Reaction method of colloidal chemical raw materials
Technical Field
The invention relates to a chemical reaction device, in particular to a colloidal chemical raw material reaction method, and belongs to the technical field of chemical equipment application.
Background
The human beings have close relationship with chemical engineering and are popularized in various aspects of life. In modern life, chemical products can not be left at all times and places, and the chemical products are needed to serve from material life such as clothes, food, live, and walk to mental life such as culture, art and entertainment. Some chemical products play an epoch-making important role in the development history of human beings. The chemical reaction device is a holding reaction device which is specially used for mutual reaction of liquid chemical raw materials.
But current chemical reaction device still has certain defect when using, and current chemical reaction device can the splendid attire reaction, but current chemical reaction device exists the phenomenon that the heating is not even enough, if the inside reaction liquid of reaction tank is heated inequality and will influence chemical reaction's efficiency and quality, and current chemical reaction device has the phenomenon that the reaction liquid contacts inadequately moreover.
Especially to the reaction that gelatineous industrial chemicals participated in, easily appear reacting unevenly among the existing equipment, the insufficient condition, this mainly is related to with the characteristic of gelatineous industrial chemicals's thick form, and at present most chemical production enterprises still adopt traditional retort to react, also lack the reaction equipment to this kind of industrial chemicals among the prior art for be in comparatively awkward state all the time to gelatineous industrial chemicals's reaction.
Disclosure of Invention
In view of this, the colloidal chemical raw material reaction method provided by the invention is mainly used for chemical reaction of colloidal chemical raw materials, and well solves the problems in the background technology.
The invention realizes the aim through the following technical scheme, and the colloidal chemical raw material reaction method comprises the following steps:
a: firstly, reaction raw materials to be reacted are respectively fed into a reaction tank from a first feeding box and a second feeding box through a blanking pipe, an electric heating plate is electrified, the electric heating plate generates heat energy, and the heat energy is uniformly conducted into the reaction tank through a heat conducting rod clamped in a clamping hole;
b: when the reaction liquid in the reaction tank reaches a certain temperature, a first motor box and a second motor box are respectively electrified, the first motor box drives a knife roller connected with the first motor box to rotate clockwise through a rotating shaft, the second motor box drives the knife roller connected with the second motor box to rotate anticlockwise through the rotating shaft, the knife rollers rotating in different directions can be used for fully stirring the reaction liquid in the reaction tank, so that the reaction is more sufficient, and a heat preservation cylinder plays a role in heat preservation;
c: after the reaction is finished, opening a valve, enabling the reacted chemical liquid to flow into a collecting tank through a discharging pipe to be collected, and filtering and collecting solid impurities in the reaction liquid through a filter screen;
wherein, the reaction tank used for the stirring reaction of the colloidal chemical raw materials comprises a fixed cabinet and a reaction tank, a collecting tank is arranged inside the fixed cabinet and is used for collecting the chemical liquid which is completed by the reaction, a heat preservation cylinder is arranged above the fixed cabinet and is used for preventing the heat inside the reaction tank from losing and ensuring that the reaction tank can carry out the chemical reaction at a constant temperature, one side of the heat preservation cylinder is provided with a first motor box which is used for driving a rotating shaft clamped with the heat preservation cylinder to rotate, the other side of the heat preservation cylinder is provided with a second motor box which is used for driving the rotating shaft clamped with the heat preservation cylinder to rotate, one side of the second motor box is clamped with the rotating shaft and plays a role in transmission, a plurality of cutter rollers which are uniformly arranged are welded outside the rotating shaft, the cutter rollers rotate under the effect of the rotating shaft to stir the reaction raw materials inside the reaction tank, the upper part of the heat preservation cylinder is connected with a first feeding box, one side of the, first feeding case and second feeding bottom of the case portion all are equipped with the inlet pipe, be used for transporting chemical reaction raw materials, a plurality of stabilizer blades of the bottom welding of second motor case, support fixed second motor case, a plurality of heating staple bolts are established to the outside cover of reaction tank, and can produce heat energy after the circular telegram, heat staple bolt lateral wall block a plurality of align to grid's heat conduction stick, be used for the even conduction of heat energy to the reaction tank that will heat the staple bolt production, the inside electric plate that is equipped with of heating staple bolt, it produces the device of heat energy to heat the staple bolt, the inside card hole that sets up a plurality of sizes of running through of electric plate, the heat conduction stick is fixed to the block that is used for, the bottom of reaction tank is equipped with the unloading pipe, unloading pipe lateral wall block valve, the outflow of control reaction liquid, the inside block filter screen of unloading pipe.
Further, the equal block pivot of first motor case and second motor case, and the epaxial rotor of first motor case block and the epaxial rotor of second motor case block staggers each other to make the rotor that sets up in different epaxial rotors can not contact in rotatory, guarantee that the rotatory rotor of equidirectional can the intensive mixing reaction raw materials.
Further, the heat conduction stick is cylindrical structure, and heat conduction stick diameter and card hole diameter phase-match to make the heat conduction stick can perfect block fix in the inside in card hole, and fully heat the inside reaction raw materials of reaction tank through the heat conduction stick, improve reaction efficiency.
