CN108265834A - A kind of high-polymer self-adhesion waterproof coiled material and preparation method thereof - Google Patents
A kind of high-polymer self-adhesion waterproof coiled material and preparation method thereof Download PDFInfo
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- CN108265834A CN108265834A CN201810066490.3A CN201810066490A CN108265834A CN 108265834 A CN108265834 A CN 108265834A CN 201810066490 A CN201810066490 A CN 201810066490A CN 108265834 A CN108265834 A CN 108265834A
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- coiled material
- waterproof coiled
- polymer self
- adhesion waterproof
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- E—FIXED CONSTRUCTIONS
- E04—BUILDING
- E04B—GENERAL BUILDING CONSTRUCTIONS; WALLS, e.g. PARTITIONS; ROOFS; FLOORS; CEILINGS; INSULATION OR OTHER PROTECTION OF BUILDINGS
- E04B1/00—Constructions in general; Structures which are not restricted either to walls, e.g. partitions, or floors or ceilings or roofs
- E04B1/62—Insulation or other protection; Elements or use of specified material therefor
- E04B1/66—Sealings
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L95/00—Compositions of bituminous materials, e.g. asphalt, tar, pitch
-
- E—FIXED CONSTRUCTIONS
- E04—BUILDING
- E04D—ROOF COVERINGS; SKY-LIGHTS; GUTTERS; ROOF-WORKING TOOLS
- E04D5/00—Roof covering by making use of flexible material, e.g. supplied in roll form
- E04D5/10—Roof covering by making use of flexible material, e.g. supplied in roll form by making use of compounded or laminated materials, e.g. metal foils or plastic films coated with bitumen
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/24—Acids; Salts thereof
- C08K3/26—Carbonates; Bicarbonates
- C08K2003/265—Calcium, strontium or barium carbonate
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Civil Engineering (AREA)
- Architecture (AREA)
- Structural Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Materials Engineering (AREA)
- Electromagnetism (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Adhesives Or Adhesive Processes (AREA)
Abstract
The present invention relates to waterproof roll fields, more particularly to a kind of high-polymer self-adhesion waterproof coiled material and preparation method thereof, including the asphalt adhesive bed of material, the macromolecular sheet material and isolation film of both sides above and below the asphalt adhesive bed of material, the asphalt adhesive bed of material includes the component of following parts by weight：70 parts~85 parts of pitch；2 parts~10 parts of styrene butadiene styrene block copolymer (SBS)；2 parts~10 parts of plasticizer；5 parts~10 parts of tackifier；5 parts~15 parts of filler；1 part~5 parts of polyamide wax；2 parts~10 parts of nano silicon dioxide；1 part~5 parts of nano zeolite.Waterproof roll of the present invention by adding in the polyamide wax, nano silicon dioxide and nano zeolite of certain content in formula, can effectively improve seam peel strength, low temperature flexibility and the water resistance of waterproof roll.
Description
Technical field
The present invention relates to waterproof roll fields, and in particular to a kind of high-polymer self-adhesion waterproof coiled material and preparation method thereof.
Background technology
Waterproof roll is mainly used for construction wall, roofing and tunnel, highway, refuse landfill etc., plays and resists
A kind of rollable flexible building material product into web-like of extraneous rainwater, underground water leakage, as between engineering foundation and building
Ne-leakage connects, and is first of barrier of entire engineering waterproofing, entire engineering is played a crucial role.Macromolecule waterproof
Coiled material is the generally acknowledged waterproof material haveing excellent performance, and is widely used in waterproof and dampproof, the macromolecule of industry and residential construction area
Adhesive waterproof coil is by macromolecular sheet material (PVC, HDPE, EVA, EPDM, TPO etc. are produced for raw material), self-adhesive glue layer and isolation film
Composition, can the compound fabric reinforcement on macromolecular sheet material as needed.
Maximum intensity when seam peel strength refers to coiled material with being torn at coiled material lapping, embodies the good of coiled material performance
Bad, existing waterproof roll is because formula for raw stock is single, simple for process, and after construction, seam peel strength is poor, when base expands,
It can be pulled open in lap-joint, overlap joint failure so as to which seam crossing be caused to seep water, makes building waterproof layer be faced with formidable challenges,
Even wreck.Further, since various environmental factors or human factor, asphalt felt product is artificially trampled often in construction
It destroys, damage coil waterproof layer quality is easy to when coiled material surface is acted on by violent or unexpected external force and reduces or loses
The original water resistance of coiled material, and encountered at the destruction temperature it is relatively low when, be destroyed on coiled material and locate further serious, coiled material surface
Waterproof layer is cracked.Therefore, the excellent waterproof roll of a kind of low temperature flexibility and water resistance is developed to be even more important
Invention content
For the above-mentioned shortcoming of the prior art, a kind of high-polymer self-adhesion waterproof coiled material of present invention institute, by being formulated
Middle polyamide wax, nano silicon dioxide and the nano zeolite for adding in certain content can effectively improve the seam stripping of waterproof roll
From intensity, low temperature flexibility and water resistance.
