CN107287608A - Filter case rusty stain cleaning cream and preparation method thereof - Google Patents
Filter case rusty stain cleaning cream and preparation method thereof Download PDFInfo
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- CN107287608A CN107287608A CN201710542680.3A CN201710542680A CN107287608A CN 107287608 A CN107287608 A CN 107287608A CN 201710542680 A CN201710542680 A CN 201710542680A CN 107287608 A CN107287608 A CN 107287608A
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23G—CLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
- C23G5/00—Cleaning or de-greasing metallic material by other methods; Apparatus for cleaning or de-greasing metallic material with organic solvents
- C23G5/02—Cleaning or de-greasing metallic material by other methods; Apparatus for cleaning or de-greasing metallic material with organic solvents using organic solvents
- C23G5/032—Cleaning or de-greasing metallic material by other methods; Apparatus for cleaning or de-greasing metallic material with organic solvents using organic solvents containing oxygen-containing compounds
Abstract
Filter case recycling cleaning fluid, is mainly prepared from including following components：100 130 parts of the mixture of sour 50 56 parts of disodium hydrogen, water and alcohol, 30 50 parts of butyl glycol ether, 230 250 parts of hand cleanser, 20 25 parts of propylene glycol monobutyl ether, 10 15 parts of trimethylolpropane, 40% 460 550 parts of aqueous solution of nitric acid, 80 100 parts of ammoniacal liquor, 50 90 parts of hydrogen peroxide, 70 100 parts of starch, 15 65 parts of citric acid, 20 50 parts of tartaric acid, 30 80 parts of phosphoric acid, special 500 700 parts of distillate.Configuration is convenient, and cost is low, non-hazardous, and water saving is not hurt hands, cleaning process is safe and simple, and cleaning performance is good, corrosion-free effect, and small, natural rust remover is influenceed on human health, wipe, rinsed with water, prepare simplicity, safety non-toxic has good rust removing function to metal.
Description
Technical field：
Reclaim and reuse the present invention relates to cleaner, and in particular to filter case rusty stain cleaning cream and its preparation side
Method.
Background technology：
At present, domestic and international automobile and the cleaner of engineering machinery were used to maintenance period change after, generally as scrapping place
Reason, causes very big waste, and the only filtering material of usage cycles is really achieved in fact, and other parts are by strict inspection
Secondary it can be utilized after looking into, it is therefore necessary to recovery is carried out to it and remanufactured, it is necessary to be cleaned to shell after recovery, merely
Water be difficult remove case surface impurity, it is therefore desirable to a kind of special cleaning agent.
The content of the invention：
The technical problems to be solved by the invention are to overcome the defect of prior art, and there is provided a kind of filter case rusty stain
Cleaning cream and preparation method thereof.
The technical problems to be solved by the invention are realized using following technical scheme.
Filter case rusty stain cleaning cream, it is characterised in that：Mainly it is prepared from including following components：Sour disodium hydrogen 50-
56 parts, 100-130 parts of the mixture of water and alcohol, 30-50 parts of butyl glycol ether, 230-250 parts of hand cleanser, propylene glycol monobutyl ether
20-25 parts, 10-15 parts of trimethylolpropane, 460-550 parts of 40% aqueous solution of nitric acid, 80-100 parts of ammoniacal liquor, hydrogen peroxide 50-90
Part, 70-100 parts of starch, 15-65 parts of citric acid, 20-50 parts of tartaric acid, 30-80 parts of phosphoric acid, special distillate 500-700 parts.
Mainly it is prepared from including following components：100 parts of the mixture of sour 50 parts of disodium hydrogen, water and alcohol, butyl glycol ether
30 parts, 230 parts of hand cleanser, 20 parts of propylene glycol monobutyl ether, 10 parts of trimethylolpropane, 460 parts of 40% aqueous solution of nitric acid, ammoniacal liquor 80
Part, 50 parts of hydrogen peroxide, 70 parts of starch, 15 parts of citric acid, 20 parts of tartaric acid, 30 parts of phosphoric acid, special 500 parts of distillate.
