CN107286753A - Meet water color shifting ink, tipping paper and preparation method - Google Patents

Meet water color shifting ink, tipping paper and preparation method Download PDF

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Publication number
CN107286753A
CN107286753A CN201710586629.2A CN201710586629A CN107286753A CN 107286753 A CN107286753 A CN 107286753A CN 201710586629 A CN201710586629 A CN 201710586629A CN 107286753 A CN107286753 A CN 107286753A
Authority
CN
China
Prior art keywords
water color
shifting ink
color shifting
chance water
tipping paper
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710586629.2A
Other languages
Chinese (zh)
Inventor
徐善水
赵荣艳
杨江涛
杨立新
曹萼
杨二果
王超
王云龙
郭飞
姜亚洲
余四军
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
ANHUI GENUINE PAPER PACKING Co Ltd
Original Assignee
ANHUI GENUINE PAPER PACKING Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by ANHUI GENUINE PAPER PACKING Co Ltd filed Critical ANHUI GENUINE PAPER PACKING Co Ltd
Priority to CN201710586629.2A priority Critical patent/CN107286753A/en
Publication of CN107286753A publication Critical patent/CN107286753A/en
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00Inks
    • C09D11/50Sympathetic, colour changing or similar inks
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00Inks
    • C09D11/02Printing inks
    • C09D11/10Printing inks based on artificial resins
    • C09D11/102Printing inks based on artificial resins containing macromolecular compounds obtained by reactions other than those only involving unsaturated carbon-to-carbon bonds
    • C09D11/103Printing inks based on artificial resins containing macromolecular compounds obtained by reactions other than those only involving unsaturated carbon-to-carbon bonds of aldehydes, e.g. phenol-formaldehyde resins
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H27/00Special paper not otherwise provided for, e.g. made by multi-step processes
    • D21H27/18Paper- or board-based structures for surface covering
    • D21H27/22Structures being applied on the surface by special manufacturing processes, e.g. in presses

Abstract

A kind of chance water color shifting ink and tipping paper that the present invention is provided, wherein, the chance water color shifting ink includes the component of following parts by weight:65~85 parts of water-base resin liquid;5~15 parts of filler auxiliary agent;Colour former 4~10;5~10 parts of water.Above-mentioned tipping paper, with the chance water color-changing anti-counterfeit layer formed by chance water color shifting ink.Water discoloration can be met by meeting water photochromic layer, and discoloration condition is easily achieved, and can easily verify the true and false, exercisable convenience is good.

