CN108164349A - A kind of nutrient matrix cultivated for Ornamental Bamboo and preparation method thereof - Google Patents
A kind of nutrient matrix cultivated for Ornamental Bamboo and preparation method thereof Download PDFInfo
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- CN108164349A CN108164349A CN201810219532.2A CN201810219532A CN108164349A CN 108164349 A CN108164349 A CN 108164349A CN 201810219532 A CN201810219532 A CN 201810219532A CN 108164349 A CN108164349 A CN 108164349A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
- C05D9/00—Other inorganic fertilisers
Abstract
The invention discloses a kind of for nutrient matrix of Ornamental Bamboo cultivation and preparation method thereof, include the raw material of following parts by weight:30~40 parts of dredging silt, 20~30 parts of bamboo shoot shell, 10~15 parts of cinder powder, 10~15 parts of fresh pig dung, 5~10 parts of rape cake, 5~8 parts of pine bark, 3~5 parts of attapulgite clay/chitosan particle.The content of phenolic acid is low in nutrient matrix prepared by the present invention, and photosynthetic rate, chlorophyll content, cauline leaf growth, root system development and the biomass accumulation of bamboo will not be suppressed, and the growth and development ability of bamboo is strong, and the survival rate of bamboo cultivation is high;In addition the present invention prepares that nutrient matrix water imbibition, water-retaining property are strong, can promote the water suction and development of bamboo root system, while the light-weight of nutrient matrix, quality are loose, more convenient to be transported in packing box, promotes the aerobic respiration of bamboo root system.
Description
Technical field
The present invention relates to technical field of agricultural cultivation more particularly to a kind of nutrient matrixes and its system for Ornamental Bamboo cultivation
Preparation Method.
Background technology
Bamboo belongs to grass family (Poaceae) Bambusoideae (Bambusoideae) perennial evergreen plant, the whole world there are about
70 belong to more than 1200 kinds, are distributed mainly on Asia.Bamboo is the important component of the forest reserves, and China is the center producing region of bamboo
One of, the good reputation of " bamboo kingdom " is known as, either《The Book of Songs》In " order order this card, faint South Mountain " or Soviet Union and Eastern Europe slope it is " peaceful
Edible no meat, can not occupy no bamboo ", all it is seen that Chinese bamboo culture trace of long standing and well established.As bamboo resource in the world most
Abundant country, China have more than 500 kinds of bamboo class of category, bamboo grove Class area estimation more than 40 to have as many as more than 400 ten thousand hectares, be mainly distributed on China
Southern each province accounts for about the 3% of the national forest gross area, accounts for the 25% of world's bamboo grove gross area.With higher economic use value
Mao bamboon (Phyllostachys pubescens) woods have 2,800,000 hectares, account for 70% or so.
Bamboo is fast-growing type plant resources, and growth soon, is easily bred, the period is short, per unit area yield is high, and disposable cultivation is afforested, every year
Go out the long bamboo of bamboo shoot, become a useful person within 3 or five years, annual reasonable intermediate cutting can continuously utilize decades.Bamboo is with its unique biology, ecology
And the features such as multipurpose, the attention of people is increasingly subject to, is just being played in Sustainable Development Strategy of China more and more important
Effect.
However, the phenolic acid containing higher concentration in existing nutrient matrix, and photosynthetic rate of the phenolic acid to bamboo, chlorophyll
Content, cauline leaf growth, root system development and biomass accumulation etc. have inhibiting effect, are unfavorable for the growth and development of bamboo, and seek
Content of beary metal is big in foster matrix, be easy to cause the heavy metal pollution of soil.
Invention content
In view of this, the object of the present invention is to provide a kind of nutrient matrix and preparation method thereof for Ornamental Bamboo cultivation,
To reduce the content of phenolic acid in nutrient matrix, inhibition of the reduction phenolic acid to bamboo growth and development improves the survival rate that bamboo is cultivated,
The content of beary metal in nutrient matrix is reduced simultaneously, improves the feature of environmental protection of nutrient matrix.
The present invention solves above-mentioned technical problem by following technological means:
A kind of nutrient matrix for Ornamental Bamboo cultivation includes the raw material of following parts by weight:30~40 parts of dredging silt,
20~30 parts of bamboo shoot shell, 10~15 parts of cinder powder, 10~15 parts of fresh pig dung, 5~10 parts of rape cake, 5~8 parts of pine bark, concave convex rod
Stone clay/3~5 parts of chitosan particle.