Mainly it is prepared from including following components：130 parts of the mixture of sour 56 parts of disodium hydrogen, water and alcohol, butyl glycol ether
50 parts, 250 parts of hand cleanser, 25 parts of propylene glycol monobutyl ether, 15 parts of trimethylolpropane, 550 parts of 40% aqueous solution of nitric acid, ammoniacal liquor
100 parts, 90 parts of hydrogen peroxide, 100 parts of starch, 65 parts of citric acid, 50 parts of tartaric acid, 80 parts of phosphoric acid, special 700 parts of distillate.
The preparation method of filter case rusty stain cleaning cream, it is characterised in that：Comprise the following steps that：
Ammoniacal liquor is added to the water, 90 DEG C -110 DEG C are warming up to；
Hydrogen peroxide, citric acid, tartaric acid, phosphoric acid are sequentially added, 20-30min is stirred in the solution of gained；
Using the mixture of sour disodium hydrogen crushing water and alcohol as extraction, leaching liquor is concentrated under reduced pressure, and recycling design is extremely
Without alcohol taste；
By gained without alcohol taste solution, spent glycol butyl ether is obtained by extraction corresponding extract, extract is concentrated under reduced pressure, obtains
Powdered extract；
By gained powdered extract through being washed to eluent it is colourless after, sling with long cloth, residual moisture filtered off, to not dripping
During water, then the elution by hand cleanser of volumetric concentration, collect eluent and be simultaneously concentrated and dried, when dried object；
Take propylene glycol monobutyl ether and the aqueous solution of nitric acid of 100-110 parts 40% to be placed in agitator tank A to stir, mixing speed is
3000r/mim, whipping temp is 60-65 DEG C, 5 minutes time, adds solution, stirs 10 parts, obtain A liquid；
Meanwhile, take trimethylolpropane, the aqueous solution of nitric acid of 360-400 parts 40% to be placed in agitator tank B, mixing speed is
1000r/mim, whipping temp is 60-65 DEG C, 5 minutes time, adds dried object and special distillate, stirs 10 parts, obtain B liquid
Body；
After A fluid temperatures rise to 50 DEG C of stabilizations, starch is added, is got cleaning fluid from system with circulating collection pump, passed through
Enter cleaning agent make-up tank after Filter Press solid particle；
Citric acid is prepared, formulated pump squeezes into oxidation furnace, the circulation of passivating solution low discharge is made to boiler by circulating collection pump
Coil pipe is passivated；
Take filter press apart, reclaim the solid particle of Filter Press；
Solid particle and B liquid are taken, according to 1:0.6-0.8 ratios are added in agitator tank C, stirring, and mixing speed is
1000r/mim, whipping temp is 60-65 DEG C, 2 minutes time, is eventually adding 3-5 parts of surfactants, mixing speed is
2500r/mim, whipping temp is 80-90 DEG C, 10 minutes time；
Filtering, collects the water distillation that liquid mixes 10 times of liquid, in the pasty state, cools down, into cream.
Strong 20-25 parts of glycerine, 20-25 parts of ammonium sulfate, 30-35 parts of magnesium sulfate, 30-35 parts of melamine, zinc stearate
30-35 parts, 50% 30-35 parts of sodium hydroxide, 3-5 parts of PLA, HEDP5-6 parts of 1-hydroxy ethylidene-1,1-diphosphonic acid, polyacrylic acid PAA9-
16 parts, NaOH30-39 parts of piece alkali, 1-6 parts of BTA, 12-18 parts of sodium sulfite.
Further technology：Described special distillate is prepared from including following components：Strong 20 parts of glycerine, ammonium sulfate 20
Part, 30 parts of magnesium sulfate, 30 parts of melamine, 30 parts of zinc stearate, 50% 30 parts of sodium hydroxide, 3 parts of PLA, hydroxy ethylidene two
HEDP5 parts of phosphoric acid, PAA9 parts of polyacrylic acid, NaOH30 parts of piece alkali, 1 part of BTA, 12 parts of sodium sulfite.