Description

Meet water color shifting ink, tipping paper and preparation method
Technical field
It is more particularly to a kind of to meet water color shifting ink, tipping paper and preparation method the present invention relates to tipping paper technical field.
Background technology
Cigarette tipping paper is the important cigarette auxiliary material in cigarette manufacturing process, and with the fast development of tobacco product, cigarette is used Tipping paper has been used not only for connecting the effect of cigaratte filter and cigarette, further plays the false proof and attractive in appearance of cigarette Function.For high-grade, high-quality cigarette, false proof demand is just further urgent.At present, cigarette tipping paper is assigned anti-fraud functional Method has many kinds, for example, different embossings are prepared using embossing technique on the surface of tipping paper, but its manufacture craft is multiple It is miscellaneous, and forgeability is high, antifalse effect is poor;And for example, there is the word or pattern of warm change/light change function by surface printing, But this method for anti-counterfeit is relatively fixed because warm change condition, light become condition, is verified that the operable convenience of the true and false is poor, is unfavorable for Consumer operates.
The content of the invention
Based on this, it is necessary to poor for the operable convenience of traditionally anti-counterfeiting technology antifalse effect difference or the checking true and false Problem meets water color shifting ink, tipping paper and preparation method there is provided one kind.
A kind of chance water color shifting ink that the present invention is provided, wherein, the water color shifting ink of meeting includes following parts by weight Component:
In one of which embodiment, the water-base resin liquid is included in phenolic modified resin, aldehydic acid modified resin It is one or two kinds of.
In one of which embodiment, the filler auxiliary agent includes one or both of precipitated calcium carbonate, talcum powder.
In one of which embodiment, the chance water color shifting ink also includes:Drier, substrate wetting agents and levelling One or more in agent.
In one of which embodiment, the colour former includes naphthalene anhydride class pigment.
In one of which embodiment, the colour former has polyvinyl alcohol clad.
In one of which embodiment, the fineness for meeting water color shifting ink is less than or equal to 15 μm.
The present invention also provides a kind of tipping paper, wherein, the tipping paper includes water color shifting ink as described above of meeting and printed Chance water color-changing anti-counterfeit layer.
In one of which embodiment, the thickness of dry film for meeting water color-changing anti-counterfeit layer is 0.5 μm~4 μm.
The present invention is also provided in a kind of preparation method of tipping paper, its spy, and the tipping paper is using as above any one institute It is 0.4MPa, paper migration that the chance water color shifting ink stated, which prints the platen pressure to be formed in chance water color-changing anti-counterfeit layer, printing process, Speed is 80~120m/min, and drying temperature is 90~120 DEG C, and inking grammes per square metre is 0.5~1.0g/m2
Above-mentioned chance water color shifting ink, includes the component of following parts by weight:Water-base resin liquid 65~85;Filler auxiliary agent 5~ 15;Colour former 4~10.The chance water color-changing anti-counterfeit layer being printed as by the chance water color shifting ink can meet water discoloration, and discoloration condition is easy In realization, the true and false can be easily verified, exercisable convenience is good.
Above-mentioned tipping paper, with water color-changing anti-counterfeit layer is met, the chance water photochromic layer can meet water discoloration, and discoloration condition is easy to real It is existing, the true and false can be easily verified, exercisable convenience is good.
Embodiment
In order to make the purpose , technical scheme and advantage of the present invention be clearer, by the following examples, to the present invention Chance water color shifting ink and tipping paper and preparation method be further elaborated.It should be appreciated that described herein specific Embodiment only to explain the present invention, is not intended to limit the present invention.
A kind of chance water color shifting ink that the present invention is provided, meeting water color shifting ink includes the component of following parts by weight:
The pattern and/or word being printed as by the chance water color shifting ink can meet water discoloration, and discoloration condition is easily achieved, energy Enough easily to verify the true and false, exercisable convenience is good.
As a kind of optional embodiment, water-base resin liquid is included in phenolic modified resin liquid, aldehydic acid modified resin liquid It is one or two kinds of.
Alternatively, water-base resin liquid is phenolic modified resin liquid and aldehydic acid modified resin liquid mass ratio is 1:1~1:3 it is mixed Compound, the solid content of mixture is 10%~20%, and water color shifting ink solid content height, viscosity are met as made from the water-base resin liquid It is low, good film-forming property.
As a kind of optional embodiment, filler auxiliary agent includes one or both of precipitated calcium carbonate, talcum powder.Such Filler auxiliary agent and water-base resin liquid phase capacitive are good, by increasing capacitance it is possible to increase the abundant degree of the printing of ink printed layer, improve printing quality, enhancing Meet the contrast before and after water discoloration.Alternatively, the particle diameter of precipitated calcium carbonate is 5~10 μm.In the particle size range, water discoloration is met Ink has optimal printability.
Alternatively, the particle diameter of talcum powder is 5~10 μm.
As a kind of optional embodiment, meeting water color shifting ink also includes:In drier, substrate wetting agents and levelling agent One or more.
