CN107555930A - One kind is high-strength, block water air entrained concrete building block and preparation method - Google Patents
One kind is high-strength, block water air entrained concrete building block and preparation method Download PDFInfo
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Abstract
The present invention proposes a kind of high-strength, air entrained concrete building block and the preparation method of blocking water are by gypsum, quick lime, cement, flyash is ground to below 10 μm of particle diameter, make its activation, add papermaking wastewater and aluminium powder, got angry by aluminium powder in slurry, organic saponified foaming in papermaking wastewater, fine active calcium material is promoted to generate spherical afwillite hard wall material with siliceous material hydro-thermal, overcome existing air-entrained concrete building block exist it is hygroscopic, low intensity, the high technological deficiency of construction requirement, so as to obtain the high-strength air entrained concrete building block to block water, further, preparation technology of the present invention is simple, raw material sources are extensive, turn waste into wealth, technique is compatible with the Preparation equipment of existing building building block, it is easily achieved scale industrial production.
Description
Technical field
The present invention relates to building material manufacture field, and in particular to it is a kind of it is high-strength, block water air entrained concrete building block and
Preparation method.
Background technology
New Building Materials are caused a new generation's upgrading construction material, main bag on the basis of traditional building material
Include novel wall material, heat preserving and insulating material, waterproof and sealing material and decorating and renovating material etc..When the low-carbon epoch arrive,
In the case where country advocates energy-saving, Transformation Development overall background, green low-carbon, energy-conserving and environment-protective, which have become building material, to return
The mission kept away.For this, with it is green, sharp it is useless, heat-insulated, insulation, fire prevention, it is light, high-strength, substitute, cost is cheap, section is native, save
Ground therefrom obtains huge development new opportunities for the building material of target.The industrial output value of building material is more than 600,000,000,000 yuan, year
14% is grown beyond, family more than 5000 of working enterprise.At present, constantly there is building material to be developed, particularly some Composites,
Multifunction, energy-saving, greenization, the building material of high-strength light occupy the proportion of traditional construction material more than 50%.
Air-entrained concrete building block as a kind of novel wall material, due to good thermal and insulating performance, it is in light weight,
The advantages that anti-seismic performance is good, applied in the filling wall and load bearing wall of building, to improving the heat-insulating property of building structure, reducing
Building load has obvious action.Air-entrained concrete building block is mainly with sand, rubble, flyash and containing silicon tailings and calcareous material
The gel of material is primary raw material, fills foaming agent aluminium powder, passes through the works such as dispensing, stirring, cast, precuring, cutting, steam pressure, maintenance
Light porous silicate product made of skill process.
But when specifically used, air-entrained concrete building block is because having more insertion space, therefore it is high to absorb water, it is difficult to hinders
Long-term immersion is kept off, thus it is high to the waterproof requirement of wall.In addition, air-entrained concrete building block surface strength is low, surface holds
Powder is easily played, is not easy to preferably bond with mortar during use, it usually needs special mortar is bonded.Therefore, it is existing to add
Gas concrete segment is high to use and construction technical requirement, is widely applied so as to hinder it.
Chinese invention application number 201510754705.7 discloses a kind of good autoclave aerated concrete building block of mechanical strength
And preparation method thereof, the hydroxyl to dissociate in cellulose is enclosed by carrying out acetylization reaction to cypress fiber, improves material
Hydrophobic performance and heat endurance, then coordinate physical modification method to add other active ingredients, improve fiber steam pressurized
Durability and dispersiveness in concrete so that aerated-block has splendid mechanical strength, excellent heat-resisting quantity and water proofing property
Energy.But the hydrophobic performance of material and heat endurance depend on cypress fiber progress acetylization reaction degree in the program, furthermore
Hardening strength is carried out using string to be limited.
Therefore, the high technological deficiency of hygroscopic, low intensity, construction requirement be present for existing air-entrained concrete building block, open
Send out new preparation method a kind of and can effectively manufacture and produce that high-strength, the air-entrained concrete building block that blocks water is significant.
