CN107670630B - A kind of swing solid-liquid reaction kettle - Google Patents

A kind of swing solid-liquid reaction kettle Download PDF

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Publication number
CN107670630B
CN107670630B CN201711069336.3A CN201711069336A CN107670630B CN 107670630 B CN107670630 B CN 107670630B CN 201711069336 A CN201711069336 A CN 201711069336A CN 107670630 B CN107670630 B CN 107670630B
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CN
China
Prior art keywords
autoclave
fixed frame
gear
motor
reaction kettle
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Application number
CN201711069336.3A
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Chinese (zh)
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CN107670630A (en
Inventor
茆康建
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Fuyang Jindi Rubber and Plastic Additives Co., Ltd.
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Fuyang Jindi Rubber And Plastic Additives Co Ltd
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Priority to CN201711069336.3A priority Critical patent/CN107670630B/en
Publication of CN107670630A publication Critical patent/CN107670630A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/28Moving reactors, e.g. rotary drums
    • B01J19/285Shaking or vibrating reactors; reactions under the influence of low-frequency vibrations or pulsations
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers

Abstract

The invention discloses a kind of swing solid-liquid reaction kettles, including pedestal, stabilizer blade, autoclave body, inlet tube, feed inlet and drain pipe, the left and right ends of the pedestal have been respectively fixedly connected with left fixed frame, right fixed frame, left fixed frame, autoclave body is equipped between right fixed frame, gear is arranged in left rotary shaft, the lower section of gear is equipped with half gear, the right side wall of left fixed frame is fixedly connected with first motor, the upper surface of autoclave body is fixedly connected with the second motor, the axle stretch end of second motor is fixedly connected with agitating shaft, agitating shaft passes through to be protruded into autoclave body at the top of autoclave body, several main breaking-edges are distributed on agitating shaft, the lower end of agitating shaft is fixedly connected with grinding head, utilize main breaking-edge, secondary breaking-edge crushes solid reactant, expand the contact area of solid reactant and liquid reactants, keep reaction more abundant, during the reaction, kettle Body swings back and forth, further such that solid reactant is sufficiently mixed with liquid reactants, keeps reaction more abundant.

