CN108165051B - A kind of high distillation is high to wash yellowish-brown disperse dye composition, dye preparations and application - Google Patents
A kind of high distillation is high to wash yellowish-brown disperse dye composition, dye preparations and application Download PDFInfo
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- CN108165051B CN108165051B CN201810113526.9A CN201810113526A CN108165051B CN 108165051 B CN108165051 B CN 108165051B CN 201810113526 A CN201810113526 A CN 201810113526A CN 108165051 B CN108165051 B CN 108165051B
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- 239000000986 disperse dye Substances 0.000 title claims abstract description 48
- 239000000203 mixture Substances 0.000 title claims abstract description 40
- 239000000975 dye Substances 0.000 title claims abstract description 38
- 238000004821 distillation Methods 0.000 title claims abstract description 36
- 238000002360 preparation method Methods 0.000 title abstract description 13
- 150000001875 compounds Chemical class 0.000 claims abstract description 27
- 238000005406 washing Methods 0.000 claims abstract description 19
- 238000004043 dyeing Methods 0.000 claims abstract description 15
- 230000002209 hydrophobic effect Effects 0.000 claims abstract description 8
- 239000002657 fibrous material Substances 0.000 claims abstract description 6
- 239000000047 product Substances 0.000 claims description 16
- 239000012752 auxiliary agent Substances 0.000 claims description 11
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims description 6
- 239000007859 condensation product Substances 0.000 claims description 6
- NVVZQXQBYZPMLJ-UHFFFAOYSA-N formaldehyde;naphthalene-1-sulfonic acid Chemical compound O=C.C1=CC=C2C(S(=O)(=O)O)=CC=CC2=C1 NVVZQXQBYZPMLJ-UHFFFAOYSA-N 0.000 claims description 3
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 2
- 229920001732 Lignosulfonate Polymers 0.000 claims description 2
- -1 alkyl naphthalene sulfonic acid formaldehyde Chemical compound 0.000 claims description 2
- 229910052736 halogen Inorganic materials 0.000 claims description 2
- 150000002367 halogens Chemical class 0.000 claims description 2
- 229910052739 hydrogen Inorganic materials 0.000 claims description 2
- 239000001257 hydrogen Substances 0.000 claims description 2
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims description 2
- 125000001797 benzyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C([H])([H])* 0.000 claims 1
- 239000002131 composite material Substances 0.000 abstract description 2
- 230000007613 environmental effect Effects 0.000 abstract description 2
- 238000000034 method Methods 0.000 description 10
- VGKYEIFFSOPYEW-UHFFFAOYSA-N 2-methyl-4-[(4-phenyldiazenylphenyl)diazenyl]phenol Chemical compound Cc1cc(ccc1O)N=Nc1ccc(cc1)N=Nc1ccccc1 VGKYEIFFSOPYEW-UHFFFAOYSA-N 0.000 description 9
- 239000004744 fabric Substances 0.000 description 9
- 230000000052 comparative effect Effects 0.000 description 8
- 239000002270 dispersing agent Substances 0.000 description 7
- 238000000859 sublimation Methods 0.000 description 7
- 230000008022 sublimation Effects 0.000 description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
- 238000002156 mixing Methods 0.000 description 6
- 238000000227 grinding Methods 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- 238000001694 spray drying Methods 0.000 description 5
- 238000009826 distribution Methods 0.000 description 4
- 229920005610 lignin Polymers 0.000 description 4
- 239000004576 sand Substances 0.000 description 3
- 230000002195 synergetic effect Effects 0.000 description 3
- 238000004040 coloring Methods 0.000 description 2
- 230000007812 deficiency Effects 0.000 description 2
- 238000010017 direct printing Methods 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 239000000178 monomer Substances 0.000 description 2
- 229920000728 polyester Polymers 0.000 description 2
- 239000005020 polyethylene terephthalate Substances 0.000 description 2
- 238000007639 printing Methods 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 239000002002 slurry Substances 0.000 description 2
- NMDKWAQVRNUKQH-UHFFFAOYSA-N 2-benzylnaphthalene-1-sulfonic acid formaldehyde Chemical compound C=O.C(C1=CC=CC=C1)C1=C(C2=CC=CC=C2C=C1)S(=O)(=O)O NMDKWAQVRNUKQH-UHFFFAOYSA-N 0.000 description 1