Further, the electric plate is circular structure, and the electric plate passes through the wire and is electric connection with external power source, thereby make the electric plate can have sufficient electric energy and normally work, the heating heat conduction stick, a plurality of rotor blades all set up the inside at the reacting tank, and a plurality of rotor blades pass through the pivot respectively with first motor case, the second motor case is the rotation and is connected, thereby make a plurality of rotor blades can realize not equidirectional rotation respectively through first motor case and second motor case, make the inside raw materials of reacting tank can be by intensive mixing, the second motor case passes through the stabilizer blade setting in the top of fixed cabinet, thereby make the second motor case can be fixed more firmly, guarantee the stability of second motor case.
Further, the pivot is provided with two and is driven by first motor case and second motor case respectively, the rotor is the flabellum shape structure, and a plurality of rotor are the spiral along the pivot and arrange, and a plurality of rotor are used for the chemical raw materials of gluing to one end propelling movement, and two epaxial rotor arrange opposite direction, realize the clockwise circulation or the anticlockwise circulation of chemical raw materials of gluing.
Further, the center of pivot is equipped with the through-hole, the root of rotor is equipped with the venthole, and the venthole is linked together with the through-hole, and the through-hole is connected with the air supply through the pipeline, lets in gas in to the through-hole and can realize clearing up the gelatineous raw materials of rotor root to guarantee the abundant reaction.
Furthermore, a liquid suction rod is arranged in the reaction tank, the liquid suction rod is telescopic, and the liquid suction rod is used for sucking out useless liquid generated by the reaction, so that the full reaction is ensured.
Further, it is articulated through universal ball between first feeding case and the second feeding case and the reaction tank, and be connected with between first feeding case and second feeding case and the reaction tank and rock the cylinder, it is used for driving first feeding case and second feeding case and rocks to rock the cylinder, avoids the gelatineous raw materials to stew to increase the mobility of gelatineous raw materials.
Compared with the prior art, the invention has the beneficial effects that:
1. according to the invention, the first motor box and the second motor box are respectively arranged above the fixed cabinet, so that the two motor boxes rotating in different directions can be used for driving the knife rolls on the rotating shaft to rotate and stir in different directions, reaction raw materials in the reaction tank can be fully contacted, and the reaction efficiency and the reaction quality are effectively improved.
2. According to the invention, the reaction tank is fully heated by the heat conducting rod through the plurality of heating hoops sleeved outside the reaction tank and connected with each other through the heat conducting rod, so that reaction raw materials in the reaction tank can be rapidly heated, and the reaction efficiency and the reaction quality are effectively improved.
Drawings
FIG. 1 is a schematic view of the overall structure of the present invention;
FIG. 2 is a schematic view of a heating hoop structure according to the present invention;
FIG. 3 is a schematic cross-sectional view of a heating hoop according to the present invention;
fig. 4 is an enlarged view of the area a of the present invention 1.
In the figure: the device comprises a fixed cabinet 1, a reaction tank 2, a collecting tank 3, a heat-insulating cylinder 4, a first motor box 5, a second motor box 6, a rotating shaft 7, a knife roll 8, a first feeding box 9, a second feeding box 10, a discharging pipe 11, support legs 12, a heating hoop 13, a heat conducting rod 14, a clamping hole 15, an electric heating plate 16, a discharging pipe 17, a valve 18 and a filter screen 19.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
As shown in fig. 1 to 4, the colloidal chemical raw material reaction method of the present invention includes the following steps:
a: firstly, reaction raw materials to be reacted are respectively put into a reaction tank 2 from a first feeding box 9 and a second feeding box 10 through a blanking pipe 11, an electric heating plate 16 is electrified, the electric heating plate 16 generates heat energy, and the heat energy is uniformly conducted into the reaction tank 2 through a heat conduction rod 14 clamped in a clamping hole 15;
b: when the reaction liquid in the reaction tank 2 reaches a certain temperature, a first motor box 5 and a second motor box 6 are respectively electrified, the first motor box 5 drives a knife roll 8 connected with the first motor box to rotate clockwise through a rotating shaft 7, the second motor box 6 drives the knife roll 8 connected with the second motor box to rotate anticlockwise through the rotating shaft 7, the knife rolls 8 rotating in different directions can be used for fully stirring the reaction liquid in the reaction tank 2 to enable the reaction to be more sufficient, and the heat preservation cylinder 4 plays a role in heat preservation;
c: after the reaction is finished, opening a valve 18, enabling the reacted chemical liquid to flow into a collecting tank 3 through a discharge pipe 17 to be collected, and filtering and collecting solid impurities in the reaction liquid through a filter screen 19;
