CN107497382A - A kind of reactor reacted jointly for various materials - Google Patents
A kind of reactor reacted jointly for various materials Download PDFInfo
- Publication number
- CN107497382A CN107497382A CN201710790156.8A CN201710790156A CN107497382A CN 107497382 A CN107497382 A CN 107497382A CN 201710790156 A CN201710790156 A CN 201710790156A CN 107497382 A CN107497382 A CN 107497382A
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- China
- Prior art keywords
- kettle
- auxiliary
- spindle motor
- reaction warehouse
- various materials
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
- B01F23/70—Pre-treatment of the materials to be mixed
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/05—Stirrers
- B01F27/07—Stirrers characterised by their mounting on the shaft
- B01F27/074—Stirrers characterised by their mounting on the shaft having two or more mixing elements being concentrically mounted on the same shaft
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/05—Stirrers
- B01F27/09—Stirrers characterised by the mounting of the stirrers with respect to the receptacle
- B01F27/091—Stirrers characterised by the mounting of the stirrers with respect to the receptacle with elements co-operating with receptacle wall or bottom, e.g. for scraping the receptacle wall
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/05—Stirrers
- B01F27/11—Stirrers characterised by the configuration of the stirrers
- B01F27/17—Stirrers with additional elements mounted on the stirrer, for purposes other than mixing
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
- B01F27/805—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis wherein the stirrers or the receptacles are moved in order to bring them into operative position; Means for fixing the receptacle
- B01F27/806—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis wherein the stirrers or the receptacles are moved in order to bring them into operative position; Means for fixing the receptacle with vertical displacement of the stirrer, e.g. in combination with means for pivoting the stirrer about a vertical axis in order to co-operate with different receptacles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
- B01F27/87—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis the receptacle being divided into superimposed compartments
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
- B01F27/90—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with paddles or arms
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/10—Maintenance of mixers
- B01F35/12—Maintenance of mixers using mechanical means
- B01F35/123—Maintenance of mixers using mechanical means using scrapers for cleaning mixers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/006—Baffles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/008—Feed or outlet control devices
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00076—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
- B01J2219/00085—Plates; Jackets; Cylinders
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00162—Controlling or regulating processes controlling the pressure
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Mixers Of The Rotary Stirring Type (AREA)
Abstract
The invention discloses a kind of reactor reacted jointly for various materials, it is related to pressure vessel field, including kettle, spindle motor and auxiliary spindle motor, the baffle plate that kettle is divided into premix feed bin and reaction warehouse is provided with the kettle, the baffle plate is provided with the material outlet of two solenoid valve controls, the spindle motor is connected with the telescopic rotating shaft that autoclave body bottom is extended to through baffle plate, agitating paddle is connected with the telescopic rotating shaft, the agitating paddle has setting in reaction warehouse and premix feed bin, the auxiliary spindle motor is connected with transmission component, the transmission device, which is connected with, auxiliary stirs device, the present invention can be such that material is slightly mixed in feed bin is premixed, comprehensive stirring is then carried out in reaction warehouse, material is fully contacted, efficiently reacted.
Description
Technical field
The present invention relates to pressure vessel field, more particularly, to a kind of reactor reacted jointly for various materials.
Background technology
Reactor is a kind of conventional consersion unit in chemical plant, be for completing to vulcanize, nitrifying, hydrogenating, hydrocarbonylation, polymerization,
The pressure vessel of the technical process such as condensation, it is typically by kettle, transmission device, agitating device, heater, cooling device, close
Seal apparatus etc. forms, and relies primarily on motor driven agitating shaft during the course of the reaction and reactant is stirred, it is fully reacted
Obtain required product.
For existing most of reactor course of reaction for material is sequentially added in reactor, being directly stirred makes its anti-
Should, first put into the material that puts into afterwards in different levels, material stirring can be caused insufficient, cause material to be not sufficiently reacted,
More accessory substance is often derived, both wastes raw material, is difficult to separate so as to influence product quality with product again, just at last can
Separated by separable programming, such separable programming can also increase the workload of worker, waste corporate resource.
