CN107285495A - 一种锂离子电池生产废水处理装置 - Google Patents
一种锂离子电池生产废水处理装置 Download PDFInfo
- Publication number
- CN107285495A CN107285495A CN201710608165.0A CN201710608165A CN107285495A CN 107285495 A CN107285495 A CN 107285495A CN 201710608165 A CN201710608165 A CN 201710608165A CN 107285495 A CN107285495 A CN 107285495A
- Authority
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- China
- Prior art keywords
- filter membrane
- pond
- ion battery
- water
- lithium ion
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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- HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium Ion Chemical compound data:image/svg+xml;base64,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 data:image/svg+xml;base64,PD94bWwgdmVyc2lvbj0nMS4wJyBlbmNvZGluZz0naXNvLTg4NTktMSc/Pgo8c3ZnIHZlcnNpb249JzEuMScgYmFzZVByb2ZpbGU9J2Z1bGwnCiAgICAgICAgICAgICAgeG1sbnM9J2h0dHA6Ly93d3cudzMub3JnLzIwMDAvc3ZnJwogICAgICAgICAgICAgICAgICAgICAgeG1sbnM6cmRraXQ9J2h0dHA6Ly93d3cucmRraXQub3JnL3htbCcKICAgICAgICAgICAgICAgICAgICAgIHhtbG5zOnhsaW5rPSdodHRwOi8vd3d3LnczLm9yZy8xOTk5L3hsaW5rJwogICAgICAgICAgICAgICAgICB4bWw6c3BhY2U9J3ByZXNlcnZlJwp3aWR0aD0nODVweCcgaGVpZ2h0PSc4NXB4JyB2aWV3Qm94PScwIDAgODUgODUnPgo8IS0tIEVORCBPRiBIRUFERVIgLS0+CjxyZWN0IHN0eWxlPSdvcGFjaXR5OjEuMDtmaWxsOiNGRkZGRkY7c3Ryb2tlOm5vbmUnIHdpZHRoPSc4NS4wJyBoZWlnaHQ9Jzg1LjAnIHg9JzAuMCcgeT0nMC4wJz4gPC9yZWN0Pgo8dGV4dCB4PSczNS40JyB5PSc1My42JyBjbGFzcz0nYXRvbS0wJyBzdHlsZT0nZm9udC1zaXplOjIzcHg7Zm9udC1zdHlsZTpub3JtYWw7Zm9udC13ZWlnaHQ6bm9ybWFsO2ZpbGwtb3BhY2l0eToxO3N0cm9rZTpub25lO2ZvbnQtZmFtaWx5OnNhbnMtc2VyaWY7dGV4dC1hbmNob3I6c3RhcnQ7ZmlsbDojM0I0MTQzJyA+TDwvdGV4dD4KPHRleHQgeD0nNTAuNicgeT0nNTMuNicgY2xhc3M9J2F0b20tMCcgc3R5bGU9J2ZvbnQtc2l6ZToyM3B4O2ZvbnQtc3R5bGU6bm9ybWFsO2ZvbnQtd2VpZ2h0Om5vcm1hbDtmaWxsLW9wYWNpdHk6MTtzdHJva2U6bm9uZTtmb250LWZhbWlseTpzYW5zLXNlcmlmO3RleHQtYW5jaG9yOnN0YXJ0O2ZpbGw6IzNCNDE0MycgPmk8L3RleHQ+Cjx0ZXh0IHg9JzU2LjcnIHk9JzQ0LjMnIGNsYXNzPSdhdG9tLTAnIHN0eWxlPSdmb250LXNpemU6MTVweDtmb250LXN0eWxlOm5vcm1hbDtmb250LXdlaWdodDpub3JtYWw7ZmlsbC1vcGFjaXR5OjE7c3Ryb2tlOm5vbmU7Zm9udC1mYW1pbHk6c2Fucy1zZXJpZjt0ZXh0LWFuY2hvcjpzdGFydDtmaWxsOiMzQjQxNDMnID4rPC90ZXh0Pgo8L3N2Zz4K [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 title claims abstract description 25
- 229910001416 lithium ion Inorganic materials 0.000 title claims abstract description 25
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 24