In addition, the present invention also provides a kind of preparation method of the nutrient matrix for Ornamental Bamboo cultivation, including following step
Suddenly:
1) processing of raw material:Bamboo shoot shell, rape cake, pine bark are dried, then is crushed with pulverizer and crosses 120 mesh sieve, is obtained
Mixed-powder takes fresh pig dung to add in mixed-powder, is stirred evenly under the rotating speed of 300~500r/min, obtain fermentation material;
2) decomposed fermentation:1) fermentation material obtained in is poured into the porose fermenter in bottom, is uniformly blended into fermentation material
The zymophyte of 1.2% times of weight, then watering wetting fermentation material, makes fermentation material water content reach 75~80%, then at 45~55
15~20d of continuing fermentation at DEG C, obtains decomposed manure;
3) degradation of phenolic acid:2) decomposed manure that will be obtained in adds in the Fenton reagent of 2~3% times of weight of fermentation material,
It is uniformly mixed, 30~60min is reacted under room temperature;
4) preparation of nutrient matrix:First cinder powder, attapulgite clay/chitosan particle and dredging silt are uniformly mixed
It closes, the decomposed manure in then adding in 3) after the degradation treatment of phenolic acid, pH value is adjusted to 5~6, then at 40~50 DEG C
Drying is to get to nutrient matrix
Further, the zymophyte in step 2) includes EM bacterium, ferment bacterium and Gymboree zymophyte.
Further, during the decomposed fermentation in step 2), a stirring and moisturizing is carried out every 3~5d, keeps fermentation material
Water content 50~80%.
Further, the preparation method of attapulgite clay/chitosan particle described in step 4) is as follows:
Step 1, the activation of attapulgite clay:Attapulgite clay is taken, crush and crosses 120 mesh sieve, at 750 DEG C
1h is roasted, is cooled to room temperature, is then immersed in the hydrochloric acid of 10 times of volume 1mol/L, 3h is stirred at 80 DEG C, centrifugation goes demineralizing acid molten
Liquid, the multiple water of precipitation deionization rinse, then the precipitation after flushing is immersed the oxalic acid solution that mass fraction is 10%, in room temperature
It is lower to use supersonic oscillations 2h, it then filters except oxalic acid solution, the multiple water of precipitation deionization rinses, then dry in 110 DEG C
To activation attapulgite clay powder;
Step 2, the preparation of chitosan colloidal sol:Chitosan is taken to immerse the oxalic acid solution that 10 times of volume mass scores are 10%
In, it is fully dissolved under 50 DEG C of magnetic agitation, obtains chitosan colloidal sol;
Step 3, the load of chitosan:The chitosan colloidal sol that step 2 obtains is taken to add in isometric deionized water dilution,
The activation attapulgite that the step of being sufficiently stirred, obtaining chitosan colloidal sol dilution, take 6~10 times of weight of chitosan one obtains sticks
Native powder is added to chitosan colloidal sol dilution, then persistently stirs 5h, then stand 5h while stirring, removes supernatant, will be heavy
It forms sediment and pours into the NaOH solution of 5 times of volume 1mol/L, after stirring 30min under the rotating speed of 1500~3000r/min, it is molten to filter removal
Then agent, then rinsed with deionized water to neutrality is dried in vacuo to get to attapulgite clay/chitosan particle.
Further, the power of the ultrasonic wave in step 1 is 120W, frequency of oscillation 50kHz.
Further, the vacuum drying condition of step 3 is:Temperature 60 C, vacuum degree 0.09MPa~0.1MPa, time
20h。
Beneficial effects of the present invention:
1. the content of phenolic acid is low in nutrient matrix prepared by the present invention, the photosynthetic rate of bamboo, chlorophyll content, cauline leaf life
Long, root system development and biomass accumulation will not be suppressed, and the growth and development ability of bamboo is strong, the survival rate of bamboo cultivation
It is high;
2. prepared by the present invention, nutrient matrix water imbibition, water-retaining property are strong, can promote the water suction and development of bamboo root system, simultaneously
The light-weight of nutrient matrix, quality are loose, more convenient to be transported in packing box, promote the aerobic respiration of bamboo root system;
3. nutrient matrix prepared by the present invention utilizes dredging silt, bamboo shoot shell, cinder powder, fresh pig dung and rape cake the like waste
In not only contain containing abundant cellulose, also containing needed for a variety of bamboo growth and development such as abundant N, P, K, Zn, Cu, Mn, Se
Nutrient can not only realize these wastes useless by decomposed fermentation processing into the nutrient matrix for cultivating bamboo cultivation
The regeneration of gurry, moreover it is possible to alleviate a large amount of wastes immense pressure caused by environmental protection;
4. attapulgite clay prepared by the present invention/chitosan particle heavy metal adsorption performance is strong, can fully adsorb
Heavy metal in nutrient matrix improves the feature of environmental protection of nutrient matrix;Simultaneously because the antibacterial action of chitosan, can duration kill
The harmful levels of pathogens to go out in nutrient matrix, the bamboo root for preventing germ from invading, prevents bamboo from symptom occur, while can extend battalion
Support the shelf-life of matrix.