Description

A kind of swing solid-liquid reaction kettle
Technical field
The present invention relates to a kind of chemical equipment technical field, specifically a kind of swing solid-liquid reaction kettle.
Background technique
The broad understanding of reaction kettle has the rustless steel container physically or chemically reacted, according to different process conditions demands The structure design and parameter configuration of container are carried out, design condition, process, inspection and manufacture, examination are needed according to Its Relevant Technology Standards, To realize the mixture response function of heating, evaporation that technique requires, cooling and low high speed, reaction kettle is widely used in petroleum, changes Work, rubber, pesticide, dyestuff, medicine, food, for completing the technical process such as vulcanization, nitrification, hydrogenation, hydrocarbonylation, polymerization, condensation Pressure vessel, such as reactor, reaction pot, decomposition pot, polymeric kettle etc.;Material generally has carbon manganese steel, stainless steel, zirconium, Ni-based conjunction Often there is material and mix non-uniform situation in golden and other composite materials, existing frequently-used solid-liquid reaction kettle, reaction is caused to be imitated Rate is low, it is difficult to meet the daily production requirement of people.
Summary of the invention
The purpose of the present invention is to provide a kind of swing solid-liquid reaction kettles, to solve mentioned above in the background art ask Topic.
To achieve the above object, the invention provides the following technical scheme:
A kind of swing solid-liquid reaction kettle, including pedestal, stabilizer blade, autoclave body, inlet tube, feed inlet and drain pipe, the base The left and right ends of seat have been respectively fixedly connected with left fixed frame, right fixed frame, and autoclave body, kettle are equipped between left fixed frame, right fixed frame Left rotary shaft, right spindle are respectively fixedly connected at left and right sides of body, the left end of left rotary shaft and left fixed frame are rotatablely connected, right spindle Right end and right fixed frame be rotatablely connected, left rotary shaft, right spindle center line coincide, gear, gear are arranged in left rotary shaft Lower section be equipped with half gear, half gear engage with gear, and half gear is by shaft and the rotation connection of left fixed frame, under half gear End is fixedly connected with fixed plate, and the right side wall of left fixed frame is fixedly connected with first motor, and the axle stretch end of first motor is fixed to be connected It is connected to turntable, the right side wall of turntable is fixedly connected with hold-down bars close to edge, sliding slot is offered in fixed plate, hold-down bars is embedded in In sliding slot, the upper surface of autoclave body is fixedly connected with the second motor, and the left side of the second motor is equipped with inlet tube, and inlet tube and autoclave body connect Logical, the right side of the second motor is equipped with feed inlet, and feed inlet is connected to autoclave body, and the axle stretch end of the second motor is fixedly connected with stirring Axis, agitating shaft passes through to be protruded into autoclave body at the top of autoclave body, and several main breaking-edges are distributed on agitating shaft, set below main breaking-edge There is scraper plate, scraper plate is fixedly connected with agitating shaft, and the side wall of autoclave body is equipped with observation window, the other end of scraper plate and the inner wall of observation window It abuts, the lower section of scraper plate is equipped with spiral plate, and spiral plate is fixedly connected with agitating shaft, and the lower end of agitating shaft is fixedly connected with grinding Head, grinding head is eccentrically mounted, and the bottom of autoclave body is equipped with drain pipe.
As a further solution of the present invention: the lower surface of the pedestal is fixedly connected with stabilizer blade.
As further scheme of the invention: being equipped with valve on the inlet tube.
As further scheme of the invention: several secondary breaking-edges, main breaking-edge, pair is distributed in the inner wall of the autoclave body Breaking-edge is interspersed.
As further scheme of the invention: grinding protrusion is distributed in the side wall of the grinding head.
As further scheme of the invention: being equipped with valve on the drain pipe.
Compared with prior art, the beneficial effects of the present invention are: using main breaking-edge, secondary breaking-edge to solid reactant into Row crushes, and expands the contact area of solid reactant and liquid reactants, keeps reaction more abundant, can be observed using observation window The intracorporal response situation of kettle, can remove the reactant being attached on observation window using scraper plate, drive solid-liquid mixed using spiral plate Close object to seethe up and down, be sufficiently mixed reactant, improve reaction efficiency, using grinding head to the solid reactant of autoclave body bottom into Row, which squeezes, to be crushed, and is contacted solid reactant with liquid reactants more abundant, is kept reaction more abundant, during the reaction, Autoclave body swings back and forth, further such that solid reactant is sufficiently mixed with liquid reactants, keeps reaction more abundant.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of swing solid-liquid reaction kettle;
Fig. 2 is the right view of swing solid-liquid reaction kettle turntable;
Fig. 3 is the top view of grinding head in swing solid-liquid reaction kettle.
In figure: 1- pedestal;2- stabilizer blade;The left fixed frame of 3-;The right fixed frame of 4-;5- autoclave body;6- left rotary shaft;7- right spindle;8- Gear;Half gear of 9-;10- first motor;11- turntable;12- hold-down bars;13- fixed plate;14- inlet tube;15- feed inlet;16- Second motor;17- agitating shaft;The main breaking-edge of 18-;19- pair breaking-edge;20- scraper plate;21- observation window;22- spiral plate;23- is ground Bistrique;24- grinding protrusion;25- drain pipe.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other Embodiment shall fall within the protection scope of the present invention.