- 238000004065 wastewater treatment Methods 0.000 title claims abstract description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances data:image/svg+xml;base64,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 data:image/svg+xml;base64,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 O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 73
- 239000012528 membrane Substances 0.000 claims abstract description 58
- 239000002351 wastewater Substances 0.000 claims abstract description 35
- 239000005416 organic matter Substances 0.000 claims abstract description 33
- OKTJSMMVPCPJKN-UHFFFAOYSA-N carbon Chemical compound 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[C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 26
- 239000003960 organic solvent Substances 0.000 claims abstract description 22
- 238000010438 heat treatment Methods 0.000 claims abstract description 11
- WHXSMMKQMYFTQS-UHFFFAOYSA-N lithium Chemical compound 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[Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 claims abstract description 11
- 229910052744 lithium Inorganic materials 0.000 claims abstract description 11
- 239000002253 acid Substances 0.000 claims abstract description 8
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 8
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt Chemical compound 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[Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims abstract description 8
- 229910052803 cobalt Inorganic materials 0.000 claims abstract description 8
- 239000010941 cobalt Substances 0.000 claims abstract description 8
- 239000003814 drug Substances 0.000 claims abstract description 6
- 238000007789 sealing Methods 0.000 claims abstract description 4
- SECXISVLQFMRJM-UHFFFAOYSA-N n-methylpyrrolidone Chemical compound 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CN1CCCC1=O SECXISVLQFMRJM-UHFFFAOYSA-N 0.000 claims description 14
- VZGDMQKNWNREIO-UHFFFAOYSA-N Carbon tetrachloride Chemical group 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O=C1CCCN1 HNJBEVLQSNELDL-UHFFFAOYSA-N 0.000 description 1
- 241000196171 Hydrodictyon reticulatum Species 0.000 description 1
- 239000000356 contaminant Substances 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 238000005868 electrolysis reaction Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000002349 favourable Effects 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000001764 infiltration Methods 0.000 description 1
- 238000011068 load Methods 0.000 description 1
- 238000005461 lubrication Methods 0.000 description 1