The content of the invention
It is more to improve existing reactor input the invention provides a kind of reactor reacted jointly for various materials
The problem of insufficient is stirred during kind material.
In order to solve the above-mentioned technical problem, the technical solution adopted by the present invention is summarized as follows:
A kind of reactor reacted jointly for various materials, including kettle, spindle motor and auxiliary spindle motor, the kettle
Inside is provided with the baffle plate that kettle is divided into the premix feed bin on upper strata and the reaction warehouse of lower floor, and the baffle plate is provided with two and reaction
The material outlet by solenoid valve control of storehouse connection, the spindle motor are connected with decelerator, and the decelerator is connected with through baffle plate
Extend to the telescopic rotating shaft of reaction warehouse, the telescopic rotating shaft axis body and axle bottom are respectively equipped with agitating paddle and consistent with bottom shape
Scraper, the agitating paddle premix feed bin and reaction warehouse in have setting, be additionally provided with the reaction warehouse it is some it is auxiliary stir device,
The auxiliary device that stirs is connected with transmission component, and the transmission component is connected with auxiliary spindle motor, in spindle motor at the top of the kettle
Both sides are respectively provided with an identical charging aperture, and the autoclave body bottom is provided with a discharging opening and support base.
Further, the reactor is externally provided with electric heating cover, and the temperature of reactor can be regulated and controled, in order to
Material is fully reacted.
Further, the auxiliary device half of stirring rotates clockwise, and half rotates counterclockwise, and the auxiliary device that stirs stirs dress with master
Put mutual cooperation so that dead angle is not present in stirring, and material can fully be reacted.
Further, the auxiliary spindle motor is connected with decelerator, for the different phase of material reaction, can pass through tune
Save decelerator and change mixing speed, in order to avoid influence material reaction.
Further, pressure gauge is provided with the kettle, the pressure gauge is connected with through baffle plate and extends to reaction
Inductor in storehouse, reacting kettle inner pressure can be monitored in real time, in order to avoid there is the situation of the excessive and fried kettle of pressure.
In summary, by adopting the above-described technical solution, the beneficial effects of the invention are as follows:
1. two charging apertures can add different materials simultaneously, and paddle is provided with feed bin is premixed, make material
It can slightly be mixed in feed bin is premixed, be advantageous to material and fully reacted in reaction warehouse;
2. in reaction warehouse be provided with it is some it is auxiliary stir device, they with telescopic rotating shaft agitating paddle mutual cooperation be stirred,
Simultaneous retractable rotating shaft bottom is also connected with the scraper consistent with bottom shape, can prevent materials from bonding can not be fully anti-in bottom
Should, meanwhile, telescopic rotating shaft can control the position of scraper and paddle in kettle, and such device to stir without dead angle,
Material can fully be reacted;
3. electric heating cover can provide endlessly heat for reactor, the temperature of reactor is set to maintain most suitable thing
Expect the position of reaction;
4. pressure gauge can be monitored in real time to the pressure in reactor, worker can be reminded to carry out pressure release behaviour when pressure is high
Make, avoid the generation for the situation that fried kettle is produced because of hypertonia in kettle.
Brief description of the drawings
Fig. 1 internal structure schematic diagrams of the present invention;
In figure mark for:1st, kettle;2nd, charging aperture;3rd, spindle motor;4th, decelerator;5th, telescopic rotating shaft;6th, baffle plate;7th, it is pre-
Blending bunker;9th, material outlet;10th, pressure gauge;11st, inductor;12nd, electric heating cover;13rd, auxiliary spindle motor;15th, transmission component;16、
Agitating paddle;17th, it is auxiliary to stir device;18th, scraper;19th, discharging opening;20th, support base;21st, reaction warehouse.