Further technology：Described special distillate is prepared from including following components：Strong 25 parts of glycerine, ammonium sulfate 25
Part, 35 parts of magnesium sulfate, 35 parts of melamine, 35 parts of zinc stearate, 50% 35 parts of sodium hydroxide, 5 parts of PLA, hydroxy ethylidene two
HEDP6 parts of phosphoric acid, PAA16 parts of polyacrylic acid, NaOH39 parts of piece alkali, 6 parts of BTA, 18 parts of sodium sulfite.
Further technology：Prepared by described special distillate comprises the following steps：
1-hydroxy ethylidene-1,1-diphosphonic acid HEDP, polyacrylic acid PAA, piece alkali NaOH, BTA, sodium sulfite mix 300 parts
Water, is stirred, and filtering, by filter press press filtration, obtains powder；
Strong glycerine, ammonium sulfate, magnesium sulfate, melamine, zinc stearate, 50% sodium hydroxide are well mixed, and are placed in close
In envelope, hermetic bag is placed under mud and buried, hermetic bag is taken out after 3 days, hermetic bag is punctured, then by PLA at cut
Add, after 1 hour, be placed under sunlight and be exposed to the sun 1 hour, the mixture in hermetic bag is taken out；
Mixed with powder, stand 2 days, by distillation, constantly field adds water in still-process, collects distillate.
The beneficial effects of the present invention are：
Configuration is convenient, and cost is low, non-hazardous, and water saving is not hurt hands, cleaning process is safe and simple, cleaning performance is good, corrosion-free
Effect, small, natural rust remover is influenceed on human health, is wiped, is rinsed with water, prepares easy, safety non-toxic, to gold
Accessory has good rust removing function.
Contrast existing cleaning products：
It is widely applicable for full effect cleaning agent, whether greasy dirt, dust or becomes rusty stain, can easily solve.But generally it
All contain ethylene glycol monobutyl ether solvent, skin disruption red blood cell can be passed through.Some consumers do not see the description of product, are not added with dilute
Release, dosage used is bigger, endanger bigger.Some sprays contain carcinogenic substance formaldehyde.
Laundry product.Washing powder, softener etc. may contain carcinogenic substance formaldehyde, and short-period used can induce allergy and asthma.
Degreasing agent.Degreasing agent may stimulate lungs, or burn skin and eyes, it is also possible to some containing carcinogenic components
Crystalline cleaning agent may blinding or fatal, or produce hazardous chemical reaction.Skin, eyes, mucous membrane and clothing should be avoided contact to
Thing.To avoid gulping down or sucking by mistake spraying when using, rubber gloves must be taken, and keep room ventilation as far as possible.
Cleaning agent prepared by this law.Corrosion-free effect, small, natural rust remover is influenceed on human health, is wiped, is used water
Flushing.
Embodiment：
In order that the technical means, the inventive features, the objects and the advantages of the present invention are easy to understand, tie below
Specific embodiment is closed, the present invention is expanded on further.
Embodiment 1：Filter case rusty stain cleaning cream, is mainly prepared from including following components：Sour 50 parts of disodium hydrogen, water
With 100 parts of the mixture of alcohol, 30 parts of butyl glycol ether, 230 parts of hand cleanser, 20 parts of propylene glycol monobutyl ether, trimethylolpropane 10
Part, 460 parts of 40% aqueous solution of nitric acid, 80 parts of ammoniacal liquor, 50 parts of hydrogen peroxide, 70 parts of starch, 15 parts of citric acid, 20 parts of tartaric acid, phosphorus
30 parts of acid, special 500 parts of distillate.