- 239000002075 main ingredient Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000008213 purified water Substances 0.000 description 1
- -1 small molecule organosilane ester Chemical class 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
Classifications
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F9/00—Multistage treatment of water, waste water, or sewage
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/26—Treatment of water, waste water, or sewage by extraction
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/28—Treatment of water, waste water, or sewage by sorption
- C02F1/283—Treatment of water, waste water, or sewage by sorption using coal, charred products, or inorganic mixtures containing them
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/44—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/44—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis
- C02F1/442—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis by nanofiltration
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/44—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis
- C02F1/444—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis by ultrafiltration or microfiltration
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2101/00—Nature of the contaminant
- C02F2101/10—Inorganic compounds
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2101/00—Nature of the contaminant
- C02F2101/30—Organic compounds
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2101/00—Nature of the contaminant
- C02F2101/30—Organic compounds
- C02F2101/34—Organic compounds containing oxygen
Abstract
本发明提供一种锂离子电池生产废水处理装置，包括有机物分离池、蒸馏塔和深度净水池；有机物分离池顶端密封连接池盖，池盖顶端设有药剂添加口；有机溶剂通过管道输送至蒸馏塔，蒸馏塔包括加热罐和回流分离塔；深度净水池包括深度净水池池体，其内部沿废水输送方向依次设有活性炭过滤板、第一过滤膜、第二过滤膜和第三过滤膜；第一过滤膜、第二过滤膜和第三过滤膜的孔径依次减小，活性炭过滤板、第一过滤膜、第二过滤膜和第三过滤膜的间距依次减小；管道装有流量调节阀，管道中溶液的输送动力由电泵提供。本发明的有益效果是：该设计能够专门针对锂离子电池生产废水中含有钴酸锂、NMP、碳粉等主要成分进行净化处理，以提高净水效率，降低净化成本。
Description
一种锂离子电池生产废水处理装置
技术领域
[0001]本发明涉及锂离子电池生产技术领域，尤其是涉及一种锂离子电池生产废水处理 装置。
背景技术
[0002]目前，企业中生产锂离子电池的废水来源主要为锂电池阳极生产过程中产生的清 洗废水和阴极生产中产生的清洗废水。这些废水中的主要成份为钴酸锂、NMP (甲基吡咯烷 酮）、碳粉等，废水量为3〇m3/d。锂电废水，排放为间歇性，水质变化波动较大。目前，对锂离 子电池生产废水净化一种是成本较高的化学氧化、药剂电解再配合活性炭吸附、反渗透等 技术处理方式，另一种则是与生活污水一起净化。但是与生活污水一起净化则净化周期就 会显著延长，所以处理效率还是比较低。由此可见，如何研宄出一种锂离子电池生产废水处 理装置，能够专门针对锂离子电池生产废水中含有钴酸锂、NMP、碳粉这些主要物质进行净 化处理，从而提高净水效率，降低净化成本，是目前本领域技术人员亟待解决的问题。
发明内容
[0003] 为了解决上述问题，本发明提供了一种锂离子电池生产废水处理装置。