- WODGMMJHSAKKNF-UHFFFAOYSA-N 2-methylnaphthalene-1-sulfonic acid Chemical compound C1=CC=CC2=C(S(O)(=O)=O)C(C)=CC=C21 WODGMMJHSAKKNF-UHFFFAOYSA-N 0.000 description 1
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Polymers C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 1
- 229920004934 Dacron® Polymers 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- 229920004933 Terylene® Polymers 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000013329 compounding Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000002203 pretreatment Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
- 238000009941 weaving Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0033—Blends of pigments; Mixtured crystals; Solid solutions
- C09B67/0046—Mixtures of two or more azo dyes
- C09B67/0051—Mixtures of two or more azo dyes mixture of two or more monoazo dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/16—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
- D06P1/18—Azo dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/34—Material containing ester groups
- D06P3/52—Polyesters
- D06P3/54—Polyesters using dispersed dyestuffs
Landscapes
- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
Abstract
The invention discloses a kind of yellowish-brown disperse dye composition of the high washing of high distillation, dye preparations and applications.The dye composite, including component A, component B, component C, component A is selected from one or both of compound shown in formula (I), component B is selected from least one of compound shown in formula (II -1)~(II -3), and component C is selected from least one of compound shown in formula (III -1)~(III -3)；Based on component A, component B and component C, by weight, the content of component A is 30~95 parts, and the content of component B is 1~70 part, and the content of component C is 1~40 part.(I),(II -1),(II -2),(II -3),(III -1),(III -2),(III -3).When the yellowish-brown disperse dye composition of the present invention and dye preparations are applied to hydrophobic fiber material dyeing or stamp, have the characteristics that environmental protection, every fastness is excellent, lifting force is good.
Description
Technical field
The present invention relates to a kind of yellowish-brown disperse dye composition of the high washing of high distillation, dye preparations and applications, are suitble to application
Dyeing or stamp in hydrophobic fiber material.
Background technique
Requirement recently as terylene and blend polyester fabric to environmental protection and fastness increasingly improves, to the ring of disperse dyes
It protects and fastness requirement is also higher and higher, the good disperse dyes of sublimation reliability are commonly used in middle deep colour dyeing and stamp, but existing product
Often there are some disadvantages in kind, especially washing fastness is inadequate.Height distillation is high wash yellowish-brown disperse dyes send out as hot spot it
One.
For disperse yellow brown S-4RL (C.I. Disp.Orange 30) although properties are excellent, polystream phenol is exceeded (no
Meet 100 standard of OKO-TEX), and sublimation reliability and washing fastness slightly owe deficiency.
Disperse yellow S-6G 200%(C.I.Disp.Yellow 114) it is one beautiful in colour, the outstanding kind of fastness is main
Be used for disseminate and pattern-printing and dyeing, receive praises from customers always for a long time, but the coloring intensity of the dyestuff is not high, lifting force compared with
Difference, it is difficult to obtain darker, and price is higher, which is used as always based on monochromatic yellows use.
It needs a kind of high high yellowish-brown disperse dyes of fastness of distillation in a hurry in the market, is applied to dyeing especially stamp, has good
Good fastness performance and with spectrum stability when other dyestuff compatibilities.
For the effect of disperse dyes compound synergic already to be familiar, blending dyestuff can obtain more preferable dyeability and jail
Degree becomes the project of dyestuff worker research and the power of innovation.