Alternatively, the parts by weight of drier, substrate wetting agents and levelling agent that chance water color shifting ink includes are:
Drier 2~3;
Substrate wetting agents 2~3;
Levelling agent 1~3.
Wherein, drier can select commercially available aqueous drier, and substrate wetting agents can select commercially available wetting agent, example Such as can be that enlightening is high by 245, levelling agent can select commercially available levelling agent, for example, can be BYK-333.
As a kind of optional embodiment, colour former includes naphthalene anhydride class pigment.Alternatively, naphthalene anhydride class pigment can meet water Clear, colorless is changed into from colors such as yellow, green, red or the face such as yellow, green, red are changed into from clear, colorless Color or the mutual phase inversion between the colors such as yellow, green, red.
As a kind of optional embodiment, colour former has polyvinyl alcohol clad, and polyvinyl alcohol cladding colour former can Improve the stability of colour former.
As a kind of optional embodiment, the fineness for meeting water color shifting ink is less than or equal to 15 μm.
Alternatively, it is 18~25 (English 2# tea grace cups) to meet the viscosity of water color shifting ink, and fineness is 5~15 μm, solid content For 15%~25%.The chance water color shifting ink of above-mentioned viscosity, fineness and solid content, can cooperate with the print for improving and meeting water color shifting ink Brush adaptive so that meeting water color shifting ink has more preferably levelability and film forming.
The present invention also provides a kind of tipping paper, including the chance water color-changing anti-counterfeit printed by above-mentioned chance water color shifting ink Layer.Alternatively, when the humidity >=63% of tipping paper, meet water color-changing anti-counterfeit layer and change colour.
Tipping paper is included by the above-mentioned chance water color-changing anti-counterfeit layer for meeting the printing of water color shifting ink.Alternatively, water is met to become The thickness of dry film of color false proof layer is 0.5 μm~4 μm.
Further, meet water color-changing anti-counterfeit layer and form at least one of pattern and word shape.
The tipping paper of the embodiment of the present invention one includes base paper layer, printing layer, false proof display layer and the chance water stacked gradually Color-changing anti-counterfeit layer.
The base paper for tipping paper that base paper layer is selected, the body paper requires that its grammes per square metre is 32~40g/m2, machine direction tensile strength is 1.6 ~5KN/m2, longitudinal tensile strain rate is 1%~2%, and moisture is 5.0%~7.0%.
Printing layer is printed with the content such as pattern and character of tipping paper design, and the content such as the pattern and character can be directly in tipping paper Upper display.Alternatively, printing layer, remainder antiforge display layer are locally printed with base paper layer.
False proof display layer is printed on base paper layer with the shape of pattern and/or word.
Water color-changing anti-counterfeit layer is met to be covered on false proof display layer.When tipping paper does not meet water, due to meeting the false proof photochromic layer of water It is covered on false proof display layer, the color of the false proof photochromic layer of water is met in tipping paper display, false proof display layer can not be observed.When connecing When filling paper chance water, meet the false proof photochromic layer of water and be changed into transparent, false proof display layer, which can show that, to be come, so as to directly be observed Arrive.
The tipping paper of the embodiment, chance water color-changing anti-counterfeit layer is eclipsed under certain humidity or chance water condition to be changed into transparent, from And the color of its covering part is shown, and it on the one hand can be used in verifying the true or false of cigarette, it is easy to operate, on the other hand, Add the enjoyment in smoking process.
The tipping paper of the embodiment of the present invention two includes base paper layer, printing layer and the chance water color-changing anti-counterfeit layer stacked gradually.
The base paper for tipping paper that base paper layer is selected, the body paper requires that its grammes per square metre is 32~40g/m2, machine direction tensile strength is 1.6 ~5KN/m2, longitudinal tensile strain rate is 1%~2%, and moisture is 5.0%~7.0%.
Printing layer is printed with the content such as pattern and character of tipping paper design, and the content such as the pattern and character can be directly in tipping paper Upper display.
Water color-changing anti-counterfeit layer local complexity is met in printing layer.When tipping paper does not meet water, meeting the false proof photochromic layer of water is Bright, the full content of printing layer can be directly observed.
When tipping paper meets water, meet the false proof photochromic layer of water and developed the color by transparent become, so that shield portions print layer segment, display Go out to meet pattern and/or word that water color-changing anti-counterfeit layer is formed.
The tipping paper of the embodiment, meets water color-changing anti-counterfeit layer and is changed into colour developing from transparent under certain humidity or chance water condition, So as to show the color of the pattern and/or word of meeting the layer formation of water color-changing anti-counterfeit, it on the one hand can be used in verifying the true of cigarette Puppet, it is easy to operate, on the other hand, also increase the enjoyment in smoking process.
The tipping paper of the embodiment of the present invention three includes base paper layer, printing layer and the chance water color-changing anti-counterfeit layer stacked gradually.
The base paper for tipping paper that base paper layer is selected, the body paper requires that its grammes per square metre is 32~40g/m2, machine direction tensile strength is 1.6 ~5KN/m2, longitudinal tensile strain rate is 1%~2%, and moisture is 5.0%~7.0%.