The content of the invention
The defects of hygroscopic, low intensity, high construction requirement be present for existing air-entrained concrete building block, the present invention proposes one
Kind is high-strength, block water air entrained concrete building block and preparation method, and gypsum, quick lime, cement, flyash are ground into particle diameter 10
Below μm, make its activation, add papermaking wastewater and aluminium powder, got angry by aluminium powder in slurry, it is organic saponified in papermaking wastewater
Foaming, fine active calcium material is promoted to generate spherical afwillite hard wall material with siliceous material hydro-thermal, so that gram
Taken existing air-entrained concrete building block and the high technological deficiency of hygroscopic, low intensity, construction requirement be present, obtain it is high-strength block water plus
Gas concrete building blocks.
To solve the above problems, the present invention uses following technical scheme:
On the one hand offer one kind is high-strength, block water air entrained concrete building block, and the air entrained concrete building block is by including under
Row raw material is prepared:Gypsum 10-25 parts, quick lime 13-25 parts, cement 15-20 parts, flyash 15-25 parts, aluminium powder
5-15 parts, papermaking wastewater 15-60 parts, surfactant 1-2 parts.
Preferably, papermaking wastewater concentration be quality solid content 10-25%, and main component is alkali lye and wooden on a small quantity
Element, lignocellulosic.
Preferably, the surfactant is one kind in sulfonated polystyrene, sulfonated acetone formaldehyde condensation products.
On the other hand, there is provided a kind of high-strength, the air entrained concrete building block that blocks water preparation method, comprise the following steps:
(1)Each raw material is weighed in proportion, gypsum, quick lime are crushed, and adds flyash, cement mixing is ground into ball mill
Powdery, surfactant is sprayed into thereto, be uniformly mixed in spray, obtain active powder material, penetrating speed is 0.1-3m/s;
(2)Papermaking wastewater and aluminium powder are added into step(1)Active powder material in, continue to be stirred slurry, by aluminium powder in slurry
In got angry with the acid reaction in papermaking wastewater, while discharge amount of heat, heating mixed slurry is to 50-65 DEG C, in papermaking wastewater
Organic acid and alkaline calcium salt saponification bubble, be stirred continuously to slurry and no longer produce gas;
(3)By step(2)The slurry cast of preparation to base substrate in-mold molding, 12-24 hours reach cutting intensity after be stripped, enter
Shaping blank is made in row cutting;
(4)Above-mentioned shaping embryo material is delivered to drying box, finished product is made in 75-85 DEG C of drying 10-15 hour.
Preferably, after using ball mill grinding, gypsum, quick lime, cement, gypsum, flyash be ground to 10 μm of particle diameter with
Under.
Preferably, after the slurry cast enters mould, it is compacted using pressure head, moulding pressure 15-300KPa.
There is the high technological deficiency of hygroscopic, low intensity, construction requirement in existing air-entrained concrete building block, the present invention proposes one
Kind is high-strength, block water air entrained concrete building block and preparation method, and gypsum, quick lime, cement, flyash are ground into particle diameter 10
Below μm, make its activation, add papermaking wastewater and aluminium powder, got angry by aluminium powder in slurry, it is organic saponified in papermaking wastewater
Foaming, fine active calcium material is promoted to generate spherical afwillite hard wall material with siliceous material hydro-thermal, so as to
To the high-strength air entrained concrete building block to block water.Its significant advantage is handled by miniaturization so that calcareous material and silicon
Material is sufficiently activated, and promotion forms more afwillite hard wall materials, so as to improve the strong of air-entrained concrete building block
Degree;Meanwhile using papermaking wastewater, twice laid, and organic saponified and colloid substances foaming therein are not only realized, is promoted
Fine active calcium material generates spherical closing afwillite hard wall material with siliceous material hydro-thermal, so as to prevent water
Intrusion.