The preparation method of filter case rusty stain cleaning cream, is comprised the following steps that：
Ammoniacal liquor is added to the water, 90 DEG C -110 DEG C are warming up to；
Hydrogen peroxide, citric acid, tartaric acid, phosphoric acid are sequentially added, 20-30min is stirred in the solution of gained；
Using the mixture of sour disodium hydrogen crushing water and alcohol as extraction, leaching liquor is concentrated under reduced pressure, and recycling design is extremely
Without alcohol taste；
By gained without alcohol taste solution, spent glycol butyl ether is obtained by extraction corresponding extract, extract is concentrated under reduced pressure, obtains
Powdered extract；
By gained powdered extract through being washed to eluent it is colourless after, sling with long cloth, residual moisture filtered off, to not dripping
During water, then the elution by hand cleanser of volumetric concentration, collect eluent and be simultaneously concentrated and dried, when dried object；
Take propylene glycol monobutyl ether and the aqueous solution of nitric acid of 100-110 parts 40% to be placed in agitator tank A to stir, mixing speed is
3000r/mim, whipping temp is 60-65 DEG C, 5 minutes time, adds solution, stirs 10 parts, obtain A liquid；
Meanwhile, take trimethylolpropane, the aqueous solution of nitric acid of 360-400 parts 40% to be placed in agitator tank B, mixing speed is
1000r/mim, whipping temp is 60-65 DEG C, 5 minutes time, adds dried object and special distillate, stirs 10 parts, obtain B liquid
Body；
After A fluid temperatures rise to 50 DEG C of stabilizations, starch is added, is got cleaning fluid from system with circulating collection pump, passed through
Enter cleaning agent make-up tank after Filter Press solid particle；
Citric acid is prepared, formulated pump squeezes into oxidation furnace, the circulation of passivating solution low discharge is made to boiler by circulating collection pump
Coil pipe is passivated；
Take filter press apart, reclaim the solid particle of Filter Press；
Solid particle and B liquid are taken, according to 1:0.6-0.8 ratios are added in agitator tank C, stirring, and mixing speed is
1000r/mim, whipping temp is 60-65 DEG C, 2 minutes time, is eventually adding 3-5 parts of surfactants, mixing speed is
2500r/mim, whipping temp is 80-90 DEG C, 10 minutes time；
Filtering, collects the water distillation that liquid mixes 10 times of liquid, in the pasty state, cools down, into cream.
Special distillate is prepared from including following components：Strong 20 parts of glycerine, 20 parts of ammonium sulfate, 30 parts of magnesium sulfate, three
30 parts of poly cyanamid, 30 parts of zinc stearate, 50% 30 parts of sodium hydroxide, 3 parts of PLA, HEDP5 parts of 1-hydroxy ethylidene-1,1-diphosphonic acid, poly- third
PAA9 parts of olefin(e) acid, NaOH30 parts of piece alkali, 1 part of BTA, 12 parts of sodium sulfite.
Prepared by special distillate comprises the following steps：
1-hydroxy ethylidene-1,1-diphosphonic acid HEDP, polyacrylic acid PAA, piece alkali NaOH, BTA, sodium sulfite mix 300 parts
Water, is stirred, and filtering, by filter press press filtration, obtains powder；
Strong glycerine, ammonium sulfate, magnesium sulfate, melamine, zinc stearate, 50% sodium hydroxide are well mixed, and are placed in close
In envelope, hermetic bag is placed under mud and buried, hermetic bag is taken out after 3 days, hermetic bag is punctured, then by PLA at cut
Add, after 1 hour, be placed under sunlight and be exposed to the sun 1 hour, the mixture in hermetic bag is taken out；
Mixed with powder, stand 2 days, by distillation, constantly field adds water in still-process, collects distillate.