Please refer to Fig. 1-3, in the embodiment of the present invention, a kind of swing solid-liquid reaction kettle, including pedestal 1, stabilizer blade 2, autoclave body 5, inlet tube 14, feed inlet 15 and drain pipe 25, the lower surface of the pedestal 1 are fixedly connected with stabilizer blade 2, pedestal 1, left and right two End has been respectively fixedly connected with left fixed frame 3, right fixed frame 4, and autoclave body 5 is equipped between left fixed frame 3, right fixed frame 4, autoclave body 5 The left and right sides has been respectively fixedly connected with left rotary shaft 6, right spindle 7, and the left end of left rotary shaft 6 and left fixed frame 3 are rotatablely connected, right spindle 7 right end and right fixed frame 4 are rotatablely connected, left rotary shaft 6, right spindle 7 center line coincide, autoclave body 5 can be around left rotary shaft 6, right spindle 7 rotates, and gear 8 is arranged in left rotary shaft 6, and the lower section of gear 8 is equipped with half gear 9, and half gear 9 is engaged with gear 8, Half gear 9 is rotatablely connected by shaft and left fixed frame 3, and the lower end of half gear 9 is fixedly connected with fixed plate 13, left fixed frame 3 Right side wall be fixedly connected with first motor 10, the axle stretch end of first motor 10 is fixedly connected with turntable 11, the right side of turntable 11 Wall is fixedly connected with hold-down bars 12 close to edge, sliding slot is offered in fixed plate 13, hold-down bars 12 is in sliding slot, hold-down bars 12 can be free to slide along sliding slot, drives turntable 11 to rotate when first motor 10 is run, and then hold-down bars 12 is driven to rotate, Gu Determine to drive fixed plate 13 to swing while stick 12 rotates, so that half gear, 9 positive and negative rotation is driven, and then with 8 positive and negative rotation of moving gear, from And 6 positive and negative rotation of left rotary shaft is driven, final that autoclave body 5 is driven to swing back and forth, the upper surface of autoclave body 5 is fixedly connected with the second motor 16, The left side of second motor 16 is equipped with inlet tube 14, and inlet tube 14 is connected to autoclave body 5, valve is equipped on inlet tube 14, liquid is anti- Object is answered to enter in autoclave body 5 by inlet tube 14, the right side of the second motor 16 is equipped with feed inlet 15, and feed inlet 15 is connected to autoclave body 5, Solid reactant is entered in autoclave body 5 by feed inlet 15, and the axle stretch end of the second motor 16 is fixedly connected with agitating shaft 17, agitating shaft 17 tops for passing through autoclave body 5 are protruded into autoclave body 5, several main breaking-edges 18 are distributed on agitating shaft 17, the inner wall of autoclave body 5 is distributed with Several pair breaking-edges 19, main breaking-edge 18, secondary breaking-edge 19 are interspersed, and 17 turns of agitating shaft are driven when the second motor 16 is run It is dynamic, and then main breaking-edge 18 is driven to rotate, solid reactant is put into autoclave body 5 from feed inlet 15, utilizes main breaking-edge 18, secondary powder Broken sword 19 crushes solid reactant, and the lower section of main breaking-edge 18 is equipped with scraper plate 20, scraper plate 20 and the fixed company of agitating shaft 17 It connects, the side wall of autoclave body 5 is equipped with observation window 21, and the other end of scraper plate 20 is abutted with the inner wall of observation window 21, utilizes observation window 21 The response situation in autoclave body 5 can be observed, can remove the reactant being attached on observation window 21 using scraper plate 20, scraper plate 20 Lower section is equipped with spiral plate 22, and spiral plate 22 is fixedly connected with agitating shaft 17, and the lower end of agitating shaft 17 is fixedly connected with grinding head 23, Grinding head 23 is eccentrically mounted, and grinding protrusion 24 is distributed in the side wall of grinding head 23, using grinding head 23 to the solid reaction of bottom Object carries out extruding crushing, and the bottom of autoclave body 5 is equipped with drain pipe 25, is equipped with valve on drain pipe 25.
The working principle of the invention is: liquid reactants being injected in autoclave body 5 by inlet tube 14, solid reactant is led to It crosses feed inlet 15 to pour into autoclave body 5, starts the second motor 16, drive agitating shaft 17 to rotate when the second motor 16 is run, and then band It moves main breaking-edge 18 to rotate, solid reactant is put into autoclave body 5 from feed inlet 15, right using main breaking-edge 18, secondary breaking-edge 19 Solid reactant is crushed, and the contact area of solid reactant and liquid reactants is expanded, and is kept reaction more abundant, is utilized sight Response situation in autoclave body 5 can be observed by examining window 21, be can remove the reactant being attached on observation window 21 using scraper plate 20, stirred Mixing when axis 17 rotates drives spiral plate 22 to rotate, and drives solidliquid mixture to seethe up and down, is sufficiently mixed reactant, improves reaction Efficiency drives grinding head 23 to rotate when agitating shaft 17 rotates, and utilizes grinding head 23, the solid of raised 24 pairs of 5 bottoms of autoclave body of grinding Reactant carries out extruding crushing, contacts solid reactant with liquid reactants more abundant, keeps reaction more abundant, the first electricity It drives turntable 11 to rotate when machine 10 is run, and then hold-down bars 12 is driven to rotate, fixed plate 13 is driven while hold-down bars 12 rotates It swings, so that half gear, 9 positive and negative rotation is driven, and then with 8 positive and negative rotation of moving gear, so that 6 positive and negative rotation of left rotary shaft is driven, it is final to drive Autoclave body 5 swings back and forth, further such that solid reactant is sufficiently mixed with liquid reactants, keeps reaction more abundant.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power Benefit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent elements of the claims Variation is included within the present invention.Any reference signs in the claims should not be construed as limiting the involved claims.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art The other embodiments being understood that.