By experiment test, the air entrained concrete building block compression strength of gained is 2.5-5.8MPa, density 0.6-
0.7g/cm3,Water absorption rate is 0.33-0.52%.
One kind of the invention is high-strength, block water air entrained concrete building block and preparation method, and compared with prior art, it is protruded
The characteristics of and excellent effect be:
1st, the present invention proposes that one kind is high-strength, block water air entrained concrete building block, and the building block surface is by spherical hydration silicon
Sour calcium hard wall material parcel, so as to ensure water resistance characteristic and improve the intensity of air-entrained concrete building block.
2nd, this programme uses papermaking wastewater, not only realizes twice laid, and utilize therein organic saponified in aluminium
Bubbled in the presence of powder, promote fine active calcium material to generate spherical closing hard wall material with siliceous material hydro-thermal, keep away
The additional chemical reaction of addition material water-proof material is exempted from.
3rd, scheme preparation technology disclosed by the invention is simple, and raw material sources are extensive, turn waste into wealth, and technique is built with existing building
The Preparation equipment of block is compatible, it is easy to accomplish scale industrial production.
Embodiment
Below by way of embodiment, the present invention is described in further detail, but this should not be interpreted as to the present invention
Scope be only limitted to following example.In the case where not departing from above method thought of the present invention, according to ordinary skill
The various replacements or change that knowledge and customary means are made, should be included in the scope of the present invention.
Embodiment 1
(1)Each raw material is weighed by weight:Take 22 parts of gypsum, 15 parts of quick lime, 18 parts of cement, 22 parts of flyash, 10 parts of aluminium powder,
60 parts of papermaking wastewater, sulfonated polystyrene 1-2 parts.Gypsum, quick lime are crushed, add flyash, cement mixing in ball mill
In be ground into powdery below 10 μm of particle diameter, spray into sulfonated polystyrene thereto, be uniformly mixed in spray, obtain activity
Powder, penetrating speed are 2.3m/s;
(2)Papermaking wastewater and aluminium powder are added into step(1)Active powder material in, continue to be stirred slurry, by aluminium powder in slurry
In got angry with the acid reaction in papermaking wastewater, while discharge amount of heat, heating mixed slurry is to 50-65 DEG C, in papermaking wastewater
Organic acid and alkaline calcium salt saponification bubble, be stirred continuously to slurry and no longer produce gas;
(3)By step(2)In the slurry cast of preparation to base substrate mould, it is compacted using pressure head, moulding pressure 15kPa, 24 is small
When shaping reach cutting intensity after be stripped, cut into length 600mm, height 240mm, thickness 200mm specifications into parison
Material;
(4)Above-mentioned shaping embryo material is delivered to drying box, finished product is obtained within 15 hours in 75 DEG C of drying.
To length 600mm, height 240mm, thickness 200mm sample block carry out performance test, air entrained concrete building block
Density is 0.65g/cm3, compression strength 5.8MPa, water absorption rate 0.52%.
Embodiment 2
(1)Each raw material is weighed by weight:Take 18 parts of gypsum, 22 parts of quick lime, 18 parts of cement, 18 parts of flyash, 7 parts of aluminium powder,
55 parts of papermaking wastewater, 1 part of sulfonated acetone formaldehyde condensation products.Gypsum, quick lime are crushed, add flyash, cement mixing in ball
The powdery being ground into grinding machine below 10 μm of particle diameter, sulfonated acetone formaldehyde condensation products are sprayed into thereto, be stirred in spray
It is even, active powder material is obtained, penetrating speed is 2.5m/s;
(2)Papermaking wastewater and aluminium powder are added into step(1)Active powder material in, continue to be stirred slurry, by aluminium powder in slurry
In got angry with the acid reaction in papermaking wastewater, while discharge amount of heat, heating mixed slurry is to 60 DEG C, having in papermaking wastewater
Machine acid bubbles with alkaline calcium salt saponification, is stirred continuously to slurry and no longer produces gas;
(3)By step(2)In the slurry cast of preparation to base substrate mould, it is compacted using pressure head, moulding pressure 100kPa, 15 is small
When shaping reach cutting intensity after be stripped, cut into length 600mm, height 240mm, thickness 200mm specifications into parison
Material;
(4)Above-mentioned shaping embryo material is delivered to drying box, is dried 15 hours at 80 DEG C, finished product is made.