Embodiment 2：Filter case rusty stain cleaning cream, is mainly prepared from including following components：Sour 56 parts of disodium hydrogen, water
With 130 parts of the mixture of alcohol, 50 parts of butyl glycol ether, 250 parts of hand cleanser, 25 parts of propylene glycol monobutyl ether, trimethylolpropane 15
Part, 550 parts of 40% aqueous solution of nitric acid, 100 parts of ammoniacal liquor, 90 parts of hydrogen peroxide, 100 parts of starch, 65 parts of citric acid, 50 parts of tartaric acid,
80 parts of phosphoric acid, special 700 parts of distillate.
The preparation method of filter case rusty stain cleaning cream, is comprised the following steps that：
Ammoniacal liquor is added to the water, 90 DEG C -110 DEG C are warming up to；
Hydrogen peroxide, citric acid, tartaric acid, phosphoric acid are sequentially added, 20-30min is stirred in the solution of gained；
Using the mixture of sour disodium hydrogen crushing water and alcohol as extraction, leaching liquor is concentrated under reduced pressure, and recycling design is extremely
Without alcohol taste；
By gained without alcohol taste solution, spent glycol butyl ether is obtained by extraction corresponding extract, extract is concentrated under reduced pressure, obtains
Powdered extract；
By gained powdered extract through being washed to eluent it is colourless after, sling with long cloth, residual moisture filtered off, to not dripping
During water, then the elution by hand cleanser of volumetric concentration, collect eluent and be simultaneously concentrated and dried, when dried object；
Take propylene glycol monobutyl ether and the aqueous solution of nitric acid of 100-110 parts 40% to be placed in agitator tank A to stir, mixing speed is
3000r/mim, whipping temp is 60-65 DEG C, 5 minutes time, adds solution, stirs 10 parts, obtain A liquid；
Meanwhile, take trimethylolpropane, the aqueous solution of nitric acid of 360-400 parts 40% to be placed in agitator tank B, mixing speed is
1000r/mim, whipping temp is 60-65 DEG C, 5 minutes time, adds dried object and special distillate, stirs 10 parts, obtain B liquid
Body；
After A fluid temperatures rise to 50 DEG C of stabilizations, starch is added, is got cleaning fluid from system with circulating collection pump, passed through
Enter cleaning agent make-up tank after Filter Press solid particle；
Citric acid is prepared, formulated pump squeezes into oxidation furnace, the circulation of passivating solution low discharge is made to boiler by circulating collection pump
Coil pipe is passivated；
Take filter press apart, reclaim the solid particle of Filter Press；
Solid particle and B liquid are taken, according to 1:0.6-0.8 ratios are added in agitator tank C, stirring, and mixing speed is
1000r/mim, whipping temp is 60-65 DEG C, 2 minutes time, is eventually adding 3-5 parts of surfactants, mixing speed is
2500r/mim, whipping temp is 80-90 DEG C, 10 minutes time；
Filtering, collects the water distillation that liquid mixes 10 times of liquid, in the pasty state, cools down, into cream.
Special distillate is prepared from including following components：Strong 25 parts of glycerine, 25 parts of ammonium sulfate, 35 parts of magnesium sulfate, three
35 parts of poly cyanamid, 35 parts of zinc stearate, 50% 35 parts of sodium hydroxide, 5 parts of PLA, HEDP6 parts of 1-hydroxy ethylidene-1,1-diphosphonic acid, poly- third
PAA16 parts of olefin(e) acid, NaOH39 parts of piece alkali, 6 parts of BTA, 18 parts of sodium sulfite.
Prepared by special distillate comprises the following steps：
1-hydroxy ethylidene-1,1-diphosphonic acid HEDP, polyacrylic acid PAA, piece alkali NaOH, BTA, sodium sulfite mix 300 parts
Water, is stirred, and filtering, by filter press press filtration, obtains powder；
Strong glycerine, ammonium sulfate, magnesium sulfate, melamine, zinc stearate, 50% sodium hydroxide are well mixed, and are placed in close
In envelope, hermetic bag is placed under mud and buried, hermetic bag is taken out after 3 days, hermetic bag is punctured, then by PLA at cut
Add, after 1 hour, be placed under sunlight and be exposed to the sun 1 hour, the mixture in hermetic bag is taken out；
Mixed with powder, stand 2 days, by distillation, constantly field adds water in still-process, collects distillate.