Based on disperse yellow S-6G 200%(C.I.Disp.Yellow 114) compounding dyestuff research work for a long time
But ignored always.The study found that increasing with the disperse dyes height distillation yellow red kind of high washing fastness, utilizes disperse yellow S-
6G 200% compounds yellow commercially available some excellent feux rouges and orange and red kind in the excellent color development in the region 400-450NM, can be with
The power that gets a promotion is good, and the yellowish-brown kind that metamerism is good and every fastness ability is excellent substantially improves disperse yellow S-6G
200% deficiency can satisfy the market demand as a kind of novel yellowish-brown kind.
Summary of the invention
To solve the above problems, the present invention provides a kind of yellowish-brown disperse dye compositions of the high washing of high distillation, dyestuff system
Product and application when being applied to hydrophobic fiber material dyeing or stamp, have the spies such as environmentally friendly, every fastness is excellent, lifting force is good
Point.
In order to achieve the above object, the technical solution adopted by the present invention is that: a kind of high distillation is high to wash yellowish-brown disperse dyes
Composition, including component A, component B and component C, wherein the component A be selected from one of compound shown in formula (I) or
Two kinds, the component B is selected from least one of compound shown in formula (II -1)~(II -3), and the component C is selected from formula (III -
1) at least one of compound shown in~(III -3)；Based on the component A, component B and component C, by weight, component
The content of A is 30~95 parts, and the content of component B is 1~70 part, and the content of component C is 1~40 part:
(I),
(II -1),
(II -2),
(II -3),
(III -1),
(III -2),
(III -3)；
In formula (I):
R1、R2、R3Respectively stand alone as hydrogen,、Or halogen, wherein Ph is phenyl；N is
1~4, m are 1~3.
Further, the component A is preferably one of dye composition shown in following formula (I-l)~(I -15) or two
Kind or more mixture:
(I -1),
(I -2),
(I -3),
(I -4),
(I -5),
(I -6),
(I -7),
(I -8),
(I -9),
(I -10),
(I -11),
(I -12),
(I -13),
(I -14),
(Ⅰ-15)。
Further, the high yellowish-brown disperse dye composition of washing of the high distillation further includes component D, and component D is selected from formula
(III-4) or formula (III-5) compound represented, based on the component A, component B, component C and component D, by weight,
The content of component D is 0.1~3 part；
(III-4),
(III-5)。
Further, the high distillation it is high wash yellowish-brown disperse dye composition by component A, component B, component C and
Component D composition, based on the component A, component B, component C and component D, by weight, the content of component A is 40~90
Part, the content of component B is 1~50 part, and the content of component C is 1~25 part, and the content of component D is 0.1~3 part.
High distillation of the present invention is high to wash yellowish-brown disperse dye composition, as commodity selling or is applied to weaving material
When material coloring, usually also needs that auxiliary agent is added and post-processed.Therefore, the present invention also provides a kind of high washing of high distillation is yellowish-brown
Disperse dyes product washes yellowish-brown disperse dye composition and auxiliary agent, auxiliary agent and high distillation Gao Shui containing the high distillation height
The weight ratio for washing yellowish-brown disperse dye composition is 0.2~5:1.Preferably, the high distillation is high washes yellowish-brown dispersion dye
Material products are made of the yellowish-brown disperse dye composition of the high washing of high distillation and auxiliary agent.The auxiliary agent is multiple for disperse dyes
The common dispersing agent of timing, diffusant and other surfactants etc., preferably are selected from one of following or in which two or more mixing
Object: lignosulfonates (lignin 85A, lignin 83A etc.), alkyl naphthalene sulfonic acid formaldehyde condensation products (such as methyl naphthalene sulfonic acid and formaldehyde
Condensation product (Dispersant MF)), naphthalene sulfonic acid-formaldehyde condensation product (dispersing agent NNO), benzyl naphthalene sulfonic acid-formaldehyde condensation product (dispersing agent CNF)
Deng.