To length 600mm, height 240mm, thickness 200mm sample block carry out performance test, air entrained concrete building block
Density is 0.7g/cm3, compression strength 4.5MPa, water absorption rate 0.42%.
Embodiment 3
(1)Each raw material is weighed by weight:Take 25 parts of gypsum, 15 parts of quick lime, 15 parts of cement, 25 parts of flyash, 10 parts of aluminium powder,
60 parts of papermaking wastewater, 2 parts of sulfonated polystyrene.Gypsum, quick lime are crushed, add flyash, cement mixing in ball mill
The powdery being ground into below 10 μm of particle diameter, sprays into sulfonated polystyrene thereto, is uniformly mixed in spray, obtains activity powder
Material, penetrating speed is 0.8m/s;
(2)Papermaking wastewater and aluminium powder are added into step(1)Active powder material in, continue to be stirred slurry, by aluminium powder in slurry
In got angry with the acid reaction in papermaking wastewater, while discharge amount of heat, heating mixed slurry is to 60 DEG C, having in papermaking wastewater
Machine acid bubbles with alkaline calcium salt saponification, is stirred continuously to slurry and no longer produces gas;
(3)By step(2)In the slurry cast of preparation to base substrate mould, it is compacted using pressure head, moulding pressure 150kPa, 18 is small
When shaping reach cutting intensity after be stripped, cut into length 600mm, height 240mm, thickness 200mm specifications into parison
Material;
(4)Above-mentioned shaping embryo material is delivered to drying box, is dried 12 hours at 79 DEG C, finished product is made.
To length 600mm, height 240mm, thickness 200mm sample block carry out performance test, air entrained concrete building block
Density is 0.68g/cm3, compression strength 3.2MPa, water absorption rate 0.33%.
Embodiment 4
(1)Each raw material is weighed by weight:Take 10 parts of gypsum, 25 parts of quick lime, 20 parts of cement, 15 parts of flyash, 5 parts of aluminium powder,
18 parts of papermaking wastewater, 1 part of sulfonated acetone formaldehyde condensation products.Gypsum, quick lime are crushed, add flyash, cement mixing in ball
The powdery being ground into grinding machine below 10 μm of particle diameter, sulfonated acetone formaldehyde condensation products are sprayed into thereto, be stirred in spray
It is even, active powder material is obtained, penetrating speed is 3m/s;
(2)Papermaking wastewater and aluminium powder are added into step(1)Active powder material in, continue to be stirred slurry, by aluminium powder in slurry
In got angry with the acid reaction in papermaking wastewater, while discharge amount of heat, heating mixed slurry is to 55 DEG C, having in papermaking wastewater
Machine acid bubbles with alkaline calcium salt saponification, is stirred continuously to slurry and no longer produces gas;
(3)By step(2)In the slurry cast of preparation to base substrate mould, it is compacted using pressure head, moulding pressure 15KPa, 12 is small
When shaping reach cutting intensity after be stripped, cut into length 600mm, height 240mm, thickness 200mm specifications into parison
Material;
(4)Above-mentioned shaping embryo material is delivered to drying box, is dried 15 hours at 75 DEG C, finished product is made.
To length 600mm, height 240mm, thickness 200mm sample block carry out performance test, air entrained concrete building block
Density is 0.63g/cm3, compression strength 2.8MPa, water absorption rate 0.42%.