A kind of high-polymer self-adhesion waterproof coiled material of the present invention, including the asphalt adhesive bed of material, above and below the asphalt adhesive bed of material
The macromolecular sheet material and isolation film of both sides, the asphalt adhesive bed of material include the component of following parts by weight：70 parts~85 parts of pitch；
2 parts~10 parts of Styrene-Butadiene-Styrene Block Copolymer (SBS)；2 parts~10 parts of plasticizer；5 parts~10 parts of tackifier；
5 parts~15 parts of filler；1 part~5 parts of polyamide wax；2 parts~10 parts of nano silicon dioxide；1 part~5 parts of nano zeolite.
Preferably, the pitch is the mixture of following parts by weight of component：No. 10 25 parts~30 parts of pitches；No. 100 pitches
50 parts~55 parts.
Preferably, the plasticizer is polyisobutene or naphthenic oil.
Preferably, the tackifier are rosin or terpene resin.
Preferably, the filler is selected from one or more of light calcium carbonate powder, dicalcium powder and talcum powder.
Preferably, the macromolecular sheet material be ethylene-vinyl acetate copolymer (EVA), polyvinyl chloride (PVC) and highly dense
Spend one or more of polyethylene (HDPE).
The present invention also provides a kind of preparation methods of high-polymer self-adhesion waterproof coiled material, include the following steps：
Pitch is squeezed into material-compound tank stirring, plasticizer is added in when temperature rises to 160 ± 5 DEG C；Treat that temperature rises to 180 ± 5
DEG C when add in Styrene-Butadiene-Styrene Block Copolymer (SBS), stir 1~2 hour, temperature control 185~200
DEG C, it is ground 1~2 hour with colloid mill while stirring；Tackifier are added in agitator tank and are stirred 0.5~1 hour, are raised in temperature
At 175 DEG C~180 DEG C, filler, polyamide wax, nano silicon dioxide and nano zeolite are blended into, stirring is dropped after 10~30 minutes
When temperature is to 150 ± 5 DEG C, asphalt size is made；
The asphalt adhesive bed of material is prepared by raw material of asphalt size, high molecular sheet is covered each by the both sides up and down of the asphalt adhesive bed of material
Material and isolation film are crimped, are packaged to be waterproof roll.
The present invention, which is compared with the prior art, to be had the advantage that：The present invention by adding in the poly- of certain content in formula
Amide waxe, nano silicon dioxide and nano zeolite can significantly improve the properties of waterproof roll, with being individually added into polyamide
Wax or the waterproof roll of nano material are compared, and are particularly obtained in low temperature flexibility, impermeability and seam peel strength
Significantly promoted.
Specific embodiment
The invention discloses a kind of high-polymer self-adhesion waterproof coiled material and preparation method thereof, those skilled in the art can use for reference
Present disclosure is suitably modified technological parameter realization.In particular, it should be pointed out that all similar substitutions and modifications are to this field skill
It is it will be apparent that they are considered as being included in the present invention for art personnel.The present invention method and application by compared with
Good embodiment is described, related personnel significantly can not depart from the content of present invention, in spirit and scope to as described herein
Methods and applications are modified or suitably changed with combining, to realize and using the technology of the present invention.
Experimental method in following embodiments is conventional method unless otherwise instructed.The examination that following embodiments are related to
Agent, equipment or raw material are common commercially available product unless otherwise noted, can all be bought and obtained by market.Specific case is carried out below
Example is implemented, but the present invention is not limited to these following cases.
Embodiment 1
10# pitch 25kg, 100# pitches 50kg is squeezed into material-compound tank stirring, cycloalkanes is added in when temperature rises to 160 ± 5 DEG C
Oily 2kg；SBS glue 10kg are added in when temperature rises to 180 ± 5 DEG C, are stirred 1.5 hours, temperature is controlled at 185~200 DEG C, while stirring
Side colloid mill is mixed to grind 1.5 hours；10kg terpene resins are added in agitator tank and are stirred 0.5 hour, 175 are raised in temperature~
At 180 DEG C, talcum powder 15kg, polyamide wax 5kg, nano silicon dioxide 2kg and nano zeolite 5kg are blended into, stirs 25 minutes, stirs
Cool down after mixing fully, when temperature is down to 150 ± 5 DEG C to get asphalt size；
According to forming technology of coiled material, by asphalt size obtained for waterproof roll, the upper and lower surface of asphalt size is distinguished
Macromolecular sheet material (ethylene-vinyl acetate copolymer) and isolation film are covered, is crimped, packs up to the adhesive polymer
Waterproof roll.