Specific embodiment
Below with reference to embodiment, the present invention is described in detail:
The preparation embodiment one of attapulgite clay/chitosan particle
Attapulgite clay is taken, crush and crosses 120 mesh sieve, 1h is roasted at 750 DEG C, is cooled to room temperature, be then immersed in
The hydrochloric acid of 10 times of volume 1mol/L stirs 3h, centrifugation removal hydrochloric acid solution at 80 DEG C, and the multiple water of precipitation deionization rinses,
The precipitation after flushing is immersed into the oxalic acid solution that mass fraction is 10% again, is at room temperature 120W with power, frequency of oscillation is
Then the supersonic oscillations 2h of 50kHz is filtered except oxalic acid solution, the multiple water of precipitation deionization rinses, then in 110 DEG C of dryings
Obtain activation attapulgite clay powder;Chitosan is taken to immerse in the oxalic acid solution that 10 times of volume mass scores are 10%, in 50
DEG C magnetic agitation under fully dissolve, obtain chitosan colloidal sol;Obtained chitosan colloidal sol is added in isometric deionized water
Dilution, is sufficiently stirred, obtains chitosan colloidal sol dilution, the activation attapulgite clay powder of 6 times of weight of chitosan is taken, while stirring
It mixes side and is added to chitosan colloidal sol dilution, then persistently stir 5h, then stand 5h, remove supernatant, precipitation is poured into 5 times of bodies
Product 1mol/L NaOH solution, under the rotating speed of 1500~3000r/min stir 30min after, filter removal solvent, then spend from
Sub- water is rinsed to neutrality, and then dry 20h sticks to get to attapulgite under 60 DEG C, the vacuum condition of 0.09MPa~0.1MPa
Soil/chitosan particle.
The preparation embodiment two of attapulgite clay/chitosan particle
Attapulgite clay is taken, crush and crosses 120 mesh sieve, 1h is roasted at 750 DEG C, is cooled to room temperature, be then immersed in
The hydrochloric acid of 10 times of volume 1mol/L stirs 3h, centrifugation removal hydrochloric acid solution at 80 DEG C, and the multiple water of precipitation deionization rinses,
The precipitation after flushing is immersed into the oxalic acid solution that mass fraction is 10% again, is at room temperature 120W with power, frequency of oscillation is
Then the supersonic oscillations 2h of 50kHz is filtered except oxalic acid solution, the multiple water of precipitation deionization rinses, then in 110 DEG C of dryings
Obtain activation attapulgite clay powder;Chitosan is taken to immerse in the oxalic acid solution that 10 times of volume mass scores are 10%, in 50
DEG C magnetic agitation under fully dissolve, obtain chitosan colloidal sol;Obtained chitosan colloidal sol is added in isometric deionized water
Dilution, is sufficiently stirred, obtains chitosan colloidal sol dilution, take the activation attapulgite clay powder of 10 times of weight of chitosan, side
Stirring side is added to chitosan colloidal sol dilution, then persistently stirs 5h, then stand 5h, removes supernatant, precipitation is poured into 5 times
The NaOH solution of volume 1mol/L after stirring 30min under the rotating speed of 1500~3000r/min, filters removal solvent, then spend
Ionized water is rinsed to neutrality, then under 60 DEG C, the vacuum condition of 0.09MPa~0.1MPa dry 20h to get to attapulgite
Clay/chitosan particle.