Embodiment 5
(1)Each raw material is weighed by weight:Take 25 parts of gypsum, 13 parts of quick lime, 20 parts of cement, 25 parts of flyash, 5 parts of aluminium powder,
15 parts of papermaking wastewater, 2 parts of sulfonated polystyrene.Gypsum, quick lime are crushed, add flyash, cement mixing in ball mill
The powdery being ground into below 10 μm of particle diameter, sprays into sulfonated polystyrene thereto, is uniformly mixed in spray, obtains activity powder
Material, penetrating speed is 0.1m/s;
(2)Papermaking wastewater and aluminium powder are added into step(1)Active powder material in, continue to be stirred slurry, by aluminium powder in slurry
In got angry with the acid reaction in papermaking wastewater, while discharge amount of heat, heating mixed slurry is to 50 DEG C, having in papermaking wastewater
Machine acid bubbles with alkaline calcium salt saponification, is stirred continuously to slurry and no longer produces gas;
(3)By step(2)In the slurry cast of preparation to base substrate mould, it is compacted using pressure head, moulding pressure 300KPa, 24 is small
When shaping reach cutting intensity after be stripped, cut into length 600mm, height 240mm, thickness 200mm specifications into parison
Material;
(4)Above-mentioned shaping embryo material is delivered to drying box, is dried 10 hours at 85 DEG C, finished product is made.
To length 600mm, height 240mm, thickness 200mm sample block carry out performance test, air entrained concrete building block
Density is 0.7g/cm3, compression strength 5.2MPa, water absorption rate 0.41%.
Claims (5)
1. it is a kind of it is high-strength, block water air entrained concrete building block, it is characterised in that the air entrained concrete building block by including
Following raw materials in part by weight is prepared:Gypsum 10-25 parts, quick lime 13-25 parts, cement 15-20 parts, flyash 15-25 parts, aluminium
Powder 5-15 parts, papermaking wastewater 15-60 parts, surfactant 1-2 parts;The papermaking wastewater concentration is quality solid content 10-25%;
The surfactant is one kind in sulfonated polystyrene, sulfonated acetone formaldehyde condensation products.
2. high-strength, the air entrained concrete building block that blocks water the preparation method described in a kind of any one of claim 1-4, its feature
It is, comprises the following steps:
(1)Each raw material is weighed in proportion, gypsum, quick lime are crushed, and adds flyash, cement mixing is ground into ball mill
Powdery, surfactant is sprayed into thereto, be uniformly mixed in spray, obtain active powder material, penetrating speed is 0.1-3m/s;
(2)Papermaking wastewater and aluminium powder are added into step(1)Active powder material in, continue to be stirred slurry, by aluminium powder in slurry
In got angry with the acid reaction in papermaking wastewater, while discharge amount of heat, heating mixed slurry is to 50-65 DEG C, in papermaking wastewater
Organic acid and alkaline calcium salt saponification bubble, be stirred continuously to slurry and no longer produce gas;
(3)By step(2)The slurry cast of preparation to base substrate in-mold molding, 12-24 hours reach cutting intensity after be stripped, enter
Shaping blank is made in row cutting;
(4)Above-mentioned shaping embryo material is delivered to drying box, 10-15 hours are dried at 75-85 DEG C, in by 600-800 DEG C of kiln
Firing obtains finished product.
3. a kind of high-strength, the air entrained concrete building block that blocks water preparation method according to claim 2, its feature exist
In after ball mill grinding, gypsum, quick lime, cement, gypsum, flyash are ground to below 10 μm of particle diameter.
4. a kind of high-strength, the air entrained concrete building block that blocks water preparation method according to claim 2, its feature exist
In the papermaking wastewater is by hypochlorous acid, sodium hypochlorite, hydrogen peroxide bleaching pretreatment.
5. a kind of high-strength, the air entrained concrete building block that blocks water preparation method according to claim 2, its feature exist
After, the slurry cast enters mould, it is compacted using pressure head, moulding pressure 15-300KPa.
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CN108164206A (en) * | 2018-01-17 | 2018-06-15 | 重庆京纬再生资源有限公司 | A kind of preparation method of strong concrete building block |
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