Embodiment 2
10# pitch 30kg, 100# pitches 55kg is squeezed into material-compound tank stirring, cycloalkanes is added in when temperature rises to 160 ± 5 DEG C
Oily 10kg；SBS glue 5kg are added in when temperature rises to 180 ± 5 DEG C, are stirred 1.5 hours, temperature is controlled at 185~200 DEG C, while stirring
Side colloid mill is mixed to grind 1.5 hours；5kg rosin is added in agitator tank and is stirred 0.5 hour, 175~180 DEG C are raised in temperature
When, dicalcium powder 10kg, polyamide wax 2kg, nano silicon dioxide 8kg and nano zeolite 1kg are blended into, is stirred 25 minutes, stirring is filled
Cool down after point, when temperature is down to 150 ± 5 DEG C to get asphalt size；
According to forming technology of coiled material, by asphalt size obtained for waterproof roll, the upper and lower surface of asphalt size is distinguished
Macromolecular sheet material (polyvinyl chloride) and isolation film are covered, is crimped, packs up to the high-polymer self-adhesion waterproof coiled material.
Comparative example 1
10# pitch 25kg, 100# pitches 50kg is squeezed into material-compound tank stirring, cycloalkanes is added in when temperature rises to 160 ± 5 DEG C
Oily 2kg；SBS glue 10kg are added in when temperature rises to 180 ± 5 DEG C, are stirred 1.5 hours, temperature is controlled at 185~200 DEG C, while stirring
Side colloid mill is mixed to grind 1.5 hours；10kg terpene resins are added in agitator tank and are stirred 0.5 hour, 175 are raised in temperature~
At 180 DEG C, talcum powder 15kg, nano silicon dioxide 2kg and nano zeolite 5kg are blended into, is stirred 25 minutes, is carried out after stirring fully
Cooling, when temperature is down to 150 ± 5 DEG C to get asphalt size；
According to forming technology of coiled material, by asphalt size obtained for waterproof roll, the upper and lower surface of asphalt size is distinguished
Macromolecular sheet material (ethylene-vinyl acetate copolymer) and isolation film are covered, is crimped, packs up to the adhesive polymer
Waterproof roll.
Comparative example 2
10# pitch 25kg, 100# pitches 50kg is squeezed into material-compound tank stirring, cycloalkanes is added in when temperature rises to 160 ± 5 DEG C
Oily 2kg；SBS glue 10kg are added in when temperature rises to 180 ± 5 DEG C, are stirred 1.5 hours, temperature is controlled at 185~200 DEG C, while stirring
Side colloid mill is mixed to grind 1.5 hours；10kg terpene resins are added in agitator tank and are stirred 0.5 hour, 175 are raised in temperature~
At 180 DEG C, talcum powder 15kg and polyamide wax 5kg are blended into, is stirred 25 minutes, cools down after stirring fully, is down in temperature
To get asphalt size at 150 ± 5 DEG C；
According to forming technology of coiled material, by asphalt size obtained for waterproof roll, the upper and lower surface of asphalt size is distinguished
Macromolecular sheet material (ethylene-vinyl acetate copolymer) and isolation film are covered, is crimped, packs up to the adhesive polymer
Waterproof roll.
Above-described embodiment 1-2 and comparative example the 1-2 waterproof roll prepared are detected respectively, testing result such as table 1
Shown in：
Table 1
Pass through table 1：1-2 of the embodiment of the present invention by adding in polyamide wax, the nanometer two of certain content in formula
Silica and nano zeolite can significantly improve the properties of waterproof roll, with being individually added into polyamide wax or nano material
Waterproof roll compare, be greatly improved in low temperature flexibility, impermeability and seam peel strength.
More than case study on implementation be to the present invention be specifically described for example, technical staff belonging to the present invention can be with
Various concrete cases are modified or supplemented.
Claims (7)
1. a kind of high-polymer self-adhesion waterproof coiled material, which is characterized in that including the asphalt adhesive bed of material, the both sides above and below the asphalt adhesive bed of material
Macromolecular sheet material and isolation film, the asphalt adhesive bed of material includes the component of following parts by weight：70 parts~85 parts of pitch；Benzene second
2 parts~10 parts of alkene-butadiene-styrene block copolymer (SBS)；2 parts~10 parts of plasticizer；5 parts~10 parts of tackifier；Filling
5 parts~15 parts of agent；1 part~5 parts of polyamide wax；2 parts~10 parts of nano silicon dioxide；1 part~5 parts of nano zeolite.
2. a kind of high-polymer self-adhesion waterproof coiled material according to claim 1, which is characterized in that the pitch is following weight
The mixture of part component：No. 10 25 parts~30 parts of pitches；No. 100 50 parts~55 parts of pitches.