The preparation embodiment three of attapulgite clay/chitosan particle
Attapulgite clay is taken, crush and crosses 120 mesh sieve, 1h is roasted at 750 DEG C, is cooled to room temperature, be then immersed in
The hydrochloric acid of 10 times of volume 1mol/L stirs 3h, centrifugation removal hydrochloric acid solution at 80 DEG C, and the multiple water of precipitation deionization rinses,
The precipitation after flushing is immersed into the oxalic acid solution that mass fraction is 10% again, is at room temperature 120W with power, frequency of oscillation is
Then the supersonic oscillations 2h of 50kHz is filtered except oxalic acid solution, the multiple water of precipitation deionization rinses, then in 110 DEG C of dryings
Obtain activation attapulgite clay powder;Chitosan is taken to immerse in the oxalic acid solution that 10 times of volume mass scores are 10%, in 50
DEG C magnetic agitation under fully dissolve, obtain chitosan colloidal sol;Obtained chitosan colloidal sol is added in isometric deionized water
Dilution, is sufficiently stirred, obtains chitosan colloidal sol dilution, the activation attapulgite clay powder of 8 times of weight of chitosan is taken, while stirring
It mixes side and is added to chitosan colloidal sol dilution, then persistently stir 5h, then stand 5h, remove supernatant, precipitation is poured into 5 times of bodies
Product 1mol/L NaOH solution, under the rotating speed of 1500~3000r/min stir 30min after, filter removal solvent, then spend from
Sub- water is rinsed to neutrality, and then dry 20h sticks to get to attapulgite under 60 DEG C, the vacuum condition of 0.09MPa~0.1MPa
Soil/chitosan particle.
Attapulgite clay/chitosan particle that 5g embodiments one to embodiment three is taken to obtain respectively, tests its shell respectively
Glycan load factor (%), heavy metal adsorption rate (%) and germ killing rate (%), test result is as shown in table 1:
Table 1
By data above analysis it is found that in attapulgite clay/chitosan particle that embodiment one to embodiment three obtains,
The load factor of chitosan is 40% or so, and heavy metal adsorption rate reaches more than 90%, and germ killing rate reaches more than 95.
The preparation example IV of nutrient matrix
A kind of nutrient matrix for Ornamental Bamboo cultivation includes the raw material of following parts by weight:30 parts of dredging silt, bamboo shoot shell
20 parts, 10 parts of cinder powder, 10 parts of fresh pig dung, 5 parts of rape cake, 5 parts of pine bark, 3 parts of attapulgite clay/chitosan particle.Its
Preparation method is as follows:
Bamboo shoot shell, rape cake, pine bark are dried, then is crushed with pulverizer and crosses 120 mesh sieve, mixed-powder is obtained, takes fresh
Pig manure is added in mixed-powder, is stirred evenly under the rotating speed of 300~500r/min, is obtained fermentation material;The fermentation material that will be obtained
It pours into the porose fermenter in bottom, EM bacterium, ferment bacterium and the Gymboree for being uniformly blended into 1.2% times of weight of fermentation material are zymogenic
Mixed Microbes, then watering wetting fermentation material, makes fermentation material water content reach 75~80%, ferments at 45~55 DEG C, during which
A stirring and moisturizing are carried out every 3~5d, the water content of fermentation material is kept to be obtained after 50~80%, 15~20d of continuing fermentation
To decomposed manure;The decomposed manure that will be obtained adds in the Fenton reagent of 2% times of weight of fermentation material, is uniformly mixed, in room temperature
30~60min of lower reaction;First cinder powder, attapulgite clay/chitosan particle and dredging silt are uniformly mixed, then added in
Decomposed manure after the degradation treatment of phenolic acid adjusts pH value to 5~6, is then dried at 40~50 DEG C to get to nutrition
Matrix.
The preparation embodiment five of nutrient matrix
A kind of nutrient matrix for Ornamental Bamboo cultivation includes the raw material of following parts by weight:40 parts of dredging silt, bamboo shoot shell
30 parts, 15 parts of cinder powder, 15 parts of fresh pig dung, 10 parts of rape cake, 8 parts of pine bark, 5 parts of attapulgite clay/chitosan particle.Its
Preparation method is as follows:
Bamboo shoot shell, rape cake, pine bark are dried, then is crushed with pulverizer and crosses 120 mesh sieve, mixed-powder is obtained, takes fresh
Pig manure is added in mixed-powder, is stirred evenly under the rotating speed of 300~500r/min, is obtained fermentation material;The fermentation material that will be obtained
It pours into the porose fermenter in bottom, EM bacterium, ferment bacterium and the Gymboree for being uniformly blended into 1.2% times of weight of fermentation material are zymogenic
Mixed Microbes, then watering wetting fermentation material, makes fermentation material water content reach 75~80%, ferments at 45~55 DEG C, during which
A stirring and moisturizing are carried out every 3~5d, the water content of fermentation material is kept to be obtained after 50~80%, 15~20d of continuing fermentation
To decomposed manure;The decomposed manure that will be obtained adds in the Fenton reagent of 3% times of weight of fermentation material, is uniformly mixed, in room temperature
30~60min of lower reaction;First cinder powder, attapulgite clay/chitosan particle and dredging silt are uniformly mixed, then added in
Decomposed manure after the degradation treatment of phenolic acid adjusts pH value to 5~6, is then dried at 40~50 DEG C to get to nutrition
Matrix.