General principle, principal character and the advantages of the present invention of the present invention has been shown and described above.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the simply explanation described in above-described embodiment and specification is originally
The principle of invention, without departing from the spirit and scope of the present invention, various changes and modifications of the present invention are possible, these changes
Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its
Equivalent thereof.
Claims (8)
1. filter case recycling cleaning fluid, it is characterised in that：Mainly it is prepared from including following components：Sour disodium hydrogen
50-56 parts, 100-130 parts of the mixture of water and alcohol, 30-50 parts of butyl glycol ether, 230-250 parts of hand cleanser, propyleneglycol monobutyl
20-25 parts of ether, 10-15 parts of trimethylolpropane, 460-550 parts of 40% aqueous solution of nitric acid, 80-100 parts of ammoniacal liquor, hydrogen peroxide 50-
90 parts, 70-100 parts of starch, 15-65 parts of citric acid, 20-50 parts of tartaric acid, 30-80 parts of phosphoric acid, special distillate 500-700
Part.
2. the filter case recycling cleaning fluid according to claim 1, it is characterised in that：Mainly include following
Component is prepared from：100 parts of the mixture of sour 50 parts of disodium hydrogen, water and alcohol, 30 parts of butyl glycol ether, 230 parts of hand cleanser, the third two
20 parts of alcohol monobutyl ether, 10 parts of trimethylolpropane, 460 parts of 40% aqueous solution of nitric acid, 80 parts of ammoniacal liquor, 50 parts of hydrogen peroxide, starch 70
Part, 15 parts of citric acid, 20 parts of tartaric acid, 30 parts of phosphoric acid, special 500 parts of distillate.
3. the filter case recycling cleaning fluid according to claim 1, it is characterised in that：Mainly include following
Component is prepared from：130 parts of the mixture of sour 56 parts of disodium hydrogen, water and alcohol, 50 parts of butyl glycol ether, 250 parts of hand cleanser, the third two
25 parts of alcohol monobutyl ether, 15 parts of trimethylolpropane, 550 parts of 40% aqueous solution of nitric acid, 100 parts of ammoniacal liquor, 90 parts of hydrogen peroxide, starch
100 parts, 65 parts of citric acid, 50 parts of tartaric acid, 80 parts of phosphoric acid, special 700 parts of distillate.
4. the preparation method of the filter case recycling cleaning fluid according to claim 1, it is characterised in that：Tool
Body step is as follows：
Ammoniacal liquor is added to the water, 90 DEG C -110 DEG C are warming up to；
Hydrogen peroxide, citric acid, tartaric acid, phosphoric acid are sequentially added, 20-30min is stirred in the solution of gained；
Using the mixture of sour disodium hydrogen crushing water and alcohol as extraction, leaching liquor is concentrated under reduced pressure, and recycling design is to without alcohol
Taste；
By gained without alcohol taste solution, spent glycol butyl ether is obtained by extraction corresponding extract, extract is concentrated under reduced pressure, and obtains drying
Medicinal extract；
By gained powdered extract through being washed to eluent it is colourless after, sling with long cloth, residual moisture filtered off, to not dripping
When, then eluted by hand cleanser of volumetric concentration, collect eluent and be concentrated and dried, when dried object；
Take propylene glycol monobutyl ether and the aqueous solution of nitric acid of 100-110 parts 40% to be placed in agitator tank A to stir, mixing speed is 3000r/
Mim, whipping temp is 60-65 DEG C, 5 minutes time, adds solution, stirs 10 parts, obtain A liquid；
Meanwhile, take trimethylolpropane, the aqueous solution of nitric acid of 360-400 parts 40% to be placed in agitator tank B, mixing speed is 1000r/
Mim, whipping temp is 60-65 DEG C, 5 minutes time, adds dried object and special distillate, stirs 10 parts, obtain B liquid；
After A fluid temperatures rise to 50 DEG C of stabilizations, starch is added, is got cleaning fluid from system with circulating collection pump, through press filtration
Enter cleaning agent make-up tank after machine filtering solid particles；
Citric acid is prepared, formulated pump squeezes into oxidation furnace, the circulation of passivating solution low discharge is made to coil tubes by circulating collection pump
It is passivated；
Take filter press apart, reclaim the solid particle of Filter Press；
Solid particle and B liquid are taken, according to 1:0.6-0.8 ratios are added in agitator tank C, stirring, and mixing speed is 1000r/
Mim, whipping temp is 60-65 DEG C, 2 minutes time, is eventually adding 3-5 parts of surfactants, mixing speed is 2500r/mim,
Whipping temp is 80-90 DEG C, 10 minutes time；
Filtering, collects the water distillation that liquid mixes 10 times of liquid, in the pasty state, cools down, into cream.
