite weighed up, porous ceramic grain, sepiolite powder, mica powder are mixed first Then 10min adds water and waterproofing agent to stir 5min, add cement, thickener stirring 5min, obtain mixture slurry;
(2)Above-mentioned mixture slurry is heated to 62 degree and keeps the temperature 22min, be then cooled to after room temperature be added composite reinforcing fiber and Dispersant, continue stirring until fiber dispersity it is good, without conglomeration, obtain fibrous mixture slurry;
(3)By step(2)Gained mixture slurry pours into die for molding, is demoulded after standing 4.5h, and it is 25 degree, humidity to be put into temperature 90% or more fog room carries out standard curing 28d to get wall waterproof fireproofing thermal insulation material.
In conclusion wall provided by the invention waterproof fireproofing thermal insulation material, natural inorganic material is selected, tasteless, Pollution-free nonirritant, and good permeability, thermal coefficient are small, coefficient of heat insulation is big, adhesion strength height not only energy conservation and environmental protection but also safety It is applicable in.
The foregoing is only a preferred embodiment of the present invention, is not intended to restrict the invention, although with reference to aforementioned reality Applying example, invention is explained in detail, for those skilled in the art, still can be to aforementioned each implementation Technical solution recorded in example is modified or equivalent replacement of some of the technical features.All essences in the present invention With within principle, any modification, equivalent replacement, improvement and so on should all be included in the protection scope of the present invention god.

Claims (10)

1. a kind of wall waterproof fireproofing thermal insulation material, which is characterized in that the raw material composition including following parts by weight:Cement 10-20 parts, 30-50 parts of expanded perlite, 15-25 parts of porous ceramic grain, 7-15 parts of composite reinforcing fiber, 6-14 parts of sepiolite powder, 12-18 parts of 4-10 parts of mica powder, 1-5 parts of waterproofing agent, 2-5 parts of dispersant, 0.5-3.5 parts of thickener and water.
2. wall according to claim 1 waterproof fireproofing thermal insulation material, which is characterized in that including following parts by weight Raw material forms:15 parts of cement, 40 parts of expanded perlite, 20 parts of porous ceramic grain, 11 parts of composite reinforcing fiber, 10 parts of sepiolite powder, 15 parts of 7 parts of mica powder, 3 parts of waterproofing agent, 3.5 parts of dispersant, 2 parts of thickener and water.
3. wall according to claim 1 waterproof fireproofing thermal insulation material, which is characterized in that the cement is aluminosilicate Cement.
4. wall according to claim 1 waterproof fireproofing thermal insulation material, which is characterized in that the expanded perlite is anti- Water carbonizes closed-cell expanded perlite, grain size 0.6-1.2mm, unit weight 100-200kg/m3, 9-14 times of expansion multiple.
5. wall according to claim 1 waterproof fireproofing thermal insulation material, which is characterized in that the porous ceramic grain is by powder Porous ceramic grain of the coal ash as main material, grain size 10-15mm.
6. wall according to claim 1 waterproof fireproofing thermal insulation material, which is characterized in that the composite reinforcing fiber is Weight ratio is 2-4:1 carbon fiber and the composition of polyimide fiber.
7. wall according to claim 1 waterproof fireproofing thermal insulation material, which is characterized in that the waterproofing agent is stearic acid Calcium, aluminum stearate or sodium methyl silicate.
8. wall according to claim 1 waterproof fireproofing thermal insulation material, which is characterized in that the dispersant is six inclined phosphorus Sour sodium.
9. wall according to claim 1 waterproof fireproofing thermal insulation material, which is characterized in that the thickener is cellulose Ether.
10. a kind of according to claim 1-9 any one of them wall preparation method of waterproof fireproofing thermal insulation material, feature It is, includes the following steps:
(1)In parts by weight, 10- is mixed in the expanded perlite weighed up, porous ceramic grain, sepiolite powder, mica powder first Then 20min adds water and waterproofing agent to stir 3-5min, add cement, thickener stirring 3-5min, obtain mixture slurry;
(2)Above-mentioned mixture slurry is heated to 60-70 degree and keeps the temperature 20-30min, composite strengthening is added after being then cooled to room temperature Fiber and dispersant, continue stirring until fiber dispersity it is good, without conglomeration, obtain fibrous mixture slurry;
(3)By step(2)Gained mixture slurry pours into die for molding, is demoulded after standing 4-6h, and it is 25 degree, humidity to be put into temperature 90% or more fog room carries out standard curing 28d to get wall waterproof fireproofing thermal insulation material.
CN201810388416.3A 2018-04-26 2018-04-26 A kind of wall waterproof fireproofing thermal insulation material and preparation method thereof Withdrawn CN108341648A (en)

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CN201810388416.3A CN108341648A (en) 2018-04-26 2018-04-26 A kind of wall waterproof fireproofing thermal insulation material and preparation method thereof

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Application Number Priority Date Filing Date Title
CN201810388416.3A CN108341648A (en) 2018-04-26 2018-04-26 A kind of wall waterproof fireproofing thermal insulation material and preparation method thereof

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110357569A (en) * 2019-07-13 2019-10-22 张家港市盛港绿色防火建材有限公司 A kind of fire prevention wall interior panel and preparation method thereof
CN110482952A (en) * 2019-08-29 2019-11-22 徐州金盟新型建材有限公司 A kind of fire-proof and thermal-insulation materials for wall for building
CN113666770A (en) * 2021-08-18 2021-11-19 顾青林 Hydraulic engineering heat insulation material and preparation method thereof
CN114180894A (en) * 2021-12-31 2022-03-15 常德集智生物科技有限公司 Light heat-insulating fireproof brick plate and preparation method thereof

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110357569A (en) * 2019-07-13 2019-10-22 张家港市盛港绿色防火建材有限公司 A kind of fire prevention wall interior panel and preparation method thereof
CN110357569B (en) * 2019-07-13 2021-11-09 张家港市盛港绿色防火建材有限公司 Fireproof enclosure plate and preparation method thereof
CN110482952A (en) * 2019-08-29 2019-11-22 徐州金盟新型建材有限公司 A kind of fire-proof and thermal-insulation materials for wall for building
CN113666770A (en) * 2021-08-18 2021-11-19 顾青林 Hydraulic engineering heat insulation material and preparation method thereof
CN114180894A (en) * 2021-12-31 2022-03-15 常德集智生物科技有限公司 Light heat-insulating fireproof brick plate and preparation method thereof

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