High distillation of the present invention is high wash yellowish-brown disperse dyes product the preparation method is as follows: will the high distillation of composition it is high
Wash yellowish-brown disperse dye composition dye monomer compound (former dyestuff) mix according to the ratio after, in the presence of auxiliary agent, water
Corpusculed is carried out with pulverizers such as sand mill or grinders；It in addition can also be by dye monomer compound respectively in auxiliary agent, water
In the presence of carry out corpusculed processing with pulverizers such as sand mill or grinders after mixed in proportion.Height of the present invention
Distillation is high to wash yellowish-brown disperse dyes product, with being liquid after sand mill or grinder grinding, after spray drying can for powdery,
Granular, this is well known to those skilled in the art preparation method, due to can not be by the de- of moisture 100% in spray-drying process
It removes, so even being still to allow that there are a certain amount of moisture in powdery or granular dye preparations.
Due to the particularity of dye industry, it is difficult also It is not necessary to which sterling is made, it will usually in some preparation process
Impurity, dye preparations of the invention also allow that there are micro impurity.
High distillation of the present invention is high to wash yellowish-brown disperse dye composition, also allows further to compound with other dyestuffs
New composition is made in synergy, or other red, yellow or the shading components such as orange are added.
In the present invention, formula (I), (II -1)~(II -3), dye composition is convenient to shown in (III -1)~(III -5)
It is synthesized by mode well known to those skilled in the art, commercial goods can also be used.
The present invention provides the high yellowish-brown disperse dye compositions and dye preparations washed of the high distillation in hydrophobic fibre
Application in dyeing material or stamp.
It, can be by ways customary in industry to hydrophobic fiber material using dyestuff made of dye composite of the invention
(such as polyester and its blended fabric) is dyed, and is such as dyed using common dip method or high-temperature and high pressure dyeing process, can also
For direct printing.Wherein, common dip method such as pre-processes hydrophobic fiber material, is put into dye vat and is disseminated,
Dye finishes, and cold water wash to neutrality squeezes out, and restores again cleaning, dries；Fabric is such as carried out dye pre-treatment by direct printing, is dried
Dry, shape prints disperse dyes mill base on printing machine, then is evaporated, and the dye fixing on fabric is made in the way of decatize, finally
Washing, stentering forming.
High distillation of the invention is high, and to wash several component compatibilities in yellowish-brown disperse dye composition preferable, according to molecule it
Between synergistic effect, select specified chemical structure component be combined, after component A, component B, component C three's compatibility, entirely
Disperse dye composition shows good washing fastness, sublimation reliability, perspiration fastness and lifting force.Component is further added
It can make dye preparations that there is better lifting force after D, meanwhile, component D also has the function of adjusting coloured light.
High distillation provided by the invention is high to wash yellowish-brown disperse dye composition and dye preparations, is applied to hydrophobic fibre
When dyeing material or stamp, there is the features such as lifting force is good and water-fastness, perspiration fastness and fastness to sublimation are excellent.
Detailed description of the invention
Attached drawing 1 is the lifting force comparison diagram of the disperse dyes of Examples 1 to 3 and comparative example 1~2.
Specific embodiment
The present invention is described further combined with specific embodiments below, but protection scope of the present invention is not limited in
This:
Embodiment 1:
By 51 grams of formulas (I -1) compound, 41 grams of formula (II -3) compounds, 7.65 grams of formula (III -1) compounds, 0.35 gram of formula
(III -4) compound, 170 grams of Dispersant MF, after adding 200 grams of water blendings, grinding distribution, spray drying to get finished product, this at
Product can provide fabric yellowish-brown tone.
Embodiment 2:
By 86.2 grams of formulas (I -2) compound, 4.3 grams of formula (II -1) compounds, 9.33 grams of formula (III -1) compounds, 0.12 gram
Formula (III -5) compound, 113 grams of Dispersant MF, after adding 200 grams of water blendings, grinding distribution, spray drying, should to get finished product
Finished product can provide fabric yellowish-brown tone.
Embodiment 3:
By 60.3 grams of formulas (I -5) compound, 26.33 grams of formula (II -2) compounds, 13.1 grams of formula (III -2) compounds, 0.27
Gram formula (III -3) compound, 168 grams of Dispersant MF, after adding 200 grams of water blendings, grinding distribution, spray drying to get finished product,
The finished product can provide fabric yellowish-brown tone.