Embodiment
The present invention is described in further detail with reference to the accompanying drawings and detailed description.Embodiments of the present invention bag
Include but be not limited to the following example.
Embodiment 1
As shown in figure 1, a kind of reactor reacted jointly for various materials, including kettle 1, spindle motor 3 and auxiliary axle
Motor 13, the inside of kettle 1 are provided with the baffle plate 6 that kettle 1 is divided into the premix feed bin 7 on upper strata and the reaction warehouse 21 of lower floor,
The baffle plate 6 is provided with two material outlets 9 by solenoid valve control connected with reaction warehouse 21, and the spindle motor 3, which is connected with, to be subtracted
Fast device 4, the decelerator 4 are connected with the telescopic rotating shaft 5 that reaction warehouse 21 is extended to through baffle plate 6, the axis body of telescopic rotating shaft 5 and axle
Bottom is respectively equipped with agitating paddle 16 and the scraper 18 consistent with bottom shape, and the agitating paddle 16 is in premix feed bin 7 and reaction warehouse
Have setting in 21, be additionally provided with the reaction warehouse 21 it is some it is auxiliary stir device 17, it is described auxiliary to stir device 17 and the phase of transmission component 15
Even, the transmission component 15 is connected with auxiliary spindle motor 13, be respectively provided with the top of the kettle 1 on the both sides of spindle motor 3 one it is identical
Charging aperture 2, the autoclave body bottom is provided with a discharging opening 19 and support base 20.
Operation principle of the present invention:Material needed for reaction is added in premix feed bin 7 by charging aperture 2, motor 3 is opened, makes
Obtain agitating paddle 16 can slightly to mix material, then control electromagnetic valve switch, material is entered reaction warehouse from material outlet 9
In 21, then open auxiliary spindle motor 13 and drive the auxiliary device 17 that stirs to be stirred material by transmission component 15, while can pass through
Telescopic rotating shaft 5 adjusts the position of scraper, and bottom material is swept and is stirred reaction, will by discharging opening 19 after the completion of reaction
Material takes out.
The present embodiment by being pre-mixed to material, set it is main stir device and it is some it is auxiliary stir device, material is filled
Divide stirring, in the absence of stirring dead angle so that material can fully react, and reduce the generation of byproduct of reaction, improve reactant
Purity, saved raw material, reduced the workload of worker.
Embodiment 2
Further optimize on the basis of a kind of reactor reacted jointly for various materials described in embodiment 1, institute
State reactor and be externally provided with electric heating cover 12, can be maintained the temperature of kettle 1 during material reaction according to the demand of material
The optimum temperature of reaction so that reaction is more fully thoroughly.
Embodiment 3
Further optimize on the basis of a kind of reactor reacted jointly for various materials described in embodiment 2, institute
State the auxiliary half under the drive of auxiliary spindle motor 13 of device 17 of stirring to rotate clockwise, half rotates counterclockwise, when material enters reaction warehouse
When in 21, it is auxiliary stir device 17 and it is main stir device and can cooperate, shear agitation is carried out to material in different directions so that stir
No dead angle is mixed, material reaction is more abundant.
Embodiment 4
Further optimize on the basis of a kind of reactor reacted jointly for various materials described in embodiment 3, institute
State auxiliary spindle motor 13 and be connected with decelerator, pressure gauge 10 is provided with the kettle 1, the pressure gauge, which is connected with through baffle plate, to be prolonged
The inductor 11 in reaction warehouse is extended, when material reaction to different phase, it may be desirable to different mixing speeds, can now lead to
Cross decelerator to be controlled mixing speed, be advantageous to the abundant reaction of material, inductor 11 can be by the pressure in reactor
Situation is reacted in pressure gauge 10, and when there is the higher situation of pressure, worker can carry out pressure release processing, avoid because of pressure
The generation of phenomenon that is too high and causing fried kettle.