The preparation embodiment six of nutrient matrix
A kind of nutrient matrix for Ornamental Bamboo cultivation includes the raw material of following parts by weight:35 parts of dredging silt, bamboo shoot shell
30 parts, 12 parts of cinder powder, 13 parts of fresh pig dung, 7 parts of rape cake, 6 parts of pine bark, 4 parts of attapulgite clay/chitosan particle.Its
Preparation method is as follows:
Bamboo shoot shell, rape cake, pine bark are dried, then is crushed with pulverizer and crosses 120 mesh sieve, mixed-powder is obtained, takes fresh
Pig manure is added in mixed-powder, is stirred evenly under the rotating speed of 300~500r/min, is obtained fermentation material;The fermentation material that will be obtained
It pours into the porose fermenter in bottom, EM bacterium, ferment bacterium and the Gymboree for being uniformly blended into 1.2% times of weight of fermentation material are zymogenic
Mixed Microbes, then watering wetting fermentation material, makes fermentation material water content reach 75~80%, ferments at 45~55 DEG C, during which
A stirring and moisturizing are carried out every 3~5d, the water content of fermentation material is kept to be obtained after 50~80%, 15~20d of continuing fermentation
To decomposed manure;The decomposed manure that will be obtained adds in the Fenton reagent of 2.5% times of weight of fermentation material, is uniformly mixed, Yu Chang
30~60min of the lower reaction of temperature;First cinder powder, attapulgite clay/chitosan particle and dredging silt are uniformly mixed, Ran Houjia
Enter the decomposed manure after the degradation treatment of phenolic acid, adjust pH value to 5~6, then dried at 40~50 DEG C to get to battalion
Support matrix.
Nutrient matrix made from Example four limbs embodiment six carries out Ornamental Bamboo culture, separately takes a ordinary nutritional matrix
As a control group, the chicken feather bamboo seedling of 18~20cm high is cultivated respectively, is divided into 3 plants one clump, embodiment one is respectively adopted to implementation
Breeding apparatus prepared by four gained wood plastic composite of example is cultivated, and each molding breeding apparatus of embodiment takes 10 respectively
It is cultivated, rooting rate, survival rate, average production height, branch amount and the ground biomass product of chicken feather bamboo was counted after 6 months
It is tired;Specific test result is as shown in table 2:
Table 2
By data above analysis it is found that nutrient matrix and control group ordinary nutritional base prepared by example IV to embodiment six
Matter is compared, and rooting rate is minimum to improve 20 percentage points, and survival rate is minimum to improve 13 percentage points, and average production height is minimum
15cm is improved, branch amount is minimum to improve 6, and ground biomass accumulation is minimum to improve 25g, and indices have significantly
Raising.
The content of phenolic acid is low in nutrient matrix prepared by the present invention, the photosynthetic rate of bamboo, chlorophyll content, cauline leaf life
Long, root system development and biomass accumulation will not be suppressed, and the growth and development ability of bamboo is strong, the survival rate of bamboo cultivation
It is high;In addition the present invention prepares that nutrient matrix water imbibition, water-retaining property are strong, can promote the water suction and development of bamboo root system, seek simultaneously
It is loose to support the light-weight of matrix, quality, it is more convenient to be transported in packing box, promote the aerobic respiration of bamboo root system.
The above embodiments are merely illustrative of the technical solutions of the present invention and it is unrestricted, although with reference to preferred embodiment to this hair
It is bright to be described in detail, it will be understood by those of ordinary skill in the art that, it can modify to technical scheme of the present invention
Or equivalent replacement, without departing from the objective and range of technical solution of the present invention, the claim in the present invention should all be covered
In range.The present invention be not described in detail technology, shape, construction part be known technology.
Claims (7)
1. a kind of nutrient matrix for Ornamental Bamboo cultivation, it is characterised in that:Include the raw material of following parts by weight:Dredging silt
30~40 parts, 20~30 parts of bamboo shoot shell, 10~15 parts of cinder powder, 10~15 parts of fresh pig dung, 5~10 parts of rape cake, pine bark 5~8
Part, 3~5 parts of attapulgite clay/chitosan particle.