Embodiment 4~8:
According to method described in embodiment 1, the difference is that using the weight of component A, component B, component C, component D in table 1
Than and auxiliary agent, slurries are made after adding water blending, the solid content for controlling slurries is 35~45% to be advisable, and grinding distribution is dry, system
Finished product is obtained, the fabric uniformly good yellowish-brown tone of fastness ability can be supplied to.85A, 83A in table 1 are respectively lignin
85A, lignin 83A.
Table 1
Comparative example 1
By commercially available disperse yellow brown S-4RL 150% (C.I. DISP. ORANGE 30) dyestuff as a comparison case 1:
(1)C.I. DISP.
ORANGE 30；
Comparative example 2
By commercially available disperse yellow brown G-SF 200% (C.I. DISP. ORANGE 73) dyestuff as a comparison case 3:
(2)C.I. DISP.
ORANGE 73；
Dyeing Example 1
By the disperse dyes in disperse dyes obtained in above-described embodiment 1~8, comparative example 1, comparative example 2, using routine
High-temperature and high pressure dyeing process handles dacron, in treatment process, controls dye level (o.w.f) 2.0%, bath raio 1:40, adjusts dye bath
PH value 4~5, room temperature enter dye, are warming up to 130 DEG C with 1 DEG C/min, keep the temperature 45min, restore washing, washing, drying by well-established law, cold
But it is taken out to 70 DEG C.Observe sample cloth coloured light, and the IS0105-C10 that adopts international standards, IS0105-X11, AATCC 15-1989 points
Its water-fastness, color fastness to sublimation, fastness to perspiration is not tested, is specifically shown in Table 2:
Table 2
As shown in Table 2, the washing fastness of 1~embodiment of above-described embodiment 8 can reach 4~5 grades, and sublimation reliability can reach
To 4~5 grades, perspiration fastness can reach 5 grades, and in washing fastness, sublimation reliability and perspiration fastness, dyeability is obviously good
In comparative example 1 and comparative example 2.
Dyeing Example 2
Disperse dyes made from Examples 1 to 3 in the present invention and the disperse dyes of comparative example 1~2 are implemented according to dyeing
The method of example 1 carries out different dye level dyeing respectively, and dye level is respectively 0.5%, 1%, 2%, 4%, 6%.According to GB/
Its lifting force of T2397-2012 standard testing, gained lifting force result are as shown in Fig. 1.By attached drawing l it is found that of the present invention
The yellowish-brown disperse dyes lifting force of the high washing of height distillation and disperse yellow brown S-4RL, disperse yellow brown G-SF 200% are close, embody multiple
With synergistic effect.
The above embodiments merely illustrate the technical concept and features of the present invention, and its object is to allow person skilled in the art
Scholar cans understand the content of the present invention and implement it accordingly, and it is not intended to limit the scope of the present invention.It is all according to the present invention
Equivalent change or modification made by Spirit Essence, should be covered by the protection scope of the present invention.
Claims (7)
1. a kind of high distillation is high to wash yellowish-brown disperse dye composition, it is characterised in that: including component A, component B and component C,
Wherein, the component A is selected from one or both of compound shown in formula (I), and the component B is selected from formula (II -1)~(II -2)
At least one of shown compound, the component C are the mixture of compound shown in formula (III -2) and (III -3)；Based on described
Component A, component B and component C, by weight, the content of component A is 30~95 parts, and the content of component B is 1~70 part, group
The content for dividing C is 1~40 part:
In formula (I):
R1、R2、R3Respectively stand alone as hydrogen,Or halogen, wherein Ph is phenyl；N be 1~
4, m be 1~3.