It is embodiments of the invention as described above.The present invention is not limited to the above-described embodiments, anyone should learn that
The structure change made under the enlightenment of the present invention, the technical schemes that are same or similar to the present invention, each fall within this
Within the protection domain of invention.
Claims (5)
- A kind of 1. reactor reacted jointly for various materials, it is characterised in that:Including kettle (1), spindle motor (3) and auxiliary Kettle (1) is divided into the premix feed bin (7) on upper strata and the reaction warehouse of lower floor by spindle motor (13), internal be provided with of the kettle (1) (21) baffle plate (6), the baffle plate (6) are provided with two material outlets (9) by solenoid valve control connected with reaction warehouse (21), The spindle motor (3) is connected with decelerator (4), and the decelerator (4), which is connected with through baffle plate (6), extends to stretching for reaction warehouse (21) Contracting rotating shaft (5), telescopic rotating shaft (5) axis body and axle bottom are respectively equipped with agitating paddle (16) and the scraper consistent with bottom shape (18), the agitating paddle (16) has setting in premix feed bin (7) and reaction warehouse (21), is additionally provided with the reaction warehouse (21) It is some it is auxiliary stir device (17), the auxiliary device (17) that stirs is connected with transmission component (15), the transmission component (15) and auxiliary axle electricity Machine is connected, and an identical charging aperture (2), the kettle (1) are respectively provided with spindle motor (3) both sides at the top of the kettle (1) Bottom is provided with a discharging opening (19) and support base (20).
- A kind of 2. reactor reacted jointly for various materials as claimed in claim 1, it is characterised in that:The kettle (1) it is externally provided with electric heating cover (12).
- A kind of 3. reactor reacted jointly for various materials as claimed in claim 1, it is characterised in that:It is described auxiliary to stir dress Put (17) half to rotate clockwise, half rotates counterclockwise.
- A kind of 4. reactor reacted jointly for various materials as claimed in claim 1, it is characterised in that:The auxiliary axle electricity Machine (13) is connected with decelerator.
- A kind of 5. reactor reacted jointly for various materials as claimed in claim 1, it is characterised in that:The kettle (1) pressure gauge (10) is provided with, the pressure gauge (10) is connected with the sensing extended to through baffle plate (6) in reaction warehouse (21) Device (11).
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201710790156.8A CN107497382A (en) | 2017-09-05 | 2017-09-05 | A kind of reactor reacted jointly for various materials |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201710790156.8A CN107497382A (en) | 2017-09-05 | 2017-09-05 | A kind of reactor reacted jointly for various materials |
Publications (1)
Publication Number | Publication Date |
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CN107497382A true CN107497382A (en) | 2017-12-22 |
Family
ID=60695565
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CN201710790156.8A Withdrawn CN107497382A (en) | 2017-09-05 | 2017-09-05 | A kind of reactor reacted jointly for various materials |
Country Status (1)
Country | Link |
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CN (1) | CN107497382A (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110548473A (en) * | 2019-10-12 | 2019-12-10 | 戚江浩 | Efficient reaction kettle based on energy conservation and environmental protection |
CN116059949A (en) * | 2023-02-20 | 2023-05-05 | 广东江河生物科技有限公司 | Automatic nanometer catalyst preparation equipment |
-
2017
- 2017-09-05 CN CN201710790156.8A patent/CN107497382A/en not_active Withdrawn
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110548473A (en) * | 2019-10-12 | 2019-12-10 | 戚江浩 | Efficient reaction kettle based on energy conservation and environmental protection |
CN116059949A (en) * | 2023-02-20 | 2023-05-05 | 广东江河生物科技有限公司 | Automatic nanometer catalyst preparation equipment |
CN116059949B (en) * | 2023-02-20 | 2023-08-22 | 广东江河生物科技有限公司 | Automatic nanometer catalyst preparation equipment |
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PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
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WW01 | Invention patent application withdrawn after publication |
Application publication date: 20171222 |
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WW01 | Invention patent application withdrawn after publication |