[0004] 本发明一种锂离子电池生产废水处理装置，包括用于分离废水与废水中甲基吡咯 烷酮的有机物分离池，所述有机物分离池底部通过管道连接有蒸馏塔，所述有机物分离池 侧壁底部通过管道连接深度净水池;所述有机物分离池包括有机物分离池池体，所述有机 物分离池池体侧壁开设有原始废水入口，所述有机物分离池池体顶端密封连接有池盖，所 述池盖顶端开设有用于添加萃取甲基吡咯烷酮有机溶剂的药剂添加口；所述有机溶剂的密 度大于水的密度，且不溶于水;萃取甲基吡咯烷酮后的有机溶剂通过管道输送至所述蒸馏 塔中，所述蒸馏塔包括位于底部的加热罐和位于上端与所述加热罐相连通的回流分离塔。
[0005] 所述深度净水池包括深度净水池池体，所述深度净水池池体内沿废水进口至净化 水出口方向依次设有用于吸附残余有机物、钴酸锂和碳粉的活性炭过滤板、第一过滤膜、第 二过滤膜和第三过滤膜;所述第一过滤膜、第二过滤膜和第三过滤膜的孔径依次减小，所述 活性炭过滤板、第一过滤膜、第二过滤膜和第三过滤膜的间距依次减小;所述管道中安装有 流量调节阀，所述管道中溶液的输送动力由电泵提供。
[0006] 进一步地，所述第二过滤膜为超滤膜，所述第三过滤膜为纳滤膜。
[0007] 进一步地，所述深度净水池中设置有反洗装置，即本发明具有滤膜自清洗功能。
[0008] 进一步地，所述反洗装置包括反洗水箱、位于所述反洗水箱上端的反洗水排水管 和位于所述反洗水箱底部与所述净化水出口的接管相连通的反洗进水管，所述反洗水排水 管和反洗进水管中安装流量控制阀门。
[0009] 进一步地，所述反洗排水管包括主管和多个支管，所述支管分别与所述深度净水 池池体侧壁连通。
[0010] 进一步地，所述回流分离塔和所述加热罐侧面设有有机溶剂出口和甲基吡咯烷酮 出口。
[0011] 进一步地，用于萃取废水中甲基吡咯烷酮的所述有机溶剂为四氯化碳。
[0012] 进一步地，所述有机物分离池侧壁上开设有用于观察液位的透视窗，所述透视窗 上通密封胶连接有增强透明玻璃板。
[0013] 进一步地，用于提供废水输送动力的电栗为轴流泵。
[0014] 本发明一种锂离子电池生产废水处理装置，与现有技术相比具有以下优点： 首先，该锂离子电池生产废水处理装置中，通过采用有机溶剂将溶于废水中的甲基吡 咯烷酮成功萃取，由于有机溶剂为密度大于水的液体如四氯化碳溶液，所以其萃取完毕后 处于有机物分离池底部，这样通过管道由有机物分离池底部将存萃取液快速转移至蒸馏塔 中，利用有机溶剂沸点小于甲基吡咯烷酮沸点的特点，使两者顺利分离，分离后的有机溶剂 可以再次用于有机物分离池的萃取工作，因为其可以循环利用，所以能够显著节约废水处 理成本。
[0015] 其次，因为有机溶剂不仅可以萃取甲基吡咯烷酮，还可以萃取其他有机小分子，所 以同样可以通过蒸馈塔实现甲基吡咯烷酮与有机小分子的分离。由于主要的有机物已经被 清除，此过程可显著降低废水毒性，并且该过程为后续通过物理吸附进行深度净化提供了 有利的前提条件。
[0016]最后，该设计通过活性炭进行物理吸附，实现废水深度处理过程中的初步过滤处 理，然后通过多道滤膜进彳丁株度过滤，从而将钻酸裡、碳粉以及其它非常微小的杂质过滤 掉，以达到国家安全排放标准的目的。此外，为了降低滤膜的成本，所以在深度清洗池中安 装有反洗装置，且反洗水来源于处理后的净化水，因而本发明在降低滤膜使用成本的同时 还能够有效节约水资源。
[0017]综上所述，本发明能够专门针对锂离子电池生产废水中含有钴酸锂、NMP、碳粉这 些主要物质进行净化处理，从而提高净水效率，降低锂离子电池生产废水的净化成本。
附图说明
[0018]图1为本发明的结构示意图； 图2为本发明中深度净化池开启顶盖后的结构示意图； 图3为本发明中深度净化池的右视图； 图4为本发明的工作原理图。
[0019]图中：1、有机物分离池，2、蒸馏塔，3、深度净水池，1 • 1、原始废水入口，i . 2、药剂添 加口，1 _3、透视窗，2 • 1、加热罐，2 •2回流分离塔，3.1、深度净水池池体，3.2、活性炭过滤板， 3_3、第一过滤膜，3_4、第二过滤膜，3.5第三过滤膜，3.6、反洗水箱，3.7、反洗排水管，3.8、 反洗进水管。
具体实施方式
[0020]为了更好的理解本发明，下面结合具体实施例和附图对本发明进行进一步的描 述。
[0021]如图1-4所示，一种锂离子电池生产废水处理装置，包括用于分离废水与废水中甲 基吡咯烷酮的有机物分离池1。所述有机物分离池1底部通过管道连接有蒸馏塔2。所述有机 物分离池1侧壁底部通过管道连接深度净水池3。所述有机物分离池1包括有机物分离池池 体，所述有机物分离池池体侧壁开设有原始废水入口 1.1。
[0022]所述有机溶剂的密度大于水的密度，且不溶于水，如四氯化碳溶液。为了避免有机 溶剂挥发对外界大气造成二次污染，所以在所述有机物分离池池体顶端密封连接有池盖， 所述池盖顶端开设有用于添加萃取甲基吡咯烷酮有机溶剂的药剂添加口 1.2。
[0023]萃取甲基吡咯烷酮后的有机溶剂通过管道输送至所述蒸馏塔2中，所述有机物分 离池1侧壁上开设有用于观察液位的透视窗1.3,所述透视窗1.3上通密封胶连接有增强透 明玻璃板。这样可以使工作人员更为直观的了解有机溶剂向蒸馈塔2中的输送进度。
[0024] 所述蒸馏塔2包括位于底部的加热罐2.1和位于上端与所述加热罐2.1相连通的回 流分离塔2.2。所述回流分离塔2.2和所述加热罐2.1侧面设有有机溶剂出口和甲基吡咯烷 酮出口。这一位置设置主要是根据四氯化碳沸点小于甲基吡咯烷酮而设计。当然，所述有机 溶剂出口馏出物根据加热温度不同而分为小分子有机酯类以及四氯化碳。
[0025]由于有机物被大部分清除，所以会显著减轻后续回水处理负担。进行后续废水净 化的所述深度净水池3包括深度净水池池体3.1，所述深度净水池池体3.1内沿废水进口至 净化水出口方向依次设有用于吸附残余有机物、钴酸锂和碳粉的活性炭过滤板3.2、第一过 滤膜3.3、第二过滤膜3.4和第三过滤膜3.5。