5. the preparation method of the filter case recycling cleaning fluid according to claim 4, it is characterised in that：Institute
The special distillate stated is prepared from including following components：Strong 20-25 parts of glycerine, 20-25 parts of ammonium sulfate, magnesium sulfate 30-35
Part, 30-35 parts of melamine, 30-35 parts of zinc stearate, 50% 30-35 parts of sodium hydroxide, 3-5 parts of PLA, hydroxy ethylidene two
HEDP5-6 parts of phosphoric acid, PAA9-16 parts of polyacrylic acid, NaOH30-39 parts of piece alkali, 1-6 parts of BTA, sodium sulfite 12-18
Part.
6. the preparation method of the filter case recycling cleaning fluid according to claim 5, it is characterised in that：Institute
The special distillate stated is prepared from including following components：Strong 20 parts of glycerine, 20 parts of ammonium sulfate, 30 parts of magnesium sulfate, melamine
30 parts of amine, 30 parts of zinc stearate, 50% 30 parts of sodium hydroxide, 3 parts of PLA, HEDP5 parts of 1-hydroxy ethylidene-1,1-diphosphonic acid, polyacrylic acid
PAA9 parts, NaOH30 parts of piece alkali, 1 part of BTA, 12 parts of sodium sulfite.
7. the preparation method of the filter case recycling cleaning fluid according to claim 5, it is characterised in that：Institute
The special distillate stated is prepared from including following components：Strong 25 parts of glycerine, 25 parts of ammonium sulfate, 35 parts of magnesium sulfate, melamine
35 parts of amine, 35 parts of zinc stearate, 50% 35 parts of sodium hydroxide, 5 parts of PLA, HEDP6 parts of 1-hydroxy ethylidene-1,1-diphosphonic acid, polyacrylic acid
PAA16 parts, NaOH39 parts of piece alkali, 6 parts of BTA, 18 parts of sodium sulfite.
8. the preparation method of the filter case recycling cleaning fluid according to claim 5, it is characterised in that：Institute
Prepared by the special distillate stated comprises the following steps：
1-hydroxy ethylidene-1,1-diphosphonic acid HEDP, polyacrylic acid PAA, piece alkali NaOH, BTA, sodium sulfite mix 300 parts of water, stir
Mix, filter, by filter press press filtration, obtain powder；
Strong glycerine, ammonium sulfate, magnesium sulfate, melamine, zinc stearate, 50% sodium hydroxide are well mixed, and are placed in hermetic bag
It is interior, hermetic bag is placed under mud and buried, hermetic bag is taken out after 3 days, hermetic bag is punctured, then PLA is added at cut
Enter, after 1 hour, be placed under sunlight and be exposed to the sun 1 hour, the mixture in hermetic bag is taken out；
Mixed with powder, stand 2 days, by distillation, constantly field adds water in still-process, collects distillate.
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