Claims (6)

1. a kind of swing solid-liquid reaction kettle, including pedestal (1), stabilizer blade (2), autoclave body (5), inlet tube (14), feed inlet (15) With drain pipe (25);It is characterized in that, the left and right ends of the pedestal (1) have been respectively fixedly connected with left fixed frame (3), right fixation Frame (4), is equipped with autoclave body (5) between left fixed frame (3), right fixed frame (4), and autoclave body has been respectively fixedly connected at left and right sides of (5) Left rotary shaft (6), right spindle (7), the left end and left fixed frame (3) of left rotary shaft (6) are rotatablely connected, the right end of right spindle (7) and the right side Fixed frame (4) rotation connection, left rotary shaft (6), right spindle (7) center line coincide, gear (8) are arranged in left rotary shaft (6), The lower section of gear (8) is equipped with half gear (9), and half gear (9) is engaged with gear (8), and half gear (9) passes through shaft and left fixed frame (3) it is rotatablely connected, the lower end of half gear (9) is fixedly connected with fixed plate (13), and the right side wall of left fixed frame (3) is fixedly connected with First motor (10), the axle stretch end of first motor (10) are fixedly connected with turntable (11), and the right side wall of turntable (11) leans on proximal edge Place is fixedly connected with hold-down bars (12), and sliding slot is offered in fixed plate (13), and hold-down bars (12) is embedded in sliding slot, autoclave body (5) Upper surface is fixedly connected with the second motor (16), and the left side of the second motor (16) is equipped with inlet tube (14), inlet tube (14) and kettle The right side of body (5) connection, the second motor (16) is equipped with feed inlet (15), and feed inlet (15) is connected to autoclave body (5), the second motor (16) axle stretch end is fixedly connected with agitating shaft (17), and agitating shaft (17), which passes through, to be protruded at the top of autoclave body (5) in autoclave body (5), is stirred Mix and several main breaking-edges (18) be distributed on axis (17), the lower section of main breaking-edge (18) is equipped with scraper plate (20), scraper plate (20) with stir It mixes axis (17) to be fixedly connected, the side wall of autoclave body (5) is equipped with observation window (21), the other end and observation window (21) of scraper plate (20) Inner wall abuts, and the lower section of scraper plate (20) is equipped with spiral plate (22), and spiral plate (22) is fixedly connected with agitating shaft (17), agitating shaft (17) lower end is fixedly connected with grinding head (23), and grinding head (23) is eccentrically mounted, and the bottom of autoclave body (5) is equipped with drain pipe (25).
2. swing solid-liquid reaction kettle according to claim 1, which is characterized in that the lower surface of the pedestal (1) is fixed It is connected with stabilizer blade (2).
3. swing solid-liquid reaction kettle according to claim 1, which is characterized in that be equipped with valve on the inlet tube (14) Door.
4. swing solid-liquid reaction kettle according to claim 1, which is characterized in that the inner wall of the autoclave body (5) is distributed with Several pair breaking-edges (19), main breaking-edge (18), secondary breaking-edge (19) are interspersed.
5. swing solid-liquid reaction kettle according to claim 1, which is characterized in that the side wall of the grinding head (23) is distributed There is grinding raised (24).
6. swing solid-liquid reaction kettle according to claim 1, which is characterized in that be equipped with valve on the drain pipe (25) Door.
CN201711069336.3A 2017-11-03 2017-11-03 A kind of swing solid-liquid reaction kettle Active CN107670630B (en)