2. a kind of preparation method of nutrient matrix for Ornamental Bamboo cultivation, it is characterised in that:Include the following steps:
1) processing of raw material:Bamboo shoot shell, rape cake, pine bark are dried, then is crushed with pulverizer and crosses 120 mesh sieve, is mixed
Powder takes fresh pig dung to add in mixed-powder, is stirred evenly under the rotating speed of 300~500r/min, obtain fermentation material;
2) decomposed fermentation:1) fermentation material obtained in is poured into the porose fermenter in bottom, is uniformly blended into 1.2% times of fermentation material
The zymophyte of weight, then watering wetting fermentation material, makes fermentation material water content reach 75~80%, continues at 45~55 DEG C
Ferment 15~20d, obtains decomposed manure;
3) degradation of phenolic acid:2) decomposed manure that will be obtained in adds in the Fenton reagent of 2~3% times of weight of fermentation material, mixing
Uniformly, 30~60min is reacted under room temperature;
4) preparation of nutrient matrix:First cinder powder, attapulgite clay/chitosan particle and dredging silt are uniformly mixed, so
Decomposed manure in adding in 3) afterwards after the degradation treatment of phenolic acid, adjusting pH value to 5~6, is then dried at 40~50 DEG C,
Obtain nutrient matrix.
3. a kind of preparation method of nutrient matrix for Ornamental Bamboo cultivation according to claim 2, it is characterised in that:Step
It is rapid 2) described in zymophyte include EM bacterium, ferment bacterium and Gymboree zymophyte.
4. a kind of preparation method of nutrient matrix for Ornamental Bamboo cultivation according to claim 2, it is characterised in that:Step
It is rapid 2) described in decomposed fermentation during, carry out a stirring and moisturizing every 3~5d, keep the water content of fermentation material 50~
80%.
5. a kind of preparation method of nutrient matrix for Ornamental Bamboo cultivation according to claim 2, it is characterised in that:Step
It is rapid 4) described in attapulgite clay/chitosan particle preparation method it is as follows:
Step 1, the activation of attapulgite clay:Attapulgite clay is taken, crush and crosses 120 mesh sieve, is roasted at 750 DEG C
1h is cooled to room temperature, and is then immersed in the hydrochloric acid of 10 times of volume 1mol/L, and 3h is stirred at 80 DEG C, and centrifugation removal hydrochloric acid solution sinks
Deionization multiple water in shallow lake rinses, then the precipitation after flushing is immersed the oxalic acid solution that mass fraction is 10%, uses at room temperature
Then supersonic oscillations 2h filters except oxalic acid solution, the multiple water of precipitation deionization rinse, is then dried to obtain work in 110 DEG C
Change attapulgite clay powder;
Step 2, the preparation of chitosan colloidal sol:Chitosan is taken to immerse in the oxalic acid solution that 10 times of volume mass scores are 10%, in
It is fully dissolved under 50 DEG C of magnetic agitation, obtains chitosan colloidal sol;
Step 3, the load of chitosan:The chitosan colloidal sol that step 2 obtains is taken to add in isometric deionized water dilution, fully
One obtained activation attapulgite clay powder of the step of stirring, obtaining chitosan colloidal sol dilution, take 6~10 times of weight of chitosan
End is added to chitosan colloidal sol dilution, then persistently stirs 5h, then stand 5h while stirring, removes supernatant, and precipitation is fallen
Enter the NaOH solution of 5 times of volume 1mol/L, after stirring 30min under the rotating speed of 1500~3000r/min, filter removal solvent,
It is rinsed to neutrality, is then dried in vacuo to get to attapulgite clay/chitosan particle with deionized water again.
6. a kind of preparation method of nutrient matrix for Ornamental Bamboo cultivation according to claim 5, it is characterised in that:Step
The power of ultrasonic wave described in rapid one is 120W, frequency of oscillation 50kHz.
7. a kind of preparation method of nutrient matrix for Ornamental Bamboo cultivation according to claim 5, it is characterised in that:Step
Vacuum drying condition described in rapid three is:Temperature 60 C, vacuum degree 0.09MPa~0.1MPa, time 20h.
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CN111066580A (en) * | 2020-01-19 | 2020-04-28 | 上海炎地农业科技有限公司 | Advanced oxidation process-based edible fungus culture material pretreatment process and application |
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