3. a kind of high-polymer self-adhesion waterproof coiled material according to claim 1 or 2, which is characterized in that the plasticizer is
Polyisobutene or naphthenic oil.
4. a kind of high-polymer self-adhesion waterproof coiled material according to claim 1 or 2, which is characterized in that the tackifier are pine
Fragrant or terpene resin.
5. a kind of high-polymer self-adhesion waterproof coiled material according to claim 1 or 2, which is characterized in that the filler is selected from
One or more of light calcium carbonate powder, dicalcium powder and talcum powder.
A kind of 6. high-polymer self-adhesion waterproof coiled material according to claim 1 or 2, which is characterized in that the macromolecular sheet material
For one kind in ethylene-vinyl acetate copolymer (EVA), polyvinyl chloride (PVC) and high density polyethylene (HDPE) (HDPE).
7. the preparation method of a kind of high-polymer self-adhesion waterproof coiled material according to claim 1, which is characterized in that including following
Step：
Pitch is squeezed into material-compound tank stirring, plasticizer is added in when temperature rises to 160 ± 5 DEG C；When temperature rises to 180 ± 5 DEG C
Styrene-Butadiene-Styrene Block Copolymer (SBS) is added in, is stirred 1~2 hour, temperature control is at 185~200 DEG C, side
Side is stirred to be ground 1~2 hour with colloid mill；Tackifier are added in agitator tank and are stirred 0.5~1 hour, 175 DEG C are raised in temperature
At~180 DEG C, filler, polyamide wax, nano silicon dioxide and nano zeolite are blended into, stirring is cooled to after 10~30 minutes
At 150 ± 5 DEG C, asphalt size is made；
Prepare the asphalt adhesive bed of material by raw material of asphalt size, be covered each by the both sides up and down of the asphalt adhesive bed of material macromolecular sheet material and
Isolation film is crimped, is packaged to be waterproof roll.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201810066490.3A CN108265834B (en) | 2018-01-24 | 2018-01-24 | High-molecular self-adhesive waterproof coiled material and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810066490.3A CN108265834B (en) | 2018-01-24 | 2018-01-24 | High-molecular self-adhesive waterproof coiled material and preparation method thereof |
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| CN108265834A true CN108265834A (en) | 2018-07-10 |
| CN108265834B CN108265834B (en) | 2020-06-23 |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109401342A (en) * | 2018-09-25 | 2019-03-01 | 天津市禹神建筑防水材料有限公司 | A kind of root-resistant puncturing adhesive waterproof coil and preparation method thereof |
| CN111234539A (en) * | 2020-01-13 | 2020-06-05 | 浙江圣帝亚建筑科技有限公司 | Modified asphalt for waterproof coiled material and preparation method thereof |
| CN114672264A (en) * | 2022-04-06 | 2022-06-28 | 安徽省奥佳建材有限公司 | Elastic self-adhesive waterproof roll and preparation method thereof |
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| US9382704B2 (en) * | 2009-09-30 | 2016-07-05 | Sealanttech | Protective air barrier sealant for conditioned and unconditioned building walls |
| CN106280893A (en) * | 2016-08-29 | 2017-01-04 | 山东帝高漆业有限公司 | A kind of coal tar epoxide Colophonium finish paint and production method thereof |
| CN107418229A (en) * | 2017-07-17 | 2017-12-01 | 湖北大学 | A kind of granulated solid pitch and preparation method thereof |
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2018
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| CN1876723A (en) * | 2005-06-07 | 2006-12-13 | 锦湖石油化学株式会社 | Drainage pavement asphalt modifier with improved viscosity and method for preparing same |
| US9382704B2 (en) * | 2009-09-30 | 2016-07-05 | Sealanttech | Protective air barrier sealant for conditioned and unconditioned building walls |
| CN102220023A (en) * | 2011-05-13 | 2011-10-19 | 广西金雨伞防水装饰有限公司 | Preparation method of star-shaped SBS (styrene butadiene styrene block polymer)-modified asphalt and production method of waterproof coiled material |
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| CN107418229A (en) * | 2017-07-17 | 2017-12-01 | 湖北大学 | A kind of granulated solid pitch and preparation method thereof |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109401342A (en) * | 2018-09-25 | 2019-03-01 | 天津市禹神建筑防水材料有限公司 | A kind of root-resistant puncturing adhesive waterproof coil and preparation method thereof |
| CN111234539A (en) * | 2020-01-13 | 2020-06-05 | 浙江圣帝亚建筑科技有限公司 | Modified asphalt for waterproof coiled material and preparation method thereof |
| CN114672264A (en) * | 2022-04-06 | 2022-06-28 | 安徽省奥佳建材有限公司 | Elastic self-adhesive waterproof roll and preparation method thereof |
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| CN108265834B (en) | 2020-06-23 |
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