Printing layer is printed with the content such as pattern and character of tipping paper design, and the content such as the pattern and character can be directly in tipping paper Upper display.Alternatively, printing layer is partly printed with base paper layer, it is anti-that the formation chance water discoloration of water color shifting ink is met in remainder printing Pseudo- layer.Water color-changing anti-counterfeit layer local complexity is met on base paper layer.When tipping paper does not meet water, meet the false proof photochromic layer of water and be shown as one Color is planted, when tipping paper meets water, the false proof photochromic layer of water is met and is changed into another color, so as to show the pattern for meeting water discoloration And/or word.
The tipping paper of the embodiment, meets water color-changing anti-counterfeit layer and is changed into another from a kind of color under certain humidity or chance water condition A kind of color, so as to show the color of the pattern and/or word of meeting the layer formation of water color-changing anti-counterfeit, on the one hand can be used in checking The true or false of cigarette, it is easy to operate, on the other hand, also increase the enjoyment in smoking process.
The present invention also provides a kind of preparation method of above-mentioned tipping paper, and tipping paper prints shape using above-mentioned chance water color shifting ink Platen pressure in Cheng Yushui color-changing anti-counterfeits layer, printing process is 0.4MPa, and paper migration rate is 80~120m/min, drying Temperature is 90~120 DEG C, and inking grammes per square metre is 0.5~1.0g/m2
Chance water color shifting ink, tipping paper and the preparation method of the present invention are further described with reference to embodiment:
Embodiment one
Various raw materials, phenolic modified resin liquid 80g, nano level light calcium carbonate 7g, drier are weighed by formula as below amount 2g, printing ink reducer 2g, colour former 5g and 15 grams of water.
Above-mentioned raw materials are poured into agitator, stirring mixing 40min is transferred in oscillator and grinds 80min, fineness of grind <15 μm, filtering is made and meets water color shifting ink.
Picture and text are locally carried out on base paper layer using common ink to print to form printing layer, remainder is inked using conventional oil Scopiform is into false proof display layer.Print to form chance water color-changing anti-counterfeit layer using chance water color shifting ink in false proof viewing area.
In above-mentioned printing process by the way of intaglio printing, typography parameter is as follows:Pressure roller pressure during machine on paper Power is 0.4MPa, and machine speed is 120m/min, and oven temperature is 100 DEG C.
The semi-finished product paper of printing is subjected to gold stamping, cutting, punching, tipping paper product is made.
Embodiment two
Various raw materials, phenolic modified resin liquid 25g, aldehydic acid resin liquid 50g, nanoscale talcum powder are weighed by formula as below amount 12 grams of 10g, printing ink reducer 5g, drier 5g, levelling agent 5g, colour former 8g and water.
Above-mentioned raw materials are poured into agitator, stirring mixing 30min is transferred in oscillator and grinds 80min, fineness of grind <15 μm, filtering is made and meets water color shifting ink.
Full version picture and text are carried out on base paper layer using common ink to print to form printing layer.Above-mentioned chance water is used in printing layer Color shifting ink is locally printed, and forms chance water color-changing anti-counterfeit layer of the local complexity in printing layer,
In above-mentioned printing process by the way of intaglio printing, typography parameter is as follows:Pressure roller pressure during machine on paper Power is 0.4MPa, and machine speed is 110m/min, and oven temperature is 120 DEG C.
The semi-finished product paper of printing is subjected to gold stamping, cutting, punching, tipping paper product is prepared.
Embodiment three
Various raw materials, phenolic modified resin liquid 30g, aldehydic acid resin liquid 40g, precipitated calcium carbonate are weighed by formula as below amount 8g, nanoscale talcum powder 7g, printing ink reducer 5g, drier 5g, levelling agent 5g and colour former 8g.
Above-mentioned raw materials are poured into agitator, stirring mixing 30min is transferred in oscillator and grinds 80min, fineness of grind <15 μm, filtering is made and meets water color shifting ink.
Picture and text are locally carried out on base paper layer using common ink to print to form printing layer, remainder is using chance water discoloration oil Water color-changing anti-counterfeit layer is met in ink print formation.
In above-mentioned printing process by the way of intaglio printing, typography parameter is as follows:Pressure roller pressure during machine on paper Power is 0.4MPa, and machine speed is 110m/min, and oven temperature is 120 DEG C.
The semi-finished product paper of printing is subjected to gold stamping, cutting, punching, tipping paper product is prepared.
Meanwhile, the term of cited such as " on ", " under " in this specification, "left", "right", " centre " and " one ", also Only understanding for ease of narration, and be not used to limit enforceable scope of the invention, its relativeness is altered or modified, in nothing Under essence change technology contents, when being also considered as enforceable category of the invention.
Embodiment described above only expresses the several embodiments of the present invention, and it describes more specific and detailed, but simultaneously Therefore the limitation to the scope of the claims of the present invention can not be interpreted as.It should be pointed out that for one of ordinary skill in the art For, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to the guarantor of the present invention Protect scope.Therefore, the protection domain of patent of the present invention should be determined by the appended claims.