wherein, the retort used for the stirring reaction of the colloidal chemical raw materials comprises a fixed cabinet 1 and a reaction tank 2, a collecting tank 3 is arranged inside the fixed cabinet 1 and is used for collecting the chemical liquid after the reaction is finished, a heat-preserving cylinder is arranged above the fixed cabinet 1 and is used for preventing the heat loss inside the reaction tank 2 and ensuring that the reaction tank 2 can carry out the chemical reaction at a constant temperature, a first motor box 5 is arranged on one side of the heat-preserving cylinder 4 and is used for driving a rotating shaft 7 clamped with the first motor box to rotate, a second motor box 6 is arranged on the other side of the heat-preserving cylinder 4 and is used for driving a rotating shaft 7 clamped with the second motor box to rotate, the rotating shaft 7 is clamped on one side of the second motor box 6 and plays a role in transmission, a plurality of knife rolls 8 which are uniformly arranged are welded outside the rotating shaft 7, and the knife rolls 8 rotate under the action of the rotating shaft 7 to stir the reaction raw materials inside the reaction tank 2, a second feeding box 10 is arranged on one side of a first feeding box 9, the two feeding boxes are used for feeding chemical reaction raw materials, feeding pipes 11 are arranged at the bottoms of the first feeding box 9 and the second feeding box 10 and used for transporting the chemical reaction raw materials, a plurality of support legs 12 are welded at the bottom of a second motor box 6 and used for supporting and fixing the second motor box 6, a plurality of heating hoops 13 are sleeved outside a reaction tank 2 and can generate heat energy after being electrified, a plurality of heat conducting rods 14 which are uniformly arranged are clamped on the side walls of the heating hoops 13 and used for uniformly conducting the heat energy generated by the heating hoops 13 to the reaction tank 2, an electric heating plate 16 is arranged inside the heating hoops 13 and is a device for generating the heat energy by the heating hoops 13, a plurality of clamping holes 15 which are uniform in size are arranged inside the electric heating plate 16 in a penetrating manner and used for clamping and fixing the heat conducting rods 14, a discharging pipe 17 is arranged at the bottom of the reaction tank 2, the interior of the discharge pipe 17 is clamped with a filter screen 19 for filtering solid impurities in the liquid.
Further, first motor case 5 and the equal block pivot 7 of second motor case 6, and the rotor 8 on the pivot 7 of 5 blocks of first motor case staggers each other with the rotor 8 on the pivot 7 of 6 blocks of second motor case to make the rotor 8 that sets up on different pivots 7 can not contact in the time of the rotation, guarantee that the rotatory rotor 8 of equidirectional not can fully stir reaction raw materials.
Further, heat conduction stick 14 is cylindrical structure, and heat conduction stick 14 diameter and the 15 diameter phase-matchs of card hole to make heat conduction stick 14 can perfectly block to fix in the inside of card hole 15, and through the inside reaction raw materials of heat conduction stick 14 fully heating reaction tank 2, improve reaction efficiency.
Further, electric plate 16 is circular structure, and electric plate 16 is electric connection through wire and external power source, thereby make electric plate 16 can have sufficient electric energy normal work, heat conduction stick 14, a plurality of rotor blades 8 all set up the inside at reaction tank 2, and a plurality of rotor blades 8 respectively with first motor case 5 through pivot 7, second motor case 6 is the rotation and is connected, thereby make a plurality of rotor blades 8 can realize not equidirectional rotation respectively through first motor case 5 and second motor case 6, make the inside raw materials of reaction tank 2 can be by intensive mixing, second motor case 6 passes through stabilizer blade 12 and sets up the top at fixed cabinet 1, thereby make second motor case 6 can be fixed more firm, guarantee the stability of second motor case 6.
Further, pivot 7 is provided with two and is driven by first motor case 5 and second motor case 6 respectively, rotor 8 is the fan blade shape structure, and a plurality of rotor 8 are the spiral along pivot 7 and arrange, and a plurality of rotor 8 are used for the chemical raw materials of gluing to one end propelling movement, and two epaxial rotor 8 of pivot arrange opposite direction, realize the clockwise circulation or the anticlockwise circulation of chemical raw materials of gluing.
Further, the center of pivot 7 is equipped with the through-hole, the root of rotor 8 is equipped with the venthole, and the venthole is linked together with the through-hole, and the through-hole is connected with the air supply through the pipeline, lets in gas in to the through-hole and can realize clearing up the gelatineous raw materials of rotor 8 root to guarantee the abundant reaction.
Furthermore, a liquid suction rod is arranged in the reaction tank 2 and can stretch out and draw back, and the liquid suction rod is used for sucking out useless liquid generated by the reaction, so that the full reaction is ensured.
Further, it is articulated through universal ball between first feeding case 9 and second feeding case 10 and the reaction tank 2, and be connected with between first feeding case 9 and second feeding case 10 and the reaction tank 2 and rock the cylinder, it is used for driving first feeding case 9 and second feeding case 10 and rocks to rock the cylinder, avoids the gelatineous raw materials to ste to increase the mobility of gelatineous raw materials.
The foregoing illustrates and describes the principles, general features, and advantages of the present invention. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, which are given by way of illustration of the principles of the present invention, and that various changes and modifications may be made without departing from the spirit and scope of the invention as defined by the appended claims. The scope of the invention is defined by the appended claims and equivalents thereof.