[0026] 为了提升所述第一过滤膜3.3、第二过滤膜3.4和第三过滤膜3.5的过滤能力所以 将所述第一过滤膜3.3、第二过滤膜3.4和第三过滤膜3.5的孔径依次减小。并根据杂质含量 的高低而将所述活性炭过滤板3.2、第一过滤膜3.3、第二过滤膜3.4和第三过滤膜3.5的间 距设计为依次减小。该设计在符合流体动力学基础上能够合理利用所述深度净水池3的内 部空间。
[0027]为了使由所述深度净水池3的净水出口排出的水流具备高度净化的特点，所以将 所述第二过滤膜3.4设计为超滤膜，将所述第三过滤膜3.5设计为纳滤膜。
[0028] 为了节约所述第一过滤膜3.3、第二过滤膜3.4和第三过滤膜3 • 5的应用成本，所以 在所述深度净水池3中设置有反洗装置。所述反洗装置包括反洗水箱3.6、位于所述反洗水 箱3.6上端的反洗水排水管3.7和位于所述反洗水箱3.6底部与所述净化水出口的接管相连 通的反洗进水管3.8，所述反洗水排水管3.7和反洗进水管3.8中安装流量控制阀门。
[0029]上述设置可以使反洗水来自废水净化水，从而能达到节约用水的目的。为了使反 洗水流进入所述深度清洗池3时流速更为平稳，所以将所述反洗排水管3.7包括主管和多个 支管，所述支管分别与所述深度净水池池体3.1侧壁连通。
[0030]由于废水为间歇性的，所以为了使管道中的液体输送流速可控，在所述管道中安 装有流量调节阀。此外，所述管道中溶液的输送动力由电栗提供。本实施例中用于提供废水 输送动力电栗为轴流泵。
[0031] 这种电栗能够输送pH值4-10的污水，适用性更强。另外，轴流泵具有双重机械密 封，可靠的防止漏水，其采用专用推力轴承，结构设计合理，润滑充分，散热良好，轴承使用 寿命长。最后，轴流泵还具有机泵一体化的特点，所以安装维修省时省工，进而能够达到节 省成本的目的。
[0032]以上对本发明的实施例进行了详细说明，但所述内容仅为本发明的较佳实施例， 不能被认为用于限定本发明的实施范围。凡依本发明范围所作的均等变化与改进等，均应 仍归属于本专利涵盖范围之内。
Claims (9)
1. 一种锂离子电池生产废水处理装置，其特征在于:包括用于分离废水与废水中甲基 吡咯烷酮的有机物分离池（1)，所述有机物分离池（1)底部通过管道连接有蒸馏塔(2)，所述 有机物分离池(1)侧壁底部通过管道连接深度净水池(3); 所述有机物分离池（1)包括有机物分离池池体，所述有机物分离池池体侧壁开设有原 始废水入口（1.1)，所述有机物分离池池体顶端密封连接池盖，所述池盖顶端开设有用于添 加萃取甲基吡咯烷酮有机溶剂的药剂添加口（1.» ; 所述有机溶剂的密度大于水的密度，且不溶于水;萃取甲基吡咯烷酮后的有机溶剂通 过管道输送至所述蒸馏塔(2)中，所述蒸馏塔(2)包括位于底部的加热罐(2.1)和位于上端 与所述加热罐(2.1)相连通的回流分离塔(2 • 2); 所述深度净水池(3)包括深度净水池池体(3.1)，所述深度净水池池体(3.1)内沿其废 水进口至净化水出口方向依次设有用于吸附残余有机物、钴酸锂和碳粉的活性炭过滤板 (3.2) 、第一过滤膜(3.3)、第二过滤膜(3.4)和第三过滤膜(3.5); 所述第一过滤膜(3 • 3)、第二过滤膜(3 • 4)和第三过滤膜(3.5)的孔径依次减小，所述活 性炭过滤板(3 • 2)、第一过滤膜(3.3)、第二过滤膜(3 • 4)和第三过滤膜(3 • 5)的间距依次减 小； 所述管道中安装有流量调节阀，所述管道中溶液的输送动力由电泵提供。
2. 根据权利要求1所述的锂离子电池生产废水处理装置，其特征在于:所述第二过滤膜 (3.4)为超滤膜，所述第三过滤膜(3.5)为纳滤膜。
3. 根据权利要求1所述的锂离子电池生产废水处理装置，其特征在于:所述深度净水池 (3)中设置有反洗装置。
4. 根据权利要求3所述的锂离子电池生产废水处理装置，其特征在于:所述反洗装置包 括反洗水箱(3 • 6)、位于所述反洗水箱(3.6)上端的反洗水排水管(3.7)和位于所述反洗水 箱（3.6)底部与所述净化水出口的接管相连通的反洗进水管（3.8)，所述反洗水排水管 (3.7) 和反洗进水管(3 • 8)中安装流量控制阀门。
5. 根据权利要求4所述的锂离子电池生产废水处理装置，其特征在于:所述反洗排水管 (3.7) 包括主管和多个支管，所述支管分别与所述深度净水池池体(3.1)侧壁连通。
6. 根据权利要求1所述的锂离子电池生产废水处理装置，其特征在于:所述回流分离塔 (2.2) 和所述加热罐(2 • 1)侧面设有有机溶剂出口和甲基吡咯烷酮出口。
7. 根据权利要求1所述的锂离子电池生产废水处理装置，其特征在于:用于萃取废水中 甲基吡咯烷酮的所述有机溶剂为四氯化碳。
8. 根据权利要求1所述的锂离子电池生产废水处理装置，其特征在于:所述有机物分离 池（1)侧壁上开设有用于观察液位的透视窗（1.3)，所述透视窗（1.3)上通密封胶连接有增 强透明玻璃板。
9. 根据权利要求1-8中任意一项所述的锂离子电池生产废水处理装置，其特征在于：用 于提供废水输送动力的电栗为轴流泵。
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| CN111847707A (zh) * | 2020-07-03 | 2020-10-30 | 安徽南都华铂新材料科技有限公司 | 一种废水中重金属回收装置及其使用方法 |
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| CN108059292A (zh) * | 2017-11-28 | 2018-05-22 | 南京环保产业创新中心有限公司 | 锂离子电池生产废水零排放的处理方法 |
| CN111847707A (zh) * | 2020-07-03 | 2020-10-30 | 安徽南都华铂新材料科技有限公司 | 一种废水中重金属回收装置及其使用方法 |
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