Claims (10)

1. one kind meets water color shifting ink, it is characterised in that the chance water color shifting ink includes the component of following parts by weight:
2. chance water color shifting ink according to claim 1, it is characterised in that the water-base resin liquid includes phenol aldehyde modified tree One or both of fat and aldehydic acid modified resin.
3. it is according to claim 1 chance water color shifting ink, it is characterised in that the filler auxiliary agent include precipitated calcium carbonate and One or both of talcum powder.
4. chance water color shifting ink according to claim 1, it is characterised in that the chance water color shifting ink also includes:Urge dry One or more in agent, substrate wetting agents and levelling agent.
5. chance water color shifting ink according to claim 1, it is characterised in that the colour former includes naphthalene anhydride class pigment.
6. chance water color shifting ink according to claim 1, it is characterised in that the colour former has polyvinyl alcohol cladding Layer.
7. it is according to claim 1 chance water color shifting ink, it is characterised in that the fineness of the chance water color shifting ink be less than or Equal to 15 μm.
8. a kind of tipping paper, it is characterised in that the tipping paper is included as the chance water as described in claim 1 to 7 any one The chance water color-changing anti-counterfeit layer of color shifting ink printing.
9. tipping paper according to claim 8, it is characterised in that the thickness of dry film of the chance water color-changing anti-counterfeit layer is 0.5 μ M~4 μm.
10. a kind of preparation method of tipping paper, it is characterised in that the tipping paper is used such as claim 1 to 7 any one institute It is 0.4MPa, paper migration that the chance water color shifting ink stated, which prints the platen pressure to be formed in chance water color-changing anti-counterfeit layer, printing process, Speed is 80~120m/min, and drying temperature is 90~120 DEG C, and inking grammes per square metre is 0.5~1.0g/m2
CN201710586629.2A 2017-07-18 2017-07-18 Meet water color shifting ink, tipping paper and preparation method Pending CN107286753A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109294332A (en) * 2018-09-13 2019-02-01 广东中烟工业有限责任公司 A kind of cigarette with anti-fake color shifting ink with and preparation method thereof and cigarette tipping paper
CN109692670A (en) * 2018-12-29 2019-04-30 中国烟草总公司郑州烟草研究院 A kind of temperature response type cigarette filter functional material and preparation method thereof, cigarette filter

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20080113862A1 (en) * 2003-10-06 2008-05-15 Nocopi Technologies, Inc. Invisible Ink And Scratch Pad
CN102898896A (en) * 2012-11-09 2013-01-30 天津环球磁卡股份有限公司 Fluorescence penetrable color-applying ink and preparation method thereof
CN102898895A (en) * 2012-11-09 2013-01-30 天津环球磁卡股份有限公司 Ink capable of developing color in presence of water and preparation method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20080113862A1 (en) * 2003-10-06 2008-05-15 Nocopi Technologies, Inc. Invisible Ink And Scratch Pad
CN102898896A (en) * 2012-11-09 2013-01-30 天津环球磁卡股份有限公司 Fluorescence penetrable color-applying ink and preparation method thereof
CN102898895A (en) * 2012-11-09 2013-01-30 天津环球磁卡股份有限公司 Ink capable of developing color in presence of water and preparation method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109294332A (en) * 2018-09-13 2019-02-01 广东中烟工业有限责任公司 A kind of cigarette with anti-fake color shifting ink with and preparation method thereof and cigarette tipping paper
CN109692670A (en) * 2018-12-29 2019-04-30 中国烟草总公司郑州烟草研究院 A kind of temperature response type cigarette filter functional material and preparation method thereof, cigarette filter

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Application publication date: 20171024