2. a kind of high distillation according to claim 1 is high to wash yellowish-brown disperse dye composition, it is characterised in that: described group
Divide A for the mixture of one or more of dye composition shown in following formula (I -5), (I -10), (I -15):
3. a kind of high distillation according to claim 1 is high to wash yellowish-brown disperse dye composition, it is characterised in that: the height
The high yellowish-brown disperse dye composition of washing of distillation further includes component D, and component D, which is selected from shown in formula (III-4) or formula (III-5), to be changed
Object is closed, based on the component A, component B, component C and component D, by weight, the content of component D is 0.1~3 part；
4. a kind of high distillation according to claim 3 is high to wash yellowish-brown disperse dye composition, it is characterised in that: the height
Distillation is high to wash yellowish-brown disperse dye composition and is made of component A, component B, component C and component D, based on the component A,
Component B, component C and component D, by weight, the content of component A are 40~90 parts, and the content of component B is 1~50 part, component
The content of C is 1~25 part, and the content of component D is 0.1~3 part.
5. a kind of high distillation is high to wash yellowish-brown disperse dyes product, distil containing height described in Claims 1 to 4 any one
Height washes yellowish-brown disperse dye composition and auxiliary agent, auxiliary agent and the high weight ratio for washing yellowish-brown disperse dye composition of high distillation
For 0.2~5:1.
6. a kind of high distillation according to claim 5 is high to wash yellowish-brown disperse dyes product, it is characterised in that: the auxiliary agent
It is condensed selected from lignosulfonates, alkyl naphthalene sulfonic acid formaldehyde condensation products, naphthalene sulfonic acid-formaldehyde condensation product and benzyl naphthalenesulfonateformaldehyde formaldehyde
Any one in object or two or more mixtures.
7. the distillation of height described in any one is high according to claim 1~4 washes yellowish-brown disperse dye composition or according to right
It is required that the distillation of height described in 5~6 any one is high to wash yellowish-brown disperse dyes product in the dyeing or print of hydrophobic fiber material
Application in spending.
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| JP2004339252A (en) * | 2003-05-12 | 2004-12-02 | Dystar Japan Ltd | Disperse dye mixture suitable for dyeing composite material of polyurethane and polyester |
| CN1328326C (en) * | 2004-12-16 | 2007-07-25 | 浙江龙盛集团股份有限公司 | Disperse red dye composition |
| CN101735664B (en) * | 2009-12-23 | 2013-04-24 | 浙江龙盛染料化工有限公司 | Disperse scarlet dye composition |
| CN101880476B (en) * | 2010-06-29 | 2013-09-11 | 浙江龙盛染料化工有限公司 | Yellow-to-orange disperse dye composition |
| DE102011008683A1 (en) * | 2011-01-15 | 2012-07-19 | Dystar Colours Distribution Gmbh | Disperse dye mixtures, their preparation and use |
| CN102277012B (en) * | 2011-04-29 | 2014-10-29 | 浙江闰土股份有限公司 | Disperse purplish-red dye composition |
| KR101346852B1 (en) * | 2012-05-23 | 2014-01-02 | 공명도 | Black and navy blue disperse dye composition having excellent moisture resistance |
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| CN104194396B (en) * | 2014-09-02 | 2015-07-29 | 浙江花蝶化学股份有限公司 | A kind of dispersion high washing black dye composition |
| CN105062137A (en) * | 2015-07-31 | 2015-11-18 | 杭州福莱蒽特精细化工有限公司 | Disperse yellow brown dye composition with high dyeing degree |
| CN105153748B (en) * | 2015-07-31 | 2018-06-19 | 杭州福莱蒽特精细化工有限公司 | A kind of high disperse black dye composition of dye uptake |
| CN106479219B (en) * | 2015-08-24 | 2018-06-29 | 杭州福莱蒽特精细化工有限公司 | A kind of high dye uptake it is dark blue to black disperse dye composition |
| CN106700648A (en) * | 2016-12-07 | 2017-05-24 | 浙江昱泰染化科技有限公司 | Black disperse dye composition |
| CN107312357B (en) * | 2017-06-23 | 2018-08-17 | 浙江山峪科技股份有限公司 | A kind of dark color azoic dye disperse dye composition |
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