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Application Number Priority Date Filing Date Title
CN201711069336.3A CN107670630B (en) 2017-11-03 2017-11-03 A kind of swing solid-liquid reaction kettle

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Application Number Priority Date Filing Date Title
CN201711069336.3A CN107670630B (en) 2017-11-03 2017-11-03 A kind of swing solid-liquid reaction kettle

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CN107670630B true CN107670630B (en) 2019-07-19

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Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108380115A (en) * 2018-03-01 2018-08-10 吴迪 A kind of oscillatory type building coating agitating device
CN108404775A (en) * 2018-03-01 2018-08-17 吴迪 A kind of swing type building coating agitating device
CN108408722A (en) * 2018-06-05 2018-08-17 李训祺 A kind of graphene oxide preparation method
CN108994066A (en) * 2018-07-12 2018-12-14 蒋友裕 A kind of swing type soil remediation equipment
CN110306419A (en) * 2019-07-16 2019-10-08 燕明月 A kind of swing type lines on road surface equipment
CN111022925A (en) * 2019-11-18 2020-04-17 大连理工大学 Visual swing kettle device and method for inhibiting pipeline hydrate blockage

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN203507872U (en) * 2013-08-20 2014-04-02 中国石油化工股份有限公司 Stirring device for integrated pulping of solid crushing and solid-liquid mixing
CN204735218U (en) * 2015-06-02 2015-11-04 山东同创精细化工股份有限公司 Novel reagent reation kettle for movable paper making chemical
CN205700581U (en) * 2016-05-05 2016-11-23 常州高特新材料有限公司 Reactor turning device
CN106552575A (en) * 2016-10-17 2017-04-05 无锡市日升化工有限公司 A kind of good industrial chemicals reactor of mixing effect

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN203507872U (en) * 2013-08-20 2014-04-02 中国石油化工股份有限公司 Stirring device for integrated pulping of solid crushing and solid-liquid mixing
CN204735218U (en) * 2015-06-02 2015-11-04 山东同创精细化工股份有限公司 Novel reagent reation kettle for movable paper making chemical
CN205700581U (en) * 2016-05-05 2016-11-23 常州高特新材料有限公司 Reactor turning device
CN106552575A (en) * 2016-10-17 2017-04-05 无锡市日升化工有限公司 A kind of good industrial chemicals reactor of mixing effect

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Effective date of registration: 20190624

Address after: 236000 South Side of Weisan Road, Yingdong Economic Development Zone, Fuyang City, Anhui Province

Applicant after: Fuyang Jindi Rubber and Plastic Additives Co., Ltd.

Address before: Unit 302, No. 70 Tongguan South Road, Haizhou District, Lianyungang City, Jiangsu Province

Applicant before: Mao Kangjian

Effective date of registration: 20190624

Address after: 236000 South Side of Weisan Road, Yingdong Economic Development Zone, Fuyang City, Anhui Province

Applicant after: Fuyang Jindi Rubber and Plastic Additives Co., Ltd.

Address before: Unit 302, No. 70 Tongguan South Road, Haizhou District, Lianyungang City, Jiangsu Province

Applicant before: Mao Kangjian

GR01 Patent grant
GR01 Patent grant
PE01 Entry into force of the registration of the contract for pledge of patent right
PE01 Entry into force of the registration of the contract for pledge of patent right

Denomination of invention: Swinging solid-liquid reaction kettle

Effective date of registration: 20200420

Granted publication date: 20190719

Pledgee: Anhui Funan Rural Commercial Bank Co., Ltd. Santa sub branch

Pledgor: Fuyang Jindi Rubber and Plastic Additives Co.,Ltd.

Registration number: Y2020980001640